CN104312501B - A kind of preparation method of curry glue - Google Patents
A kind of preparation method of curry glue Download PDFInfo
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- CN104312501B CN104312501B CN201410584836.0A CN201410584836A CN104312501B CN 104312501 B CN104312501 B CN 104312501B CN 201410584836 A CN201410584836 A CN 201410584836A CN 104312501 B CN104312501 B CN 104312501B
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Abstract
The preparation method of a kind of curry glue of the present invention, the percentage by weight of curry collagen material is: macromolecule resin 1% to 15%, gel 3% to 12%, thinner 0.1% to 5%, antifreeze 1% to 10%, and all the other are water.Its preparation method comprises the following steps: step one, preparation raw material；Step 2, joining in stirred tank by thinner and water, stirring at normal temperature 5 minutes to 10 minutes is to being completely dissolved；Step 3, in stirred tank add gel, stirring at normal temperature 10 minutes to 40 minutes；Step 4, in stirred tank, add antifreeze and macromolecule resin, and stirring at normal temperature is completely dissolved to 90 minutes to resin for 30 minutes；Step 5, the liquid mixture filling and package that will obtain in step 4, obtain curry glue after standing 12 hours to 36 hours.Curry glue of the present invention, without poisonous and harmful substance, very easily rinses, and is highly suitable as student stationery and office appliance；Production process completes at normal temperatures, and technique is simple, with short production cycle；It is the liquid of good fluidity when having produced, it is easy to fill, in gel after standing.
Description
Technical field
The present invention relates to a kind of stationery, the specifically preparation method of a kind of curry glue.
Background technology
Current stationery class adhesive is mainly PVA liquid glue and solid glue stick.
But relatively low mostly needs of PVA liquid glue production cost adds formaldehyde reaction, and formaldehyde has toxicity, Producer and user is all had certain harm, especially the Producer for Long Term Contact, and hazardness is bigger.It addition, PVA liquid glue is in use difficult to well control flow, often it is coated with out a lot of rate of drying very slow；In carrying and using, the outflow that PVA liquid glue is easily unnecessary from bottle, brings worry to user.
Although solid gum relative liquid glue uses and carries more convenient, but relating to a lot of reacting by heating process in producing, complex process power consumption is relatively big, runs counter to the theory of energy-conserving and environment-protective, sustainable development；And, solid gum is not easy to fill.
Summary of the invention
The technical problem to be solved is for above-mentioned prior art present situation, and provides that formula is simple, produce easy, nontoxic a kind of curry glue, and its preparation method completes at normal temperatures, and technique is simple, with short production cycle, and fill is easy.
This invention address that the technical scheme that above-mentioned technical problem adopts is:
A kind of curry glue, the percentage by weight of each raw material is: macromolecule resin 1% to 15%, gel 3% to 12%, thinner 0.1% to 5%, antifreeze 1% to 10%, and all the other are water.
For optimizing technique scheme, the measure taked also includes:
Above-mentioned macromolecule resin is the one in polyvinylpyrrolidone and polyvinyl alcohol, or both mixture.
Above-mentioned polyvinylpyrrolidone be molecular weight 10000000 to 13000000 polyvinylpyrrolidonepowder powder；In embodiment, polyvinyl alcohol is the trade mark is the pva powder of 1788.
Above-mentioned gel is the one in lithium magnesium silicate and aluminium-magnesium silicate, or both mixture.
Above-mentioned thinner is one or more mixture in sodium hexameta phosphate, sodium pyrophosphate and sodium polyphosphate.
Above-mentioned antifreeze is one or more mixture in ethylene glycol, propylene glycol, glycerol.
The preparation method of a kind of curry glue: comprise the following steps:
Step one, preparation raw material；
Step 2, joining in stirred tank by thinner and water, stirring at normal temperature 5 minutes to 10 minutes is to being completely dissolved；
Step 3, in stirred tank add gel, stirring at normal temperature 10 minutes to 40 minutes；
Step 4, in stirred tank, add antifreeze and macromolecule resin, and stirring at normal temperature is completely dissolved to 90 minutes to resin for 30 minutes；
Step 5, the liquid mixture filling and package that will obtain in step 4, obtain curry glue after standing 12 hours to 36 hours.
Compared with prior art, it is an advantage of the current invention that the advantages of nontoxic raw materials of this curry glue is harmless, high safety.This curry glue only need to stir at normal temperatures when producing and make raw material fully dissolve and mix homogeneously, and technique is simple, with short production cycle；It is the liquid of good fluidity when having produced, it is easy to fill, in gel after standing, no longer there is mobility, it is possible to effectively prevent from carrying the outflow unnecessary with in use procedure.
It addition, curry glue of the present invention is without poisonous and harmful substance, very easily rinse, be highly suitable as student stationery and office appliance.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
A kind of curry glue, the percentage by weight of each raw material is: macromolecule resin 1% to 15%, gel 3% to 12%, thinner 0.1% to 5%, antifreeze 1% to 10%, and all the other are water.
In embodiment, macromolecule resin is the one in polyvinylpyrrolidone and polyvinyl alcohol, or both mixture.
In embodiment, polyvinylpyrrolidone be molecular weight 10000000 to 13000000 polyvinylpyrrolidonepowder powder；In embodiment, polyvinyl alcohol is the trade mark is the pva powder of 1788.
In embodiment, gel is the one in lithium magnesium silicate and aluminium-magnesium silicate, or both mixture.
In embodiment, thinner is one or more mixture in sodium hexameta phosphate, sodium pyrophosphate and sodium polyphosphate.
In embodiment, antifreeze is one or more mixture in ethylene glycol, propylene glycol, glycerol.
The preparation method of a kind of curry glue: comprise the following steps:
Step one, preparation raw material；
Step 2, joining in stirred tank by thinner and water, stirring at normal temperature 5 minutes to 10 minutes is to being completely dissolved；
Step 3, in stirred tank add gel, stirring at normal temperature 10 minutes to 40 minutes；
Step 4, in stirred tank, add antifreeze and macromolecule resin, and stirring at normal temperature is completely dissolved to 90 minutes to resin for 30 minutes；
Step 5, the liquid mixture filling and package that will obtain in step 4, obtain curry glue after standing 12 hours to 36 hours.
Embodiment one:
Step one, according to following percentage by weight prepare raw material:
Macromolecule resin: polyvinylpyrrolidone 5%
Thinner: sodium pyrophosphate 0.8%
Gel: lithium magnesium silicate 6%
Antifreeze: propylene glycol 5%
All the other are water.
Step 2, adding in stirred tank by sodium pyrophosphate and water, stirring at normal temperature 5 minutes to 10 minutes is to being completely dissolved；
Step 3, in stirred tank add lithium magnesium silicate, stirring at normal temperature 10 minutes to 40 minutes；
Step 4, in stirred tank, add propylene glycol and polyvinylpyrrolidone, and stirring at normal temperature is completely dissolved to 90 minutes to resin for 30 minutes；
Step 5, the liquid mixture filling and package that will obtain in step 4, obtain gelatinous curry glue after standing 12 hours to 36 hours.
Embodiment two:
Step one, according to following percentage by weight prepare raw material:
Macromolecule resin: polyvinyl alcohol 17888%
Thinner: sodium pyrophosphate 0.8%
Gel: lithium magnesium silicate 6%
Antifreeze: ethylene glycol 6%
All the other are water.
Step 2, adding in stirred tank by sodium pyrophosphate and water, stirring at normal temperature 5 minutes to 10 minutes is to being completely dissolved；
Step 3, in stirred tank add lithium magnesium silicate, stirring at normal temperature 10 minutes to 40 minutes；
Step 4, in stirred tank, add ethylene glycol and polyvinyl alcohol 1788, and stirring at normal temperature is completely dissolved to 90 minutes to resin for 30 minutes；
Step 5, the liquid mixture filling and package that will obtain in step 4, obtain gelatinous curry glue after standing 12 hours to 36 hours.
Embodiment three,
Step one, according to following percentage by weight prepare raw material:
Macromolecule resin: polyvinyl alcohol 17888%
Polyvinylpyrrolidone 2%
Thinner: sodium hexameta phosphate 0.2%
Sodium pyrophosphate 1%
Gel: aluminium-magnesium silicate 8%
Antifreeze: glycerol 7%
All the other are water.
Adding in stirred tank together with step 2, the thinner mixed with sodium pyrophosphate by sodium hexameta phosphate and water, stirring at normal temperature 5 minutes to 10 minutes is to being completely dissolved；
Step 3, in stirred tank add aluminium-magnesium silicate, stirring at normal temperature 10 minutes to 40 minutes；
Step 4, in stirred tank, add glycerol and the macromolecule resin that mixed by polyvinyl alcohol 1788 and polyvinylpyrrolidone, and stirring at normal temperature is completely dissolved to 90 minutes to resin for 30 minutes；
Step 5, the liquid mixture filling and package that will obtain in step 4, obtain gelatinous curry glue after standing 12 hours to 36 hours.
Embodiment four:
Step one, according to following percentage by weight prepare raw material:
Macromolecule resin: polyvinyl alcohol 17881%
Polyvinylpyrrolidone 5%
Thinner: sodium polyphosphate 0.5%
Sodium pyrophosphate 0.5%
Gel: aluminium-magnesium silicate 3%
Lithium magnesium silicate 3%
Antifreeze: ethylene glycol 2%
Propylene glycol 4%
All the other are water.
Adding in stirred tank together with step 2, the thinner mixed with sodium pyrophosphate by sodium polyphosphate and water, stirring at normal temperature 5 minutes to 10 minutes is to being completely dissolved；
Step 3, in stirred tank, add the gel mixed by aluminium-magnesium silicate and lithium magnesium silicate, stirring at normal temperature 10 minutes to 40 minutes；
Step 4, in stirred tank, add the antifreeze by ethylene glycol and mixed with propylene glycol and the macromolecule resin mixed by polyvinyl alcohol 1788 and polyvinylpyrrolidone, and stirring at normal temperature is completely dissolved to 90 minutes to resin for 30 minutes；
Step 5, the liquid mixture filling and package that will obtain in step 4, obtain gelatinous curry glue after standing 12 hours to 36 hours.
Embodiment five:
Curry glue in the present embodiment, composed as follows according to percentage by weight raw material:
Macromolecule resin: polyvinylpyrrolidone 8%
Thinner: sodium pyrophosphate 1.2%
Gel: aluminium-magnesium silicate 2%
Lithium magnesium silicate 5%
Antifreeze: glycerol 7%
All the other are water.
Embodiment six:
Curry glue in the present embodiment, composed as follows according to percentage by weight raw material:
Macromolecule resin: polyvinylpyrrolidone 10%
Thinner: sodium pyrophosphate 0.3%
Sodium polyphosphate 0.5%
Sodium hexameta phosphate 0.2%
Gel: aluminium-magnesium silicate 2%
Lithium magnesium silicate 5%
Antifreeze: propylene glycol 10%
All the other are water.
Embodiment seven:
Curry glue in the present embodiment, composed as follows according to percentage by weight raw material:
Macromolecule resin: polyvinyl alcohol 17881%
Polyvinylpyrrolidone 5%
Gel: sodium polyphosphate 1.5%
Gel: lithium magnesium silicate 3%
Antifreeze: ethylene glycol 3%
Propylene glycol 3%
Glycerol 4%
All the other are water.
Highly preferred embodiment of the present invention illustrates, those of ordinary skill in the art the various changes made or remodeling are all without departing from the scope of the present invention.
Claims (6)
1. the preparation method of a curry glue: it is characterized in that: the percentage by weight of each raw material of curry glue is: macromolecule resin 1% to 15%, gel 3% to 12%, thinner 0.1% to 5%, antifreeze 1% to 10%, and all the other are water；The preparation method of curry glue comprises the following steps:
Step one, preparation raw material；
Step 2, joining in stirred tank by thinner and water, stirring at normal temperature 5 minutes to 10 minutes is to being completely dissolved；
Step 3, in stirred tank add gel, stirring at normal temperature 10 minutes to 40 minutes；
Step 4, in stirred tank, add antifreeze and macromolecule resin, and stirring at normal temperature is completely dissolved to 90 minutes to resin for 30 minutes；
Step 5, the liquid mixture filling and package that will obtain in step 4, obtain curry glue after standing 12 hours to 36 hours.
2. the preparation method of a kind of curry glue according to claim 1, is characterized in that: described macromolecule resin is the one in polyvinylpyrrolidone and polyvinyl alcohol, or both mixture.
3. the preparation method of a kind of curry glue according to claim 2, is characterized in that: described polyvinylpyrrolidone be molecular weight 10000000 to 13000000 polyvinylpyrrolidonepowder powder；Described polyvinyl alcohol is the trade mark is the pva powder of 1788.
4. the preparation method of a kind of curry glue according to claim 3, is characterized in that: described gel is the one in lithium magnesium silicate and aluminium-magnesium silicate, or both mixture.
5. the preparation method of a kind of curry glue according to claim 4, is characterized in that: described thinner is one or more mixture in sodium hexameta phosphate, sodium pyrophosphate and sodium polyphosphate.
6. the preparation method of a kind of curry glue according to claim 5, is characterized in that: described antifreeze is one or more mixture in ethylene glycol, propylene glycol, glycerol.
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| CN201410584836.0A CN104312501B (en) | 2014-10-28 | 2014-10-28 | A kind of preparation method of curry glue |
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| CN201410584836.0A CN104312501B (en) | 2014-10-28 | 2014-10-28 | A kind of preparation method of curry glue |
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| CN104312501A CN104312501A (en) | 2015-01-28 |
| CN104312501B true CN104312501B (en) | 2016-06-29 |
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| CN201410584836.0A Expired - Fee Related CN104312501B (en) | 2014-10-28 | 2014-10-28 | A kind of preparation method of curry glue |
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| CN108485597A (en) * | 2018-03-14 | 2018-09-04 | 东莞市东彩印刷包装有限公司 | A kind of environmental protection fruit juice gel and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1192460A (en) * | 1996-12-17 | 1998-09-09 | 株式会社寿 | Solid adhesive |
| CN101220252A (en) * | 2008-01-25 | 2008-07-16 | 中北大学 | A kind of solid glue stick and preparation method thereof |
| CN101608103A (en) * | 2008-06-18 | 2009-12-23 | 宁波松鹤文具有限公司 | A kind of allochroic solid adhesive and preparation method thereof |
| CN102321443A (en) * | 2011-09-15 | 2012-01-18 | 宋仕良 | Environmental protection type transparent solid glue and preparation method thereof |
-
2014
- 2014-10-28 CN CN201410584836.0A patent/CN104312501B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1192460A (en) * | 1996-12-17 | 1998-09-09 | 株式会社寿 | Solid adhesive |
| CN101220252A (en) * | 2008-01-25 | 2008-07-16 | 中北大学 | A kind of solid glue stick and preparation method thereof |
| CN101608103A (en) * | 2008-06-18 | 2009-12-23 | 宁波松鹤文具有限公司 | A kind of allochroic solid adhesive and preparation method thereof |
| CN102321443A (en) * | 2011-09-15 | 2012-01-18 | 宋仕良 | Environmental protection type transparent solid glue and preparation method thereof |
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Granted publication date: 20160629 Termination date: 20171028 |