CN104170933B - A kind of containing mantis shrimp head, the health-care moon cake and preparation method thereof of Squilla Oratoria Shell - Google Patents
A kind of containing mantis shrimp head, the health-care moon cake and preparation method thereof of Squilla Oratoria Shell Download PDFInfo
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- CN104170933B CN104170933B CN201410393088.8A CN201410393088A CN104170933B CN 104170933 B CN104170933 B CN 104170933B CN 201410393088 A CN201410393088 A CN 201410393088A CN 104170933 B CN104170933 B CN 104170933B
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Abstract
The present invention relates to a kind of containing mantis shrimp head, the health-care moon cake and preparation method thereof of Squilla Oratoria Shell, including dough cover, it is wrapped in the stuffing material within dough cover, the composition of raw materials of described dough cover is by weight percentage: flour 38～60%, mantis shrimp enzymolysis protein powder 9～13%, glucosamine hydrochloride 6.5～10%, Bidismutose 9～13%, seed oil of Herba Apii graveolentis 10～15%, Herba Cymbopogonis Citrari grass meal 5～9.5%, psyllium seed gum 0.5～1.5%；By the manufacturing process of number of ways, above-mentioned raw materials being made moon cake dough cover, fat content and heat low, Antimicrobial preservative and gelling ability are strong, good water-retaining property, make moon cake storage and will not go mouldy for 12 months.And not having local flavor, more preferably, aromatic flavor, tasty, nutrient is more rich, and health care is more prominent, is more beneficial for digestion and the absorption of human body for mouthfeel.The most edible health-care effect that can reach building body, life lengthening.And comprehensive utilization of waste material, contain huge society, ecology, environment and economic benefit.
Description
Technical field
The present invention relates to a kind of moon cake and preparation method thereof, particularly relate to a kind of containing mantis shrimp head,
Health-care moon cake of Squilla Oratoria Shell and preparation method thereof.
Background technology
Moon cake comes across the Tang Dynasty, is eaten the Mid-autumn Festival as sacrificial offerings, after gradually at folklore,
Become a kind of traditional food must eaten the Mid-autumn Festival.Along with the raising of people's living standard, moon cake no longer office
Being limited to the food just tasted the Mid-autumn Festival, moon cake has become the cake that people like in daily life,
Giving the vitality that moon cake is flourishing, kind emerges in an endless stream, such as beans moon cake, vegetable moon cake, low sugar
Moon cake, fruit moon cake, flower mooncake, edible fungi moon cake etc..Although the materials of these moon cakes are increasingly
Abundant, component difference is very big, but the structure of moon cake and processing method are the most close, are essentially all
The raw materials such as employing flour, white sugar, vegetable oil are modulated into after dough cover wraps up stuffing material closing in again to toast and form.
In order to improve taste flavor and the nourishing healthy diversification of moon cake, only pay attention to the structure to moon cake
Regulation, but have ignored moon cake dough cover and contains abundant oils and fats and sugar, and not only heat is high, nondigestible,
Nutrient is few, does not has a health care, and easily cooperating microorganisms, even moldy metamorphism, guarantee the quality
Phase is short, thus seriously constrains the development of moon cake industry.
Mantis shrimp is commonly called as squilla, squill, squilla oratoria etc., Along Zhejiang Coast one band be commonly called as rely urine shrimp,
Shrimp pulls out bullet, crawfish hook bullet, is subordinate to Arthropoda, Crustachia, Stomatopoda, Gu Xia section, perennial sea
Industry Ji shell-fish.Happiness is dwelt in Yu Qianchao and deep-sea silt or reef crack, and distribution is extremely wide, from
Muscovite big Peter bay is to Japan and coastal area of china, Philippine, the Malay Peninsula, Hawaiian Islands
All having distribution, the Huanghai Sea, the Bohai Sea, Hainan and East Sea kind with China are most.Mantis shrimp fine and tender taste is fresh
U.S., individual big, it is divided into cephalothorax and abdominal part two parts, altogether 20 body segments of tool, head 5 saves, chest
8 joints, abdominal part 7 saves, and before head and chest, 4 joint healings form cephalothoraxes, carapace cover on it,
After chest, 4 joints expose outside carapace, the front end of carapace 2 pairs of feelers, the 1 pair of big jaw, 2
To small palate and the compound eye of band handle, abdominal part is slightly put down flat, is made up of with 1 flat periproct 6 uromeres, anus
It is opened on the periproct outside of belly.Squilla Oratoria Shell fleshiness is few, can produce substantial amounts of mantis shrimp during processing, eating
Head, Squilla Oratoria Shell (accounting for 65%～the 75% of mantis shrimp body weight).Only have at present and be used on a small quantity producing feedstuff
Deng low value product, major part is dropped, and causes environmental pollution.It is true that mantis shrimp head, shrimp
Mqb shell is if Appropriate application, and it is worth not under its meat, except containing protein, chitin,
Outside the mineral such as astaxanthin, calcium, zinc, magnesium and phosphorus, mantis shrimp head possibly together with abundant cephalin, fat,
[Zhang Qiang, " mantis shrimp head the fatty acid analysis " " threpsologys such as the various aminoacid of carotene and needed by human
Report " the 1st phase in 1998].Its biologic activity and pharmacological action are confirmed by the experimental results, tool
It is improved immunity of organisms, antioxidation, antibacterial, defying age, antitumor, improves cerebral function, carry
High memory, blood pressure lowering, fat-reducing liver-protecting and prevention effect such as cardiovascular and cerebrovascular disease, and safe to the human body
Property is high.Therefore, recent domestic scholar is devoted to seek mantis shrimp head, Squilla Oratoria Shell deep processing
Technology, is concentrated mainly on " research preparing chitin and chitosan from Squilla Oratoria Shell " [Yang Dan etc., " food
Product science " 12 phases in 2006] and mantis shrimp head be processed into mantis shrimp oil, mantis shrimp head powder, mantis shrimp head beans,
Aspect [Guo's civil division etc., " cultivation of coastal area of china mantis shrimp and the comprehensive utilizations such as mixed feed, extraction protein
With " " extraordinary Economic animals and plants " o. 11th in 2011].But directly it is processed into mantis shrimp head powder, nutriture value
It is worth low, only as common or low-grade feedstuff；If extracting protein in mantis shrimp head by enzymatic isolation method,
Heavier bitter off-flavors, weak flavor is often produced, it is impossible to as foodstuff base material in hydrolytic process.Through inspection
Rope, up to now, there is not yet and mantis shrimp head, Squilla Oratoria Shell are carried out biotechnology process and are used for making the moon
The document of cake was published, and also had no that Related product lists.
Summary of the invention
Present invention aims to current mantis shrimp head, Squilla Oratoria Shell develops the deficiency existed,
There is provided a kind of containing mantis shrimp head, the health-care moon cake and preparation method thereof of Squilla Oratoria Shell, both solved mantis shrimp enzymolysis
Protein liquid bitter off-flavors weight, weak flavor, it is impossible to as the problem of foodstuff base material, improve again moon cake antibacterial,
Make moon cake healthy nutritive value even better while anticorrosion, preservativity, and fat content and heat
Low, do not have local flavor, mouthfeel is more preferably, more easily digested.
In order to realize the purpose of the present invention, the present inventor is studied by lot of experiments and persistent exploration,
It is finally obtained following technical scheme:
A kind of containing mantis shrimp head, the health-care moon cake of Squilla Oratoria Shell, including dough cover, it is wrapped in inside dough cover
Stuffing material, the composition of raw materials of described skin material dough cover is by weight percentage: flour 38～60%, shrimp
Mqb enzymolysis protein powder 9～13%, glucosamine hydrochloride 6.5～10%, Bidismutose 9～13%,
Seed oil of Herba Apii graveolentis 10～15%, Herba Cymbopogonis Citrari grass meal 5～9.5%, psyllium seed gum 0.5～1.5%；Its making
Method comprises the following steps that:
1. prepare mantis shrimp enzymolysis protein powder, gather fresh mantis shrimp head, clean, pour pot for solvent extraction into,
And add the nose heave amount of mantis shrimp 2～the water of 5 times, boil 10～20 minutes, filter, filtering residue colloid mill
Carrying out defibrination, limit edging adds filtering residue weight 3～the water of 6 times, pH regulator to 7.5～9, adds
Filtering residue weight 0.2～the trypsin of 1.1%, enzymolysis 2～5 hours under the conditions of 40～75 DEG C, 80～
Enzyme denaturing 20 minutes under the conditions of 95 DEG C, centrifugal, take supernatant, add supernatant weight 3～the turnip of 7%
The citric acid of polysaccharide, 0.1～0.3% and 0.3～the de-bitter eliminating sargassum smell of glycine of 0.6%, concentrating under reduced pressure,
It is spray-dried, obtains mantis shrimp enzymolysis protein powder；
2. prepare glucosamine hydrochloride: gather fresh Squilla Oratoria Shell, clean, dry, pulverize
Become 15～25 mesh shell pieces to pour pot for solvent extraction into, and be 3～7wt by 3～6 times amount addition concentration of shell pieces weight
The hydrochloric acid solution of %, soaks 12～16 hours under room temperature, is washed to neutrality, drains, then by shell pieces weight
2～5 times amount add the NaOH solution that concentration are 3～7wt%, hydrolyze 3 little under the conditions of 85～95 DEG C
Time, filtering, filtering residue is washed to neutrality, is dried, and the concentration adding filtering residue weight 3～6 times is 25～37wt
The hydrochloric acid solution of %, 50～65 DEG C of ultrasonic water bath 35 minutes, it is subsequently adding the activity of filtering residue weight 3%
Charcoal decolours, filtered while hot, when filtrate is concentrated into 1/3 volume, adds 4 times of volumes of concentrated solution
Concentration is the ethanol of 80～95wt%, after stirring 5 minutes, stands and is cooled to 3～6 DEG C, separates out crystallization,
Slough ethanol, collect crystallization, be dried, obtain glucosamine hydrochloride；
3. prepare seed oil of Herba Apii graveolentis: gather the celery seed without going mouldy, dry to water content less than 3%,
It is ground into 70～90 mesh fine powders, passes through supercritical CO2The method of extracting prepares seed oil of Herba Apii graveolentis；
4. Herba Cymbopogonis Citrari grass meal is prepared: gather the Herba Cymbopogonis Citrari of fresh state, roguing, clean, send into and beat
Pulp grinder, and add Herba Cymbopogonis Citrari weight 2～the water of 9 times, making beating, squeezing, obtain pressed liquor and press residue,
Press residue 65 DEG C of hot water extraction 1～3 hours, filter, obtain squeezing juice, and squeezing juice merges with pressed liquor,
Filtrate crosses D101 macroporous adsorptive resins, first with water, after with the ethanol elution that concentration is 35～75wt%,
Collect alcohol eluen, concentrating under reduced pressure, be spray-dried, obtain Herba Cymbopogonis Citrari grass meal；
5. weigh Bidismutose by formula, glucosamine hydrochloride, psyllium seed gum are poured container into and are stirred
Mix uniformly, add Bidismutose, glucosamine hydrochloride, the water of psyllium seed gum three's gross weight 2 times
It is mixed into sucrose solution liquid, decocts under the conditions of 85～95 DEG C, be concentrated into sucrose solution liquid when amassing 2/3, cooling,
Add the seed oil of Herba Apii graveolentis mixing of above-mentioned formula ratio, obtain sugar and oil slurry；
6. weigh flour, mantis shrimp enzymolysis protein powder, Herba Cymbopogonis Citrari grass meal by formula, and fall according to this order
After entering dough mixing machine mixing, adding step sugar and oil slurry 5., and water use regulation humidity, synthesis has
Bonding and plastic dough cover dough, its subsequent processing operations moon cake manufacturing procedure routinely operates, i.e.
Make containing mantis shrimp head, the health-care moon cake of Squilla Oratoria Shell.
In above-mentioned preparation method, the de-bitter eliminating sargassum smell mechanism of action of mantis shrimp enzymolysis protein powder is that turnip is many
Sugar as suppression fishy smell generation antioxidant, can effectively remove the free radical in enzymolysis solution, prevention or
Person delays the oxidation of unsaturated fatty acid；Glycine has the characteristic of antioxidation and anti-corrosive properties, and it is with climing
There is between cyanines polysaccharide good synergism, preferably play seasoning, improve the effect of taste, then
Can optimize and slough bitter off-flavors effect；Citric acid is that local flavor regulates additive so that enzymolysis solution presents Fructus Citri Limoniae
Fragrance, tart up, improve mouthfeel；Its reaction condition is gentle, nutrition and the activity to enzymolysis solution
Composition is protected to greatest extent.The most again with nutritional labeling and the active substance of Herba Cymbopogonis Citrari
Compatibility, has complementary functions, Synergistic, makes bitter off-flavors base in the case of ensureing protein losses minimum
This removing, and there is the fresh effect of increasing of rendering palatable.
The mantis shrimp enzymolysis protein powder obtained by above-mentioned preparation method, be a kind of micromolecule polypeptide,
The mixture of aminoacid, flavour nucleotide, multivitamin and trace element.Its molecular weight is little, raw
Thing activity is high, and in human body, almost all is directly absorbed.In regulation gastrointestinal movement, improvement
Physiological function, regulate immune system, improve cerebral function, slow down aging, blood fat reducing, blood pressure lowering,
Antibacterial, antioxidation, resisting fatigue, antiviral, anticancer, remove free radical and promote that mineral element absorbs
Improve the aspects such as bioavailability to play an important role.
The glucosamine hydrochloride obtained by above-mentioned preparation method, is natural known to one
Mucopolysaccharide, molecule is less, it is easy to digest and assimilate, and has antiinflammatory, antioxidation, anticorrosion, antibacterial, anti-
The multiple pharmacological effect such as tumor.To staphylococcus aureus, escherichia coli, bacillus subtilis, Huang
21 kinds of antibacterials, mycetes such as aspergillosis all have obvious antibacterial action [Chen Xin etc., " glucosamine hydrochloric acid
The anti-corrosive antibacterial effect of salt " phase " fine chemistry industry " calendar year 2001 02], it is again the sweeting agent of food, antioxygen
Agent.
Inventors of the present invention have surprisingly found that, appropriate variable glucosamine hydrochloride, bifid
Sugar, the formula proportion of psyllium seed gum, except sugariness is equivalent to 100～200 times of white sugar, calorific value is only
Outside the 1/200 of sucrose, and present extremely significantly synergistic tackifying, gelation and film property, make
Dough coheres complexation power to be strengthened, and increases gelling ability and the water-retaining property of moon cake, improves moon cake and bake performance；
Meanwhile, also having antibacterial, anticorrosion, preservativity, suppression protein, crude fat, aminoacid etc. are no
Become sour and aoxidize, preventing the degraded of flavone compound, significantly improving the health care of moon cake.
Herba Cymbopogonis Citrari in above-mentioned raw materials is rich in soaping agents, saccharide, protein, phlegmatic temperament, phenol
Material and volatile oil component.Its volatility main body of oil have citral, neral, linalool,
Menthone, d-citronellol, dilute, the L-Borneol of L-lemon etc..Have strong citris aromas, fragrance strong and
Persistently.There is antibacterial, anticancer, dispelling wind to relieve the exterior syndrome, eliminating blood stasis and smoothing collaterals, digestion-promoting spleen-invigorating stomach, diuretic antihypertensive,
The effects such as cough-relieving pain relieving, Titian.
The present inventor is it has been unexpectedly discovered that Herba Cymbopogonis Citrari grass meal and mantis shrimp enzymolysis protein
Powder compatibility, effect is complementary, make while increasing moon cake alimentary health-care function antioxidation, antibacterial, point
Solve and absorption has synergistic function, to the effect effect going flavor and enhancing flavor, Antimicrobial preservative to show addition
Really, the bitter off-flavors in mantis shrimp enzymolysis protein powder is the most effectively sloughed so that it is there is natural flavor, have more
Unique local flavor and the fresh effect of increasing, inhibit again microbial reproduction, extend the shelf-life of moon cake.
Seed oil of Herba Apii graveolentis in above-mentioned raw materials is a kind of plants essential oil extracted from celery seed, has
Unique fragrance, its be mainly composed of flavone compound, α-selinene, myrcene, limonene,
Elemene, caryophyllene, butylphthalide, parsley apiole, cadinol, Folium eucalypti globueli (Eucalyptus globulus Labill.) diene, coumarin and bean steroid
Alcohol etc.；Have slow down aging, strengthen cardiovascular function, antiinflammatory, antioxidation, antiallergic, antibacterial,
The effects such as uric acid resisting, blood sugar lowering, radioprotective and antitumor, to staphylococcus aureus, escherichia coli,
Bacillus subtilis, [Li Nan etc. be " celery seed quintessence oil for antibacterial, the equal inhibitory action of mycete such as Aspergillus flavus
Antibacterial and Study on antioxidation " " China's flavoring agent " the 2nd phase in 2012].
The present inventor conducts in-depth research discovery, is added in the dough cover of moon cake
Seed oil of Herba Apii graveolentis, has persistently and more tempting fragrance, can remove flavor and enhancing flavor, easily causes the appetite of people,
Having again stronger emulsibility, it is had an effect with protein, starch in flour, delays protein, shallow lake
The aging of powder, improves the problem that moon cake dough cover structure is the most hardening, moreover it is possible to form stable water-oil body with water
System, enhances the retentiveness of moon cake, effectively prevents the moisture of moon cake to move outside to moon cake dough cover
Move and volatilize, thus keep the freshness of moon cake, extend the shelf life of moon cake.
The present invention extracts mantis shrimp enzymolysis by the manufacturing process of number of ways from mantis shrimp head, Squilla Oratoria Shell
Egg albumen powder, glucosamine hydrochloride, slough bitter off-flavors so that it is can not only be used for the basic of people's life
Food has again nutrition health-care functions good to human body, it is achieved the comprehensive utilization to waste material, further
Improve mantis shrimp head, the added value of Squilla Oratoria Shell, contain huge society, ecology, environment and economic effect
Benefit.
The present invention by the raw materials such as mantis shrimp head, Squilla Oratoria Shell, Herba Cymbopogonis Citrari, celery seed by process after,
Add to flour added with Bidismutose, psyllium seed gum, rutabaga polysaccharide, citric acid and glycine compatibility
Work moon cake dough cover out, each composition plays a role and brings out the best in each other, Synergistic, fat content and heat
Measuring low, Antimicrobial preservative and gelling ability are strong, good water-retaining property, and the moon cake made by the present invention stores 12
The moon will not go mouldy.And not having local flavor, more preferably, aromatic flavor, tasty, nutrition is first for mouthfeel
Element is more rich, and health care is more prominent, is more beneficial for digestion and the absorption of human body.Often eat and can increase
Add immunity of organisms, nourishing the stomach to promote the production of body fluid, the kidney invigorating and essence nourishing, heart tonifying and brain strengthening, reach building body, benefit of prolonging life
The health-care effect in longevity.To preventing and treating hyperlipidemia, cardiovascular and cerebrovascular disease, diabetes, joint disease, digestive tract
Disease, the bone density that increases, improve that bone structure, toxin expelling are anticancer, alleviate osteoporosis, anti-lipid peroxy
Change, antiviral, anticancer, the synthesis of promotion protein in body and fat-reducing etc. all play an important role.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is expanded on further.But these embodiments are only limitted to
The present invention is described rather than limits the scope of the invention.
Embodiment one
1. raw material prepares:
1. prepare mantis shrimp enzymolysis protein powder, gather fresh mantis shrimp head, clean, pour pot for solvent extraction into,
And add the water of the nose heave amount of mantis shrimp 5 times, and boiling 20 minutes, filter, filtering residue colloid mill carries out defibrination,
Limit edging adds the water of filtering residue weight 3 times, pH regulator to 8, adds the pancreas egg of filtering residue weight 0.9%
White enzyme, enzymolysis 5 hours under the conditions of 50 DEG C, enzyme denaturing 20 minutes under the conditions of 90 DEG C, centrifugal, take supernatant
Liquid, the glycine adding the rutabaga polysaccharide of supernatant weight 5%, the citric acid of 0.15% and 0.3% takes off
Bitter eliminating sargassum smell, concentrating under reduced pressure, it is spray-dried, obtains mantis shrimp enzymolysis protein powder；
2. prepare glucosamine hydrochloride: gather fresh Squilla Oratoria Shell, clean, dry, pulverize
Become 25 mesh shell pieces to pour pot for solvent extraction into, and it is molten to add, by 5 times amount of shell pieces weight, the hydrochloric acid that concentration is 3wt%
Liquid, soaks 16 hours under room temperature, is washed to neutrality, drains, then adds dense by 5 times amount of shell pieces weight
Degree is the NaOH solution of 3wt%, hydrolyzes 3 hours under the conditions of 90 DEG C, filters, and filtering residue is washed to neutrality,
It is dried, adds the hydrochloric acid solution that concentration is 25wt% of filtering residue weight 3 times, 65 DEG C of ultrasonic water bath 35 points
Clock, the activated carbon being subsequently adding filtering residue weight 3% decolours, filtered while hot, and filtrate is concentrated into 1/3
During volume, add the ethanol that concentration is 90wt% of 4 times of volumes of concentrated solution, after stirring 5 minutes, quiet
Put and be cooled to 5 DEG C, separate out crystallization, slough ethanol, collect crystallization, be dried, obtain glucosamine salt
Hydrochlorate；
3. prepare seed oil of Herba Apii graveolentis: gather the celery seed without going mouldy, dry to water content less than 3%,
It is ground into 90 mesh fine powders, passes through supercritical CO2The method of extracting prepares seed oil of Herba Apii graveolentis；
4. Herba Cymbopogonis Citrari grass meal is prepared: gather the Herba Cymbopogonis Citrari of fresh state, roguing, clean, send into and beat
Pulp grinder, and add the water of Herba Cymbopogonis Citrari weight 6 times, making beating, squeezing, obtain pressed liquor and press residue, pressure
Marc, with 65 DEG C of hot water extraction 3 hours, filters, obtains squeezing juice, and squeezing juice merges with pressed liquor, filters
Liquid crosses D101 macroporous adsorptive resins, first with water, after be the ethanol elution of 45wt% by concentration, collect
Alcohol eluen, concentrating under reduced pressure, it is spray-dried, obtains Herba Cymbopogonis Citrari grass meal.
2. composition of raw materials:
Flour 62kg, mantis shrimp enzymolysis protein powder 10kg, glucosamine hydrochloride 8kg, bifid
Sugar 12kg, seed oil of Herba Apii graveolentis 10kg, Herba Cymbopogonis Citrari grass meal 7.5kg, psyllium seed gum 0.5kg.
3. making step:
1. weigh Bidismutose 12kg, glucosamine hydrochloride 8kg, psyllium seed gum 0.5kg fall
Entering container to mix thoroughly, the water adding 41kg is mixed into sucrose solution liquid, decocts, be concentrated under the conditions of 90 DEG C
When sucrose solution liquid amasss 2/3, cooling, add seed oil of Herba Apii graveolentis 10kg mixing, obtain sugar and oil slurry；
2. weigh flour 62kg, mantis shrimp enzymolysis protein powder 10kg, Herba Cymbopogonis Citrari grass meal 7.5kg, and depend on
This order is poured into after mixing in dough mixing machine, adds step sugar and oil slurry 1., and water use regulation humidity,
Synthesis has bonding and plastic dough cover dough, its subsequent processing operations moon cake manufacturing procedure routinely
Operation, i.e. makes containing mantis shrimp head, the health-care moon cake of Squilla Oratoria Shell.
Embodiment two
1. raw material prepares:
1. prepare mantis shrimp enzymolysis protein powder, gather fresh mantis shrimp head, clean, pour pot for solvent extraction into,
And add the water of the nose heave amount of mantis shrimp 3 times, and boiling 15 minutes, filter, filtering residue colloid mill carries out defibrination,
Limit edging adds the water of filtering residue weight 5 times, pH regulator to 8.5, adds the pancreas of filtering residue weight 0.6%
Protease, enzymolysis 2 hours under the conditions of 65 DEG C, enzyme denaturing 20 minutes under the conditions of 95 DEG C, centrifugal, take
Clear liquid, adds the rutabaga polysaccharide of supernatant weight 3%, the citric acid of 0.1% and the glycine of 0.4%
De-bitter eliminating sargassum smell, concentrating under reduced pressure, it is spray-dried, obtains mantis shrimp enzymolysis protein powder；
2. prepare glucosamine hydrochloride: gather fresh Squilla Oratoria Shell, clean, dry, pulverize
Become 15 mesh shell pieces to pour pot for solvent extraction into, and it is molten to add, by 3 times amount of shell pieces weight, the hydrochloric acid that concentration is 5wt%
Liquid, soaks 12 hours under room temperature, is washed to neutrality, drains, then adds dense by 3 times amount of shell pieces weight
Degree is the NaOH solution of 5wt%, hydrolyzes 3 hours under the conditions of 95 DEG C, filters, and filtering residue is washed to neutrality,
It is dried, adds the hydrochloric acid solution that concentration is 30wt% of filtering residue weight 3 times, 50 DEG C of ultrasonic water bath 35 points
Clock, the activated carbon being subsequently adding filtering residue weight 3% decolours, filtered while hot, and filtrate is concentrated into 1/3
During volume, add the ethanol that concentration is 95wt% of 4 times of volumes of concentrated solution, after stirring 5 minutes, quiet
Put and be cooled to 3 DEG C, separate out crystallization, slough ethanol, collect crystallization, be dried, obtain glucosamine salt
Hydrochlorate；
3. prepare seed oil of Herba Apii graveolentis: gather the celery seed without going mouldy, dry to water content less than 3%,
It is ground into 75 mesh fine powders, passes through supercritical CO2The method of extracting prepares seed oil of Herba Apii graveolentis；
4. Herba Cymbopogonis Citrari grass meal is prepared: gather the Herba Cymbopogonis Citrari of fresh state, roguing, clean, send into and beat
Pulp grinder, and add the water of Herba Cymbopogonis Citrari weight 6 times, making beating, squeezing, obtain pressed liquor and press residue, pressure
Marc, with 65 DEG C of hot water extraction 2 hours, filters, obtains squeezing juice, and squeezing juice merges with pressed liquor, filters
Liquid crosses D101 macroporous adsorptive resins, first with water, after be the ethanol elution of 35wt% by concentration, collect
Alcohol eluen, concentrating under reduced pressure, it is spray-dried, obtains Herba Cymbopogonis Citrari grass meal.
2. composition of raw materials:
Flour 46kg, mantis shrimp enzymolysis protein powder 12kg, glucosamine hydrochloride 10kg, bifid
Sugar 9kg, seed oil of Herba Apii graveolentis 15kg, Herba Cymbopogonis Citrari grass meal 6.8kg, psyllium seed gum 1.2kg.
3. making step:
1. weigh Bidismutose 9kg, glucosamine hydrochloride 10kg, psyllium seed gum 1.2kg fall
Entering container to mix thoroughly, the water adding 40.4kg is mixed into sucrose solution liquid, decocts under the conditions of 95 DEG C, concentrates
To sucrose solution liquid amass 2/3 time, cooling, add seed oil of Herba Apii graveolentis 15kg mixing, obtain sugar and oil slurry；
2. weigh flour 46kg, mantis shrimp enzymolysis protein powder 12kg, Herba Cymbopogonis Citrari grass meal 6.8kg, and depend on
This order is poured into after mixing in dough mixing machine, adds step sugar and oil slurry 1., and water use regulation humidity,
Synthesis has bonding and plastic dough cover dough, its subsequent processing operations moon cake manufacturing procedure routinely
Operation, i.e. makes containing mantis shrimp head, the health-care moon cake of Squilla Oratoria Shell.
Claims (1)
1., containing mantis shrimp head, a health-care moon cake for Squilla Oratoria Shell, including dough cover, it is wrapped within dough cover
Stuffing material, it is characterised in that the composition of raw materials of described dough cover is by weight percentage: flour 38～60
%, mantis shrimp enzymolysis protein powder 9～13%, glucosamine hydrochloride 6.5～10%, Bidismutose 9～
13%, seed oil of Herba Apii graveolentis 10～15%, Herba Cymbopogonis Citrari grass meal 5～9.5%, psyllium seed gum 0.5～1.5%；It
Manufacture method comprise the following steps that:
1. prepare mantis shrimp enzymolysis protein powder, gather fresh mantis shrimp head, clean, pour pot for solvent extraction into, and add
Entering the nose heave amount of mantis shrimp 2～the water of 5 times, boil 10～20 minutes, filter, filtering residue colloid mill is carried out
Defibrination, limit edging adds filtering residue weight 3～the water of 6 times, pH regulator to 7.5～9, adds filtering residue
Weight 0.2～the trypsin of 1.1%, enzymolysis 2～5 hours under the conditions of 40～75 DEG C, 80～95
Enzyme denaturing 20 minutes under the conditions of DEG C, centrifugal, take supernatant, add supernatant weight 3～7% turnip many
Sugar, 0.1～the citric acid of 0.3% and 0.3～the de-bitter eliminating sargassum smell of glycine of 0.6%, concentrating under reduced pressure, spray
Mist is dried, and obtains mantis shrimp enzymolysis protein powder；
2. prepare glucosamine hydrochloride: gather fresh Squilla Oratoria Shell, clean, dry, pulverize into 15～
25 mesh shell pieces pour pot for solvent extraction into, and add, by 3～6 times amount of shell pieces weight, the salt that concentration is 3～7wt%
Acid solution, soaks 12～16 hours under room temperature, is washed to neutrality, drains, then by the 2～5 of shell pieces weight
Times amount adds the NaOH solution that concentration is 3～7wt%, hydrolyzes 3 hours under the conditions of 85～95 DEG C, filters,
Filtering residue is washed to neutrality, is dried, and adds filtering residue weight 3～the hydrochloric acid that concentration is 25～37wt% of 6 times
Solution, 50～65 DEG C of ultrasonic water bath 35 minutes, the activated carbon being subsequently adding filtering residue weight 3% takes off
Color, filtered while hot, when filtrate is concentrated into 1/3 volume, add 4 times of volumes of concentrated solution concentration be 80～
The ethanol of 95wt%, after stirring 5 minutes, stands and is cooled to 3～6 DEG C, separate out crystallization, slough ethanol,
Collect crystallization, be dried, obtain glucosamine hydrochloride；
3. prepare seed oil of Herba Apii graveolentis: gather the celery seed without going mouldy, dry to water content less than 3%, pulverize
Become 70～90 mesh fine powders, pass through supercritical CO2The method of extracting prepares seed oil of Herba Apii graveolentis；
4. Herba Cymbopogonis Citrari grass meal is prepared: gather the Herba Cymbopogonis Citrari of fresh state, roguing, clean, send into beater,
And add Herba Cymbopogonis Citrari weight 2～the water of 9 times, and making beating, squeezing, obtain pressed liquor and press residue, press residue
With 65 DEG C of hot water extraction 1～3 hours, filtering, obtain squeezing juice, squeezing juice merges with pressed liquor, filtrate
Cross D101 macroporous adsorptive resins, first with water, after with the ethanol elution that concentration is 35～75wt%, receive
Collection alcohol eluen, concentrating under reduced pressure, it is spray-dried, obtains Herba Cymbopogonis Citrari grass meal；
5. weigh Bidismutose by formula, glucosamine hydrochloride, psyllium seed gum pour container stirring into all
Even, add the water mixing of Bidismutose, glucosamine hydrochloride, psyllium seed gum three's gross weight 2 times
Become sucrose solution liquid, decoct under the conditions of 85～95 DEG C, be concentrated into sucrose solution liquid when amassing 2/3, cooling, add
Enter the seed oil of Herba Apii graveolentis mixing of above-mentioned formula ratio, obtain sugar and oil slurry；
6. weigh flour, mantis shrimp enzymolysis protein powder, Herba Cymbopogonis Citrari grass meal by formula, and according to this order pour into
After the machine mixing of face, adding step sugar and oil slurry 5., and water use regulation humidity, synthesis has bonding
With plastic dough cover dough, its subsequent processing operations moon cake manufacturing procedure routinely operates, i.e. makes
Containing mantis shrimp head, the health-care moon cake of Squilla Oratoria Shell.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410393088.8A CN104170933B (en) | 2014-07-31 | 2014-07-31 | A kind of containing mantis shrimp head, the health-care moon cake and preparation method thereof of Squilla Oratoria Shell |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410393088.8A CN104170933B (en) | 2014-07-31 | 2014-07-31 | A kind of containing mantis shrimp head, the health-care moon cake and preparation method thereof of Squilla Oratoria Shell |
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| Publication Number | Publication Date |
|---|---|
| CN104170933A CN104170933A (en) | 2014-12-03 |
| CN104170933B true CN104170933B (en) | 2016-09-14 |
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|---|---|---|---|
| CN201410393088.8A Expired - Fee Related CN104170933B (en) | 2014-07-31 | 2014-07-31 | A kind of containing mantis shrimp head, the health-care moon cake and preparation method thereof of Squilla Oratoria Shell |
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| CN116210882B (en) * | 2023-02-27 | 2025-03-21 | 江苏恒顺醋业股份有限公司 | A kind of seafood flavor sauce and preparation method thereof |
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Effective date of registration: 20170707 Address after: 515000 Guangdong province Shantou Jinping Jinyuan Industrial Zone on the west side of 10A2B2 road in the Chaozhou Shantou area 1-4 Patentee after: Guangdong taste Village Food Co., Ltd. Address before: 315326 Zhejiang province Cixi City Road No. 9 Shi Ningbo Tuobang electric wire & Cable Co. Ltd. Patentee before: Lu Siye |
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