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CN104445777A - Multi-effect evaporation condensed water recycling method - Google Patents

Multi-effect evaporation condensed water recycling method Download PDF

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Publication number
CN104445777A
CN104445777A CN201410691909.6A CN201410691909A CN104445777A CN 104445777 A CN104445777 A CN 104445777A CN 201410691909 A CN201410691909 A CN 201410691909A CN 104445777 A CN104445777 A CN 104445777A
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Prior art keywords
water
boiler
condensation
effect
condensed water
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CN201410691909.6A
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Chinese (zh)
Inventor
董利刚
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Dacha Danjili Chemical Co ltd
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Dacha Danjili Chemical Co ltd
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Priority to CN201410691909.6A priority Critical patent/CN104445777A/en
Publication of CN104445777A publication Critical patent/CN104445777A/en
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/26Multiple-effect evaporating
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/02Treatment of water, waste water, or sewage by heating
    • C02F1/04Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/001Processes for the treatment of water whereby the filtration technique is of importance
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2301/00General aspects of water treatment
    • C02F2301/08Multistage treatments, e.g. repetition of the same process step under different conditions

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)

Abstract

本发明公开了一种多效蒸发冷凝水回收利用方法,包括:一次冷凝水返回锅炉再利用;二次冷凝水部分用作泵冷却水,部分经过滤后可用作锅炉补水,少部分作为生活用水。此方法使得多效蒸发过程基本无污水排放,且设备改装简便,投入较少,节能环保效果较好。

The invention discloses a method for recycling condensed water from a multiple-effect evaporation process, including: returning primary condensed water to the boiler for reuse; using part of the secondary condensed water as pump cooling water, part of the water as boiler replenishment water after filtration, and a small part as domestic water. This method allows the multiple-effect evaporation process to have substantially no sewage discharge, and the equipment modification is simple, the investment is small, and the energy-saving and environmental protection effects are good.

Description

多效蒸发冷凝水回收利用方法Multi-effect evaporation condensed water recycling method

技术领域 technical field

本发明涉及一种冷凝水回收利用方法,尤其是多效蒸发冷凝水回收利用方法。 The invention relates to a method for recycling condensed water, in particular to a method for recycling condensed water of multi-effect evaporation.

背景技术 Background technique

在柴达木盆地化工生产中,一般企业对多效蒸发所产生的冷凝水等废水都采取外排的处理方式,这样不仅增加排放量,对外部环境产生较大影响,同时也增加企业生产成本,对本来就缺水的柴达木地区增加用水负担。随着盐湖化工的不断发展,企业用水量越来越大,节约用水、合理用水、一水多用成为各生产企业十分关心和重视的问题。 In the chemical production in the Qaidam Basin, general enterprises adopt the method of discharging waste water such as condensed water produced by multi-effect evaporation, which not only increases the discharge volume, but also has a great impact on the external environment, and also increases the production cost of the enterprise , Increase the water burden on the Qaidam area, which is already short of water. With the continuous development of salt lake chemical industry, the water consumption of enterprises is increasing. Water conservation, rational use of water, and multiple uses of one water have become issues of great concern and attention to all production enterprises.

在大多数情况下,蒸汽输送过程、热交换过程和冷凝水输送过程不会产生污染。因此,冷凝水在没有污染的情况下符合锅炉水的水质要求,可以直接用作锅炉用水。另外,由于冷凝水的水温较高,通常在60~80℃范围内,有的情况下可以达到80℃以上。因此,冷凝水含有较大余热量,这在能源紧张的今天应该成为废水综合利用时必须要考虑的因素。 In most cases, the steam transfer process, the heat exchange process and the condensate transfer process do not generate pollution. Therefore, the condensed water meets the water quality requirements of boiler water without pollution, and can be directly used as boiler water. In addition, due to the high temperature of condensed water, it is usually in the range of 60-80°C, and in some cases it can reach above 80°C. Therefore, condensed water contains a large amount of residual heat, which should be a factor that must be considered in the comprehensive utilization of waste water in today's energy shortage.

发明内容 Contents of the invention

本发明的目的在于提供一种应用于化工生产领域的,能全面综合回收利用多效蒸发冷凝水的方法。 The purpose of the present invention is to provide a method that can comprehensively recycle and utilize the condensed water of multi-effect evaporation, which is applied in the field of chemical production.

本发明的目的由以下技术方案实现: The purpose of the present invention is achieved by the following technical solutions:

多效蒸发冷凝水回收利用方法,包括两部分: The multi-effect evaporation condensate recycling method includes two parts:

(1)                   加热锅炉产生的蒸汽进入一效加热室加热料液,加热完毕后经过表面冷凝器产生一次冷凝水并进入一次冷凝水罐中,将一次冷凝水通过冷凝水泵打入一效预热器预热一效进料后流入锅炉补水池,然后再返回锅炉作为锅炉用水重新利用; (1) The steam generated by the heating boiler enters the first-effect heating chamber to heat the feed liquid. After heating, the primary condensed water is generated through the surface condenser and enters the primary condensed water tank. The primary condensed water is pumped into the primary-effect preheater through the condensed water pump After preheating the first-effect feed, it flows into the boiler make-up water pool, and then returns to the boiler as boiler water for reuse;

(2)                   二效加热室出来的冷凝水进入表面冷凝器闪发,其未蒸发的部分与表面冷凝器产生的冷凝水合为二次冷凝水一起进入二次冷凝水罐,由冷凝水泵将二次冷凝水打入二效预热器预热一效进料后进入凉水池冷却降温,待温度降到一定程度后进入冷却水池,冷却水池中的部分回收水用于各泵冷却水并回收至冷却水池,富余部分去废水池贮存,废水池中的废水经过滤机过滤后可去锅炉补水池用于锅炉补水,锅炉补水池中的部分水还可作为澡堂用水,澡堂废水又回收至废水池形成水循环。 (2) The condensed water from the second-effect heating chamber enters the surface condenser to flash, and the unevaporated part combines with the condensed water produced by the surface condenser to form the secondary condensed water and enters the secondary condensed water tank together, and the condensed water pump transfers the secondary condensed water The condensed water enters the second-effect preheater to preheat the first-effect feed material and enters the cooling water pool to cool down. After the temperature drops to a certain level, it enters the cooling water pool. Part of the recovered water in the cooling water pool is used for cooling water of each pump and recycled to the cooling water tank For the water pool, the excess part is stored in the waste water pool. After being filtered by the filter, the waste water in the waste water pool can be sent to the boiler make-up water pool for boiler water replenishment. Part of the water in the boiler make-up water pool can also be used as bath water, and the bath waste water is recycled to the waste water pool to form water cycle.

相比现有技术,本发明具有以下优点: Compared with the prior art, the present invention has the following advantages:

1、多效蒸发是一个利用低压蒸汽密封运行的设备装置,在运行过程中增加冷凝水回收装置,将本来外排的冷凝水回收再利用,可以减少外排量,回收率达到80%,达到防止环境污染,节省能源的目的; 1. Multi-effect evaporation is an equipment device that uses low-pressure steam to operate in a sealed manner. During operation, a condensed water recovery device is added to recycle and reuse the condensed water that was originally discharged, which can reduce the external discharge. The recovery rate reaches 80%, reaching The purpose of preventing environmental pollution and saving energy;

2、节约水资源,改善柴达木盆地土地沙漠化的情况; 2. Save water resources and improve the desertification of the Qaidam Basin;

3、节约生产成本,企业可减少购水成本及废水处理成本。 3. Saving production costs, enterprises can reduce water purchase costs and waste water treatment costs.

附图说明 Description of drawings

图1为本发明的方法流程图。 Fig. 1 is a flow chart of the method of the present invention.

具体实施方式 Detailed ways

下面结合附图对本发明的技术方案作进一步的详细描述: Below in conjunction with accompanying drawing, technical scheme of the present invention is described in further detail:

如图1所示,多效蒸发冷凝水回收利用方法,包括两部分: As shown in Figure 1, the multi-effect evaporation condensate recycling method includes two parts:

(1)                   锅炉蒸发出来1.0MPa蒸汽进入一效加热室加热料液,加热完毕后经过表面冷凝器产生一次冷凝水并进入一次冷凝水罐中,将一次冷凝水通过冷凝水泵打入一效预热器预热一效进料后流入锅炉补水池,然后再返回锅炉作为锅炉用水重新利用; (1) 1.0MPa steam evaporated from the boiler enters the first-effect heating chamber to heat the feed liquid. After heating, the primary condensed water is generated through the surface condenser and enters the primary condensed water tank. The primary condensed water is pumped into the primary-effect preheating through the condensed water pump After preheating the first-effect feed, it flows into the boiler make-up water tank, and then returns to the boiler as boiler water for reuse;

二效加热室出来的冷凝水进入表面冷凝器闪发,其未蒸发的部分与表面冷凝器产生的冷凝水合为二次冷凝水一起进入二次冷凝水罐,由冷凝水泵将二次冷凝水打入二效预热器预热一效进料后进入凉水池冷却降温,待温度降到低于各工作泵表面温度后进入冷却水池,冷却水池中的部分回收水用于各泵冷却水并回收至冷却水池,富余部分去废水池贮存,废水池中的废水经过滤机过滤后可去锅炉补水池用于锅炉补水,锅炉补水池中的部分水还可作为澡堂用水,澡堂废水又回收至废水池形成水循环。 The condensed water from the two-effect heating chamber enters the surface condenser for flashing, and the non-evaporated part combines with the condensed water produced by the surface condenser to form secondary condensed water and enters the secondary condensed water tank together, and the secondary condensed water is pumped by the condensed water pump After entering the second-effect preheater to preheat the first-effect feed material, it enters the cooling water pool to cool down. After the temperature drops below the surface temperature of each working pump, it enters the cooling water pool. Part of the recovered water in the cooling water pool is used for the cooling water of each pump and recycled. To the cooling water pool, the excess part is stored in the waste water pool. After being filtered by the filter, the waste water in the waste water pool can be sent to the boiler make-up water pool for boiler water replenishment. Part of the water in the boiler make-up water pool can also be used as bath water, and the bath waste water is recycled to waste water The pool forms a water cycle.

Claims (1)

1. multiple-effect evaporation condensation Water Sproading Application way, is characterized in that described method comprises the steps:
The steam that heating boiler produces enters an effect oven heats feed liquid, produce a water of condensation through surface condenser after heating and enter in a condensate water pot, water of condensation is squeezed into after an effect preheater preheats one imitates charging by condensate pump and flows into boiler replenishing water pond, and then return boiler and re-use as boiler feed water;
Two effect heating chambers water of condensation out enters surface condenser shwoot, the water of condensation that its unevaporated part and surface condenser produce is combined into together with time condensation water and enters time condensation water pot, by condensate pump time condensation water squeezed into and enter cooling pond after two effect preheater preheats one imitate charging and cool, drop to until temperature and to a certain degree afterwards enter cooling basin, partially recycled water in cooling basin is used for each pump water coolant and is recycled to cooling basin, flap portion goes wastewater disposal basin to store, waste water in wastewater disposal basin can go to boiler replenishing water pond for boiler replenishing water after filter filters, part water in boiler replenishing water pond also can be used as publilc baths water, publilc baths waste water is recycled to again wastewater disposal basin and forms water cycle.
CN201410691909.6A 2014-11-27 2014-11-27 Multi-effect evaporation condensed water recycling method Pending CN104445777A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105536277A (en) * 2016-03-14 2016-05-04 许达人 Evaporation and concentration technology and device for cellosolve NMMO (N-methylmorpholine-N-oxide) aqueous solution
CN107469374A (en) * 2017-09-01 2017-12-15 湖北合加环境设备有限公司 A kind of MVR vapo(u)rization systems of quick self-picketing energy imbalance

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EP0034920A1 (en) * 1980-02-20 1981-09-02 E.I. Du Pont De Nemours And Company Water evaporation process
CN101041443A (en) * 2007-03-09 2007-09-26 中盐制盐工程技术研究院 Vacuum salt producing technique of salt-field saturated bittern direct ingress into evaporation tank
CN101450266A (en) * 2007-12-04 2009-06-10 石家庄工大化工设备有限公司 Sodium sulfide evaporation concentration system and method
CN101935077A (en) * 2010-08-27 2011-01-05 南通京通石墨设备有限公司 Waste acid concentration multistage treatment method
CN102617381A (en) * 2012-02-23 2012-08-01 洛阳鸿安生化科技有限公司 Method for evaporating hydroxybenzene glycine
CN103435226A (en) * 2013-08-27 2013-12-11 自贡市轻工业设计研究院有限责任公司 Comprehensive treatment technology for formation water in natural gas extraction
CN203355316U (en) * 2013-06-06 2013-12-25 山东元鸣生物科技有限公司 Continuous quarternary-stage evaporation and crystallization device for manufacturing sodium gluconate
CN203355317U (en) * 2013-06-13 2013-12-25 苏州乔发蒸发器制造有限公司 Four-effect crystallizing evaporator
CN203668036U (en) * 2013-12-20 2014-06-25 四川省洪雅青衣江元明粉有限公司 Recycling device of multiple-effect evaporation system condensed water for meeting requirement for boiler high-quality water
CN203833652U (en) * 2014-03-27 2014-09-17 上海问鼎水处理工程有限公司 Device for treating chitin soda boiling waste water
CN203935631U (en) * 2014-05-30 2014-11-12 江苏嘉泰蒸发结晶设备有限公司 Multi-effect evaporation system steam condensate (SC) heat energy recycling device
CN203935630U (en) * 2014-05-30 2014-11-12 江苏嘉泰蒸发结晶设备有限公司 Multi-effect evaporation system evaporation condensed water heat energy recycling device

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0034920A1 (en) * 1980-02-20 1981-09-02 E.I. Du Pont De Nemours And Company Water evaporation process
CN101041443A (en) * 2007-03-09 2007-09-26 中盐制盐工程技术研究院 Vacuum salt producing technique of salt-field saturated bittern direct ingress into evaporation tank
CN101450266A (en) * 2007-12-04 2009-06-10 石家庄工大化工设备有限公司 Sodium sulfide evaporation concentration system and method
CN101935077A (en) * 2010-08-27 2011-01-05 南通京通石墨设备有限公司 Waste acid concentration multistage treatment method
CN102617381A (en) * 2012-02-23 2012-08-01 洛阳鸿安生化科技有限公司 Method for evaporating hydroxybenzene glycine
CN203355316U (en) * 2013-06-06 2013-12-25 山东元鸣生物科技有限公司 Continuous quarternary-stage evaporation and crystallization device for manufacturing sodium gluconate
CN203355317U (en) * 2013-06-13 2013-12-25 苏州乔发蒸发器制造有限公司 Four-effect crystallizing evaporator
CN103435226A (en) * 2013-08-27 2013-12-11 自贡市轻工业设计研究院有限责任公司 Comprehensive treatment technology for formation water in natural gas extraction
CN203668036U (en) * 2013-12-20 2014-06-25 四川省洪雅青衣江元明粉有限公司 Recycling device of multiple-effect evaporation system condensed water for meeting requirement for boiler high-quality water
CN203833652U (en) * 2014-03-27 2014-09-17 上海问鼎水处理工程有限公司 Device for treating chitin soda boiling waste water
CN203935631U (en) * 2014-05-30 2014-11-12 江苏嘉泰蒸发结晶设备有限公司 Multi-effect evaporation system steam condensate (SC) heat energy recycling device
CN203935630U (en) * 2014-05-30 2014-11-12 江苏嘉泰蒸发结晶设备有限公司 Multi-effect evaporation system evaporation condensed water heat energy recycling device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105536277A (en) * 2016-03-14 2016-05-04 许达人 Evaporation and concentration technology and device for cellosolve NMMO (N-methylmorpholine-N-oxide) aqueous solution
CN105536277B (en) * 2016-03-14 2017-11-21 许达人 A kind of evaporating and concentrating process and device of the cellulose solvent NMMO aqueous solution
CN107469374A (en) * 2017-09-01 2017-12-15 湖北合加环境设备有限公司 A kind of MVR vapo(u)rization systems of quick self-picketing energy imbalance

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Application publication date: 20150325