CN104189397B - Remove scorching tincture and preparation method thereof - Google Patents
Remove scorching tincture and preparation method thereof Download PDFInfo
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- CN104189397B CN104189397B CN201410463501.3A CN201410463501A CN104189397B CN 104189397 B CN104189397 B CN 104189397B CN 201410463501 A CN201410463501 A CN 201410463501A CN 104189397 B CN104189397 B CN 104189397B
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- Cosmetics (AREA)
Abstract
The present invention relates to scorching tincture and preparation method thereof is removed, belong to technical field of traditional Chinese medicines.This goes scorching tincture to include following component in parts by weight：22 26 parts of Paris polyphylla, 32 34 parts of rheum officinale, 45 parts of safflower, 7 10 parts of the root of Dahurain angelica, 15 18 parts of giant knotweed, 79 parts of Asian puccoon, 79 parts of radix aconiti agrestis, 11 14 parts of RADIX PSAMMOSILENE, 23 parts of vomiting nut, 16 18 parts of arisacma consanguineum schott, 16 18 parts of kuh-seng, 15 18 parts of the red sage root, 47 parts of short-pedicel aconite root.The present invention goes the preparation method of scorching tincture simply, and obtained to go scorching tincture to have good removing damp-heat, purging intense heat and detonicating is promoting blood circulation and removing blood stasis, the effect of swelling and pain relieving and anti-inflammatory apocenosis.
Description
Technical field
The invention belongs to technical field of traditional Chinese medicines, and in particular to remove scorching tincture and preparation method thereof.
Background technology
Existing in the market has promoting blood circulation to remove blood stasis, although the external used medicine of swelling and pain relieving effect is a lot, their function compared with
To be limited, such as Yunnan Baiyao aerosol, although with promoting blood circulation to remove blood stasis, swelling and pain relieving effect, for traumatic injury, blood stasis and swelling pain,
DOMS and rheumatalgia pain, but trauma infection contamination, ulcer, boil, bite by mosquitos, itchy skin eruption are may not be usable for, with office
It is sex-limited.
The existing medicine for itchy skin eruption is generally western medicine composition such as antiallergy class, steroids class on the market at present, its
Side effect is big.Therefore the problem of the deficiencies in the prior art are current technical field of traditional Chinese medicines urgent need to resolve how is overcome.
The content of the invention
The invention aims to solve the deficiencies in the prior art there is provided one kind to remove scorching tincture and preparation method thereof.This goes
The preparation method of scorching tincture is simple, and obtained to go scorching tincture to have good removing damp-heat, purging intense heat and detonicating is promoting blood circulation and removing blood stasis, swelling and pain relieving
With the effect of anti-inflammatory apocenosis, available for traumatic injury, trauma infection contamination, ulcer, boil, bite by mosquitos, itchy skin eruption.With existing skill
Art is compared, and removes scorching tincture for pure Chinese medicinal preparation, Small side effects, and production technology is easy, cheap.
The technical solution adopted by the present invention is as follows：
Go scorching tincture, including following component in parts by weight：22-26 parts of Paris polyphylla, 32-34 parts of rheum officinale, safflower 4-5
Part, 7-10 parts of the root of Dahurain angelica, 15-18 parts of giant knotweed, 7-9 parts of Asian puccoon, 7-9 parts of radix aconiti agrestis, 11-14 parts of RADIX PSAMMOSILENE, 2-3 parts of vomiting nut, raw south
16-18 parts of star, 16-18 parts of kuh-seng, 15-18 parts of the red sage root, 4-7 parts of short-pedicel aconite root.
It is further preferred that described goes scorching tincture, including following component in parts by weight：It is 25 parts of Paris polyphylla, big
Yellow 33.3 parts, 4.2 parts of safflower, 8.4 parts of the root of Dahurain angelica, 16.7 parts of giant knotweed, 8.4 parts of Asian puccoon, 8.4 parts of radix aconiti agrestis, 12.5 parts of RADIX PSAMMOSILENE, Strychnos nux-vomica
2.5 parts of son, 16.7 parts of arisacma consanguineum schott, 16.7 parts of kuh-seng, 16.7 parts of the red sage root, 5.8 parts of short-pedicel aconite root.
The present invention also provides a kind of preparation method for removing scorching tincture, comprises the following steps：
Step（1）, by Paris polyphylla, rheum officinale, safflower, the root of Dahurain angelica, giant knotweed, Asian puccoon, radix aconiti agrestis, RADIX PSAMMOSILENE, vomiting nut, arisacma consanguineum schott, hardship
Ginseng, the red sage root and short-pedicel aconite root are ground into coarse powder together；
Step（2）, 62-68% ethanol as solvent is used, by step（1）Obtained coarse powder steeped overnight, is then added into
In percolator, add 62-68% ethanol to liquid level and be higher by medicinal material surface, place 20-26 hours；
Step（3）, through step（2）After placement, percolation extraction is carried out using ethanol as solvent is leached, regulation extract solution contains
Alcohol amount is 55-65%, stands, produces.
It is further preferred that described step（3）In using 63% ethanol be used as leach solvent.
It is further preferred that described step（3）Middle time of repose is 12-24h.
It is further preferred that the described preparation method for removing scorching tincture, comprises the following steps：
Step（1）, by Paris polyphylla, rheum officinale, safflower, the root of Dahurain angelica, giant knotweed, Asian puccoon, radix aconiti agrestis, RADIX PSAMMOSILENE, vomiting nut, arisacma consanguineum schott, hardship
Ginseng, the red sage root and short-pedicel aconite root are ground into coarse powder together；
Step（2）, 65% ethanol as solvent is used, by step（1）Obtained coarse powder steeped overnight, is then added into diacolation
In cylinder, add 65% ethanol to liquid level and be higher by medicinal material surface, place 24 hours；
Step（3）, through step（2）After placement, percolation extraction is carried out using ethanol as solvent is leached, regulation extract solution contains
Alcohol amount is 55-65%, stands, produces.
Product composition of the present invention differentiates：
（1）Product 20ml of the present invention is taken, is evaporated, residue adds 2mol/L hydrochloric acid 30ml, is heated to reflux 1 hour, is filtered, filtrate
Plus the shaking of 30ml ether is extracted, water bath method ether, then make dissolving with chloroform 1ml, it is used as need testing solution.Separately take Dioscin
First reference substance, solution of every 1ml containing 2mg is made of chloroform, reference substance solution is used as.According to thin-layered chromatography（Chinese Pharmacopoeia one
Annex VI B）Experiment, draws each 10 μ l of above two solution, puts respectively on same silica gel g thin-layer plate, with chloroform-methanol
（Volume ratio is 95：5）For solvent, deploy, take out, dry, developed the color with 5% phosphomolybdic acid ethanol solution, about 10 points are dried at 105 DEG C
In clock, test sample chromatogram, on position corresponding with reference substance chromatogram, show the spot of same color.
（2）Take discriminating（1）Sample liquid makees need testing solution under.Separately rheum emodin, Chrysophanol reference substance is taken to be made of chloroform
Per each solution containing 1mg of 1ml, reference substance solution is used as.According to thin-layered chromatography（One annex VI B of Chinese Pharmacopoeia）Experiment, respectively
Each 10 μ l of above two solution are drawn, are put respectively on same silica gel g thin-layer plate, with petroleum ether-ethyl acetate-formic acid（Body
Product is than being 15：5：1）Upper solution be solvent, deploy, take out, dry, put and inspected under uviol lamp, in test sample chromatogram,
On position corresponding with control chromatogram, show the spot of same color.
In this product chromatogram, with corresponding reference substance chromatogram relevant position, showing the spot of same color.
Compared with prior art, its advantage is the present invention：（1）The present invention goes the preparation method of scorching tincture simple, is made
Go scorching tincture that there is good removing damp-heat, purging intense heat and detonicating is promoting blood circulation and removing blood stasis, the effect of swelling and pain relieving and anti-inflammatory apocenosis；（2）This hair
Bright product cures mainly traumatic injury, trauma infection contamination, ulcer, boil, bite by mosquitos, itchy skin eruption；（3）Compared with prior art, go
Scorching tincture is pure Chinese medicinal preparation, Small side effects, and production technology is easy, cheap.
Embodiment
With reference to embodiment, the present invention is described in further detail.
Embodiment 1
Go scorching tincture, including following component in parts by weight：22 parts of Paris polyphylla, 32 parts of rheum officinale, 4 parts of safflower, the root of Dahurain angelica 7
Part, 15 parts of giant knotweed, 7 parts of Asian puccoon, 7 parts of radix aconiti agrestis, 11 parts of RADIX PSAMMOSILENE, 2 parts of vomiting nut, 16 parts of arisacma consanguineum schott, 16 parts of kuh-seng, the red sage root 15
Part, 4 parts of short-pedicel aconite root.
The present embodiment goes the preparation method of scorching tincture, comprises the following steps：
Step（1）, by Paris polyphylla, rheum officinale, safflower, the root of Dahurain angelica, giant knotweed, Asian puccoon, radix aconiti agrestis, RADIX PSAMMOSILENE, vomiting nut, arisacma consanguineum schott, hardship
Ginseng, the red sage root and short-pedicel aconite root are ground into coarse powder together；
Step（2）, 68% ethanol as solvent is used, by step（1）Obtained coarse powder steeped overnight, is then added into diacolation
In cylinder, add 62% ethanol to liquid level and be higher by medicinal material surface, place 20 hours；
Step（3）, through step（2）After placement, percolation extraction is carried out using 63% ethanol as solvent is leached, regulation is extracted
Liquid alcohol content is 55%, stands 24h, produces.
Embodiment 2
Go scorching tincture, including following component in parts by weight：26 parts of Paris polyphylla, 34 parts of rheum officinale, 5 parts of safflower, the root of Dahurain angelica 10
Part, 18 parts of giant knotweed, 9 parts of Asian puccoon, 9 parts of radix aconiti agrestis, 14 parts of RADIX PSAMMOSILENE, 3 parts of vomiting nut, 18 parts of arisacma consanguineum schott, 18 parts of kuh-seng, the red sage root 18
Part, 7 parts of short-pedicel aconite root.
The present embodiment goes the preparation method of scorching tincture, comprises the following steps：
Step（1）, by Paris polyphylla, rheum officinale, safflower, the root of Dahurain angelica, giant knotweed, Asian puccoon, radix aconiti agrestis, RADIX PSAMMOSILENE, vomiting nut, arisacma consanguineum schott, hardship
Ginseng, the red sage root and short-pedicel aconite root are ground into coarse powder together；
Step（2）, 62% ethanol as solvent is used, by step（1）Obtained coarse powder steeped overnight, is then added into diacolation
In cylinder, add 68% ethanol to liquid level and be higher by medicinal material surface, place 26 hours；
Step（3）, through step（2）After placement, percolation extraction is carried out using 63% ethanol as solvent is leached, regulation is extracted
Liquid alcohol content is 65%, stands 12h, produces.
Embodiment 3
Go scorching tincture, including following component in parts by weight：It is 25 parts of Paris polyphylla, 33.3 parts of rheum officinale, 4.2 parts of safflower, white
8.4 parts of the root of Dahurian angelica, 16.7 parts of giant knotweed, 8.4 parts of Asian puccoon, 8.4 parts of radix aconiti agrestis, 12.5 parts of RADIX PSAMMOSILENE, 2.5 parts of vomiting nut, 16.7 parts of arisacma consanguineum schott,
16.7 parts of kuh-seng, 16.7 parts of the red sage root, 5.8 parts of short-pedicel aconite root.
The present embodiment goes the preparation method of scorching tincture, comprises the following steps：
Step（1）, by Paris polyphylla, rheum officinale, safflower, the root of Dahurain angelica, giant knotweed, Asian puccoon, radix aconiti agrestis, RADIX PSAMMOSILENE, vomiting nut, arisacma consanguineum schott, hardship
Ginseng, the red sage root and short-pedicel aconite root are ground into coarse powder together；
Step（2）, 65% ethanol as solvent is used, by step（1）Obtained coarse powder steeped overnight, is then added into diacolation
In cylinder, add 65% ethanol to liquid level and be higher by medicinal material surface, place 24 hours；
Step（3）, through step（2）After placement, percolation extraction is carried out using 63% ethanol as solvent is leached, regulation is extracted
Liquid alcohol content is 60%, stands 18h, produces.
Product of the present invention is the supernatant liquid of yellowish-brown, after testing, amount of alcohol：55%~65%；Total solid：Remaining residue should
It is not less than 2.0%；Other：Every regulation relevant under tincture should be met（One annex I N of Chinese Pharmacopoeia version in 2010）.
Product usage of the present invention is external application, for several times daily, sprays or puts affected part on the skin.Sealing, puts shady place storage.The term of validity is 12
Individual month.Pregnant and lactant women is disabled.
To the itchy skin eruption patient of different symptoms, spraying treatment is carried out using product of the present invention, it is specific such as table 1.
Table 1
Infected patient is hindered to 100 exceptions using product of the present invention simultaneously and carries out spraying treatment, it is specific such as table 2.
Claims (6)
1. remove scorching tincture, it is characterised in that be made and formed by following component in parts by weight：22-26 parts of Paris polyphylla, rheum officinale
32-34 parts, 4-5 parts of safflower, 7-10 parts of the root of Dahurain angelica, 15-18 parts of giant knotweed, 7-9 parts of Asian puccoon, 7-9 parts of radix aconiti agrestis, RADIX PSAMMOSILENE 11-14
Part, 2-3 parts of vomiting nut, 16-18 parts of arisacma consanguineum schott, 16-18 parts of kuh-seng, 15-18 parts of the red sage root, 4-7 parts of short-pedicel aconite root.
2. remove scorching tincture according to claim 1, it is characterised in that be made by following component in parts by weight and
Into：25 parts of Paris polyphylla, 33.3 parts of rheum officinale, 4.2 parts of safflower, 8.4 parts of the root of Dahurain angelica, 16.7 parts of giant knotweed, 8.4 parts of Asian puccoon, radix aconiti agrestis 8.4
Part, 12.5 parts of RADIX PSAMMOSILENE, 2.5 parts of vomiting nut, 16.7 parts of arisacma consanguineum schott, 16.7 parts of kuh-seng, 16.7 parts of the red sage root, upper one of snow
5.8 parts of wormwood artemisia.
3. the preparation method for removing scorching tincture described in claim 1, it is characterised in that comprise the following steps：Step（1）, by weight
Building, rheum officinale, safflower, the root of Dahurain angelica, giant knotweed, Asian puccoon, radix aconiti agrestis, RADIX PSAMMOSILENE, vomiting nut, arisacma consanguineum schott, kuh-seng, the red sage root and short-pedicel aconite root one
Rise and be ground into coarse powder；
Step（2）, 62-68% ethanol as solvent is used, by step（1）Obtained coarse powder steeped overnight, is then added into diacolation
In cylinder, add 62-68% ethanol to liquid level and be higher by medicinal material surface, place 20-26 hours；
Step（3）, through step（2）After placement, percolation extraction is carried out using ethanol as solvent is leached, extract solution alcohol content is adjusted
For 55-65%, stand, produce.
4. the preparation method for removing scorching tincture according to claim 3, its feature is in described step（3）In with 63% ethanol
It is used as leaching solvent.
5. the preparation method for removing scorching tincture according to claim 3, its feature is in described step（3）Middle time of repose is
12-24h。
6. the preparation method for removing scorching tincture according to claim 3, it is characterised in that comprise the following steps：
Step（1）, by Paris polyphylla, rheum officinale, safflower, the root of Dahurain angelica, giant knotweed, Asian puccoon, radix aconiti agrestis, RADIX PSAMMOSILENE, vomiting nut, arisacma consanguineum schott, kuh-seng, pellet
Ginseng and short-pedicel aconite root are ground into coarse powder together；
Step（2）, 65% ethanol as solvent is used, by step（1）Obtained coarse powder steeped overnight, is then added into percolator
In, add 65% ethanol to liquid level and be higher by medicinal material surface, place 24 hours；
Step（3）, through step（2）After placement, percolation extraction is carried out using ethanol as solvent is leached, extract solution alcohol content is adjusted
For 55-65%, stand, produce.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410463501.3A CN104189397B (en) | 2014-09-12 | 2014-09-12 | Remove scorching tincture and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410463501.3A CN104189397B (en) | 2014-09-12 | 2014-09-12 | Remove scorching tincture and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104189397A CN104189397A (en) | 2014-12-10 |
| CN104189397B true CN104189397B (en) | 2017-09-29 |
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| EP2441440A1 (en) * | 2010-10-18 | 2012-04-18 | Luigina Straccia | Natural pharmacological aid for prevention of periodontal inflammatory disease |
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| EP2441440A1 (en) * | 2010-10-18 | 2012-04-18 | Luigina Straccia | Natural pharmacological aid for prevention of periodontal inflammatory disease |
| CN102861217A (en) * | 2012-09-25 | 2013-01-09 | 黄盛焕 | External emplastrum for treating malignant boil, sores and carbuncles |
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| 去炎酊治疗痈疽疗疖的临床观察;王吉侯;《新中医》;19940115(第01期);第52页左栏"治疗方法"、右栏"体会" * |
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