CN104382223A - Solvent suitable for preparing fruit-flavored e-cigarette liquid and the prepared e-liquid and e-cigarette - Google Patents
Solvent suitable for preparing fruit-flavored e-cigarette liquid and the prepared e-liquid and e-cigarette Download PDFInfo
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- CN104382223A CN104382223A CN201410564970.4A CN201410564970A CN104382223A CN 104382223 A CN104382223 A CN 104382223A CN 201410564970 A CN201410564970 A CN 201410564970A CN 104382223 A CN104382223 A CN 104382223A
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- solvent
- tobacco juice
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- cigarette liquid
- liquid
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- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 45
- 239000002904 solvent Substances 0.000 title claims abstract description 39
- 239000007788 liquid Substances 0.000 title abstract description 38
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 25
- 241000208125 Nicotiana Species 0.000 claims abstract description 19
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 19
- 239000000779 smoke Substances 0.000 claims abstract description 16
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract 13
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 24
- 239000000796 flavoring agent Substances 0.000 claims description 16
- CFNJLPHOBMVMNS-UHFFFAOYSA-N pentyl butyrate Chemical compound CCCCCOC(=O)CCC CFNJLPHOBMVMNS-UHFFFAOYSA-N 0.000 claims description 15
- PGMYKACGEOXYJE-UHFFFAOYSA-N pentyl acetate Chemical compound CCCCCOC(C)=O PGMYKACGEOXYJE-UHFFFAOYSA-N 0.000 claims description 13
- 235000011187 glycerol Nutrition 0.000 claims description 9
- HNAGHMKIPMKKBB-UHFFFAOYSA-N 1-benzylpyrrolidine-3-carboxamide Chemical compound C1C(C(=O)N)CCN1CC1=CC=CC=C1 HNAGHMKIPMKKBB-UHFFFAOYSA-N 0.000 claims description 8
- OBNCKNCVKJNDBV-UHFFFAOYSA-N butanoic acid ethyl ester Natural products CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 claims description 8
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 claims description 8
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 claims description 8
- FGPPDYNPZTUNIU-UHFFFAOYSA-N pentyl pentanoate Chemical compound CCCCCOC(=O)CCCC FGPPDYNPZTUNIU-UHFFFAOYSA-N 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- ZOCHHNOQQHDWHG-UHFFFAOYSA-N n-hexan-3-ol Natural products CCCC(O)CC ZOCHHNOQQHDWHG-UHFFFAOYSA-N 0.000 claims description 4
- 235000013355 food flavoring agent Nutrition 0.000 claims 4
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 abstract description 24
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 abstract description 15
- 235000019504 cigarettes Nutrition 0.000 abstract description 11
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 abstract description 6
- 235000019445 benzyl alcohol Nutrition 0.000 abstract description 5
- 206010013911 Dysgeusia Diseases 0.000 abstract description 3
- 239000008369 fruit flavor Substances 0.000 abstract description 3
- 230000036541 health Effects 0.000 abstract description 2
- 235000019634 flavors Nutrition 0.000 description 12
- 239000003205 fragrance Substances 0.000 description 10
- 239000000203 mixture Substances 0.000 description 4
- 230000000391 smoking effect Effects 0.000 description 4
- 229940072049 amyl acetate Drugs 0.000 description 3
- 239000008367 deionised water Substances 0.000 description 3
- 229910021641 deionized water Inorganic materials 0.000 description 3
- MNWFXJYAOYHMED-UHFFFAOYSA-M heptanoate Chemical compound CCCCCCC([O-])=O MNWFXJYAOYHMED-UHFFFAOYSA-M 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000284 extract Substances 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 230000005586 smoking cessation Effects 0.000 description 2
- 238000000889 atomisation Methods 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Preparation Of Fruits And Vegetables (AREA)
- Confectionery (AREA)
Abstract
Description
技术领域 technical field
本发明涉及电子烟技术领域,尤其涉及一种采用苯甲醇调配的果香型电子烟烟液溶剂及其配制的烟液和电子烟。 The invention relates to the technical field of electronic cigarettes, in particular to a fruity-flavored e-cigarette liquid solvent formulated with benzyl alcohol and the prepared e-cigarette liquid and electronic cigarette.
背景技术 Background technique
电子烟主要用于戒烟和替代香烟电子烟,是一种仿香烟的便携电子雾化器,通过雾化器把电子烟烟液打成雾气,直接吸入,其过程类似抽吸真实卷烟。电子烟有着与香烟一样的外观、与香烟近似的味道,甚至比一般香烟的口味要多出很多,也像香烟一样能吸出烟、吸出味道跟感觉。传统卷烟在减害降焦方面存在天生的不足,随着我国加入世界贸易组织和《烟草控制框架公约》,政府控烟力度在不断加强,各种模拟卷烟的低害产品不断涌现,电子烟作为其中一种重要的戒烟控烟产品得到大力推广。 E-cigarettes are mainly used to quit smoking and replace cigarettes. It is a portable electronic atomizer imitating cigarettes. Through the atomizer, the e-cigarette liquid is atomized and inhaled directly. The process is similar to smoking real cigarettes. Electronic cigarettes have the same appearance and taste similar to cigarettes, and even have a lot more flavor than ordinary cigarettes. They can also suck out smoke, taste and feeling like cigarettes. Traditional cigarettes have inherent deficiencies in harm reduction and coke reduction. With my country's accession to the World Trade Organization and the "Framework Convention on Tobacco Control", the government's efforts to control tobacco have been continuously strengthened, and various low-harm products that simulate cigarettes are emerging. Electronic cigarettes are one of them. An important smoking cessation and tobacco control product was vigorously promoted.
电子烟无论用于戒烟还是传统卷烟的替代品,均拥有巨大的成长空间。电子烟已经在加拿大、芬兰等50多个国家和地区合法销售,成为烟民健康吸烟的首选。虽然目前电子烟的销售仍主要集中在北美地区,但面对中国3亿多烟民和各大欧洲国家的吸烟人群,一旦市场打开,电子烟销售势必将会进一步的增长。 Whether e-cigarettes are used for smoking cessation or as substitutes for traditional cigarettes, there is huge room for growth. E-cigarettes have been legally sold in more than 50 countries and regions including Canada and Finland, and have become the first choice for smokers to smoke healthily. Although the current sales of e-cigarettes are still mainly concentrated in North America, facing the more than 300 million smokers in China and the smokers in major European countries, once the market is opened, the sales of e-cigarettes are bound to further increase.
电子烟烟液由溶剂、烟用香精香料、烟草提取物、植物提取物等组成。电子烟烟液溶剂是电子烟烟液的主要成分,主要为丙二醇、丙三醇。以丙二醇、丙三醇为溶剂调配的果香型电子烟烟液存在谐调性差、口感油腻等缺点。现有技术尚未见有采用苯甲醇作为溶剂调配果香型电子烟烟液的相关报道。 E-cigarette liquid is composed of solvents, flavors and fragrances for tobacco, tobacco extracts, plant extracts, etc. E-cigarette liquid solvent is the main component of e-cigarette liquid, mainly propylene glycol and glycerin. The fruity-flavored e-cigarette liquid prepared with propylene glycol and glycerin as solvents has disadvantages such as poor coordination and greasy taste. In the prior art, there is no related report about using benzyl alcohol as a solvent to prepare fruity-flavored e-cigarette liquid.
发明内容 Contents of the invention
为了解决上述的技术问题,本发明的一个目的是一种适用于配制果香型电子烟烟液的溶剂,应用本发明的溶剂配制的电子烟烟液香气充足,具有较好的谐调性,余味舒适,亦能产生较大的烟雾量,满足吸食者需求。本发明的第二个目的是提供采用上述溶剂配制的烟液。本发明的第三个目的是提供采用上述烟液的电子烟。 In order to solve the above-mentioned technical problems, an object of the present invention is a solvent suitable for preparing fruity-flavored e-cigarette liquid. The e-cigarette liquid prepared with the solvent of the present invention has sufficient aroma, good harmony, and excellent aftertaste. It is comfortable and can also produce a large amount of smoke to meet the needs of smokers. The second object of the present invention is to provide an e-liquid prepared with the above-mentioned solvent. The third object of the present invention is to provide an electronic cigarette using the above-mentioned e-liquid.
为了实现上述的第一个目的,本发明采用了以下的技术方案: In order to achieve the above-mentioned first purpose, the present invention adopts the following technical solutions:
一种适用于配制果香型电子烟烟液的溶剂,该溶剂按重量百分比计包括以下组分:苯甲醇40~80%,丙二醇0-30 %,丙三醇0-20 %。 A solvent suitable for preparing fruit-flavored e-cigarette liquid, the solvent includes the following components by weight percentage: 40-80% benzyl alcohol, 0-30% propylene glycol, and 0-20% glycerol.
作为优选,该溶剂按重量百分比计包括以下组分:苯甲醇50~70%,丙二醇0-20%,丙三醇0-15 %。 Preferably, the solvent comprises the following components by weight percentage: 50-70% benzyl alcohol, 0-20% propylene glycol, and 0-15% glycerol.
作为优选,该溶剂按重量百分比计还包括水0-20%。 As a preference, the solvent also includes 0-20% water by weight percentage.
作为再优选,该溶剂按重量百分比计还包括水10-20%。 As another preference, the solvent also includes 10-20% water by weight percentage.
为了实现上述的第二个目的,本发明采用了以下的技术方案: In order to achieve the above-mentioned second purpose, the present invention adopts the following technical solutions:
一种果香型电子烟烟液,该电子烟烟液包括上述的溶剂和香精香料。当然为了提高吸食的口感和效果,本发明也可以加入烟草提取物。 A fruit-flavored electronic cigarette liquid, the electronic cigarette liquid includes the above-mentioned solvent and essence and fragrance. Of course, in order to improve the taste and effect of smoking, the present invention can also add tobacco extract.
作为优选,所述的香精香料的加入量为2~10%。 As a preference, the added amount of the flavor and fragrance is 2-10%.
作为优选,所述的香精香料按重量百分比计由以下的组分构成:戊酸戊酯20~40%、丁酸戊酯20~30%、丁酸乙酯10~30%、乙酸乙酯10~20 %、乙酸戊酯1~8 %、乙酰乙酸乙酯1~5%、己醇1~5%。 Preferably, the flavor and fragrance is composed of the following components by weight percentage: 20-40% amyl valerate, 20-30% amyl butyrate, 10-30% ethyl butyrate, 10% ethyl acetate ~20%, amyl acetate 1~8%, ethyl acetoacetate 1~5%, hexanol 1~5%.
作为再优选,所述的香精香料按重量百分比计由以下的组分构成:戊酸戊酯30%、丁酸戊酯25%、丁酸乙酯20%、乙酸乙酯15 %、乙酸戊酯4 %、乙酰乙酸乙酯3%、己醇3%。 As another preference, the flavor and fragrance is composed of the following components by weight percentage: 30% pentyl valerate, 25% pentyl butyrate, 20% ethyl butyrate, 15% ethyl acetate, pentyl acetate 4%, ethyl acetoacetate 3%, hexanol 3%.
为了实现上述的第三个目的,本发明采用了以下的技术方案: In order to achieve the above-mentioned third purpose, the present invention adopts the following technical solutions:
一种果香型电子烟,该电子烟的烟液采用上述的果香型电子烟烟液。 A fruit-flavored electronic cigarette, the smoke liquid of the electronic cigarette adopts the above-mentioned fruit-flavored electronic cigarette liquid.
本发明提供了一种采用苯甲醇调配的适用于果香型电子烟烟液的溶剂。应用本发明的溶剂配制的电子烟烟液香气充足,具有较好的谐调性,余味舒适,亦能产生较大的烟雾量,满足吸食者需求。本发明提供的电子烟烟液溶剂的组分均是食品级溶剂,对吸食者健康无害。 The invention provides a solvent suitable for fruity-flavored electronic cigarette liquid formulated by benzyl alcohol. The e-cigarette liquid prepared by using the solvent of the present invention has sufficient aroma, good harmony, comfortable aftertaste, and can produce a relatively large amount of smoke to meet the needs of smokers. The components of the e-cigarette liquid solvent provided by the present invention are all food-grade solvents, which are harmless to the health of smokers.
具体实施方式 Detailed ways
通过下述实施例对本发明做进一步的说明,但实施例并不是对本发明技术方案的限定。 The present invention is further described through the following examples, but the examples are not intended to limit the technical solution of the present invention.
实施例1Example 1
一种电子烟烟液溶剂,由以下质量分数的各组分混合调制而成:苯甲醇70 %、丙二醇15%、去离子水10%。准确称取各组分,室温下充分混合均匀,加入质量分数5%的香精香料(由以下质量分数的各组分组成:戊酸戊酯30%、丁酸戊酯25%、丁酸乙酯20%、乙酸乙酯15 %、乙酸戊酯4 %、乙酰乙酸乙酯3%、己醇3%),制得果香型电子烟烟液1。 An e-cigarette liquid solvent, which is prepared by mixing the following components in mass fractions: 70% benzyl alcohol, 15% propylene glycol, and 10% deionized water. Accurately weigh each component, mix well at room temperature, add 5% flavor and fragrance by mass fraction (composed of the following components by mass fraction: 30% amyl valerate, 25% amyl butyrate, ethyl butyrate 20%, 15% ethyl acetate, 4% amyl acetate, 3% ethyl acetoacetate, 3% hexanol), to obtain the fruity-flavored e-cigarette liquid 1.
实施例2Example 2
一种电子烟烟液溶剂,由以下质量分数的各组分混合调制而成:苯甲醇50 %、丙二醇15%、丙三醇15%、去离子水15%。准确称取各组分,室温下充分混合均匀,加入质量分数5%的香精香料(由以下质量分数的各组分组成:戊酸戊酯30%、丁酸戊酯25%、丁酸乙酯20%、乙酸乙酯15 %、乙酸戊酯4 %、乙酰乙酸乙酯3%、己醇3%),制得果香型电子烟烟液2。 An e-cigarette liquid solvent, which is prepared by mixing the following components in mass fractions: 50% benzyl alcohol, 15% propylene glycol, 15% glycerol, and 15% deionized water. Accurately weigh each component, mix well at room temperature, add 5% flavor and fragrance by mass fraction (composed of the following components by mass fraction: 30% amyl valerate, 25% amyl butyrate, ethyl butyrate 20%, 15% ethyl acetate, 4% amyl acetate, 3% ethyl acetoacetate, 3% hexanol), to obtain fruity flavor e-cigarette liquid 2.
实施例3Example 3
一种电子烟烟液溶剂,由以下质量分数的各组分混合调制而成:苯甲醇60 %、丙三醇25%离子水20%。准确称取各组分,室温下充分混合均匀,加入质量分数5%的香精香料(由以下质量分数的各组分组成:戊酸戊酯30%、丁酸戊酯25%、丁酸乙酯20%、乙酸乙酯15 %、乙酸戊酯4 %、乙酰乙酸乙酯3%、己醇3%),制得果香型电子烟烟液3。 An e-cigarette liquid solvent, which is prepared by mixing the following components in mass fractions: 60% benzyl alcohol, 25% glycerol, and 20% ionized water. Accurately weigh each component, mix well at room temperature, add 5% flavor and fragrance by mass fraction (composed of the following components by mass fraction: 30% amyl valerate, 25% amyl butyrate, ethyl butyrate 20%, ethyl acetate 15%, pentyl acetate 4%, ethyl acetoacetate 3%, hexanol 3%), and the fruity flavor e-cigarette liquid 3 was obtained.
对照例Comparative example
由以下质量分数的各组分混合调制而成:丙二醇70%、丙三醇15%、去离子水10%。准确称取各组分,室温下充分混合均匀,加入质量分数5%的香精香料(由以下质量分数的各组分组成:戊酸戊酯30%、丁酸戊酯25%、丁酸乙酯20%、乙酸乙酯15 %、乙酸戊酯4 %、乙酰乙酸乙酯3%、己醇3%),制得果香型电子烟烟液对照例。 It is prepared by mixing the following components in mass fractions: 70% propylene glycol, 15% glycerin, and 10% deionized water. Accurately weigh each component, mix well and evenly at room temperature, add 5% flavor and fragrance by mass fraction (composed of the following components by mass fraction: 30% amyl valerate, 25% amyl butyrate, ethyl butyrate 20%, ethyl acetate 15%, pentyl acetate 4%, ethyl acetoacetate 3%, hexanol 3%) to prepare a fruity-flavored e-cigarette liquid control example.
将制备的电子烟烟液1、电子烟烟液2、电子烟烟液对照例添加到电子烟中进行感官评析,结果表明:与对照例相比,利用本发明溶剂配制的电子烟烟液,雾化后与果香型香精香料谐调性更好,口感不腻,具有更高的吸食品质。 The prepared e-cigarette liquid 1, e-cigarette liquid 2, and e-cigarette liquid control example were added to electronic cigarettes for sensory evaluation. After atomization, it has better harmony with fruit flavor flavors and fragrances, the taste is not greasy, and it has higher smoking quality.
以上对本发明电子烟烟液溶剂及其加工方法进行了阐述,用于帮助理解本发明,但本发明的实施方式并不受上述实施例的限制,任何未背离本发明原理下所做的改变、修改、组合均应为等效的置换方式,都包含在本发明的保护范围之内。 The e-cigarette liquid solvent and its processing method of the present invention have been described above to help understand the present invention, but the implementation of the present invention is not limited by the above examples, and any changes made without departing from the principles of the present invention, Modifications and combinations should be equivalent replacement methods, and are included in the protection scope of the present invention.
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CN111269749A (en) * | 2020-03-17 | 2020-06-12 | 四川中烟工业有限责任公司 | A kind of fruit aroma base for cigarette and its application |
CN113693262A (en) * | 2021-08-30 | 2021-11-26 | 深圳市真味生物科技有限公司 | Fruit-flavor electronic cigarette liquid solvent prepared from benzyl alcohol |
CN114343231A (en) * | 2021-12-06 | 2022-04-15 | 四川三联新材料有限公司 | Electronic cigarette liquid with citrus-flavor aroma and preparation method thereof |
WO2024066095A1 (en) * | 2022-09-28 | 2024-04-04 | 深圳市真味生物科技有限公司 | Nicotine salt and atomized liquid thereof, vape cartridge and use |
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CN107418733A (en) * | 2017-07-05 | 2017-12-01 | 湖北民族学院 | A kind of compound method of banana flavor flavouring essence for tobacco |
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CN114343231A (en) * | 2021-12-06 | 2022-04-15 | 四川三联新材料有限公司 | Electronic cigarette liquid with citrus-flavor aroma and preparation method thereof |
WO2024066095A1 (en) * | 2022-09-28 | 2024-04-04 | 深圳市真味生物科技有限公司 | Nicotine salt and atomized liquid thereof, vape cartridge and use |
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