CN104195002B - A kind of production method of mulberries brandy - Google Patents
A kind of production method of mulberries brandy Download PDFInfo
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Abstract
本发明涉及一种桑葚白兰地的生产方法,属于酿酒技术领域,包括原材料的筛选和破碎、原料成分的调整、果浆发酵、过滤分离、果渣发酵、二次过滤、调色及恒温储存、调配勾兑、冷冻澄清、低温灌装等步骤。本发明改进以往的清汁发酵方式,克服了桑葚产量低,并且含糖量低于葡萄,酸度高等特点,制得风味独特的桑葚白兰地酒,酒度在40%-43%。
The invention relates to a production method of mulberry brandy, belonging to the technical field of brewing, including screening and crushing of raw materials, adjustment of raw material components, fruit pulp fermentation, filtration separation, pomace fermentation, secondary filtration, color matching, constant temperature storage, and deployment Blending, freezing clarification, low temperature filling and other steps. The invention improves the previous clear juice fermentation method, overcomes the characteristics of low mulberry yield, lower sugar content than grapes, and high acidity, and prepares mulberry brandy with unique flavor and alcohol content of 40%-43%.
Description
技术领域technical field
本发明属于酿酒技术领域,具体是一种桑葚白兰地的生产方法。The invention belongs to the technical field of brewing, in particular to a production method of mulberry brandy.
背景技术Background technique
桑甚为红紫色或黑色椭圆型聚合果,汁浓且甜酸清香,富含硒、白黎芦醇、花青素、氨基酸、黄酮、多糖以及钙、铁、钾、磷、锌等矿物质,还含有大量游离酸和各种氨基酸以及人体所需的微量元素及胡萝卜素、果糖等。Mulberry is very reddish-purple or black oval-shaped aggregate fruit, with thick juice, sweet and sour fragrance, rich in selenium, resveratrol, anthocyanins, amino acids, flavonoids, polysaccharides, calcium, iron, potassium, phosphorus, zinc and other minerals , It also contains a large amount of free acid and various amino acids, as well as trace elements needed by the human body, carotene, fructose, etc.
我国是世界蚕桑发源地,资源丰富,桑葚产量均位居世界首位。桑葚属于热性浆果,皮薄汁多,营养丰富,但季节性强,常温下,极不耐贮藏,易腐烂变质。采摘后应及时处理,来延长其货架期,或加工生产其他桑葚产品,如桑葚罐头、桑葚膏、桑葚饮料、桑葚醋、桑葚酒等等。桑葚的价值如此高,但目前产业化的程度并不高,民间有许多制作桑葚白酒的方法,但这些桑葚白酒因其制作工艺方面存在问题,所以所酿成的酒质量及口感都较差。现有技术中,桑葚白兰地的生产大都沿用葡萄白兰地的生产,这其中也包括白兰地的调色,一般的白兰地在装瓶前都会采用橡木桶进行陈酿,这样酒液的颜色便从原来的透明无色,变成了琥珀色,由于各桶内白兰地贮存中色泽变化不同,因而需人工调整,以保持不同批产品间色泽的一致性,普遍采用的是加糖色,但我国的焦糖工业是非常落后,绝大部分产量是由作坊式的手工方法生产的,能够用比较科学的方法生产的厂家寥寥无几,而且仅能生产单一的在酱油中应用的耐盐焦糖,品质较差,卫生指标也很差。近期百事可乐中添加的焦糖色素中再次检测出了含有可能致癌的4-甲基咪唑,尽管4-甲基咪唑是否对人类致癌存在争议,但已有数据显示可能导致动物致癌。因此用焦糖色素对白兰地调色应该谨慎使用,利用天然色素对白兰地进行调色可避免市场上焦糖色素参差不齐的产品质量对白兰地产生不利人体健康的物质。除此之外,桑葚还具有产量有限、远不及葡萄的规模、含糖量低于葡萄,酸度高的特点,使其完全采用常规的工艺并不能获得好的品质。my country is the birthplace of sericulture in the world, rich in resources, and the output of mulberry ranks first in the world. Mulberry is a hot berry with thin skin, rich juice and rich nutrition. However, it has strong seasonality. It is not resistant to storage at room temperature and is easy to rot and deteriorate. After picking, it should be processed in time to extend its shelf life, or to process and produce other mulberry products, such as canned mulberry, mulberry paste, mulberry drink, mulberry vinegar, mulberry wine, etc. The value of mulberry is so high, but the degree of industrialization is not high at present. There are many methods for making mulberry liquor among the people, but these mulberry liquors have problems in the production process, so the quality and taste of the wine produced are relatively poor. In the prior art, the production of mulberry brandy mostly follows the production of grape brandy, which also includes the coloring of the brandy. General brandy will be aged in oak barrels before bottling, so that the color of the wine will change from the original transparent colorless Because of the different color changes in the storage of brandy in each barrel, manual adjustment is required to maintain the consistency of color between different batches of products. Sugaring color is generally used, but my country's caramel industry is very Backward, most of the output is produced by workshop-style manual methods, and there are very few manufacturers that can produce with more scientific methods, and can only produce a single salt-resistant caramel used in soy sauce, with poor quality and hygienic indicators Also very poor. Recently, 4-methylimidazole, which may cause cancer, was detected again in the caramel coloring added to Pepsi-Cola. Although there is controversy about whether 4-methylimidazole is carcinogenic to humans, existing data show that it may cause cancer in animals. Therefore, caramel pigments should be used with caution in coloring brandy. Using natural pigments to color brandy can prevent the uneven product quality of caramel pigments on the market from producing harmful substances to brandy. In addition, mulberry also has the characteristics of limited yield, far smaller scale than grapes, lower sugar content than grapes, and high acidity, making it impossible to obtain good quality by using conventional techniques.
发明内容Contents of the invention
本发明的目的是提供一种桑葚白兰地的生产方法,克服现有技术的缺陷,以制得口味纯正,风味独特的桑葚白兰地酒。The purpose of the present invention is to provide a kind of production method of mulberry brandy, overcome the defective of prior art, to make mulberry brandy with pure taste and unique flavor.
为实现上述目的,本发明所采取的技术方案是:一种桑葚白兰地的生产方法,包括以下步骤:In order to achieve the above object, the technical solution adopted by the present invention is: a production method of mulberry brandy, comprising the following steps:
(1)筛选、破碎:采摘、挑选成熟完好度好的桑葚果,破碎压榨成果浆;储存在不锈钢罐中,并立即加入50mg/L的SO2防止氧化和抑制杂菌生长;(1) Screening and crushing: picking and selecting mulberry fruits with good maturity and integrity, crushing and pressing into pulp; storing in stainless steel tanks, and immediately adding 50mg/L SO 2 to prevent oxidation and inhibit the growth of miscellaneous bacteria;
(2)原料成分的调整:调整桑葚果浆的糖度和pH,使发酵结束后酒精度达到8%-12%;(2) Adjustment of raw material components: adjust the sugar content and pH of the mulberry pulp, so that the alcohol content reaches 8%-12% after the fermentation is finished;
(3)果浆发酵:将桑葚果浆送入发酵罐,添加活性干酵母,使在低于22℃的条件下连续发酵10天以上,期间进行通风搅拌;发酵15天后对发酵液残糖量和挥发酸含量进行检测,并品尝原酒口味;(3) Fermentation of fruit pulp: send mulberry pulp into a fermenter, add active dry yeast, make continuous fermentation at a temperature lower than 22°C for more than 10 days, and carry out ventilation and stirring during the period; after 15 days of fermentation, the residual sugar content of the fermentation liquid and volatile acid content were tested, and the taste of the original wine was tasted;
(4)过滤分离:将发酵物料进行过滤分离,过滤所得果渣备用,分离所得原酒立即进行蒸馏,所得原酒原白兰地酒储存备用;(4) Filtration and separation: the fermented material is filtered and separated, the pomace obtained by filtration is for subsequent use, the original wine obtained after separation is immediately distilled, and the original brandy of the obtained original wine is stored for subsequent use;
(5)果渣发酵:过滤所得果渣继续在发酵罐中2℃-4℃恒温、密封条件下发酵25-30天;(5) Fermentation of pomace: the pomace obtained by filtering continues to ferment for 25-30 days in a fermenter at a constant temperature of 2°C-4°C and under sealed conditions;
(6)二次过滤:果渣发酵完成后,进行过滤,所得滤液立即进行蒸馏,所得果渣原白兰地酒储存备用;(6) secondary filtration: after the pomace fermentation is completed, filter, the gained filtrate is distilled immediately, and the former brandy of the pomace is stored for subsequent use;
(7)调色及恒温储存:用900mL稀释后的白兰地浸泡藏25g红花,每天间歇搅拌2-3次,在常温下浸泡15天后过滤获得色泽深红的澄清母液,密封储存;将母液加入到白兰地中搅拌充分混合调色,进行人工老熟操作,恒温密封储存2个月,并分期进行降酒度和储存,得到原酒白兰地和果渣白兰地。(7) Color matching and constant temperature storage: soak 25g safflower in 900mL diluted brandy, stir intermittently 2-3 times a day, soak at room temperature for 15 days, filter to obtain a clear mother liquor with dark red color, and store it in a sealed container; add the mother liquor to Stir it into the brandy, mix it thoroughly, mix the color, carry out artificial aging operation, store it in a constant temperature seal for 2 months, and reduce the alcohol content and store it in stages to obtain raw wine brandy and pomace brandy.
(8)调配勾兑:将降度和储存后的原酒白兰地酒和果渣白兰地酒进行勾兑,储存8个月,得到陈酿酒;(8) Blending and blending: blending the original wine brandy and pomace brandy after the reduction and storage, and storing for 8 months to obtain aged wine;
(9)冷冻澄清:将陈酿酒保持在-15℃的条件下7天,乘冷进行过滤,促进白兰地的稳定;(9) Frozen clarification: keep the aged wine at -15°C for 7 days, and filter while cold to promote the stability of the brandy;
(10)低温灌装:将过滤滤液在4℃的条件下进行灌装,既得产品桑葚白兰地。(10) Filling at low temperature: filling the filtered filtrate at 4°C to obtain the mulberry brandy.
在上述酿造方法中,步骤(1)所述果浆在2-4小时内进行发酵。In the above brewing method, the pulp in step (1) is fermented within 2-4 hours.
在上述酿造方法中,步骤(2)所述调整桑葚果浆糖度用脱水桑椹果或/和浓度为65°Bx的桑椹果汁进行调整;调整后原料糖度控制在23°Bx,PH值调整为3.2-3.5。In the above brewing method, the adjustment of mulberry pulp sugar content in step (2) is adjusted with dehydrated mulberry fruit or/and mulberry fruit juice with a concentration of 65°Bx; the adjusted raw material sugar content is controlled at 23°Bx, and the pH value is adjusted to 3.2 -3.5.
在上述酿造方法中,步骤(3)所述检测的发酵液残糖量<4g/L,所述检测的挥发酸含量≤0.5g/L。In the above brewing method, the detected residual sugar content of the fermentation broth in step (3) is <4g/L, and the detected volatile acid content is ≤0.5g/L.
在上述酿造方法中,步骤(4)所述原酒原白兰地酒的体积分数为65%-70%。In the above brewing method, the volume fraction of the original brandy in the step (4) is 65%-70%.
在上述酿造方法中,步骤(7)所述稀释后的白兰地酒精度为40%-43%,搅拌调色中母液的质量百分含量为2%-4%,白兰地的质量百分含量为96%-98%。In the above brewing method, the alcohol content of the diluted brandy in step (7) is 40%-43%, the mass percentage of the mother liquor in the stirring and toning is 2%-4%, and the mass percentage of the brandy is 96%. %-98%.
在上述酿造方法中,步骤(8)所述储存期间定期向勾兑的桑葚白兰地酒通入17-20mg/L的氧气。In the above-mentioned brewing method, the oxygen of 17-20 mg/L is passed into the blended mulberry brandy regularly during the storage period described in step (8).
本发明的有益效果是:The beneficial effects of the present invention are:
1)采用100%纯桑葚破碎后汁液和果渣混合发酵、过滤后果渣再次发酵的二次发酵和勾兑方式,改进以往的清汁发酵方式,克服了桑葚产量低,并且含糖量低于葡萄,酸度高等特点。1) Adopt the secondary fermentation and blending method of 100% pure mulberry crushed juice and pomace mixed fermentation, filtered fruit residue fermented again, improve the previous clear juice fermentation method, overcome the low yield of mulberries, and the sugar content is lower than that of grapes, Characterized by high acidity.
2)采用藏红花对白兰地进行调色,能够避免市场上的焦糖色素参差不起的产品质量对白兰地产生不利于人体健康的物质;并且能够使白兰地呈现金黄色,晶莹剔透,具有陈酿的果香和醇和的藏红花香气,调高了本质,丰满了口感,并促进了健康。2) Use saffron to color the brandy, which can prevent the caramel pigments on the market with uneven product quality from producing substances that are not conducive to human health; and can make the brandy golden yellow, crystal clear, and have an aged fruity aroma The mellow aroma of saffron heightens the essence, rounds out the palate, and promotes health.
3)生产的桑葚白兰地酒,酒度在40%-43%(体积分数),并且口味纯正,风味独特。3) The mulberry brandy produced has an alcohol content of 40%-43% (volume fraction), and has pure taste and unique flavor.
附图说明Description of drawings
图1为本发明方法的工艺流程框图。Fig. 1 is a process flow diagram of the method of the present invention.
具体实施方式detailed description
采用广东化州种植的桑葚原料,其100g鲜果中含有花青素含量高达250mg,具有原料比较优势。The mulberries grown in Huazhou, Guangdong are used as raw materials, and 100g of fresh fruits contain anthocyanins as high as 250mg, which has comparative advantages in raw materials.
在桑葚果成熟度达到要求时采摘,人工筛选出生青果、霉烂果,清洗,破碎打浆,2-4小时内进入发酵,以保证原料的新鲜纯正;When the maturity of the mulberry fruit reaches the requirement, it is picked manually, and the green fruit and moldy fruit are manually screened, cleaned, crushed and beaten, and fermented within 2-4 hours to ensure the freshness and purity of the raw material;
接着进行原料调整:白兰地的原料酒以11%计,原料糖度在22°Bx,糖度调整使用部分脱水果或浓缩汁;pH值调整在3.2-3.5间;Carry out raw material adjustment then: the raw material wine of brandy is in 11%, and raw material sugar content is at 22 ° of Bx, and sugar content adjustment uses part depleted fruit or concentrated juice; pH value is adjusted between 3.2-3.5;
将桑葚果浆送入发酵罐,添加0.25g/kg活性干酵母,温度控制在22℃以下连续发酵10天以上,期间进行通风搅拌;发酵15天后检测残糖和挥发酸,并品尝原酒口味,符合要求后过滤;发酵液进行过滤,分离原酒和皮渣;过滤后的原酒立即进行蒸馏,得到酒度(体积分数)为65%-70%的原酒原白兰地酒储存、备用;Put the mulberry pulp into the fermentation tank, add 0.25g/kg active dry yeast, and keep the temperature below 22°C for continuous fermentation for more than 10 days, during which ventilation and stirring are carried out; after 15 days of fermentation, detect the residual sugar and volatile acid, and taste the taste of the original wine, Filter after meeting the requirements; filter the fermented liquid to separate the original wine and skin dregs; distill the filtered original wine immediately to obtain the original brandy of the original wine with an alcohol content (volume fraction) of 65%-70% for storage and standby;
分离出的果渣在4℃恒温发酵25天,再采用二次蒸馏法得到65%-70%(体积分数)的果渣原白兰地。The isolated pomace is fermented at a constant temperature of 4° C. for 25 days, and then a secondary distillation method is used to obtain 65%-70% (volume fraction) of the original pomace brandy.
对白兰地进行调色,包括下列步骤:A.母液的制备:称25g藏红花加入900mL稀释后酒精度为40%(V/V)的白兰地中,每天间歇搅拌混合物2-3次,在常温下浸泡15天后过滤成色泽深红的澄清母液,密封贮存;B.白兰地调色:将母液加入到白兰地中搅拌充分混合,其中白兰地的质量百分含量为97.5%,母液的质量百分含量为2.5%,然后在32℃下恒温密封,储存2个月,并分两次进行降酒度,第一次降至体积分数的酒度50%左右,储存时间稍长些,第二次酒度降至40%-43%;储存期间定期通氧促进氧化反应;Brandy is carried out toning, comprises the following steps: A. the preparation of mother liquor: weigh 25g saffron and add 900mL diluted back in the brandy that alcoholic strength is 40% (V/V), stir mixture 2-3 time every day intermittently, soak at normal temperature After 15 days, filter into the clarified mother liquor of dark red color, and seal it for storage; B. brandy coloring: mother liquor is added in the brandy and stirred and fully mixed, wherein the mass percentage of brandy is 97.5%, and the mass percentage of mother liquor is 2.5% , and then sealed at a constant temperature at 32°C, stored for 2 months, and the alcohol content was reduced twice, the first time the alcohol content was reduced to about 50% of the volume fraction, the storage time was a little longer, and the second alcohol content was reduced to 50%. 40%-43%; regular oxygenation during storage to promote oxidation reaction;
之后,将备用的果渣白兰地和原酒白兰地进行勾兑,再储存8个月,定期向勾兑的酒通入18mg/L的氧气,得到陈酿酒;Afterwards, the standby pomace brandy and original wine brandy are blended, stored for another 8 months, and 18 mg/L of oxygen is regularly introduced into the blended wine to obtain aged wine;
最后,将储存后陈酿白兰地酒在冷冻室内冷冻至-15℃,放置7天,过滤其中沉淀物,并促进白兰地的稳定;在4℃下低温灌装、压盖、贴标、装箱入库,得到产品桑葚白兰地。Finally, freeze the aged brandy after storage to -15°C in the freezer, place it for 7 days, filter the sediment in it, and promote the stability of the brandy; fill, cap, label, and put it into storage at a low temperature of 4°C , to obtain the product mulberry brandy.
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