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CN104450510B - Cosmetics, food, chemical industry and agricultural biology surfactant microemulsion production system - Google Patents

Cosmetics, food, chemical industry and agricultural biology surfactant microemulsion production system Download PDF

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CN104450510B
CN104450510B CN201410650537.2A CN201410650537A CN104450510B CN 104450510 B CN104450510 B CN 104450510B CN 201410650537 A CN201410650537 A CN 201410650537A CN 104450510 B CN104450510 B CN 104450510B
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liquid
fermentation
kettle
biosurfactant
storage tank
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CN104450510A (en
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程叶红
谢宗桂
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Guangdong Gaohang Intellectual Property Operation Co ltd
Zhuhai Jiahong Technology Co ltd
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Individual
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Priority to CN201610017019.6A priority Critical patent/CN105879816B/en
Priority to CN201610016996.4A priority patent/CN105647787B/en
Priority to CN201610016998.3A priority patent/CN105505758B/en
Priority to CN201410650537.2A priority patent/CN104450510B/en
Priority to CN201610015251.6A priority patent/CN105543074B/en
Priority to CN201610017018.1A priority patent/CN105543076B/en
Priority to CN201610015551.4A priority patent/CN105505748B/en
Priority to CN201610016980.3A priority patent/CN105505757B/en
Priority to CN201610017017.7A priority patent/CN105482997B/en
Application filed by Individual filed Critical Individual
Priority to CN201610015244.6A priority patent/CN105420094B/en
Priority to CN201610014953.2A priority patent/CN105420093B/en
Priority to CN201610017026.6A priority patent/CN105543077B/en
Priority to CN201610017016.2A priority patent/CN105543075B/en
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Abstract

本发明涉及一种化妆品、食品、化工及农业用生物表活剂微乳液生产系统，用于微生物发酵生产生物表面活性剂的发酵釜；用于对发酵釜中的发酵液进行纯化分离处理的发酵液纯化设备以及用于储放纯化后的生物表面活性剂的生物表面活性剂储罐；分别用于储放助表面活性剂、碱液、水相以及油相的助表面活性剂储罐、碱液储罐、水相储罐以及油相储罐；以及表面活性剂混合液配制釜和微乳状液反应釜。上述技术方案中提供的化妆品、食品、化工及农业用生物表活剂微乳液生产系统，通过对发酵液进行纯化以及微乳化处理，从而快速制得生物表面活性剂的微乳状液。

The invention relates to a biosurfactant microemulsion production system for cosmetics, food, chemical industry and agriculture, a fermentation kettle used for microbial fermentation to produce biosurfactants; a fermentation tank used for purifying and separating the fermentation liquid in the fermentation kettle Liquid purification equipment and biosurfactant storage tanks for storing purified biosurfactants; cosurfactant storage tanks, alkali liquid storage tank, water phase storage tank and oil phase storage tank; and surfactant mixed liquid preparation kettle and microemulsion liquid reaction kettle. The biosurfactant microemulsion production system for cosmetics, food, chemical industry and agriculture provided in the above technical solution can quickly prepare the microemulsion of biosurfactant by purifying and microemulsifying the fermented liquid.

Description

化妆品、食品、化工及农业用生物表活剂微乳液生产系统Biosurfactant Microemulsion Production System for Cosmetics, Food, Chemical Industry and Agriculture

技术领域technical field

本发明涉及乳化剂生产领域，具体涉及一种化妆品、食品、化工及农业用生物表活剂微乳液生产系统。The invention relates to the field of emulsifier production, in particular to a production system of biosurfactant microemulsion for cosmetics, food, chemical industry and agriculture.

背景技术Background technique

微乳状液为透明或半透明的自发形成的热力学稳定体系，有水包油和油包水两种类型。微乳状液的形成是自发的，不需要外界提供能量，是一种热力学非常稳定的体系，因此在石油化工、化妆品、食品等领域被广泛的采用。其中，由生物表面活性剂制备的微乳状液常用于高档化妆品，其更稳定、安全性高、皮肤吸收性好。该类微乳状液的制备方法为：将生物表面活性剂(脂肽类生物表面活性剂)、助表面活性剂(C3～C5醇)与碱(氢氧化钠)混合配制成表面活性剂混合液，配制水相(一般为盐水)，配制油相(一般为烷烃、环烷烃、芳香烃)；把配制好的表面活性剂混合液加入水相中混合均匀，然后将油相逐滴滴入上述溶液中，并不断搅拌均匀，直到溶液由浑浊到澄清，即制得由生物表面活性剂组成的微乳状液，由于需要采用逐滴滴加油相，因此使得微乳状液的生产速率底，严重影响产品生产速率。Microemulsions are transparent or translucent spontaneously formed thermodynamically stable systems, and there are two types: oil-in-water and water-in-oil. The formation of microemulsion is spontaneous and does not require external energy. It is a thermodynamically very stable system, so it is widely used in petrochemical, cosmetics, food and other fields. Among them, microemulsions prepared by biosurfactants are often used in high-end cosmetics, which are more stable, high in safety, and good in skin absorption. The preparation method of this type of microemulsion is: mix biosurfactant (lipopeptide biosurfactant), co-surfactant (C3-C5 alcohol) and alkali (sodium hydroxide) to prepare surfactant mixture , prepare the water phase (generally brine), prepare the oil phase (generally alkanes, cycloalkanes, aromatic hydrocarbons); add the prepared surfactant mixture into the water phase and mix evenly, then add the oil phase drop by drop to the above solution, and keep stirring evenly until the solution is from turbid to clear, that is, a microemulsion composed of biosurfactants is obtained. Since the oil phase needs to be used drop by drop, the production rate of the microemulsion is at the bottom, which seriously affects Product production rate.

发明内容Contents of the invention

本发明的目的就是提供一种化妆品、食品、化工及农业用生物表活剂微乳液生产系统，其可快速的将微生物发酵的生物表面活性剂制成微乳状液。The purpose of the present invention is to provide a biosurfactant microemulsion production system for cosmetics, food, chemical industry and agriculture, which can quickly make microemulsions from biosurfactants fermented by microorganisms.

为实现上述目的，本发明采用了以下技术方案：To achieve the above object, the present invention adopts the following technical solutions:

一种化妆品、食品、化工及农业用生物表活剂微乳液生产系统，其特征在于，包括如下生产设备:A kind of biosurfactant microemulsion production system for cosmetics, food, chemical industry and agriculture, is characterized in that, comprises following production equipment:

用于微生物发酵生产生物表面活性剂的发酵釜；Fermentation kettles for microbial fermentation to produce biosurfactants;

用于对发酵釜中的发酵液进行纯化分离处理的发酵液纯化设备以及用于储放纯化后的生物表面活性剂的生物表面活性剂储罐；Fermentation liquid purification equipment for purifying and separating the fermentation liquid in the fermentation tank and a biosurfactant storage tank for storing the purified biosurfactant;

分别用于储放助表面活性剂、碱液、水相以及油相的助表面活性剂储罐、碱液储罐、水相储罐以及油相储罐；Co-surfactant storage tanks, lye storage tanks, water-phase storage tanks and oil-phase storage tanks for storing co-surfactant, lye, water phase and oil phase respectively;

以及表面活性剂混合液配制釜和微乳状液反应釜；发酵釜、发酵液纯化设备和生物表面活性剂储罐依次进行连接，生物表面活性剂储罐、助表面活性剂储罐以及碱液储罐的出液口均与表面活性剂混合液配制釜相连接，表面活性剂混合液配制釜和水相储罐的出液口均与微乳状液反应釜相连接。And surfactant mixture preparation kettle and microemulsion reaction kettle; fermentation kettle, fermentation liquid purification equipment and biosurfactant storage tank are connected in sequence, biosurfactant storage tank, co-surfactant storage tank and lye storage tank The liquid outlets of the tanks are all connected with the surfactant mixed liquid preparation kettle, and the liquid outlets of the surfactant mixed liquid preparation kettle and the water phase storage tank are all connected with the microemulsion reaction kettle.

上述技术方案中提供的化妆品、食品、化工及农业用生物表活剂微乳液生产系统，通过对发酵液进行纯化以及微乳化处理，从而快速制得生物表面活性剂的微乳状液。The biosurfactant microemulsion production system for cosmetics, food, chemical industry and agriculture provided in the above technical solution can quickly prepare the microemulsion of biosurfactant by purifying and microemulsifying the fermented liquid.

附图说明Description of drawings

图1为本发明的结构示意图；Fig. 1 is a structural representation of the present invention;

图2为发酵液纯化设备的结构示意图；Fig. 2 is the structural representation of fermented liquid purification equipment;

图3为第二搅拌机构、布气板件以及通气管的结构示意图；Fig. 3 is the structural representation of the second stirring mechanism, the air distribution plate and the ventilation pipe;

图4为第一搅拌机构、布液板件以及油相进液管的结构示意图；Fig. 4 is a structural schematic diagram of the first stirring mechanism, the liquid distribution plate and the oil phase liquid inlet pipe;

图5为布气板件的结构示意图；Figure 5 is a schematic structural view of the air distribution plate;

图6为布液板件的结构示意图；Figure 6 is a schematic structural view of the liquid distribution plate;

图7为卸料机构的结构示意图；Fig. 7 is the structural representation of unloading mechanism;

图8为第一卸料板下侧板面的结构示意图。Fig. 8 is a schematic structural view of the lower side plate surface of the first unloading plate.

具体实施方式detailed description

为了使本发明的目的及优点更加清楚明白，以下结合实施例对本发明进行具体说明。应当理解，以下文字仅仅用以描述本发明的一种或几种具体的实施方式，并不对本发明具体请求的保护范围进行严格限定。In order to make the objects and advantages of the present invention clearer, the present invention will be specifically described below in conjunction with examples. It should be understood that the following words are only used to describe one or several specific implementation modes of the present invention, and do not strictly limit the protection scope of the specific claims of the present invention.

本发明采取的技术方案如图1、2所示，一种化妆品、食品、化工及农业用生物表活剂微乳液生产系统，其特征在于，包括如下生产设备:The technical scheme that the present invention takes is as shown in Figure 1, 2, a kind of cosmetics, food, chemical industry and agricultural biosurfactant microemulsion production system, it is characterized in that, comprises following production equipment:

用于微生物发酵生产生物表面活性剂的发酵釜40；A fermenter 40 for microbial fermentation to produce biosurfactants;

用于对发酵釜40中的发酵液进行纯化分离处理的发酵液纯化设备90以及用于储放纯化后的生物表面活性剂的生物表面活性剂储罐10；A fermentation broth purification device 90 for purifying and separating the fermentation broth in the fermentation tank 40 and a biosurfactant storage tank 10 for storing the purified biosurfactant;

分别用于储放助表面活性剂、碱液、水相以及油相的助表面活性剂储罐80、碱液储罐50、水相储罐60以及油相储罐70；Co-surfactant storage tank 80, lye storage tank 50, water phase storage tank 60 and oil phase storage tank 70 respectively used for storing co-surfactant, lye, water phase and oil phase;

以及表面活性剂混合液配制釜20和微乳状液反应釜30；发酵釜、发酵液纯化设备和生物表面活性剂储罐依次进行连接，生物表面活性剂储罐、助表面活性剂储罐以及碱液储罐的出液口均与表面活性剂混合液配制釜相连接，表面活性剂混合液配制釜和水相储罐的出液口均与微乳状液反应釜相连接。And surfactant mixed solution preparation kettle 20 and microemulsion reaction kettle 30; Fermentation kettle, fermented liquid purification equipment and biosurfactant storage tank are connected sequentially, biosurfactant storage tank, auxiliary surfactant storage tank and alkali The liquid outlets of the liquid storage tank are all connected with the surfactant mixed solution preparation kettle, and the liquid outlets of the surfactant mixed solution preparation kettle and the water phase storage tank are both connected with the microemulsion reaction kettle.

上述技术方案中提供的化妆品、食品、化工及农业用生物表活剂微乳液生产系统，通过对发酵液进行纯化以及微乳化处理，从而快速制得生物表面活性剂的微乳状液。由于发酵的周期较长，为了保证生产的连续性，可以设置多个发酵釜，多个发酵釜的发酵液出口分别与纯化装置相连接。The biosurfactant microemulsion production system for cosmetics, food, chemical industry and agriculture provided in the above technical solution can quickly prepare the microemulsion of biosurfactant by purifying and microemulsifying the fermented liquid. Due to the long fermentation period, in order to ensure the continuity of production, multiple fermentation tanks can be installed, and the outlets of the fermentation liquid of the multiple fermentation tanks are respectively connected to the purification device.

由于发酵液成分复杂，包括菌体，未被发酵的固体培养基，未被微生物完全利用的糖类、无机盐、蛋白质，以及微生物的各种代谢产物，发酵液粘度大，对于发酵液纯化设备，具体可如图2所示，包括依次设置前后连接的稀释装置91、粗滤装置92、微滤装置93、去杂质蛋白装置94、去杂质离子装置95以及盐化装置96。稀释装置主要对发酵液进行稀释和调节PH，一般采用槽体构成；粗滤装置主要将发酵液中的菌体、未被发酵的固体培养基以及其他较大的固体杂质给去除掉，可采用离心过滤设备或者其他过滤设备，也可采用多个过滤设备连用，粗虑后的发酵液可再次进行稀释和调节PH；微滤主要去除发酵液中的小分子杂质，如色素等等，一般采用膜过滤装置进行，所采用过滤膜的孔径应根据目的生物表面活性剂的分子大小进行选取，应使得过滤膜对生物表面活性剂进行截留，一般可采用陶瓷膜；微滤过后可在此进行稀释和调节PH；去杂质蛋白装置可以是等电点沉淀装置，去杂质离子装置主要为树脂吸附装置，通过对吸附后的微生物表面活性剂进行洗脱，洗脱液与碱液在盐化装置中进行反应生成盐。当然对于不同类型的生物表面活性剂所采用的纯化设备可以不同，本法提供的具体的纯化设备主要适用于脂肽类生物表面活性剂的纯化处理。对于其他种类的生物表面活性剂(如糖类、脂蛋白类)的纯化，其大体流程也是稀释、粗虑、微滤、去除杂质蛋白和离子。Due to the complex components of the fermentation liquid, including bacteria, unfermented solid medium, sugars, inorganic salts, proteins that are not fully utilized by microorganisms, and various metabolites of microorganisms, the viscosity of the fermentation liquid is high. For fermentation liquid purification equipment Specifically, as shown in FIG. 2 , it includes a dilution device 91 , a coarse filtration device 92 , a microfiltration device 93 , an impurity protein removal device 94 , an impurity ion removal device 95 , and a salinization device 96 that are connected sequentially. The dilution device mainly dilutes and adjusts the pH of the fermentation broth, and is generally composed of a tank; the coarse filtration device mainly removes bacteria in the fermentation broth, unfermented solid medium and other large solid impurities, and can be used Centrifugal filtration equipment or other filtration equipment can also be used in conjunction with multiple filtration equipment. The fermented liquid after coarse filtration can be diluted again and the pH can be adjusted; microfiltration mainly removes small molecular impurities in the fermented liquid, such as pigments, etc. Membrane filtration device, the pore size of the filter membrane should be selected according to the molecular size of the target biosurfactant, so that the filter membrane can intercept the biosurfactant, generally a ceramic membrane can be used; after microfiltration, it can be diluted here and adjust PH; the impurity protein removal device can be an isoelectric point precipitation device, and the impurity ion removal device is mainly a resin adsorption device. By eluting the adsorbed microbial surfactant, the eluent and lye are in the salinization device The reaction produces a salt. Of course, the purification equipment used for different types of biosurfactants can be different, and the specific purification equipment provided by this method is mainly suitable for the purification treatment of lipopeptide biosurfactants. For the purification of other types of biosurfactants (such as sugars and lipoproteins), the general process is also dilution, rough filtration, microfiltration, and removal of impurity proteins and ions.

由于发酵釜内发酵液粘度大，因此传统采用气管通入空气难于保证无菌空气在发酵罐内的均匀分布。因此，本发明采用如图3、5所示的技术方进行实施：发酵釜内设置的第二搅拌机构，发酵釜的上部设置有物料投入口，发酵釜的下部设置卸料口，第二搅拌机构包括立状布置的第二搅拌轴，第二搅拌轴的外围均匀设置立状布置的通气管45，通气管45的管身上间隔设置有布气板件46，各布气板件46的中部开设有供第二搅拌轴通过的通孔，布气板件46的内部设置成空腔状且布气板件46的板面上均匀开设布气孔461，各布气孔461处设置有滤网，各通气管的管腔分别与一布气板件46的内腔相连通连接，各通气管45的上端穿过釜体后与鼓气装置相连接，发酵釜内还设置有温度传感器和PH测量组件。层状排布的布气板件46，在鼓入无菌空气时，能够从各层相发酵液中补充空气，使得发酵液中空气均匀，保证生物表面活性剂的发酵。Due to the high viscosity of the fermentation liquid in the fermenter, it is difficult to ensure the uniform distribution of sterile air in the fermenter by traditionally using a trachea to feed air. Therefore, the present invention adopts the technical side as shown in Figure 3, 5 to carry out: the second stirring mechanism that is provided with in the fermenting kettle, the top of the fermenting kettle is provided with the material inlet, the bottom of the fermenting kettle is provided with the discharge port, the second stirring The mechanism includes a vertically arranged second agitating shaft, and vertically arranged air pipes 45 are evenly arranged on the periphery of the second agitating shaft, and air distribution plates 46 are arranged at intervals on the pipe body of the air pipe 45, and the middle of each air distribution plate 46 A through hole is provided for the passage of the second stirring shaft, the inside of the air distribution plate 46 is set into a cavity shape and the air distribution hole 461 is evenly opened on the plate surface of the air distribution plate 46, and each air distribution hole 461 is provided with a filter screen, The lumens of each ventilation pipe are connected to the inner cavity of a gas distribution plate 46 respectively, and the upper ends of each ventilation pipe 45 pass through the kettle body and are connected to the gas blowing device. The fermentation kettle is also provided with a temperature sensor and a pH measuring device. components. The air distribution boards 46 arranged in layers can replenish air from the fermentation liquid of each layer when the aseptic air is blown in, so that the air in the fermentation liquid is uniform and ensures the fermentation of the biosurfactant.

优选的方案为：可以采用一开口向下的锥形罩构成布气板件，锥形罩的中部开设通孔，锥形罩的罩体内部设置成空腔状，锥形罩的外罩面上均匀设置布气孔461。这样布气的均匀性，以及水平覆盖面最大，如图5所示。所述的布气板件层状设置有三个，通气管设置有三根，通气管的上端穿过发酵釜釜体上部的电机安装座后通过四通连接头以及气管与鼓气装置相连接。The preferred solution is: a conical cover with an opening downward can be used to form the air distribution plate, a through hole is opened in the middle of the conical cover, the inside of the cover body of the conical cover is set in a cavity shape, and the outer cover surface of the conical cover The air distribution holes 461 are uniformly arranged. In this way, the uniformity of air distribution and the maximum horizontal coverage are shown in Figure 5. There are three air distribution plates in layers, and three air pipes. The upper end of the air pipe passes through the motor mounting seat on the upper part of the fermentation kettle body and is connected to the air blowing device through a four-way connector and an air pipe.

进一步的如图7、8所示，卸料口处设置有卸料机构，卸料机构包括发酵罐卸料口处上、下平行布置的圆形的第一、二卸料板42、43，第一卸料板42与发酵罐固连为一体，第二卸料板43的侧面上开设有环形槽，第二卸料板43通过环形槽内设置的钢珠组件与发酵罐绕铅垂方向构成转动配合连接，第一、二卸料板42、43的圆心位于同一铅垂线上，第一、二卸料板上同一半径大小的圆周处分别开设第一、二卸料口42a、43a，第一卸料板42的下板面设置成由第一、二台阶面421、422组合构成的台阶状，第二台阶面422与第二卸料板43的上板面相贴合，第一台阶面421与第二卸料板43上板面之间形成空腔，第一卸料口42a开设在第一台阶面421上，第一、二台阶面交合的台阶处设置有密封件423，密封件423的形状与第一、二台阶面交接处的台阶形状一致，第二卸料板43与驱动机构相连接，优选的方案为：第一、二台阶面交接处的外轮廓为弧形，这样将密封件设置为弧形，密封件可采用O形密封件，第一卸料板的上板面设置成锥状且第一卸料口处的高度最低。通过驱动机构调节第二卸料板进行转动，使得第一、二卸料板上的第一、二卸料口相对应和相异，从而实现对发酵罐的快速卸料和卸料口的闭合，实现快速卸料，从而节约时间，提高提取效率。Further as shown in Figures 7 and 8, a discharge mechanism is provided at the discharge port, and the discharge mechanism includes circular first and second discharge plates 42, 43 arranged in parallel up and down at the discharge port of the fermenter, The first unloading plate 42 is fixedly connected with the fermentation tank as a whole, and an annular groove is opened on the side of the second unloading plate 43, and the second unloading plate 43 is formed around the vertical direction by the steel ball assembly arranged in the annular groove and the fermentation tank. Rotate fit connection, the circle centers of the first and second discharge plates 42, 43 are located on the same vertical line, and the first and second discharge openings 42a, 43a are respectively opened on the circumferences of the same radius on the first and second discharge plates, The lower surface of the first unloading plate 42 is set to a stepped shape composed of the first and second stepped surfaces 421, 422, the second stepped surface 422 is attached to the upper surface of the second unloading plate 43, and the first step A cavity is formed between the surface 421 and the upper surface of the second discharge plate 43, the first discharge port 42a is opened on the first step surface 421, and a seal 423 is arranged at the step where the first and second step surfaces intersect. The shape of the part 423 is consistent with the step shape of the junction of the first and second step surfaces, and the second unloading plate 43 is connected with the driving mechanism. The preferred solution is: the outer contour of the junction of the first and second step surfaces is arc-shaped, In this way, the seal is arranged in an arc shape, and the seal can be an O-shaped seal. The upper surface of the first discharge plate is set in a cone shape and the height of the first discharge port is the lowest. The second unloading plate is adjusted to rotate through the driving mechanism, so that the first and second unloading openings on the first and second unloading plates are corresponding and different, so as to realize the fast unloading of the fermenter and the closing of the unloading opening , to achieve fast unloading, thus saving time and improving extraction efficiency.

为了提高微乳化的速率，本发明采用如图4、6所示的技术方进行实施：微乳状液反应釜，包括釜体以及釜体内设置的第一搅拌机构，第一搅拌机构包括立状布置的第一搅拌轴31，第一搅拌轴31的外围均匀设置立状布置的油相进液管35，油相进液管35的管身上间隔设置有布液板件36，各布液板件36的中部开设有供第一搅拌轴31通过的通孔，布液板件36的内部设置成空腔状且布液板件36的下板面均匀开设布液孔，各油相进液管的管腔分别与一布液板件36的内腔相连通连接，各油相进液管的上端穿过釜体后与油相储罐相连接，釜体上还设置有表面活性剂混合液进液管口以及水相进液管口。层状排布的布液板件36，在滴加油相时，油相从布液板件36上的各布液孔滴入反应釜内的混合液中，相对于传统的一滴滴的滴入显著提高生产效率。各布液孔之间应保持一定的间距，具体操作时，布液孔为布液板件36上插设的针管构成，相邻针管的长度相异。In order to improve the rate of microemulsification, the present invention adopts the technical side as shown in Figure 4, 6 to carry out: Microemulsion liquid reactor, comprises the first agitating mechanism that kettle body and kettle body are arranged, and the first agitating mechanism includes vertical arrangement The first agitating shaft 31 of the first agitating shaft 31 is evenly provided with vertically arranged oil phase inlet pipes 35 on the periphery of the first agitating shaft 31, and liquid distribution plates 36 are arranged at intervals on the pipes of the oil phase liquid inlet pipes 35, and each liquid distribution plate The middle part of 36 is provided with a through hole for the first stirring shaft 31 to pass through, the inside of the liquid distribution plate 36 is set into a cavity shape and the lower surface of the liquid distribution plate 36 is evenly provided with liquid distribution holes, and the liquid inlet pipes of each oil phase The lumens of the tubes are respectively connected with the inner cavity of a liquid distribution plate 36, and the upper ends of the oil phase liquid inlet pipes pass through the kettle body and are connected with the oil phase storage tank, and the kettle body is also provided with a surfactant mixed liquid Inlet nozzle and water phase inlet nozzle. The liquid distribution plate 36 arranged in layers, when dripping the oil phase, the oil phase drops into the mixed liquid in the reaction kettle from the liquid distribution holes on the liquid distribution plate 36, compared with the traditional dripping Significantly improve production efficiency. A certain distance should be kept between the liquid distribution holes. During specific operation, the liquid distribution holes are formed by needle tubes inserted on the liquid distribution plate 36, and the lengths of adjacent needle tubes are different.

优选的方案为：布液板件36为一开口向上的锥形罩构成，锥形罩的中部开设通孔，锥形罩的罩体内部设置成空腔状，锥形罩的外罩面上均匀设置用于构成布气孔的针管361，针管361的长度方向与锥形罩的罩面相垂直布置，针管在锥形罩的罩面上呈圈状设置，且针管的长度随锥形罩的半径增大而增大，这样滴入油相的效果最佳。所述的布液板件层状设置有三个，油相进液管设置有三根，油相进液管的上端穿过釜体后通过四通连接头以及料液输送管道与油相储罐相连接。The preferred solution is: the liquid distribution plate 36 is formed by a conical cover with an opening upward, a through hole is opened in the middle of the conical cover, the inside of the cover body of the conical cover is set in a cavity shape, and the outer cover surface of the conical cover is uniform. The needle tube 361 that is used to form the air distribution hole is arranged, and the length direction of the needle tube 361 is vertically arranged with the cover surface of the conical cover. Large and enlarged, so that the effect of dripping into the oil phase is the best. There are three liquid distribution plates in layers, and three oil phase liquid inlet pipes. The upper end of the oil phase liquid inlet pipe passes through the kettle body and connects with the oil phase storage tank through the four-way connector and the material liquid delivery pipeline. connect.

由于第一、二搅拌轴上分别设置了布气装置和布液装置，因此第一、二搅拌轴轴身上无法设置搅拌桨，因此本发明中第一、二搅拌机构采用相同的技术方案进行实施，亦即如图3、4所示，第一、二搅拌轴31、的下端辐射状设置连接杆，连接杆的末端分别立状设置搅拌杆，连接杆和/或搅拌杆上分别设置搅拌料液的搅拌桨34。具体的为搅拌杆的长度为连接杆的两倍，连接杆包括第一、二、三连接杆321、322、323，搅拌杆包括第一、二、三搅拌杆331、332、333，第一连接杆321、第二搅拌杆332的下段以及第三搅拌杆333的上段分别设置搅拌桨34，搅拌桨34为一条板片构成，这样搅拌机构能够从不同的方向对溶液进行搅拌，提高混合的均匀性。搅拌杆和连接杆均为角钢构成，这样强度大，便于搅拌桨34的安装以及搅拌机构的稳定性。Since the first and second stirring shafts are respectively provided with an air distribution device and a liquid distribution device, the shafts of the first and second stirring shafts cannot be equipped with stirring paddles. Therefore, the first and second stirring mechanisms in the present invention are implemented using the same technical solution. That is, as shown in Figures 3 and 4, the lower ends of the first and second stirring shafts 31 are radially provided with connecting rods, and the ends of the connecting rods are respectively vertically provided with stirring rods, and the connecting rods and/or the stirring rods are respectively provided with a stirring material liquid. The stirring paddle 34. Specifically, the length of the stirring rod is twice that of the connecting rod. The upper section of connecting rod 321, the second stirring rod 332 and the upper section of the third stirring rod 333 are provided with stirring paddle 34 respectively. Uniformity. Both the stirring rod and the connecting rod are made of angle steel, so the strength is high, which is convenient for the installation of the stirring paddle 34 and the stability of the stirring mechanism.

另外，对于发酵釜，发酵釜的釜壁为夹层结构，夹层结构形成的夹腔用于容纳热流体。热流体用于调节发酵釜内温度，满足微生物发酵的需求。对于微乳状液反应釜，釜体的内侧壁上设置有扰流筋，釜体的侧壁为夹层结构构成，夹层结构形成的夹腔用于容纳热流体。热流体用于调节釜内温度，适应不同微乳状液的生产。In addition, for the fermentation tank, the wall of the fermentation tank is a sandwich structure, and the sandwich cavity formed by the sandwich structure is used to accommodate the thermal fluid. The thermal fluid is used to adjust the temperature in the fermentation tank to meet the needs of microbial fermentation. For the microemulsion reaction kettle, spoiler ribs are provided on the inner wall of the kettle body, and the side wall of the kettle body is composed of a sandwich structure, and the sandwich cavity formed by the sandwich structure is used to accommodate the thermal fluid. The thermal fluid is used to adjust the temperature in the kettle to adapt to the production of different microemulsions.

表面活性剂混合液配制釜内设置有第三搅拌机构以及超声发射组件，表面活性剂配制釜的釜壁为夹层结构、夹层结构形成的夹腔用于容纳加热流体。超声发射组件对物料进行振荡，使得表面活性剂、助表面活性剂快速混匀。A third stirring mechanism and an ultrasonic emission component are arranged in the surfactant mixed solution preparation kettle, the wall of the surfactant preparation kettle is a sandwich structure, and the sandwich structure formed by the sandwich structure is used to accommodate the heating fluid. The ultrasonic emitting component vibrates the material, so that the surfactant and co-surfactant are quickly mixed.

总之，本发明可有效提高微乳状液的生产效率。In a word, the present invention can effectively improve the production efficiency of microemulsion.

以上所述仅是本发明的优选实施方式，应当指出，对于本技术领域的普通技术人员来说，在获知本发明中记载内容后，在不脱离本发明原理的前提下，还可以对其作出若干同等变换和替代，这些同等变换和替代也应视为属于本发明的保护范围。The above is only a preferred embodiment of the present invention. It should be pointed out that for those of ordinary skill in the art, after knowing the content recorded in the present invention, they can also make changes to it without departing from the principle of the present invention. Several equivalent transformations and substitutions should also be deemed to belong to the protection scope of the present invention.

Claims (1)

1.一种化妆品、食品、化工及农业用生物表活剂微乳液生产系统，其特征在于，包括如下生产设备:1. a biosurfactant microemulsion production system for cosmetics, food, chemical industry and agriculture, is characterized in that, comprises following production equipment: 用于微生物发酵生产生物表面活性剂的发酵釜；Fermentation kettles for microbial fermentation to produce biosurfactants; 用于对发酵釜中的发酵液进行纯化分离处理的发酵液纯化设备以及用于储放纯化后的生物表面活性剂的生物表面活性剂储罐；Fermentation liquid purification equipment for purifying and separating the fermentation liquid in the fermentation tank and a biosurfactant storage tank for storing the purified biosurfactant; 分别用于储放助表面活性剂、碱液、水相以及油相的助表面活性剂储罐、碱液储罐、水相储罐以及油相储罐；Co-surfactant storage tanks, lye storage tanks, water-phase storage tanks and oil-phase storage tanks for storing co-surfactant, lye, water phase and oil phase respectively; 以及表面活性剂混合液配制釜和微乳状液反应釜；发酵釜、发酵液纯化设备和生物表面活性剂储罐依次进行连接，生物表面活性剂储罐、助表面活性剂储罐以及碱液储罐的出液口均与表面活性剂混合液配制釜相连接，表面活性剂混合液配制釜和水相储罐的出液口均与微乳状液反应釜相连接；And surfactant mixture preparation kettle and microemulsion reaction kettle; fermentation kettle, fermentation liquid purification equipment and biosurfactant storage tank are connected in sequence, biosurfactant storage tank, co-surfactant storage tank and lye storage tank The liquid outlets of the tanks are all connected to the surfactant mixed liquid preparation kettle, and the liquid outlets of the surfactant mixed liquid preparation kettle and the aqueous phase storage tank are all connected with the microemulsion reaction kettle; 微乳状液反应釜包括釜体以及釜体内设置的第一搅拌机构，第一搅拌机构包括立状布置的第一搅拌轴，第一搅拌轴的外围均匀设置立状布置的油相进液管，油相进液管的管身上间隔设置有布液板件，各布液板件的中部开设有供第一搅拌轴通过的通孔，布液板件的内部设置成空腔状且布液板件的下板面均匀开设布液孔，各油相进液管的管腔分别与一布液板件的内腔相连通连接，各油相进液管的上端穿过釜体后与油相储罐相连接，釜体上还设置有表面活性剂混合液进液管口以及水相进液管口；The microemulsion reaction kettle includes a kettle body and a first stirring mechanism arranged in the kettle body. The first stirring mechanism includes a vertically arranged first stirring shaft, and a vertically arranged oil phase liquid inlet pipe is evenly arranged on the periphery of the first stirring shaft. The pipe body of the oil phase liquid inlet pipe is provided with liquid distribution plates at intervals, and the middle part of each liquid distribution plate is provided with a through hole for the first stirring shaft to pass through. The inside of the liquid distribution plate is set in a cavity shape and the liquid distribution plate The lower plate surface of the part is evenly opened with liquid distribution holes, and the lumen of each oil phase liquid inlet pipe is respectively connected with the inner cavity of a liquid distribution plate part, and the upper end of each oil phase liquid inlet pipe passes through the kettle body and connects with the oil phase The storage tanks are connected, and the kettle body is also provided with a surfactant mixed liquid inlet nozzle and a water phase inlet nozzle; 发酵液纯化设备包括依次设置前后连接的稀释装置、粗滤装置、微滤装置、去杂质蛋白装置、去杂质离子装置以及盐化装置。The fermentation broth purification equipment includes a dilution device, a rough filtration device, a microfiltration device, an impurity protein removal device, an impurity ion removal device, and a salinization device that are connected in sequence.
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