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CN104170013B - The manufacture method and information recording carrier of glass substrate for information recording medium - Google Patents

The manufacture method and information recording carrier of glass substrate for information recording medium Download PDF

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Publication number
CN104170013B
CN104170013B CN201380011847.3A CN201380011847A CN104170013B CN 104170013 B CN104170013 B CN 104170013B CN 201380011847 A CN201380011847 A CN 201380011847A CN 104170013 B CN104170013 B CN 104170013B
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Prior art keywords
grinding
glass substrate
carrier
retaining hole
information recording
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CN201380011847.3A
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CN104170013A (en
Inventor
小松隆史
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Hoya Corp
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Hoya Corp
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24BMACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
    • B24B37/00Lapping machines or devices; Accessories
    • B24B37/04Lapping machines or devices; Accessories designed for working plane surfaces
    • B24B37/07Lapping machines or devices; Accessories designed for working plane surfaces characterised by the movement of the work or lapping tool
    • B24B37/08Lapping machines or devices; Accessories designed for working plane surfaces characterised by the movement of the work or lapping tool for double side lapping
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24BMACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
    • B24B37/00Lapping machines or devices; Accessories
    • B24B37/27Work carriers
    • B24B37/28Work carriers for double side lapping of plane surfaces
    • GPHYSICS
    • G11INFORMATION STORAGE
    • G11BINFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B5/00Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
    • G11B5/84Processes or apparatus specially adapted for manufacturing record carriers
    • G11B5/8404Processes or apparatus specially adapted for manufacturing record carriers manufacturing base layers

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Manufacturing Of Magnetic Record Carriers (AREA)
  • Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
  • Magnetic Record Carriers (AREA)

Abstract

Carrier (500) has:Configure and run through retaining hole (520C) in one the 1st of near center location;Multiple 2 run through retaining hole (520P) through what retaining hole (520C) annularly configured with around the 1st, in the case where the diameter of glass substrate (1) to be set to Dmm and will be set to rmm to the distance of the 1st center (C2) for running through retaining hole (520C) from the center of carrier (500) (C1), the 1st of carrier (500) the is arranged on the opening position of the relational expression of satisfaction [(D/4)≤r≤(D/2)] through the center (C2) of retaining hole (520C).

Description

The manufacture method and information recording carrier of glass substrate for information recording medium
Technical field
The present invention relates to the manufacture method of glass substrate for information recording medium and information recording carrier, more particularly to The manufacture method of the glass substrate for information recording medium used in the manufacture of information recording carrier and possess the information record Jie The information recording carrier of matter glass substrate.
Background technology
The information recording carriers such as disk are equipped on computer etc. as hard disk.Information recording carrier is on the surface of substrate Upper to form the magnetic thin film layer comprising recording layer to manufacture, the recording layer make use of magnetic, light or optomagnetic etc. property.Note Record layer is magnetized by magnetic head, thus by defined information record in information recording carrier.
Information recording carrier is improving constantly packing density year by year.Accompany with this, for used in information recording carrier The quality of substrate, also requires high quality.As the substrate of information recording carrier, all the time using aluminium base, still, with The raising of packing density, gradually replace with the flatness of substrate surface and the glass substrate that intensity is more excellent than aluminium base.
In the manufacture method of the glass substrate of information recording carrier, have and be used to ensure higher surface configuration precision Grinding process/grinding step.In order to realize the high-precision shape quality of glass substrate, employ working process ability not Same slurry and grinding/grinding pad effectively combines, 2 grinding/grinding steps more than stage.Such as in Japan There is the conventional technology related to the manufacture of glass substrate disclosed in JP 2007-015105 publications (patent document 1).
Prior art literature
Patent document
Patent document 1:Japanese Unexamined Patent Publication 2007-015105 publications
The content of the invention
The invention problem to be solved
For the glass substrate used as information recording carrier, multiple glass substrates are typically held in carrier (carrier) grinding/grinding for running through retaining hole, carrying out glass substrate set on.In recent years, in order to cut down cost, exist Such trend:Increase the glass substrate number on each carrier used in grinding/grinding.
In addition, in order to improve the packing density of each glass substrate, or even the end face to outer circumferential side by glass substrate Neighbouring region is used as information recording area, and therefore, the shape finishing precision of the outer circumference side edge face of glass substrate also requires Higher precision.
If set for carrier in a manner of most close through retaining hole, also it is placed with the near center location of carrier Glass substrate.If glass substrate to be configured to the center of carrier, when double-sided grinding device is driven in grinding process, configuration Center glass substrate be concentrated through in grinding pad platform inner circumferential near and platform periphery near among region (with Under, referred to as Intermediate Gray region.) same position.
Glass substrate is concentrated through this case that the same position of grinding pad causing in grinding process, on grinding pad , the part that glass substrate passes through produce grinding pad (bonded-abrasive) uneven wear, so as to grinding pad middle band Domain produces the step (impression) that section is spill.
If producing step on grinding pad, easily produced on the surface of glass substrate and damage is ground as caused by the step Hinder (cut).In addition, in order to eliminate the grinding damage, prolonged processing is needed in grinding step thereafter, and (larger goes Except amount).But grinding using soft mostly in grinding step below, particularly final grinding step (precise finiss) Mill pad, if the time of final grinding step is elongated, the end surface shape of glass substrate deteriorates.
The present invention be in view of above-mentioned problem and complete, there is provided a kind of manufacture method of glass substrate for information recording medium And information recording carrier, in the grinding process of double-sided grinding device has been used, it can suppress to produce step on grinding pad.
The means used to solve the problem
In the manufacture method of the glass substrate for information recording medium based on the present invention, described information recording medium is in circle Formed with magnetic thin film layer on the main surface of the glass substrate of disk shape, in the manufacturer of described information recording medium glass substrate In method, there is surface grinding process, in the surface grinding process, using the double-sided grinding device for possessing planetary gears, Water, grinding fluid or lubricating fluid are supplied while being ground the main surface of above-mentioned glass substrate.
Above-mentioned double-sided grinding device possesses:Upper mounting plate, it is located at the upside of above-mentioned glass substrate, and in the upper of the upper mounting plate Stating glass substrate side has upside grinding pad;Lower platform, it is located at the downside of above-mentioned glass substrate, and in the above-mentioned of the lower platform Glass substrate side has downside grinding pad;And discoid carrier, it, which is provided with, protects multiple running through for the above-mentioned glass substrates of holding Hole is held, above-mentioned carrier is clipped by above-mentioned upside grinding pad and above-mentioned downside grinding pad, and enters by above-mentioned planetary gears Rotary motion as defined in row.
It is above-mentioned to have through retaining hole:Be configured in the near center location of above-mentioned carrier one the 1st runs through retaining hole; Multiple 2 run through retaining hole through what retaining hole annularly configured with around the above-mentioned 1st.
The diameter of above-mentioned glass substrate is being set to Dmm and protected running through from the center of above-mentioned carrier to the above-mentioned 1st Hold the center in hole distance be set to rmm in the case of, the above-mentioned 1st is arranged on satisfaction through the center of retaining hole The opening position of the relational expression of [(D/4)≤r≤(D/2)].
In another way, above-mentioned carrier, than annularly configured through retaining hole around the above-mentioned 1st above-mentioned the 2 opening position on the inside of radial direction of the retaining hole by above-mentioned carrier, also with diameter than above-mentioned through small auxiliary of retaining hole Help through hole.
Possess in the information recording carrier based on the present invention:Glass substrate, it is by any one above-mentioned mode institute What the manufacture method for the glass substrate for information recording medium stated obtained;And magnetic thin film layer, it is formed in above-mentioned glass substrate On main surface.
Invention effect
In accordance with the invention it is possible to provide manufacture method and information record Jie of a kind of glass substrate for information recording medium Matter, in the grinding process of double-sided grinding device has been used, it can suppress to produce step on grinding pad.
Brief description of the drawings
Fig. 1 is the stereogram for showing the glass substrate obtained by the manufacture method by the glass substrate in embodiment.
Fig. 2 is the disk for showing to possess the glass substrate obtained by the manufacture method by the glass substrate in embodiment Stereogram.
Fig. 3 is the flow chart for the manufacture method for showing the glass substrate in embodiment.
Fig. 4 is the partial perspective view of the double-sided grinding device used in grinding process.
Fig. 5 is the top view for showing the carrier in embodiment.
Fig. 6 is the top view for the size relationship for showing the carrier in embodiment.
Fig. 7 is the top view of glass substrate.
Fig. 8 is the top view for showing to refer to the carrier in technology.
Fig. 9 is the top view of the downside grinding pad in the technology that refers to.
Figure 10 is the top view for showing the carrier in another embodiment.
Figure 11 be show embodiment 1-2, end surface shape in comparative example 1-2 evaluation result figure.
Embodiment
Below, referring to the drawings, to being illustrated based on embodiments of the present invention and embodiment.In embodiment and implementation In the explanation of example, in the case where referring to number, amount etc., except in the case of having and especially recording, the scope of the present invention simultaneously differs Fixed limit is due to the number, amount etc..In the explanation of embodiment and embodiment, such situation be present:For the same part and Corresponding part, identical reference number is marked, and the explanation of repetition is not repeated.
[glass substrate/disk 10]
Referring to Figures 1 and 2, first, to the manufacture by the glass substrate for information recording medium based on present embodiment Glass substrate 1 obtained by method and the disk 10 for possessing glass substrate 1 illustrate.Fig. 1 is shown in (the reference of disk 10 The stereogram of the glass substrate 1 used in Fig. 2).Fig. 2 is to be shown as information recording carrier, possess the disk of glass substrate 1 10 stereogram.
As shown in figure 1, the glass substrate 1 (glass substrate for information recording medium) used in disk 10 is in middle heart The circular plate shape of Cheng Youkong 1H ring-type.The glass substrate 1 of disc-shape has the main surface 1A in front, back side major surface 1B, interior All end face 1C and peripheral end face 1D.
The size of glass substrate 1 is not particularly limited, for example, external diameter is 0.8 inch, 1.0 inches, 1.8 inches, 2.5 English It is very little or 3.5 inches etc..From the viewpoint of breakage is prevented, the thickness of glass substrate 1 is, for example, 0.30mm~2.2mm.This reality Applying the size of the glass substrate 1 in mode is:External diameter is about 65mm, and internal diameter is about 20mm, and thickness is about 0.8mm.Glass The thickness of glass substrate 1 is that the average of the value that is measured at any number of points by the point symmetry on glass substrate 1 calculates Value.
As shown in Fig. 2 in disk 10, formed with magnetic film on the positive main surface 1A of above-mentioned glass substrate 1, from And form the magnetic thin film layer 2 for including magnetic recording layer.In fig. 2, formed with magnetic thin film layer 2 only on the main surface 1A in front, but Can be overleaf on main surface 1B formed with magnetic thin film layer 2.
Magnetic thin film layer 2 is main by the way that the thermosetting resin for being dispersed with magnetic particle to be spun on to the front of glass substrate 1 (spin-coating method) formed on the 1A of surface.Magnetic thin film layer 2 can also be formed at glass substrate by sputtering method or electroless plating method etc. 1 positive main surface 1A.
On the thickness of the magnetic thin film layer 2 formed on the positive main surface 1A of glass substrate 1, in the case of spin-coating method It is about 0.3 μm~about 1.2 μm, is about 0.04 μm~about 0.08 μm in the case of sputtering method, in electroless plating method In the case of be about 0.05 μm~about 0.1 μm.From the viewpoint of filming and densification, preferably pass through sputtering method or change Plating method is learned to form magnetic thin film layer 2.
As the magnetic material for magnetic thin film layer 2, it is not particularly limited, known magnetic material can be used, But in order to obtain high confining force, based on the Co higher by crystalline anisotropy and to adjust relict flux density as mesh And to add Ni or Cr Co class alloys etc. proper.In addition, as the magnetic layer material suitable for thermal assisted recording, can With using the material of FePt classes.
In addition, in order to improve the smoothness of magnetic recording head, lubricant can be thinly coated on the surface of magnetic thin film layer 2. As lubricant, such as it can enumerate to be diluted as the PFPE (PFPE) of fluid lubricant by the use of the solvent of freon class etc. and obtain The lubricant arrived.
Furthermore, it is also possible to it is arranged as required to basalis or protective layer.Basalis in disk 10 selects according to magnetic film Select.As the material of basalis, such as it can enumerate what is selected from the nonmagnetic metal such as Cr, Mo, Ta, Ti, W, V, B, Al or Ni Material more than at least one.
In addition, basalis is not limited to individual layer, the multilayer for being laminated identical type or different types of layer forms can also be set to Structure.For example, the multi-layer substrates such as Cr/Cr, Cr/CrMo, Cr/CrV, NiAl/Cr, NiAl/CrMo or NiAl/CrV can be set to Layer.
As the protective layer for abrasion and the corrosion for preventing magnetic thin film layer 2, such as Cr layers, Cr alloy-layers, carbon-coating, hydrogen can be enumerated Change carbon-coating, zirconia layer or silicon dioxide layer etc..These protective layers can utilize in-line arrangement together with basalis, magnetic film etc. Sputter equipment is continuously formed.In addition, these protective layers can be set to individual layer, or it is set to by identical type or variety classes Layer form sandwich construction.
Other protective layers can be formed on above-mentioned protective layer, or substitutes above-mentioned protective layer and forms other protective layers. For example, above-mentioned protective layer can be substituted, and on Cr layers, during the solvent dilution tetraalkoxysilane with alcohol type, point Dissipate ground coating colloid silicon dioxide microparticle and be sintered, form silica (SiO2) layer.
[manufacture method of glass substrate]
Next, using the flow chart shown in Fig. 3, in present embodiment glass substrate for information recording medium (with Under, referred to simply as glass substrate.) manufacture method illustrate.Fig. 3 is the manufacture for showing the glass substrate 1 in embodiment The flow chart of method.
The manufacture method of glass substrate in present embodiment possesses glass blank preparatory process (step S10), glass base Plate formation process (step S20), grinding/grinding step (step S30), chemical enhanced process (step S40) and matting (step S50).The glass substrate that can be obtained to process chemical intensification treatment process (step S40) is (equivalent to the glass in Fig. 1 Substrate 1) implement magnetic thin film formation process (step S60).By magnetic thin film formation process (step S60), can obtain as letter Cease the disk 10 of recording medium.
Hereinafter, in the description below illustrated successively to this each step S10~S60 details, do not record The simplified cleaning suitably carried out between each step S10~S60.
(glass blank preparatory process)
In glass blank preparatory process (step S10) so that the glass material melting (step of glass substrate to be formed S11).Glass material is for example with common alumina silicate glass.Alumina silicate glass contains 58% mass percent~75% The SiO of mass percent2, the mass percent of 5% mass percent~23% Al2O3, the mass of 3% mass percent~10% The Li of percentage2O, the Na of the mass percent of 4% mass percent~13%2O is as main component.The glass material of melting exists After flowing on lower mould, punch forming (step S12) is carried out by upper die and lower die.Discoid glass is formd by punch forming Glass blank (base glass material).
Glass blank, which can utilize, to be ground grinding tool and cuts out the foliated glass formed by pulling down (down draw) method or float glass process (plate glass) and formed.In addition, glass material is not limited to alumina silicate glass, can be arbitrary material.
(glass substrate formation process)
Next, in glass substrate formation process (step S20), for the purpose of improving dimensional accuracy and form accuracy, Implement the 1st friction process (step S21) in the main surface of two sides of the glass blank formed to punch forming.Two sides of glass blank Main surface refer to main surface by each processing described later and as the positive main surface 1A in Fig. 1 and as the main table in the back side Face 1B main surface (hereinafter referred to as two main surfaces).For example, by using granularity #400 alumina abrasive grain, (particle diameter is about 40~60 μm), surface roughness Rmax is finish-machined to as 6 μm or so.
After the 1st friction process, the diamond drill machine using cylindrical shape is first-class, implements coring to the central part of glass blank (inner circumferential excision) handles (step S22).Handled by coring, can obtain opening up porose circular glass base in central part Plate.Chamfer machining as defined in can also implementing to the hole of central part.
In addition, using brush by the peripheral end face of glass substrate and inner circumferential end surface grinding into mirror-like (step S22).As Abrasive particle is ground, the slurry containing cerium oxide abrasive particle can be used.
(grinding/grinding step)
Next, in grinding/grinding step (step S30), the 2nd friction work is implemented to two main surfaces of glass substrate Sequence (step S31).2nd friction process (step S31) is carried out using double-sided grinding device, and the double-sided grinding device make use of row Star gear mechanism.Specifically, from two main surfaces that platform is pressed into glass blank up and down, by water, grinding fluid or lubrication Liquid is supplied to two main surfaces, makes glass blank and friction platform relative movement, to carry out the 2nd friction process.
By the 2nd friction process (step S31), the depth of parallelism substantially, flatness and thickness of glass substrate etc. are entered Row pre-adjustment, so as to obtain the base glass material on the main surface with general planar.In the 2nd friction process, produced to reduce Polishing scratch, use the abrasive particle finer than the 1st friction process.It is for example, solid by installing diamond grinding pad etc. on platform Determine abrasive particle, surface roughness Rmax will be refined on two faces of glass substrate as 2 μm or so.
Here, reference picture 4, is illustrated to the Sketch of double-sided grinding device 1000.Fig. 4 is in the 2nd friction process The partial perspective view of the middle double-sided grinding device 1000 used.
Double-sided grinding device 1000 possesses:Upper mounting plate (upside grinding tool keeps platform) 300;(downside grinding tool is kept lower platform Platform) 400;Upside is ground pad 310, and it is installed in the side (glass substrate side) relative with lower platform 400 of upper mounting plate 300 Lower surface on;And downside grinding pad 410, it is installed in the side (glass relative with upper mounting plate 300 of lower platform 400 Substrate-side) upper surface on.
It is to carry out grinding for two main surfaces to glass substrate 1 that upside, which is ground pad 310 and downside grinding pad 410, Machining tool.Upper mounting plate 300 and lower platform 400 mutually rotate in the opposite direction relative to the revolution direction of carrier 500.In shape Carrier 500 is configured with into the gap between upper mounting plate 300 and lower platform 400.The glass substrate 1 of multiple plate-likes is maintained at On the carrier 500.In addition, the detailed construction of carrier 500 can be described afterwards.
The surface that upside grinding pad 310 and downside grinding pad 410 can be carried out in the 2nd friction process (step S31) is clear Wash.Upside is ground pad 310 and the surface clean of downside grinding pad can be in any process in the 2nd friction process (step S31) Middle progress, can also be carried out between any process in grinding/grinding step (step S30), or, can also grinding/ Grinding step (step S30) is carried out after terminating.
After one or many grindings are carried out to the main surface of the two of glass substrate 1, in double-sided grinding device 1000 The surface clean of grinding pad 310 and downside grinding pad 410 on the upside of middle progress.Upside is ground the table of pad 310 and downside grinding pad 410 Face can be periodically cleaned in the one or many grindings of every progress, or, can also aperiodically it be cleaned.
Next, as the 1st polishing process (rough lapping), remove and remain in glass in the 2nd friction process (step S31) Cut on two main surfaces of substrate, while the warpage of glass substrate is corrected (step S33).In the 1st polishing process In, use the double-side polishing apparatus that make use of planetary gears.For example, use hard velvet, polyurethane foam part or pitch The grinding pads such as dipping suede are ground.As grinding agent, the slurry using common cerium oxide abrasive particle as main component is employed Material.
In the 2nd polishing process (precise finiss), attrition process is again carried out to glass substrate, glass is remained in eliminate (step S34) such as tiny flaws on two main surfaces of substrate.Two main surfaces of glass substrate are by being finish-machined to mirror Planar, is formed as desired flatness, and the warpage of glass substrate is also eliminated.In the 2nd polishing process, using make use of row The double-side polishing apparatus of star gear mechanism.For example, use the grinding as soft polisher using suede or velvet as material Pad, is ground.As grinding agent, use with the common colloid finer than the cerium oxide used in the 1st polishing process Silica is the slurry of main component.
(chemical enhanced process)
After glass substrate is cleaned, glass substrate is set to be impregnated in chemical intensification treatment liquid, thus the two of glass substrate Individual main surface forms chemical enhanced layer (step S40).After glass substrate 1 is cleaned, glass substrate 1 is impregnated in and is heated to 30 minutes or so in the chemical intensification treatment liquid such as 300 DEG C of potassium nitrate (70%) and the mixing liquid of sodium nitrate (30%), thus Carry out chemical enhanced.
The alkali metal ions such as the lithium ion that contains in glass substrate 1, sodium ion are by the big potassium of ratio of ionic radii these ions The alkali metal ions such as ion replace (ion-exchange).
Due to because ionic radius is different and caused by deformation, producing compression in the region after having carried out ion exchange should Power, so as to by two main surface peenings of glass substrate 1., can be from glass for example, on two main surfaces of glass substrate 1 The surface of glass substrate 1 forms chemical enhanced layer in the range of playing about 5 μm, so as to improve the rigidity of glass substrate 1.As described above Like that, the glass substrate equivalent to the glass substrate 1 shown in Fig. 1 can be obtained.
The removal amount that can also further implement to glass substrate 1 on two main surfaces is more than 0.1 μm and less than 0.5 μm Polishing., can by the way that the attachment that have passed through on the main surface that glass substrate 1 is remained in after chemical enhanced process is removed To reduce the situation that head crash is produced on the disk produced using glass substrate 1.In addition, by by the two of polishing Removal amount on individual main surface is set as more than 0.1 μm and less than 0.5 μm, will not occur on the surface because of chemical intensification treatment and Caused stress inhomogeneous.The manufacture method of glass substrate in present embodiment is formed as described above.
It is strong alternatively, it is also possible to implement chemistry between the 1st polishing process (rough lapping) and the 2nd polishing process (precise finiss) Chemical industry sequence.
(matting)
Next, glass substrate is cleaned (step S50).Using detergent, pure water, ozone, IPA (isopropanol), Or UV (ultraviolet:Ultraviolet) ozone etc. cleans to two main surfaces of glass substrate, thus, it is attached to glass Attachment on two main surfaces of substrate is removed.
Then, the attachment quantity on the surface of glass substrate 1 is checked using optical profile type flaw detection apparatus etc..
(magnetic thin film formation process)
Two main surfaces of the glass substrate (equivalent to the glass substrate 1 shown in Fig. 1) after chemical intensification treatment is completed Magnetic film is formed on (or any one main surface), is consequently formed magnetic thin film layer 2.Magnetic thin film layer is by making layers below successively Film forming and formed:It is brought into close contact layer, the soft ferromagnetic layer being made up of CoFeZr alloys by what Cr alloys were formed, taken by what Ru was formed To control basalis, the perpendicular magnetic recording layer being made up of CoCrPt alloys, the protective layer being made up of C classes and the profit being made up of F classes Slip layer.By forming magnetic thin film layer, the perpendicular magnetic recording disk equivalent to the disk 10 shown in Fig. 2 can be obtained.
Disk in present embodiment is an example of the vertical disk being made up of magnetic thin film layer.Disk can also be by magnetic Property layer etc. is configured to disk in so-called face.
(carrier 500)
Next, reference picture 5 is to Fig. 7, it is two-sided to being used in the 2nd friction process in above-mentioned grinding/grinding process The detailed construction of carrier 500 illustrates used by grinding attachment 1000.Fig. 5 is to show the carrier 500 in present embodiment Top view, Fig. 6 is the top view for the size relationship for showing the carrier in present embodiment, and Fig. 7 is the vertical view of glass substrate 1 Figure.
Reference picture 5, the carrier 500 in present embodiment have the main body 510 of disc-shape, and its thickness is about 0.30mm ~2.2mm, select the thickness of the thickness of thin of the ratio glass substrate 1 to be kept.A diameter of about 430mm of carrier 500.Main body 510 can use aramid fiber, FRP (glass epoxy resin), PC (makrolon) etc..
Being provided with carrier 500 at 23 keeps glass substrate 1 to run through retaining hole 520.In the present embodiment, run through Retaining hole 520 has:Run through retaining hole 520C for one the 1st, it is configured near the center C1 of carrier 500;With 22 Individual 2nd runs through retaining hole 520P, and they are annularly configured around the 1st through retaining hole 520C.In the present embodiment, 2 are arranged as double loop through retaining hole 520P, on interior ringed line r1, have been arranged at equal intervals 8 and have run through retaining hole 520P, on outer ringed line r2,14 have been arranged at equal intervals it and have run through retaining hole 520P.Through a diameter of big of retaining hole 520 About 66.5mm.
Here, reference picture 6, Dmm is being set to and by from the center C1 of carrier 500 to by the diameter of glass substrate 1 In the case that 1 distance for running through retaining hole 520C center C2 is set to rmm, the 1st runs through retaining hole 520C center C2 is arranged on position (shadow region represented in figure with S) place of the relational expression of satisfaction [(D/4)≤r≤(D/2)].
In the present embodiment, the diameter D of glass substrate 1 is 65mm, therefore the 1st center for running through retaining hole 520C C2 is arranged on the opening position for meeting 16.25mm≤r≤32.5mm.
Double-sided grinding device 1000 in present embodiment annularly configures 5 carriers 500 in upper mounting plate 300 with Between platform 400.The outer peripheral face of carrier 500 is provided with gear, but eliminates the diagram of gear.In addition, the half of carrier 500 Footpath refers to the size in the case of being measured at the outside circle of gear.
Here, reference picture 8 and Fig. 9, are illustrated to the double-sided grinding device 1000 in the case of following:In carrier 500 Heart position C1 and the 1st overlaps through retaining hole 520C center C2, i.e. is arranged at carrier through retaining hole 520C by the 1st 500 center.Fig. 8 shows the carrier 500 run through the 1st in the case that retaining hole 520C is arranged at the center of carrier 500.
The two-sided mill of glass substrate 1 is being carried out using the carrier 500 shown in the Fig. 8 and using double-sided grinding device 1000 In the case of cutting, as shown in figure 9, when driving double-sided grinding device 1000, configure in the case where the glass substrate 1 at center is concentrated through Side is ground same position, the i.e. Intermediate Gray region BL1 of pad 410.
Glass substrate 1 is concentrated through this case that the i.e. Intermediate Gray region BL1 of same position of downside grinding pad 410 causing In grinding process, part on the downside grinding pad 410 as bonded-abrasive, glass substrate 1 passes through, produce downside and be ground The uneven wear of pad 410, so as to produce step (pressure of the section for spill in the Intermediate Gray region BL1 of downside grinding pad 410 Trace).
If producing step on downside grinding pad 410, easily produce on the surface of glass substrate 1 and drawn by the step The grinding damage (cut) risen.In addition, in order to eliminate the grinding damage, need to process for a long time in grinding step thereafter (larger removal amount).But mostly using low in grinding step below, particularly final grinding step (precise finiss) The grinding pad of hardness, if the time of final grinding step is elongated, the end surface shape of glass substrate deteriorates.This is not limited to down Side is ground pad 410, and identical phenomenon can be also produced on upside grinding pad 410.
On the other hand, the carrier 500 in the present embodiment shown in Fig. 5 is configured to, and the 1st runs through in retaining hole 520C Heart position C2 is in the position of relational expression deviateing from the center C1 of carrier 500, meeting [(D/4)≤r≤(D/2)] (region represented in figure by S).
Thus, can also in the case of the double-side grinding of glass substrate 1 is carried out by double-sided grinding device 1000 Suppress to be ground pad 310 by upside through the glass substrate 1 that retaining hole 520C is kept by the 1st and downside is ground the identical of pad 410 The situation of position.
The result is that, it is suppressed that upside is ground the generation of the uneven wear of pad 310 and downside grinding pad 410, reduces It is ground in upside on pad 310 and downside grinding pad 410 and produces situation of the section for the step (impression) of spill, so as to suppresses Grinding damage (cut) is appeared on the surface of glass substrate 1 as caused by the step.
(embodiment)
Below, above- mentioned information recording medium is said with each embodiment and each comparative example of the manufacture method of glass substrate It is bright.In each embodiment and each comparative example as shown below, untill " the glass substrate forming process " of the S20 shown in Fig. 3, such as Above-mentioned explanation is implemented like that.The number of glass substrate is to amount to 115 for each condition.
(the 2nd friction process)
Then the process before implements the 2nd friction process.Conduct has been used in upside grinding pad and downside grinding pad Bonded-abrasive, 9 μm of abrasive grain diameter diamond grinding pad.In embodiment 1 and embodiment 2, use from carrier 500 The carrier that heart position C1 to the 1st is 20mm through retaining hole 520C center C2 distance r.On the other hand, in comparative example 1 In, used by the 1st through retaining hole 520C center C2 be arranged at carrier 500 center C1 carrier, than It is below 16.25mm i.e. 15mm carrier compared with r in example 2, has been used.
In addition, in example 2, as shown in Figure 10, such glass substrate 1 is used:Kept than running through around the 1st The 2nd opening position on the inside of radial directions of the retaining hole 520p more by carrier 500 that hole 520C is annularly configured, has straight Footpath is than through the small auxiliary through hole 520M of retaining hole 520.4 auxiliary through hole 520M are provided with the glass substrate.Auxiliary Through hole 520M a diameter of 26mm, from the center C1 of carrier 500 to the distance of auxiliary through hole 520M center For 50mm.
On auxiliary through hole 520M, only 1 the 1st is being arranged at from the center of carrier 500 through retaining hole 520C In the case of the position that position C1 deviates, the position of centre of gravity of carrier 500 deviates, so as to which there may be change for carrier in grinding process Shape, may be ground pad 310 to upside and downside grinding pad 410 causes to damage.Therefore, auxiliary through hole 520M can be arranged on So that the position of centre of gravity of carrier 500 turns into the opening position of the center of carrier 500.Thereby, it is possible to suppress because carrier 500 deforms Damage in upside grinding pad 310 caused by and and downside grinding pad 410 produces.
In addition, in each embodiment and each comparative example, it is advance using the double-sided grinding device used in the 2nd friction process Prior processing has been carried out, the condition that upper and lower grinding pad shows inherent trend is implemented into the 2nd friction process after reunification, wherein, The glass substrate outside the glass substrate used in this experiment has been used in the prior processing.Specifically, this is being carried out Before experiment, using the carrier used in each embodiment and each comparative example, and the double-side grinding used in this experiment is utilized Device, in a manner of accumulative process time respectively substantially amounts to 40 hours, prior glass substrate processing is carried out.Prior In processing, used with according to glass substrate identical glass substrate made of the process untill above-mentioned S22 processes.Pass through thing First process, can observe the embodiment/comparative example carrier abrasion intrinsic, to grinding pad.
(surface finish measurement)
After the 2nd friction process (S31) terminates, the glass substrate obtained by each embodiment and each comparative example is carried out The measurement of surface roughness.Used in the measurement of surface roughness Co., Ltd.'s KEYENCE company systems, shape measure swashs Light microscope VK9700.
Surface 1mm for measuring glass substrate2Resulting result, is all evaluated.In embodiment 1 and embodiment In 2, compared with comparative example 1 and comparative example 2, the roughness on surface is relatively low, the negligible amounts damaged more deeply confirmed.
(the 1st polishing process (rough lapping))
The 1st polishing process (rough lapping) is implemented, until reaching adding for the grinding marks disappearance for thinking to observe on the surface Untill work amount.In embodiment 1 and embodiment 2, compared with comparative example 1 and comparative example 2, required process time can be shortened.
Next, implement the 2nd polishing process (precise finiss).In each embodiment and each comparative example, make processing conditions It is identical.Here, in each embodiment and each comparative example, the removal of grinding marks is mainly realized by the 1st polishing process, although Make processing conditions identical in 2nd polishing process, but mainly using the 2nd polishing process adjustment processing capacity, even in removing grinding In the case of trace, also process time can be shortened by same method.The grinding particularly used in the 2nd polishing process In the case that the hardness of pad is lower than the grinding pad used in the 1st polishing process, in the 2nd polishing process, easily in glass base Face is produced on plate to collapse angle, still, by with the present embodiment identical method, can expect to shorten process time and prevent that face from collapsing angle Such effect.
(end surface measurement of glass substrate)
Figure 11 shows embodiment 1, embodiment 2 and comparative example 1, the evaluation result of comparative example 2.For passing through embodiment 1, reality The glass substrate obtained by example 2 and comparative example 1, comparative example 2 is applied, using contact pin type profile meter, from the center of glass substrate Towards at radial direction measurement R1 (22.25mm) this point, R2 (27.25mm) this point and R3 (31.25mm) this point The height of glass substrate, as the shape of the end face part of glass substrate, using the line of the height connected at R1 and R2 as benchmark Line, the relative shift of the height of R3 opening positions is analyzed.The analysis result is determined as the product within ± 0.18 μm Certified products.
In addition, in embodiment 1,2 and comparative example 1,2, respectively 50 glass substrates are carried out with end surface measurement, investigation is qualified The ratio of product, situation of more than 86% glass substrate within ± 0.18 μm is set as to evaluate " A ", and thinks qualified, In the case of 86%, it is set as evaluating " C ", and think unqualified.
As shown in figure 11, for the result of end surface measurement, evaluated " A " in embodiment 1 and embodiment 2.Than Compared with example 1 and comparative example 2 for evaluation " C ".
So, the result on end surface measurement, in comparative example 1 and comparative example 2, end surface shape is poor, and in embodiment 1 In embodiment 2, end surface shape is good.In comparative example 1 and comparative example 2, the process time phase of the 1st polishing process (rough lapping) Increase than embodiment 1 and embodiment 2, thereby it is thinkable that with the increase of the process time, the end surface shape of glass substrate Deteriorate.
For the grinding platform used in embodiment 1 and embodiment 2, upper and lower grinding pad is measured after formal processing Average thickness.On to upside be ground pad and downside be ground pad thickness measure, near inner circumferential, Intermediate Gray region, periphery Nearby amount to respectively at each measurement 2 at 6, and then obtained the average value of upside grinding pad and downside grinding pad.
As shown in figure 11, compared with Example 1 compared with example 2, upside grinding pad 310 and downside are ground pad 410 The average value of abrasion is smaller, is 20 μm or so.Because in the case of embodiment 2, through hole is aided in by setting 520M, the position of centre of gravity of carrier 500 is corrected to the center C1 of carrier 500, thus, the phase of carrier 500 with embodiment 1 Than the deformation of vertical direction caused by carrier 500 reduces, so as to inhibit in upside grinding pad 310 and downside grinding pad 410 Damage produce.
And then the glass substrate to being obtained by above-described embodiment 1-2 and comparative example 1-2 implements the chemistry shown in Fig. 3 Strengthen process (S40), matting (S50) and magnetic thin film formation process (S60), obtain information recording carrier.
The information recording carrier is loaded into hard disk drive, has carried out read-write experiment.Use and obtained by comparative example 1-2 The information recording carrier of glass substrate the area that can not be recorded is generated near the periphery of information recording carrier.On the other hand, The information recording carrier by the obtained glass substrates of embodiment 1-2 has been used near the periphery of information recording carrier Good record can be realized.
Embodiments of the present invention and embodiment are illustrated as described above, it should think this time disclosed and implement Mode and embodiment are all to illustrate and unrestricted in all respects.The scope of the present invention by claims, without by above-mentioned Illustrate to represent, it is intended to include being had altered in the meaning and scope equal with claim.
Label declaration
1A:The main surface in front;1B:Back side major surface;1C:Inner circumferential end face;1D:Peripheral end face;1H:Hole;2:Magnetic thin film layer; 10:Disk;300:Upper mounting plate;310:Upside grinding pad;310g、410g:Groove;400:Lower platform;410:Downside grinding pad;500: Carrier;510:Main body;520:Through retaining hole;520C:1st runs through retaining hole;520P:2nd runs through retaining hole;520M:Auxiliary Through hole;1000:Double-sided grinding device.

Claims (2)

1. a kind of manufacture method of glass substrate for information recording medium, glass base of the described information recording medium in disc-shape Formed with magnetic thin film layer on the main surface of plate, in the manufacture method of described information recording medium glass substrate,
With surface grinding process, in the surface grinding process, using the double-sided grinding device for possessing planetary gears, one Side supplies water, grinding fluid or lubricating fluid while being ground the main surface of the glass substrate,
The double-sided grinding device possesses:
Upper mounting plate, it is located at the upside of the glass substrate, and has upside grinding in the glass substrate side of the upper mounting plate Pad;
Lower platform, it is located at the downside of the glass substrate, and has downside grinding in the glass substrate side of the lower platform Pad;And
Discoid carrier, it runs through retaining hole provided with multiple holding glass substrates, and the carrier is by the upper side grinding Cut pad and the downside grinding pad clip, and by the planetary gears carry out as defined in rotary motion,
It is described to have through retaining hole:Be configured in the near center location of the carrier unique one the 1st runs through holding Hole;Multiple 2 run through retaining hole through what retaining hole annularly configured with around the described 1st,
The diameter of the glass substrate is being set to Dmm and retaining hole will be run through from the center of the carrier to the described 1st Center distance be set to rmm in the case of, the described 1st is arranged on satisfaction [(D/4) through the center of retaining hole ≤ r≤(D/2)] relational expression opening position,
The carrier, than around the described 1st through retaining hole annularly configure the described 2nd through retaining hole by described Opening position on the inside of the radial direction of carrier, also with diameter than the auxiliary through hole small through retaining hole.
2. a kind of grinding carrier, the grinding is used with carrier in the manufacture method of substrate for information recording medium, described Information recording carrier on the main surface of the substrate of disc-shape formed with magnetic thin film layer, wherein,
The grinding runs through retaining hole with carrier provided with multiple holding substrates,
It is described to have through retaining hole:Unique one the 1st of near center location for being configured in the grinding carrier runs through Retaining hole;Multiple 2 run through retaining hole through what retaining hole annularly configured with around the described 1st,
The diameter of the substrate is being set to Dmm and kept running through from the center of the grinding carrier to the described 1st In the case that the distance of the center in hole is set to rmm, the described 1st is arranged on satisfaction [(D/ through the center of retaining hole 4)≤r≤(D/2)] relational expression opening position,
The grinding with carrier, than the described 2nd running through retaining hole through what retaining hole annularly configured around the described 1st By the opening position on the inside of the radial direction of the grinding carrier, also run through with diameter than the auxiliary small through retaining hole Hole.
CN201380011847.3A 2012-03-30 2013-03-06 The manufacture method and information recording carrier of glass substrate for information recording medium Active CN104170013B (en)

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