CN104489233A - Preparation method of fluid core clamped chewy gelatinized confection - Google Patents
Preparation method of fluid core clamped chewy gelatinized confection Download PDFInfo
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- 235000009508 confectionery Nutrition 0.000 title claims abstract description 131
- 239000012530 fluid Substances 0.000 title claims abstract description 91
- 238000002360 preparation method Methods 0.000 title claims abstract description 35
- 239000000499 gel Substances 0.000 claims abstract description 107
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 62
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 62
- 230000001055 chewing effect Effects 0.000 claims abstract description 39
- 108010010803 Gelatin Proteins 0.000 claims abstract description 29
- 239000008273 gelatin Substances 0.000 claims abstract description 29
- 229920000159 gelatin Polymers 0.000 claims abstract description 29
- 235000019322 gelatine Nutrition 0.000 claims abstract description 29
- 235000011852 gelatine desserts Nutrition 0.000 claims abstract description 29
- 239000007864 aqueous solution Substances 0.000 claims abstract description 24
- 238000001035 drying Methods 0.000 claims description 28
- 102000004190 Enzymes Human genes 0.000 claims description 21
- 108090000790 Enzymes Proteins 0.000 claims description 21
- 238000001816 cooling Methods 0.000 claims description 17
- ZDXPYRJPNDTMRX-UHFFFAOYSA-N glutamine Natural products OC(=O)C(N)CCC(N)=O ZDXPYRJPNDTMRX-UHFFFAOYSA-N 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000005498 polishing Methods 0.000 claims description 5
- 238000005253 cladding Methods 0.000 claims 5
- 238000010521 absorption reaction Methods 0.000 claims 3
- 238000007493 shaping process Methods 0.000 claims 3
- 230000001681 protective effect Effects 0.000 claims 2
- 235000015111 chews Nutrition 0.000 claims 1
- 108060008539 Transglutaminase Proteins 0.000 abstract description 43
- 102000003601 transglutaminase Human genes 0.000 abstract description 43
- 238000004132 cross linking Methods 0.000 abstract description 29
- 239000010985 leather Substances 0.000 abstract description 24
- 238000002844 melting Methods 0.000 abstract description 18
- 230000008018 melting Effects 0.000 abstract description 17
- 239000003349 gelling agent Substances 0.000 abstract description 13
- 235000019640 taste Nutrition 0.000 abstract description 12
- 238000000034 method Methods 0.000 abstract description 11
- 230000008901 benefit Effects 0.000 abstract description 4
- 235000015110 jellies Nutrition 0.000 description 11
- 239000008274 jelly Substances 0.000 description 11
- 230000000694 effects Effects 0.000 description 9
- 230000002779 inactivation Effects 0.000 description 9
- 238000001179 sorption measurement Methods 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 241001465754 Metazoa Species 0.000 description 4
- 238000006555 catalytic reaction Methods 0.000 description 4
- 239000000084 colloidal system Substances 0.000 description 3
- 238000010981 drying operation Methods 0.000 description 3
- 230000002255 enzymatic effect Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000002791 soaking Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000007791 dehumidification Methods 0.000 description 2
- 125000000404 glutamine group Chemical group N[C@@H](CCC(N)=O)C(=O)* 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 229940009493 gel-one Drugs 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000000415 inactivating effect Effects 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
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Abstract
本发明公开了一种夹流体芯咀嚼凝胶糖果的制备方法,夹流体芯咀嚼凝胶糖果的皮料的主凝胶剂为明胶,制备方法的步骤包括蛋白质交联的步骤,蛋白质交联的步骤是将成型完成的夹流体芯咀嚼凝胶糖果浸泡入谷氨酰胺转胺酶水溶液中进行谷氨酰胺转胺酶吸附后进行蛋白质交联。本发明的制备方法的步骤包括蛋白质交联的步骤,蛋白质交联是通过谷氨酰胺转胺酶水溶液将皮料明胶中的小分子蛋白质交联成为大分子的蛋白质,提高糖果皮料的熔点、韧性和口感,不易粘连和熔化,糖果产品口感柔软、富有弹性。产品不易受外部环境影响,操作过程简便高效,设备成本低,具有极佳的推广使用意义,能够产生较大的经济效益。The invention discloses a preparation method of a chewable gel candy with a fluid core. The main gelling agent of the leather of the chewable gel candy with a fluid core is gelatin. The steps of the preparation method include a protein cross-linking step. The method comprises the steps of immersing the molded chewing gel candy with a fluid core in an aqueous solution of transglutaminase to absorb the transglutaminase and then carry out protein cross-linking. The steps of the preparation method of the present invention include the step of protein crosslinking. The protein crosslinking is to crosslink the small molecular protein in the skin gelatin into a macromolecular protein through an aqueous solution of transglutaminase to increase the melting point of the candy skin, Toughness and taste, not easy to stick and melt, soft and elastic confectionary products. The product is not easily affected by the external environment, the operation process is simple and efficient, and the equipment cost is low. It has excellent promotion and use significance and can generate greater economic benefits.
Description
技术领域 technical field
本发明涉及一种糖果的制备方法,具体涉及一种夹流体芯咀嚼凝胶糖果的制备方法。 The invention relates to a preparation method of a candy, in particular to a preparation method of a chewable gel candy with a fluid core.
背景技术 Background technique
咀嚼凝胶糖果是一种水分含量较高、柔软、有弹性和韧性的糖果,从凝胶剂使用上分类,分为以动物性胶体为主凝胶剂咀嚼凝胶糖果和以植物性胶体为主凝胶剂咀嚼凝胶糖果,而市场上最为普遍的是以动物性胶体为主凝胶剂的凝胶糖果,此类糖果表现出的弹性和韧性最强,是最受欢迎的咀嚼凝胶糖果之一。动物性凝胶剂目前均指明胶,明胶是由动物的皮或骨头经酸、碱、酶等方法将大分子蛋白质降解为可溶性小分子蛋白质的一类蛋白,其熔点较低,由明胶为主凝胶剂制成的咀嚼凝胶糖果如果水分含量偏高,在较高温度的环境中就会软化,甚至熔化、粘连。 Chewing gel candy is a kind of candy with high moisture content, softness, elasticity and toughness. From the use of gel agent, it can be divided into chewing gel candy with animal colloid as the main gel agent and vegetable colloid as the main gel. The main gelling agent is chewing gel candy, and the most common gel candy on the market is the gel candy with animal colloid as the main gelling agent. This type of candy shows the strongest elasticity and toughness, and is the most popular chewing gel One of the candies. Animal gels currently refer to glue. Gelatin is a type of protein that degrades large molecular proteins into soluble small molecular proteins by the skin or bones of animals through acid, alkali, enzymes, etc. It has a low melting point and is mainly composed of gelatin. If the water content of the chewing jelly candy made of gel is too high, it will soften, even melt and stick together in a higher temperature environment.
由于由明胶作为主凝胶剂制成的咀嚼凝胶糖果是目前最具弹性和韧性的咀嚼凝胶糖果之一,所以夹流体芯凝胶糖果目前皮料也都是以明胶为主凝胶剂,但由于由明胶作为主凝胶剂的咀嚼凝胶糖果在皮料水分偏高时会软化,造成产品粘连、漏陷,而皮料水分偏低时,明胶会变硬,造成产品咀嚼困难,口感差,所以目前市场上很难见到夹流体芯咀嚼软糖销售。 Since the chewing gel candy made of gelatin as the main gelling agent is currently one of the most elastic and tough chewing gel candies, the core gel candy is currently made of gelatin as the main gelling agent. , but because the chewing gel candy with gelatin as the main gelling agent will soften when the moisture content of the leather material is high, resulting in product adhesion and leakage, and when the moisture content of the leather material is low, the gelatin will harden, making the product difficult to chew. The taste is poor, so it is difficult to see chewing gummies with fluid cores on the market at present.
谷氨酰胺转胺酶是一种能使蛋白质分子发生交联,使蛋白质分子由小变大的一种食品酶制剂,谷氨酰胺转胺酶催化的是蛋白质中谷氨酰胺残基发生的反应,而明胶中含有丰富的谷氨酰胺残基;通过谷氨酰胺转胺酶的催化作用,明胶中的低熔点小分子蛋白质交联成高熔点大分子蛋白质。谷氨酰胺转胺酶目前在肉类制品中应用已非常广泛,但在糖果中应用善未见报道,如果能将谷氨酰胺转胺酶的特性应用到夹流体芯咀嚼凝胶糖果中,必将能解决目前夹流体芯凝胶糖果易熔化、粘连、漏陷的缺点,为糖果市场增加一个新亮点。 Transglutaminase is a food enzyme preparation that can cross-link protein molecules and make protein molecules from small to large. Transglutaminase catalyzes the reaction of glutamine residues in proteins. Gelatin is rich in glutamine residues; through the catalysis of transglutaminase, small molecular proteins with low melting points in gelatin are cross-linked into large molecular proteins with high melting points. Transglutaminase has been widely used in meat products, but it has not been reported in candy. If the characteristics of transglutaminase can be applied to chewing gel candy with fluid core, it must be It will be able to solve the shortcomings of the current sandwich gel candy that is easy to melt, stick and leak, and add a new bright spot to the candy market.
发明内容 Contents of the invention
本发明需要解决的技术问题就在于克服现有技术的缺陷,提供一种夹流体芯咀嚼凝胶糖果的制备方法。该制备方法克服了现有夹流体芯凝胶糖果易熔化、粘连、漏陷的缺点,通过谷氨酰胺转胺酶的催化作用,将夹流体芯凝胶糖果皮料中的明胶中的低熔点小分子蛋白质交联成高熔点大分子蛋白质,使夹流体芯凝胶糖果皮料的熔点大大提高,同时韧性也相对提高,产品不易受外部环境影响,不易熔化、粘连、漏陷,且产品口感柔软、富有弹性,具有极佳的食用效果和产品竞争力。 The technical problem to be solved by the present invention is to overcome the defects of the prior art and provide a method for preparing chewable jelly candy with a fluid core. The preparation method overcomes the shortcomings of the existing fluid core gel candy that is easy to melt, stick and leak, and through the catalysis of transglutaminase, the low melting point of the gelatin in the fluid core gel candy skin The small molecular protein is cross-linked into a high melting point macromolecular protein, which greatly increases the melting point of the sandwich gel candy skin, and at the same time, the toughness is also relatively improved. The product is not easily affected by the external environment, and is not easy to melt, stick, and leak. Soft and elastic, with excellent eating effect and product competitiveness.
为解决上述问题,本发明采用的技术方案为: In order to solve the above problems, the technical solution adopted in the present invention is:
一种夹流体芯咀嚼凝胶糖果的制备方法,夹流体芯咀嚼凝胶糖果的皮料的主凝胶剂为明胶,所述制备方法的步骤包括蛋白质交联的步骤,所述蛋白质交联的步骤是将成型完成的夹流体芯咀嚼凝胶糖果浸泡入谷氨酰胺转胺酶水溶液中进行谷氨酰胺转胺酶吸附后进行蛋白质交联。蛋白质交联是通过谷氨酰胺转胺酶水溶液将皮料明胶中的小分子蛋白质交联成为大分子的蛋白质,提高糖果皮料的熔点、韧性和口感,不易粘连和熔化,糖果产品口感柔软、富有弹性。 A method for preparing a chewable gel candy with a fluid core, the main gelling agent of the skin of the chewable gel candy with a fluid core is gelatin, the steps of the preparation method include a protein cross-linking step, the protein cross-linked The method comprises the steps of immersing the molded chewing gel candy with a fluid core in an aqueous solution of transglutaminase to absorb the transglutaminase and then carry out protein cross-linking. Protein cross-linking is to cross-link the small molecular protein in the leather gelatin into a macromolecular protein through an aqueous solution of transglutaminase, which improves the melting point, toughness and taste of the candy leather, and is not easy to stick and melt. The taste of the candy product is soft and smooth. elastic.
优选的,夹流体芯咀嚼凝胶糖果的皮料中作为主凝胶剂的明胶的质量含量为12%~14%。通过实验验证,该含量的明胶的皮料,能被谷氨酰胺转胺酶交联,且具有最佳的韧性和口感。含量低时交联效果不好或基本达不到交联后提高熔点的效果,含量高时口感会太硬,因此明胶的质量含量为12%~14%为最佳的含量比例。 Preferably, the mass content of gelatin as the main gelling agent in the leather of the chewing jelly candy with a fluid core is 12% to 14%. It is verified by experiments that the gelatin leather with this content can be cross-linked by transglutaminase, and has the best toughness and mouthfeel. When the content is low, the cross-linking effect is not good or the effect of increasing the melting point after cross-linking cannot be achieved basically. When the content is high, the taste will be too hard. Therefore, the mass content of gelatin is 12% to 14% as the best content ratio.
优选的,夹流体芯咀嚼凝胶糖果皮料的pH值为3.8~4.5。 Preferably, the pH value of the chewable gel candy shell with the fluid core is 3.8-4.5.
优选的,谷氨酰胺转胺酶水溶液的pH值为8~9。 Preferably, the pH value of the transglutaminase aqueous solution is 8-9.
优选的,成型完成的夹流体芯咀嚼凝胶糖果的皮料中水分含量为12%~14%。 Preferably, the moisture content in the leather of the formed chewing gel candy with a fluid core is 12% to 14%.
优选的,夹流体芯咀嚼凝胶糖果的内容物是水溶性内容物或油溶性内容物。 Preferably, the content of the chewable jelly candy with a fluid core is a water-soluble content or an oil-soluble content.
夹流体芯咀嚼凝胶糖果的制备方法的具体步骤为: The specific steps of the preparation method of the chewable gel candy with a fluid core are:
(1)谷氨酰胺转胺酶吸附:将成型完成的夹流体芯咀嚼凝胶糖果,送入谷氨酰胺转胺酶水溶液中浸泡;将谷氨酰胺转胺酶吸附在皮料中,使谷氨酰胺转胺酶与明胶中的蛋白质分子接触; (1) Adsorption of transglutaminase: Put the formed chewable gel candy with fluid core into transglutaminase aqueous solution for soaking; adsorb transglutaminase in the leather to make glutamine amidotransaminase contacts protein molecules in gelatin;
(2)蛋白质交联:将浸泡完成的夹流体芯咀嚼凝胶糖果送入网带式输送抽湿干燥箱中进行干燥处理,干燥至表面干爽,然后将夹流体芯咀嚼凝胶糖果用食用防粘油抛光,防止粘连而影响糖果产品质量;然后加热进行蛋白质交联,加热后,谷氨酰胺转胺酶的活性提高,使明胶中的小分子蛋白质发生交联产生大分子的蛋白质,提高糖果皮料的熔点、韧性和口感,不易粘连和熔化,糖果产品口感柔软、富有弹性; (2) Protein cross-linking: send the soaked chewing gel candy with fluid core into the mesh belt conveying dehumidification drying box for drying treatment until the surface is dry, and then put the chewing gel candy with fluid core into the food-proof Polishing with viscous oil to prevent sticking and affect the quality of candy products; then heating to carry out protein cross-linking, after heating, the activity of transglutaminase is increased, so that small molecular proteins in gelatin are cross-linked to produce large molecular proteins, improving the quality of candy The melting point, toughness and taste of leather are not easy to stick and melt, and the taste of candy products is soft and elastic;
(3)灭酶冷却:将蛋白质交联完成的夹流体芯咀嚼凝胶糖果送入网带式输送热风循环箱中高温灭酶,将谷氨酰胺转胺酶的活性丧失,避免其在产品存储过程中造成产品变质;然后冷却干燥,得到夹流体芯咀嚼凝胶糖果产品。 (3) Enzyme inactivation and cooling: send the chewing gel candy with fluid core that has completed the protein cross-linking into the mesh belt conveying hot air circulation box to inactivate the enzyme at high temperature, so as to lose the activity of transglutaminase and prevent it from being stored in the product. The product deteriorates during the process; then it is cooled and dried to obtain a chewable gel candy product with a fluid core.
优选的,谷氨酰胺转胺酶吸附的步骤中,谷氨酰胺转胺酶水溶液的温度为2℃~6℃,浓度为10000U/kg~15000U/kg;夹流体芯咀嚼凝胶糖果在谷氨酰胺转胺酶水溶液中的浸泡时间为120秒~180秒。 Preferably, in the step of transglutaminase adsorption, the temperature of the transglutaminase aqueous solution is 2°C-6°C, and the concentration is 10000U/kg-15000U/kg; The soaking time in the amidotransaminase aqueous solution is 120 seconds to 180 seconds.
优选的,蛋白质交联步骤中,干燥处理的温度10℃~20℃,湿度为35%~45%,干燥时间为20分钟~25分钟; Preferably, in the protein cross-linking step, the drying temperature is 10°C-20°C, the humidity is 35%-45%, and the drying time is 20 minutes-25 minutes;
蛋白质交联步骤中,用夹流体芯咀嚼凝胶糖果总质量的0.2%~0.3%的食用防粘油抛光夹流体芯咀嚼凝胶糖果,蛋白质交联的温度为38℃~40℃,湿度70%~75%环境中进行蛋白质交联60分钟~80分钟。 In the protein cross-linking step, use 0.2% to 0.3% of the total mass of the chewing gel candy with a fluid core to polish the edible anti-sticking oil and polish the chewing gel candy with a fluid core. Perform protein cross-linking in an environment of % to 75% for 60 minutes to 80 minutes.
优选的,灭酶冷却步骤中,夹流体芯咀嚼凝胶糖果送入网带式输送热风循环箱中灭酶的时间为40秒~60秒,灭酶条件为温度78℃~80℃,湿度70%~75%;冷却干燥的操作条件为温度10℃~20℃,湿度50%~55%,冷却干燥至皮料中的水分含量为20%~22%。 Preferably, in the enzyme-inactivating cooling step, the time for the chewing gel candy with the fluid core to be sent to the mesh-belt conveying hot air circulation box to inactivate the enzyme is 40 seconds to 60 seconds, and the conditions for inactivating the enzyme are a temperature of 78°C to 80°C and a humidity of 70°C. %~75%; the operating conditions for cooling and drying are temperature 10°C~20°C, humidity 50%~55%, and cooling and drying until the moisture content in the leather is 20%~22%.
本发明的优点和有益效果为: Advantage of the present invention and beneficial effect are:
本发明夹流体芯咀嚼凝胶糖果的制备方法,该制备方法克服了现有夹流体芯凝胶糖果易熔化、粘连、漏陷的缺点,通过谷氨酰胺转胺酶的催化作用,将夹流体芯凝胶糖果皮料中的明胶中的低熔点小分子蛋白质交联成高熔点大分子蛋白质,使夹流体芯凝胶糖果皮料的熔点大大提高,同时韧性也相对提高; The preparation method of the chewable gel candy with a fluid core of the present invention overcomes the shortcomings of the existing gel candy with a fluid core that is easy to melt, stick, and leaks, and through the catalysis of transglutaminase, the fluid can be The low-melting-point small molecular protein in the gelatin in the core gel candy skin is cross-linked into a high-melting point macromolecular protein, which greatly increases the melting point of the sandwich core gel candy skin, and at the same time the toughness is relatively improved;
本发明夹流体芯咀嚼凝胶糖果的制备方法,产品不易受外部环境影响,不易熔化、粘连、漏陷,且产品口感柔软、富有弹性,具有极佳的食用效果和产品竞争力; The preparation method of the chewing gel candy with a fluid core of the present invention is not easily affected by the external environment, and is not easy to melt, stick, or leak, and the product has a soft and elastic taste, and has excellent eating effect and product competitiveness;
本发明夹流体芯咀嚼凝胶糖果的制备方法,操作过程简便高效,设备成本低,能够在大多数糖果生产企业进行生产,具有极佳的推广使用意义,能够产生较大的经济效益和产品竞争力。 The preparation method of chewing gel candy with fluid core of the present invention has simple and efficient operation process, low equipment cost, can be produced in most candy production enterprises, has excellent promotion and use significance, and can generate greater economic benefits and product competition force.
具体实施方式 Detailed ways
下列实施例将进一步说明本发明。 The following examples further illustrate the invention.
实施例1Example 1
本发明采用技术方案为一种夹流体芯咀嚼凝胶糖果的制备方法,该制备方法的具体步骤为: The technical solution adopted by the present invention is a preparation method of a chewable gel candy with a fluid core, and the specific steps of the preparation method are:
(1)谷氨酰胺转胺酶吸附:将成型完成的夹流体芯咀嚼凝胶糖果,送入谷氨酰胺转胺酶水溶液中浸泡;将谷氨酰胺转胺酶吸附在皮料中,使谷氨酰胺转胺酶与明胶中的蛋白质分子接触; (1) Adsorption of transglutaminase: Put the formed chewable gel candy with fluid core into transglutaminase aqueous solution for soaking; adsorb transglutaminase in the leather to make glutamine amidotransaminase contacts protein molecules in gelatin;
谷氨酰胺转胺酶水溶液的温度为2℃,浓度为15000U/kg;夹流体芯咀嚼凝胶糖果在谷氨酰胺转胺酶水溶液中的浸泡时间为180秒。 The temperature of the transglutaminase aqueous solution is 2° C., and the concentration is 15000 U/kg; the immersion time of the chewable gel candy with the fluid core in the transglutaminase aqueous solution is 180 seconds.
(2)蛋白质交联:将浸泡完成的夹流体芯咀嚼凝胶糖果送入网带式输送抽湿干燥箱中进行干燥处理,干燥至表面干爽,然后将夹流体芯咀嚼凝胶糖果用食用防粘油抛光,防止粘连而影响糖果产品质量;然后加热进行蛋白质交联,加热后,谷氨酰胺转胺酶的活性提高,使明胶中的小分子蛋白质发生交联产生大分子的蛋白质,提高糖果皮料的熔点、韧性和口感,不易粘连和熔化,糖果产品口感柔软、富有弹性; (2) Protein cross-linking: send the soaked chewing gel candy with fluid core into the mesh belt conveying dehumidification drying box for drying treatment until the surface is dry, and then put the chewing gel candy with fluid core into the food-proof Polishing with viscous oil to prevent sticking and affect the quality of candy products; then heating to carry out protein cross-linking, after heating, the activity of transglutaminase is increased, so that small molecular proteins in gelatin are cross-linked to produce large molecular proteins, improving the quality of candy The melting point, toughness and taste of leather are not easy to stick and melt, and the taste of candy products is soft and elastic;
蛋白质交联步骤中,干燥处理的温度10℃,湿度为35%,干燥时间为25分钟;用夹流体芯咀嚼凝胶糖果总质量的0.2%的食用防粘油抛光夹流体芯咀嚼凝胶糖果,蛋白质交联的温度为38℃,湿度70%环境中进行蛋白质交联80分钟。 In the protein cross-linking step, the temperature of the drying treatment is 10°C, the humidity is 35%, and the drying time is 25 minutes; use 0.2% of the total mass of the chewable gel candy with the fluid core to polish the edible anti-sticking oil and polish the chewable gel candy with the fluid core , the protein cross-linking temperature was 38°C, and the protein cross-linking was carried out in an environment with a humidity of 70% for 80 minutes.
(3)灭酶冷却:将蛋白质交联完成的夹流体芯咀嚼凝胶糖果送入网带式输送热风循环箱中高温灭酶,将谷氨酰胺转胺酶的活性丧失,避免其在产品存储过程中造成产品变质;然后冷却干燥,得到夹流体芯咀嚼凝胶糖果产品。本步骤中,夹流体芯咀嚼凝胶糖果送入网带式输送热风循环箱中灭酶的时间为40秒,灭酶条件为温度80℃,湿度70%;冷却干燥的操作条件为温度10℃,湿度50%,冷却干燥至皮料中的水分含量为20%。 (3) Enzyme inactivation and cooling: send the chewing gel candy with fluid core that has completed the protein cross-linking into the mesh belt conveying hot air circulation box to inactivate the enzyme at high temperature, so as to lose the activity of transglutaminase and prevent it from being stored in the product. The product deteriorates during the process; then it is cooled and dried to obtain a chewable gel candy product with a fluid core. In this step, the chewing gel candy with the fluid core is sent to the mesh belt conveying hot air circulation box for 40 seconds to inactivate the enzyme, and the enzyme inactivation condition is a temperature of 80°C and a humidity of 70%; the operating condition of cooling and drying is a temperature of 10°C , humidity 50%, cooling and drying until the moisture content in the leather is 20%.
本实施例的制备方法中,夹流体芯咀嚼凝胶糖果的皮料的主凝胶剂为明胶,夹流体芯咀嚼凝胶糖果的皮料中作为主凝胶剂的明胶的质量含量为12%。夹流体芯咀嚼凝胶糖果皮料的pH值为3.8。谷氨酰胺转胺酶水溶液的pH值为8。成型完成的夹流体芯咀嚼凝胶糖果的皮料中水分含量为12%。夹流体芯咀嚼凝胶糖果的内容物是水溶性内容物。 In the preparation method of this embodiment, the main gelling agent of the skin of the chewing gel candy with a fluid core is gelatin, and the mass content of the gelatin as the main gelling agent in the skin of the chewing gel candy with a fluid core is 12% . The pH of the sandwiched chewable gel candy shell is 3.8. The pH value of the transglutaminase aqueous solution was 8. The moisture content in the leather of the formed sandwich fluid core chewing gel candy is 12%. The contents of the fluid core chewable gel candy are water soluble contents.
实施例2Example 2
在实施例1的基础上,本发明夹流体芯咀嚼凝胶糖果的制备方法的另一种实施例的步骤为: On the basis of Example 1, the steps of another embodiment of the preparation method of the chewable jelly candy with a fluid core of the present invention are as follows:
(1)谷氨酰胺转胺酶吸附步骤中:谷氨酰胺转胺酶水溶液的温度为6℃,浓度为10000U/kg;夹流体芯咀嚼凝胶糖果在谷氨酰胺转胺酶水溶液中的浸泡时间为120秒。 (1) In the transglutaminase adsorption step: the temperature of the transglutaminase aqueous solution is 6°C, and the concentration is 10000U/kg; The time is 120 seconds.
(2)蛋白质交联步骤中:干燥处理的温度20℃,湿度为45%,干燥时间为20分钟;用夹流体芯咀嚼凝胶糖果总质量的0.3%的食用防粘油抛光夹流体芯咀嚼凝胶糖果,蛋白质交联的温度为40℃,湿度75%环境中进行蛋白质交联60分钟。 (2) In the protein cross-linking step: the temperature of the drying treatment is 20°C, the humidity is 45%, and the drying time is 20 minutes; chewing with 0.3% of the total mass of the gel candy with an edible anti-sticking oil and polishing with a fluid core For gel candy, the temperature for protein cross-linking is 40°C and the humidity is 75% for 60 minutes.
(3)灭酶冷却步骤中:夹流体芯咀嚼凝胶糖果送入网带式输送热风循环箱中灭酶的时间为60秒,灭酶条件为温度80℃,湿度75%;冷却干燥的操作条件为温度20℃,湿度55%,冷却干燥至皮料中的水分含量为22%。 (3) In the cooling step of enzyme inactivation: the chewing gel candy with fluid core is sent to the mesh belt conveying hot air circulation box for 60 seconds to inactivate the enzyme, and the enzymatic inactivation conditions are temperature 80°C, humidity 75%; cooling and drying operation The conditions are temperature 20°C, humidity 55%, cooling and drying until the moisture content in the leather is 22%.
本实施例的制备方法中,夹流体芯咀嚼凝胶糖果的皮料中作为主凝胶剂的明胶的质量含量为14%。夹流体芯咀嚼凝胶糖果皮料的pH值为4.5。谷氨酰胺转胺酶水溶液的pH值为9。成型完成的夹流体芯咀嚼凝胶糖果的皮料中水分含量为14%。夹流体芯咀嚼凝胶糖果的内容物是油溶性内容物。 In the preparation method of this embodiment, the mass content of gelatin as the main gelling agent in the leather of the chewable jelly candy with a fluid core is 14%. The pH of the sandwiched chewable gel candy shell is 4.5. The pH value of the transglutaminase aqueous solution is 9. The moisture content in the leather of the formed sandwich fluid core chewing gel candy is 14%. The contents of the fluid core chewable gel candy are oil soluble contents.
其他部分与实施例1完全相同。 Other parts are identical with embodiment 1.
实施例3Example 3
在实施例1的基础上,本发明夹流体芯咀嚼凝胶糖果的制备方法的另一种实施例的步骤为: On the basis of Example 1, the steps of another embodiment of the preparation method of the chewable jelly candy with a fluid core of the present invention are as follows:
(1)谷氨酰胺转胺酶吸附步骤中:谷氨酰胺转胺酶水溶液的温度为4℃,浓度为12500U/kg;夹流体芯咀嚼凝胶糖果在谷氨酰胺转胺酶水溶液中的浸泡时间为150秒。 (1) In the transglutaminase adsorption step: the temperature of the transglutaminase aqueous solution is 4°C, and the concentration is 12500U/kg; The time is 150 seconds.
(2)蛋白质交联步骤中:干燥处理的温度15℃,湿度为40%,干燥时间为22分钟;用夹流体芯咀嚼凝胶糖果总质量的0.25%的食用防粘油抛光夹流体芯咀嚼凝胶糖果,蛋白质交联的温度为39℃,湿度72%环境中进行蛋白质交联70分钟。 (2) In the protein cross-linking step: the temperature of the drying treatment is 15°C, the humidity is 40%, and the drying time is 22 minutes; the edible anti-sticking oil is used for chewing with a fluid core of 0.25% of the total mass of the gel candy. For gel candy, the temperature for protein cross-linking is 39°C and the humidity is 72% for 70 minutes.
(3)灭酶冷却步骤中:夹流体芯咀嚼凝胶糖果送入网带式输送热风循环箱中灭酶的时间为50秒,灭酶条件为温度79℃,湿度72%;冷却干燥的操作条件为温度15℃,湿度52%,冷却干燥至皮料中的水分含量为21%。 (3) In the cooling step of enzyme inactivation: the chewing gel candy with fluid core is sent to the mesh belt conveying hot air circulation box for 50 seconds to inactivate the enzyme, and the enzymatic inactivation conditions are temperature 79°C, humidity 72%; cooling and drying operation The conditions are temperature 15°C, humidity 52%, cooling and drying until the moisture content in the leather is 21%.
本实施例的制备方法中,夹流体芯咀嚼凝胶糖果的皮料中作为主凝胶剂的明胶的质量含量为13%。夹流体芯咀嚼凝胶糖果皮料的pH值为4.2。谷氨酰胺转胺酶水溶液的pH值为8.5。成型完成的夹流体芯咀嚼凝胶糖果的皮料中水分含量为13%。夹流体芯咀嚼凝胶糖果的内容物是水溶性内容物。 In the preparation method of this embodiment, the mass content of gelatin as the main gelling agent in the leather of the chewable jelly candy with a fluid core is 13%. The pH of the sandwiched chewable gel candy shell is 4.2. The pH value of the transglutaminase aqueous solution was 8.5. The moisture content in the leather of the formed sandwich fluid core chewing gel candy is 13%. The contents of the fluid core chewable gel candy are water soluble contents.
其他部分与实施例1完全相同。 Other parts are identical with embodiment 1.
实施例4Example 4
在实施例1的基础上,本发明夹流体芯咀嚼凝胶糖果的制备方法的另一种实施例的步骤为: On the basis of Example 1, the steps of another embodiment of the preparation method of the chewable jelly candy with a fluid core of the present invention are as follows:
(1)谷氨酰胺转胺酶吸附步骤中:谷氨酰胺转胺酶水溶液的温度为5℃,浓度为14000U/kg;夹流体芯咀嚼凝胶糖果在谷氨酰胺转胺酶水溶液中的浸泡时间为150秒。 (1) In the transglutaminase adsorption step: the temperature of the transglutaminase aqueous solution is 5°C, and the concentration is 14000U/kg; The time is 150 seconds.
(2)蛋白质交联步骤中:干燥处理的温度17℃,湿度为41%,干燥时间为4分钟;用夹流体芯咀嚼凝胶糖果总质量的0.27%的食用防粘油抛光夹流体芯咀嚼凝胶糖果,蛋白质交联的温度为38.5℃,湿度74%环境中进行蛋白质交联74分钟。 (2) In the protein cross-linking step: the temperature of the drying treatment is 17°C, the humidity is 41%, and the drying time is 4 minutes; the edible anti-sticking oil is used for chewing with a fluid core of 0.27% of the total mass of the gel candy. For gel candy, the temperature of protein cross-linking is 38.5°C, and the temperature of protein cross-linking is 74% for 74 minutes.
(3)灭酶冷却步骤中:夹流体芯咀嚼凝胶糖果送入网带式输送热风循环箱中灭酶的时间为55秒,灭酶条件为温度79℃,湿度74%;冷却干燥的操作条件为温度17℃,湿度54%,冷却干燥至皮料中的水分含量为21%。 (3) In the cooling step of enzyme inactivation: the chewing gel candy with fluid core is sent to the mesh belt conveying hot air circulation box for 55 seconds to inactivate the enzyme, and the enzymatic inactivation conditions are temperature 79°C, humidity 74%; cooling and drying operation The conditions are temperature 17°C, humidity 54%, cooling and drying until the moisture content in the leather is 21%.
本实施例的制备方法中,夹流体芯咀嚼凝胶糖果的皮料中作为主凝胶剂的明胶的质量含量为14%。夹流体芯咀嚼凝胶糖果皮料的pH值为4.3。谷氨酰胺转胺酶水溶液的pH值为8。成型完成的夹流体芯咀嚼凝胶糖果的皮料中水分含量为12%。夹流体芯咀嚼凝胶糖果的内容物是水溶性内容物。 In the preparation method of this embodiment, the mass content of gelatin as the main gelling agent in the leather of the chewable jelly candy with a fluid core is 14%. The pH of the sandwiched chewable gel candy shell is 4.3. The pH value of the transglutaminase aqueous solution was 8. The moisture content in the leather of the formed sandwich fluid core chewing gel candy is 12%. The contents of the fluid core chewable gel candy are water soluble contents.
其他部分与实施例1完全相同。 Other parts are identical with embodiment 1.
对比例comparative example
在实施例1的基础上,将谷氨酰胺转胺酶吸附步骤中的谷氨酰胺转胺酶水溶液更换为纯净水,其他部分与实施例1完全相同。本对比例得到的夹流体芯咀嚼凝胶糖果易熔化、粘连、漏陷,熔点和韧性较低,产品易受外部环境影响,产品口感不佳。 On the basis of Example 1, the transglutaminase aqueous solution in the transglutaminase adsorption step was replaced with pure water, and the other parts were exactly the same as in Example 1. The chewable jelly candy with a fluid core obtained in this comparative example is easy to melt, stick and leak, has a low melting point and toughness, is easily affected by the external environment, and has a poor taste.
综上,本发明的夹流体芯凝胶糖果的制备方法,其制备的糖果产品由于采用谷氨酰胺转胺酶进行蛋白质交联,使糖果产品克服了现有夹流体芯凝胶糖果易熔化、粘连、漏陷的缺点,通过谷氨酰胺转胺酶的催化作用,将夹流体芯凝胶糖果皮料中的明胶中的低熔点小分子蛋白质交联成高熔点大分子蛋白质,使夹流体芯凝胶糖果皮料的熔点大大提高,同时韧性也相对提高;产品不易受外部环境影响,不易熔化、粘连、漏陷,且产品口感柔软、富有弹性,具有极佳的食用效果和产品竞争力;同时,本发明的方法操作过程简便高效,设备成本低,能够在大多数糖果生产企业进行生产,具有极佳的推广使用意义,能够产生较大的经济效益和产品竞争力。 To sum up, the preparation method of the gel candy with a fluid core of the present invention, the candy product prepared by it adopts transglutaminase to carry out protein cross-linking, so that the candy product overcomes the easy melting of the existing gel candy with a fluid core. For the shortcomings of adhesion and leakage, through the catalysis of transglutaminase, the low melting point small molecular protein in the gelatin in the sandwich gel candy skin is cross-linked into a high melting point macromolecular protein, making the sandwich core The melting point of the gel candy skin material is greatly improved, and the toughness is also relatively improved; the product is not easily affected by the external environment, and is not easy to melt, stick, and leak, and the product tastes soft and elastic, with excellent eating effect and product competitiveness; At the same time, the method of the present invention has simple and efficient operation process, low equipment cost, can be produced in most candy production enterprises, has excellent popularization and use significance, and can generate greater economic benefits and product competitiveness.
最后应说明的是:显然,上述实施例仅仅是为清楚地说明本发明所作的举例,而并非对实施方式的限定。对于所属领域的普通技术人员来说,在上述说明的基础上还可以做出其它不同形式的变化或变动。这里无需也无法对所有的实施方式予以穷举。而由此所引申出的显而易见的变化或变动仍处于本发明的保护范围之中。 Finally, it should be noted that obviously, the above-mentioned embodiments are only examples for clearly illustrating the present invention, rather than limiting the implementation. For those of ordinary skill in the art, on the basis of the above description, other changes or changes in different forms can also be made. It is not necessary and impossible to exhaustively list all the implementation manners here. However, the obvious changes or variations derived therefrom are still within the protection scope of the present invention.
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