CN104562779B - A kind of dyeing assistant improving textile color stability and preparation method thereof - Google Patents
A kind of dyeing assistant improving textile color stability and preparation method thereof Download PDFInfo
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- CN104562779B CN104562779B CN201510058057.1A CN201510058057A CN104562779B CN 104562779 B CN104562779 B CN 104562779B CN 201510058057 A CN201510058057 A CN 201510058057A CN 104562779 B CN104562779 B CN 104562779B
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- dyeing assistant
- color stability
- textile color
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- 239000004753 textile Substances 0.000 title claims abstract description 43
- 238000004043 dyeing Methods 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 20
- 239000002270 dispersing agent Substances 0.000 claims abstract description 20
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 19
- 230000000149 penetrating effect Effects 0.000 claims abstract description 19
- GFLJTEHFZZNCTR-UHFFFAOYSA-N 3-prop-2-enoyloxypropyl prop-2-enoate Chemical compound C=CC(=O)OCCCOC(=O)C=C GFLJTEHFZZNCTR-UHFFFAOYSA-N 0.000 claims abstract description 18
- -1 amido silicon Chemical compound 0.000 claims abstract description 18
- 239000003921 oil Substances 0.000 claims abstract description 18
- 229920000371 poly(diallyldimethylammonium chloride) polymer Polymers 0.000 claims abstract description 18
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims abstract description 18
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 18
- 239000010703 silicon Substances 0.000 claims abstract description 18
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims abstract description 18
- 239000008367 deionised water Substances 0.000 claims abstract description 17
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 17
- 229920002401 polyacrylamide Polymers 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- JHJUUEHSAZXEEO-UHFFFAOYSA-M sodium;4-dodecylbenzenesulfonate Chemical compound [Na+].CCCCCCCCCCCCC1=CC=C(S([O-])(=O)=O)C=C1 JHJUUEHSAZXEEO-UHFFFAOYSA-M 0.000 claims abstract description 11
- 239000000725 suspension Substances 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 7
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 claims description 4
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 4
- 229920000053 polysorbate 80 Polymers 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- QOYWCXUGVIBELA-UHFFFAOYSA-N C(CCCCCCCCCCC)(=O)OCCOCCOC(CCCCCCCCCCC)=O.C(CC(=O)C)(=O)O.C(C(=C)C)(=O)O Chemical group C(CCCCCCCCCCC)(=O)OCCOCCOC(CCCCCCCCCCC)=O.C(CC(=O)C)(=O)O.C(C(=C)C)(=O)O QOYWCXUGVIBELA-UHFFFAOYSA-N 0.000 claims 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims 1
- 239000003086 colorant Substances 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- 231100000252 nontoxic Toxicity 0.000 abstract description 3
- 230000003000 nontoxic effect Effects 0.000 abstract description 3
- SNRUBQQJIBEYMU-UHFFFAOYSA-N dodecane Chemical compound CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 12
- 238000000034 method Methods 0.000 description 7
- MZSDGDXXBZSFTG-UHFFFAOYSA-M sodium;benzenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C1=CC=CC=C1 MZSDGDXXBZSFTG-UHFFFAOYSA-M 0.000 description 6
- 239000000975 dye Substances 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- YEQBHMVRNHTCPJ-UHFFFAOYSA-N 2-methylprop-2-enoic acid;3-oxobutanoic acid Chemical group CC(=C)C(O)=O.CC(=O)CC(O)=O YEQBHMVRNHTCPJ-UHFFFAOYSA-N 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- QLNJFJADRCOGBJ-UHFFFAOYSA-N propionamide Chemical compound CCC(N)=O QLNJFJADRCOGBJ-UHFFFAOYSA-N 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
Landscapes
- Coloring (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of dyeing assistant improving textile color stability, in parts by weight, including following components: amido silicon oil 10 15 parts, polyacrylamide 15 20 parts, sodium polyacrylate 15 parts, dodecylbenzene sodium sulfonate 2 10 parts, PDDA 15 parts, penetrating agent 25 parts, dispersant 23 parts, cross-linking agent 13 parts, deionized water 20 30 parts.The invention also discloses the preparation method of this dyeing assistant.The dyeing assistant improving textile color stability that the present invention provides, can be effectively improved the color fastness of textile, make the textile bright colors after dyeing bright-coloured, soft comfortable, and material therefor is nontoxic, cheap, beneficially environmental conservation, low cost.
Description
Technical field:
The present invention relates to textile dyeing technical field, be specifically related to a kind of raising textile color
The dyeing assistant of fastness.
Background technology:
Color fastness refers to that various effects during processing and use are supported by the color of textile
Drag, it mainly includes light fastness, washing fastness, crock fastness, perspiration fastness, flatiron
Fastness etc., color fastness is good and bad, is directly related to the healthy and safe of human body, the product of color fastness difference
In wearing process, encounter rainwater, pigment that sweat will result on fabric comes off and fades, its
The molecule of middle dyestuff and heavy metal ion etc. are likely to be absorbed by the body by skin and endanger
On the other hand health, also can make other clothing staining worn, or with other clothing
Other medicated clothing dirty is contaminated when thing washs together.Therefore, how to improve the color fastness of textile, become
The problem solved it is badly in need of for textile fast development.
Summary of the invention:
It is an object of the invention to provide a kind of dyeing assistant improving textile color stability, Ke Yiyou
Effect improves the color fastness of textile, makes the textile bright colors after dyeing bright-coloured, soft comfortable,
And material therefor is nontoxic, cheap, beneficially environmental conservation, low cost.
For achieving the above object, the present invention is by the following technical solutions:
A kind of dyeing assistant improving textile color stability, in parts by weight, including following components:
Amido silicon oil 10-15 part, polyacrylamide 15-20 part,
Sodium polyacrylate 1-5 part, dodecylbenzene sodium sulfonate 2-10 part,
PDDA 1-5 part,
Penetrating agent 2-5 part, dispersant 2-3 part,
Cross-linking agent 1-3 part, deionized water 20-30 part.
Preferred as technique scheme, a kind of dyeing assistant improving textile color stability,
In parts by weight, including following components:
Amido silicon oil 10 parts, polyacrylamide 18 parts,
Sodium polyacrylate 2 parts, dodecylbenzene sodium sulfonate 5 parts,
PDDA 5 parts,
Penetrating agent 2 parts, dispersant 3 parts,
Cross-linking agent 2 parts, deionized water 30 parts.
Preferred as technique scheme, described penetrating agent is diisooctyl succinum semi-annular jade pendant acid sodium.
Preferred as technique scheme, described dispersant is span80 and Tween 80 mixed
Compound.
Preferred as technique scheme, described cross-linking agent is methacrylic acid acetoacetic acid second
Glycol dibasic acid esters.
Preferred as technique scheme, the mass ratio of span80 and Tween 80 is 1:2.
The present invention's, another purpose is to provide the preparation method of this textile dyeing auxiliary agent, bag
Include following steps:
(1) amido silicon oil, polyacrylamide and deionized water are mixed, at 10000-15000
Rev/min state under, high-speed stirred 12-24h, obtain suspension；
(2) suspension obtained toward step (1) is sequentially added into sodium polyacrylate, dodecane
Base benzene sulfonic acid sodium salt, PDDA, continue stirring, be subsequently adding penetrating agent,
Dispersant, cross-linking agent, ultrasonic 8-12h under 1000W power, it is improved textile color jail
The dyeing assistant of degree.
Compared with prior art, the method have the advantages that
The present invention use poly-propionic acid amide., sodium polyacrylate, PDDA and
Amido silicon oil mixes, and forms compositions, and said composition can be formed good by dispersant
Good dispersion, modified to dye molecule by it so that dye molecule has longer strand,
Form well crosslinking with textile by cross-linking agent, decrease dyestuff because the little entrance of molecule is spun
Inside fabric, the damage that textile fiber is caused；
The dyeing assistant that the present invention provides can be effectively improved the color fastness of textile, after making dyeing
Textile bright colors bright-coloured, soft comfortable, and material therefor is nontoxic, cheap, have
It is beneficial to environmental conservation, low cost.
Detailed description of the invention:
For a better understanding of the present invention, below by embodiment, the present invention is further described, real
Execute example only for explaining the present invention, the present invention will not be constituted any restriction.
Embodiment 1
A kind of dyeing assistant improving textile color stability, in parts by weight, including following components:
Amido silicon oil 10 parts, polyacrylamide 15 parts,
Sodium polyacrylate 1 part, dodecylbenzene sodium sulfonate 2 parts,
PDDA 1 part,
Penetrating agent 2 parts, dispersant 2 parts,
Cross-linking agent 1 part, deionized water 20 parts.
Its preparation method comprises the following steps:
(1) by amido silicon oil, polyacrylamide and deionized water mix, 10000 turns/
Under the state divided, high-speed stirred 12h, obtain suspension；
(2) suspension obtained toward step (1) is sequentially added into sodium polyacrylate, dodecane
Base benzene sulfonic acid sodium salt, PDDA, continue stirring, be subsequently adding penetrating agent,
Dispersant, cross-linking agent, under 1000W power, ultrasonic 8h, is improved textile color stability
Dyeing assistant.
Embodiment 2
A kind of dyeing assistant improving textile color stability, in parts by weight, including following components:
Amido silicon oil 15 parts, polyacrylamide 20 parts,
Sodium polyacrylate 5 parts, dodecylbenzene sodium sulfonate 10 parts,
PDDA 5 parts,
Penetrating agent 5 parts, dispersant 3 parts,
Cross-linking agent 3 parts, deionized water 30 parts.
Its preparation method comprises the following steps:
(1) by amido silicon oil, polyacrylamide and deionized water mix, 15000 turns/
Under the state divided, high-speed stirred 24h, obtain suspension；
(2) suspension obtained toward step (1) is sequentially added into sodium polyacrylate, dodecane
Base benzene sulfonic acid sodium salt, PDDA, continue stirring, be subsequently adding penetrating agent,
Dispersant, cross-linking agent, under 1000W power, ultrasonic 12h, is improved textile color stability
Dyeing assistant.
Embodiment 3
A kind of dyeing assistant improving textile color stability, in parts by weight, including following components:
Amido silicon oil 11 parts, polyacrylamide 16 parts,
Sodium polyacrylate 2 parts, dodecylbenzene sodium sulfonate 4 parts,
PDDA 2 parts,
Penetrating agent 3 parts, dispersant 3 parts,
Cross-linking agent 2 parts, deionized water 22 parts.
Its preparation method comprises the following steps:
(1) by amido silicon oil, polyacrylamide and deionized water mix, 11000 turns/
Under the state divided, high-speed stirred 14h, obtain suspension；
(2) suspension obtained toward step (1) is sequentially added into sodium polyacrylate, dodecane
Base benzene sulfonic acid sodium salt, PDDA, continue stirring, be subsequently adding penetrating agent,
Dispersant, cross-linking agent, under 1000W power, ultrasonic 9h, is improved textile color stability
Dyeing assistant.
Embodiment 4
A kind of dyeing assistant improving textile color stability, in parts by weight, including following components:
Amido silicon oil 12 parts, polyacrylamide 17 parts,
Sodium polyacrylate 3 parts, dodecylbenzene sodium sulfonate 6 parts,
PDDA 3 parts,
Penetrating agent 4 parts, dispersant 2 parts,
Cross-linking agent 2 parts, deionized water 26 parts.
Its preparation method comprises the following steps:
(1) by amido silicon oil, polyacrylamide and deionized water mix, 12000 turns/
Under the state divided, high-speed stirred 18h, obtain suspension；
(2) suspension obtained toward step (1) is sequentially added into sodium polyacrylate, dodecane
Base benzene sulfonic acid sodium salt, PDDA, continue stirring, be subsequently adding penetrating agent,
Dispersant, cross-linking agent, under 1000W power, ultrasonic 10h, is improved textile color stability
Dyeing assistant.
Embodiment 5
A kind of dyeing assistant improving textile color stability, in parts by weight, including following components:
Amido silicon oil 14 parts, polyacrylamide 18 parts,
Sodium polyacrylate 4 parts, dodecylbenzene sodium sulfonate 8 parts,
PDDA 4 parts,
Penetrating agent 4 parts, dispersant 2 parts,
Cross-linking agent 1 part, deionized water 28 parts.
Its preparation method comprises the following steps:
(1) by amido silicon oil, polyacrylamide and deionized water mix, 14000 turns/
Under the state divided, high-speed stirred 20h, obtain suspension；
(2) suspension obtained toward step (1) is sequentially added into sodium polyacrylate, dodecane
Base benzene sulfonic acid sodium salt, PDDA, continue stirring, be subsequently adding penetrating agent,
Dispersant, cross-linking agent, under 1000W power, ultrasonic 11h, is improved textile color stability
Dyeing assistant.
Below the textile after adding the dyeing assistant dyeing provided in the embodiment of the present invention is entered
Row fastness to rubbing, light fastness, washing fastness are tested, and are designated as sample 1-5 respectively, its
Textile after the dyeing assistant dyeing that middle comparative example provides for being not added with the present invention, test result
As shown in table 1:
Table 1
From the point of view of table 1, the dyeing assistant that the present invention provides, the dyeing of textile can be significantly improved
Fastness, the textile after dyeing, wearability, water-wash resistance are good.
Claims (6)
1. the dyeing assistant improving textile color stability, it is characterised in that in parts by weight, including following components:
Amido silicon oil 10-15 part, polyacrylamide 15-20 part,
Sodium polyacrylate 1-5 part, dodecylbenzene sodium sulfonate 2-10 part,
PDDA 1-5 part,
Penetrating agent 2-5 part, dispersant 2-3 part,
Cross-linking agent 1-3 part, deionized water 20-30 part；
Its preparation method comprises the following steps:
(1) amido silicon oil, polyacrylamide and deionized water are mixed, when 10000-15000 rev/min, high-speed stirred 12-24h, obtain suspension；
(2) suspension obtained toward step (1) is sequentially added into sodium polyacrylate, dodecylbenzene sodium sulfonate, PDDA, continue stirring, it is subsequently adding penetrating agent, dispersant, cross-linking agent, ultrasonic 8-12h under 1000W power, is improved the dyeing assistant of textile color stability.
A kind of dyeing assistant improving textile color stability the most as claimed in claim 1, it is characterised in that in parts by weight, including following components:
Amido silicon oil 10 parts, polyacrylamide 18 parts,
Sodium polyacrylate 2 parts, dodecylbenzene sodium sulfonate 5 parts,
PDDA 5 parts,
Penetrating agent 2 parts, dispersant 3 parts,
Cross-linking agent 2 parts, deionized water 30 parts.
A kind of dyeing assistant improving textile color stability the most as claimed in claim 1, it is characterised in that described penetrating agent is diisooctyl succinum sodium sulfonate.
A kind of dyeing assistant improving textile color stability the most as claimed in claim 1, it is characterised in that described dispersant is the mixture of span80 and Tween 80.
A kind of dyeing assistant improving textile color stability the most as claimed in claim 1, it is characterised in that described cross-linking agent is methacrylic acid acetoacetic acid diethylene glycol dilaurate.
A kind of dyeing assistant improving textile color stability the most as claimed in claim 4, it is characterised in that the mass ratio of span80 and Tween 80 is 1:2.
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| CN201510058057.1A CN104562779B (en) | 2015-02-04 | 2015-02-04 | A kind of dyeing assistant improving textile color stability and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510058057.1A CN104562779B (en) | 2015-02-04 | 2015-02-04 | A kind of dyeing assistant improving textile color stability and preparation method thereof |
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| CN104562779A CN104562779A (en) | 2015-04-29 |
| CN104562779B true CN104562779B (en) | 2016-08-31 |
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| CN110924193A (en) * | 2019-12-11 | 2020-03-27 | 苏州经贸职业技术学院 | Preparation method of reactive dye dyeing accelerating functional agent |
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