CN104529186A - Method for making film-coated gradual-change color steel glass - Google Patents
Method for making film-coated gradual-change color steel glass Download PDFInfo
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- CN104529186A CN104529186A CN201410768148.XA CN201410768148A CN104529186A CN 104529186 A CN104529186 A CN 104529186A CN 201410768148 A CN201410768148 A CN 201410768148A CN 104529186 A CN104529186 A CN 104529186A
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- 239000011521 glass Substances 0.000 title claims abstract description 67
- 238000000034 method Methods 0.000 title claims abstract description 29
- 229910000831 Steel Inorganic materials 0.000 title claims abstract description 11
- 239000010959 steel Substances 0.000 title claims abstract description 11
- 230000000694 effects Effects 0.000 claims abstract description 32
- 239000007789 gas Substances 0.000 claims abstract description 8
- 238000001755 magnetron sputter deposition Methods 0.000 claims abstract description 5
- 238000000576 coating method Methods 0.000 claims description 52
- 239000011248 coating agent Substances 0.000 claims description 39
- 238000007639 printing Methods 0.000 claims description 35
- 230000008859 change Effects 0.000 claims description 26
- 238000004544 sputter deposition Methods 0.000 claims description 20
- 239000000758 substrate Substances 0.000 claims description 17
- 239000011229 interlayer Substances 0.000 claims description 16
- 239000010410 layer Substances 0.000 claims description 13
- 239000002184 metal Substances 0.000 claims description 12
- 229910052751 metal Inorganic materials 0.000 claims description 12
- 238000004519 manufacturing process Methods 0.000 claims description 11
- 239000012752 auxiliary agent Substances 0.000 claims description 9
- 238000001035 drying Methods 0.000 claims description 9
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 8
- 239000000956 alloy Substances 0.000 claims description 5
- 229910045601 alloy Inorganic materials 0.000 claims description 5
- 150000002736 metal compounds Chemical class 0.000 claims description 5
- 230000003287 optical effect Effects 0.000 claims description 5
- 229910052786 argon Inorganic materials 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 238000007747 plating Methods 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 3
- 229910052709 silver Inorganic materials 0.000 claims description 3
- 239000004332 silver Substances 0.000 claims description 3
- 241000826860 Trapezium Species 0.000 claims description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 2
- 230000009471 action Effects 0.000 claims description 2
- 230000001154 acute effect Effects 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 238000000465 moulding Methods 0.000 claims description 2
- 230000008569 process Effects 0.000 abstract description 5
- 239000013077 target material Substances 0.000 abstract description 3
- 230000007704 transition Effects 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 15
- 239000003086 colorant Substances 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000005329 float glass Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000005355 lead glass Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000007650 screen-printing Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000005477 sputtering target Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000005341 toughened glass Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- Surface Treatment Of Glass (AREA)
Abstract
The invention relates to a method for making a film-coated gradual-change color steel glass. According to the method, a target material is sputtered to the surface of smooth glass by adopting a magnetron sputtering method, when the target materials, working gases and electrifying currents are different, different film effects are made, when special tools are different, different gradual-change effects can be made, and when ink formulas are different, different color effects can be completed by stacking ink and a combined film; in addition, different film layers can be formed on the glass surface through different processes, so that an obvious film area and a non-film area appear on the upper edge and lower edge of a product, and step-by-step transition appears in the middle of the product.
Description
Technical field
The present invention relates to a kind of manufacture method realizing plated film gradual change product on glass, this product at home, outer market belongs to novel product, will be widely used in the high-end market of current household electrical appliances color crystal glass industry; The present invention is mainly effective realizes fade effect by coating process, and the color brilliant typography of reasonable combination, and the perfect effect of the one realized, belong to glass post-processing and manufacture field.
Background technology
Some products are required to possess obvious metalluster texture, figure line gives and draws near or vision difference from the close-by examples to those far off, allly in the market want the product being carried out implementation level appearance effect by fade effect, realize by net-point printing or air brushing; The present invention is dry plate, the paste plate of avoiding print lattice-point printing process, the bad problem such as disconnected ink, PASS line of spray-drawing process, and high glittering effect can be realized in figure aspect, reach desirable metal-like, really accomplish: high-end, air, the high-end product that improves grade thus make up the market vacancy.
Summary of the invention
Technical problem: the object of the invention is to be coated with gradual change rete on glass, then combines the color brilliant silk screen printing process of tradition; The manufacture method of the color steel glass of a kind of plated film gradual change is provided.
Technical scheme: the color steel glass of gradual change of the present invention, be with magnetically controlled sputter method by target as sputter to smooth glass surface, when target, working gas and electrical current different, we can produce different rete effects; Different fade effect can be made when special fixture is different; When ink formulations is different, ink and binding film stacked adding, can complete distinct colors effect.Different technique will form different retes on the glass surface, makes the obvious rete of upper following appearance of product and non-rete district, occurs in the middle of product incremental excessive.
The manufacture method of the first gradual change rete coated glass of the present invention is, this glass be with magnetically controlled sputter method by target as sputter to smooth glass surface, adopt the design of staged unbalanced magnetic field, make magnetron sputtering plating rete thickness by thick to thin, even variation, thus generation fade effect, concrete grammar is;
The first step. local for sputtering cavity vacuum is extracted into 1.0 × 10
-4pa, pass into argon gas, make sputtering chamber pressure remain on 4Pa, under staged Nonequilibrium magnetic field action, with magnetically controlled sputter method one or more layers metal of coating, alloy or metal compound film on the glass substrate of clean dried, to change the optical property of glass to realize color gradients rete;
Second step. glass substrate, from sputtering chamber product out, lies in a horizontal plane in layer unwheeling, rete face is protected the color brilliant printing of good preparation, first carries out the printing of low-temperature printing ink coating; The interlayer of low-temperature printing ink coating is dried and back cover bake out temperature is 155 DEG C-180 DEG C;
3rd step. be arranged on table of printing machine by half tone level again, distance stock 3-8mm, regulates angle and the pressure of scraper and returning blade, the glass substrate after plated film is carried out to the low temperature coating print in rete face, finally obtain gradual change rete coated glass.
The manufacture method of the second gradual change rete coated glass of the present invention is: this glass be with magnetically controlled sputter method by target as sputter to smooth glass surface,, adopt balancing fields design, make magnetron sputtering plating rete thickness by thick to thin, even variation, thus produce fade effect;
The first step. local for sputtering cavity vacuum is extracted into 1.0 × 10
-4pa, pass into argon gas, make sputtering chamber pressure remain on 4Pa, under balancing fields effect, with magnetically controlled sputter method one or more layers metal of coating, alloy or metal compound film on the glass substrate of clean dried, to change the optical property of glass to realize colored film layer;
Second step. a fixture is set between target and glass plane materiel; Fixture material is glass, steel plate or acrylic; Fixture moulding uses right-angled trapezium or right-angle triangle, and fixture height is not more than glass plane materiel height, and special fixture assembling mode is wherein a square edge and plane-parallel, and wherein acute angle scope is 10 ° ~ 80 °.
3rd step. from sputtering chamber glass substrate product out, lie in a horizontal plane in layer unwheeling, rete face is protected, forward the printing that Cai Jing machine room carries out low-temperature printing ink coating week to; The interlayer oven dry of low-temperature printing ink coating and back cover drying parameter are at 155 DEG C-180 DEG C;
4th step. be arranged on table of printing machine by half tone level, distance stock 3-8mm, regulates angle and the pressure of scraper and returning blade, namely can carry out the low temperature coating print in rete face to the glass substrate after plated film, finally obtain gradual change rete coated glass.
Wherein:
The low-temperature printing ink of described gradual change rete printing, its mix proportion scheme presses metal colour system, glittering colour system, pure color minute surface colour system three kinds of coated designs:
Three kinds of described coatings are:
Coating a: metal colour system, quality of cathode silver accounting 1%-15%; Look ink quality accounting 1%-10%; Gloss oil quality accounting 71%-96%; Auxiliary agent quality accounting 2%-4%;
Coating b: glittering colour system, pearlescence quality accounting 1%-10%; Look ink quality accounting 1%-10%; Gloss oil quality accounting 76%-96%; Auxiliary agent quality accounting 2%-4%;
Coating c: pure color minute surface colour system, look ink quality accounting 95%-99%; Auxiliary agent quality accounting 1%-5%;
Arranging scheme: namely inter-layer coatings a+ back cover coating c shows metal-like effect;
Namely inter-layer coatings b+ back cover coating c shows luminous effect;
Namely inter-layer coatings c+ back cover coating c shows pure color effect.
The interlayer bake out temperature of described low-temperature printing ink coating prod is 155 DEG C-180 DEG C, and drying time is 4min – 8min; Back cover is dried, and parameters of temperature 165 DEG C-180 DEG C, drying time is 7min – 11min.
Beneficial effect: preparation method of the present invention is simple, except coated glass surface has metalluster, then in conjunction with the colourful technological effect of color brilliant product, realizes excellent metalluster texture; Also there is the advantage that rete is firm, the color of good endurance, rete can adjust, can use under the ultraviolet environment of long contact.Can well merge with the color crystal coating of ink.
The membranous layer ingredient of sputter coating of the present invention is simple, sputtering target material expense is low, and easily, cost is low in low-temperature printing ink allotment.
The present invention has a wide range of applications in building glass, household glass and household appliance glass industrial aspect, has a extensive future.
Accompanying drawing explanation
Fig. 1 arranges schematic diagram between target 3 of the present invention, fixture 2, glass plane materiel 1.
Embodiment
1), glass selection: when using 3-4mm float glass sheet to produce using the processing and fabricating face of the non-tin face of glass as product;
2), in airtight filming equipment, use special fixture by target and glassy product rationally separated; Maybe can by controlling the electric current that target circulates;
3), glass substrate surface through vacuum magnetic-control sputtering mode, one or more layers metal of coating, alloy or metal compound film, to change the optical property of glass, meet certain particular requirement;
4), in conjunction with the different process of the coloured silk crystalline substance printing of different ingredients, different colours, different texture, thus the fade effect of the bulk metal gloss texture of product is realized
5) to using different special fixtures to match between different transition regions.
Outside successively from glass surface, on glass, the gradual change rete of different colours is coated with magnetically controlled sputter method.
Described gradual change rete, refers to and uses different target oxidizing reaction sputtering sedimentation oxide compound plasma membranes.
The different fade effect of rete, what lean on is that fixture realizes.Here our effect of adopting fixture to produce, its advantage is much larger than the effect of its sputter area of current control regulating target; When regulating target to produce, there is the phenomenon that thickness is inconsistent in the region after sputtering and the region target do not sputtered; Gradation zone adjustment for the variant production in later stage should not control, and causes waste to target.
Color brilliant toughened glass of plated film gradual change of the present invention and preparation method thereof comprises the steps:
1) film-coated glass substrate washed with de-ionized water is first treated, dry;
2) cleaned glass substrate is put into sputtering chamber; Sputtering chamber back end vacuum is less than 2.5X10
-3pa;
3) pass into working gas and reactant gases, on the glass substrate of clean dried, be coated with color gradients rete with sputtering method;
4) special fixture interval is used between the target sputtered and glass substrate;
5) from sputtering chamber product out, lie in a horizontal plane in layer unwheeling, rete face is protected, forward the printing that Cai Jing machine room carries out low-temperature printing ink coating week to;
6) different printing press and oven dry scheme is taked according to the different qualities of ink;
7) be arranged on table of printing machine by half tone level, distance stock 3-8mm, namely the angle and the pressure that regulate scraper and returning blade can print;
8) formula of low-temperature printing ink can use arbitrary mixing ratio, arbitrary effect, adds slightly to dodge, carefully to dodge or to present stereoeffect in conjunction with lines all passable.
The low-temperature printing ink of described gradual change rete printing, its mix proportion scheme presses metal colour system, glittering colour system, pure color minute surface colour system three kinds of coated designs:
Three kinds of described coatings are:
Coating a: metal colour system, quality of cathode silver accounting 1%-15%; Look ink quality accounting 1%-10%; Gloss oil quality accounting 71%-96%; Auxiliary agent quality accounting 2%-4%;
Coating b: glittering colour system, pearlescence quality accounting 1%-10%; Look ink quality accounting 1%-10%; Gloss oil quality accounting 76%-96%; Auxiliary agent quality accounting 2%-4%;
Coating c: pure color minute surface colour system, look ink quality accounting 95%-99%; Auxiliary agent quality accounting 1%-5%;
Arranging scheme: namely inter-layer coatings a+ back cover coating c shows metal-like effect;
Namely inter-layer coatings b+ back cover coating c shows luminous effect;
Namely inter-layer coatings c+ back cover coating c shows pure color effect.
9) the interlayer drying parameter of product is at 155 DEG C-180 DEG C, and drying time is 4min – 8min; Back cover processing parameter temperature 165 DEG C-180 DEG C, drying time is 7min – 11min.
Claims (4)
1. the manufacture method of the color steel glass of plated film gradual change, it is characterized in that this glass be with magnetically controlled sputter method by target as sputter to smooth glass surface, adopt the design of staged unbalanced magnetic field, make magnetron sputtering plating rete thickness by thick to thin, even variation, thus generation fade effect, concrete grammar is;
The first step. local for sputtering cavity vacuum is extracted into 1.0 × 10
-4pa, pass into argon gas, make sputtering chamber pressure remain on 4Pa, under staged Nonequilibrium magnetic field action, with magnetically controlled sputter method one or more layers metal of coating, alloy or metal compound film on the glass substrate of clean dried, to change the optical property of glass to realize color gradients rete;
Second step. glass substrate, from sputtering chamber product out, lies in a horizontal plane in layer unwheeling, rete face is protected the color brilliant printing of good preparation, first carries out the printing of low-temperature printing ink coating; The interlayer of low-temperature printing ink coating is dried and back cover bake out temperature is 155 DEG C-180 DEG C;
3rd step. be arranged on table of printing machine by half tone level again, distance stock 3-8mm, regulates angle and the pressure of scraper and returning blade, the glass substrate after plated film is carried out to the low temperature coating print in rete face, finally obtain gradual change rete coated glass.
2. a manufacture method for the color steel glass of plated film gradual change, is characterized in that, this glass be with magnetically controlled sputter method by target as sputter to smooth glass surface,, adopt balancing fields design, make magnetron sputtering plating rete thickness by thick to thin, even variation, thus produce fade effect;
The first step. local for sputtering cavity vacuum is extracted into 1.0 × 10
-4pa, pass into argon gas, make sputtering chamber pressure remain on 4Pa, under balancing fields effect, with magnetically controlled sputter method one or more layers metal of coating, alloy or metal compound film on the glass substrate of clean dried, to change the optical property of glass to realize colored film layer;
Second step. a fixture (2) is set between target (3) and glass plane materiel (1); Fixture material is glass, steel plate or acrylic; Fixture moulding uses right-angled trapezium or right-angle triangle, and fixture height is not more than the height of glass plane materiel, and fixture assembling mode is wherein a square edge and plane-parallel, and wherein acute angle scope is 10 ° ~ 80 °.
3rd step. from sputtering chamber glass substrate product out, lie in a horizontal plane in layer unwheeling, rete face is protected, forward the printing that Cai Jing machine room carries out low-temperature printing ink coating week to; The interlayer oven dry of low-temperature printing ink coating and back cover drying parameter are at 155 DEG C-180 DEG C;
4th step. be arranged on table of printing machine by half tone level, distance stock 3-8mm, regulates angle and the pressure of scraper and returning blade, namely can carry out the low temperature coating print in rete face to the glass substrate after plated film, finally obtain gradual change rete coated glass.
3. the manufacture method of the color steel glass of a kind of plated film gradual change according to claim 1 and 2, it is characterized in that the low-temperature printing ink of described gradual change rete printing, its mix proportion scheme presses metal colour system, glittering colour system, pure color minute surface colour system three kinds of coated designs:
Three kinds of described coatings are:
Coating a: metal colour system, quality of cathode silver accounting 1%-15%; Look ink quality accounting 1%-10%; Gloss oil quality accounting 71%-96%; Auxiliary agent quality accounting 2%-4%;
Coating b: glittering colour system, pearlescence quality accounting 1%-10%; Look ink quality accounting 1%-10%; Gloss oil quality accounting 76%-96%; Auxiliary agent quality accounting 2%-4%;
Coating c: pure color minute surface colour system, look ink quality accounting 95%-99%; Auxiliary agent quality accounting 1%-5%;
Arranging scheme: namely inter-layer coatings a+ back cover coating c shows metal-like effect;
Namely inter-layer coatings b+ back cover coating c shows luminous effect;
Namely inter-layer coatings c+ back cover coating c shows pure color effect.
4. the manufacture method of the color steel glass of a kind of plated film gradual change according to claim 1 and 2, it is characterized in that the interlayer bake out temperature of described low-temperature printing ink coating prod is 155 DEG C-180 DEG C, drying time is 4min – 8min; Back cover is dried, and parameters of temperature 165 DEG C-180 DEG C, drying time is 7min – 11min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410768148.XA CN104529186A (en) | 2014-12-12 | 2014-12-12 | Method for making film-coated gradual-change color steel glass |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410768148.XA CN104529186A (en) | 2014-12-12 | 2014-12-12 | Method for making film-coated gradual-change color steel glass |
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| CN104529186A true CN104529186A (en) | 2015-04-22 |
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| CN201410768148.XA Pending CN104529186A (en) | 2014-12-12 | 2014-12-12 | Method for making film-coated gradual-change color steel glass |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109180019A (en) * | 2018-10-09 | 2019-01-11 | 江西沃格光电股份有限公司 | Cover-plate glass and filming equipment |
| CN109423607A (en) * | 2017-09-01 | 2019-03-05 | 福建省辉锐电子技术有限公司 | A method of coated cover-plate is prepared using continuous magnetron sputtering sedimentation |
| CN109422468A (en) * | 2017-09-01 | 2019-03-05 | 福建省辉锐电子技术有限公司 | A method of the coated cover-plate with two or more colors |
| CN109970357A (en) * | 2019-02-28 | 2019-07-05 | 江苏秀强玻璃工艺股份有限公司 | A kind of electrodeless gradual change coloured silk steel glass and its manufacturing method |
| CN110240417A (en) * | 2019-07-08 | 2019-09-17 | 安徽省蚌埠华益导电膜玻璃有限公司 | A kind of glass surface forms the film plating process of gradient color |
| CN111000339A (en) * | 2019-08-16 | 2020-04-14 | 豪梅拉布罗科洛梅尔 | decoration |
| US20210274670A1 (en) * | 2018-11-16 | 2021-09-02 | Shine Optoelectronics (Kunshan) Co., Ltd. | Decorative sheet and cover plate for consumer electronic product |
| CN114714786A (en) * | 2022-02-11 | 2022-07-08 | 滁州新彩家用玻璃有限公司 | Coating printing method of substrate |
| CN114875372A (en) * | 2022-05-06 | 2022-08-09 | 浙江合特光电有限公司 | Preparation method and preparation equipment of color dielectric film |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109423607A (en) * | 2017-09-01 | 2019-03-05 | 福建省辉锐电子技术有限公司 | A method of coated cover-plate is prepared using continuous magnetron sputtering sedimentation |
| CN109422468A (en) * | 2017-09-01 | 2019-03-05 | 福建省辉锐电子技术有限公司 | A method of the coated cover-plate with two or more colors |
| CN109180019A (en) * | 2018-10-09 | 2019-01-11 | 江西沃格光电股份有限公司 | Cover-plate glass and filming equipment |
| US20210274670A1 (en) * | 2018-11-16 | 2021-09-02 | Shine Optoelectronics (Kunshan) Co., Ltd. | Decorative sheet and cover plate for consumer electronic product |
| US12122131B2 (en) * | 2018-11-16 | 2024-10-22 | Shine Optoelectronics (Kunshan) Co., Ltd. | Decorative sheet and cover plate for consumer electronic product |
| CN109970357A (en) * | 2019-02-28 | 2019-07-05 | 江苏秀强玻璃工艺股份有限公司 | A kind of electrodeless gradual change coloured silk steel glass and its manufacturing method |
| CN110240417A (en) * | 2019-07-08 | 2019-09-17 | 安徽省蚌埠华益导电膜玻璃有限公司 | A kind of glass surface forms the film plating process of gradient color |
| CN111000339A (en) * | 2019-08-16 | 2020-04-14 | 豪梅拉布罗科洛梅尔 | decoration |
| CN114714786A (en) * | 2022-02-11 | 2022-07-08 | 滁州新彩家用玻璃有限公司 | Coating printing method of substrate |
| CN114875372A (en) * | 2022-05-06 | 2022-08-09 | 浙江合特光电有限公司 | Preparation method and preparation equipment of color dielectric film |
| CN114875372B (en) * | 2022-05-06 | 2023-10-27 | 浙江合特光电有限公司 | Preparation method and preparation equipment of color medium film |
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Application publication date: 20150422 |
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