CN104146887A - BB cream having long-acting moisturizing function and preparation method thereof - Google Patents
BB cream having long-acting moisturizing function and preparation method thereof Download PDFInfo
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- CN104146887A CN104146887A CN201410425432.7A CN201410425432A CN104146887A CN 104146887 A CN104146887 A CN 104146887A CN 201410425432 A CN201410425432 A CN 201410425432A CN 104146887 A CN104146887 A CN 104146887A
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- polydimethylsiloxane
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- stearoyl
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- aluminium hydroxide
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Abstract
The invention provides a BB cream having a long-acting moisturizing function. The BB cream consists following components: decamethylcyclopentasiloxane, isotridecyl isononanoate, ultrafine silicon processed titanium dioxide, nano silicon processed titanium dioxide, PEG-9 polydimenthylsiloxyethyl dimethicone, phenyl trimethicone, polydimethylsiloxane, PEG-10 polydimethylsiloxane, decamethylcyclopentasiloxane (and) polydimethylsiloxane/vinyl polydimethylsiloxane crosslinking polymer (and) polydimethylsiloxane, decamethylcyclopentasiloxane/disteardimonium hectorite/Propylene carbonate and the like. The invention also provides a preparation method of the BB cream. The BB cream is fine and smooth in skin feel, is light and weight and is air-penetrating, has a moisturizing function which can last for 8 hours, can significantly increasing moisture content in skin cuticle and can achieve long-acting moisturization without makeup floating.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of BB frost, particularly a kind of BB frost with long-acting moisture-keeping functions, and the preparation method of this BB frost.
Background technology
BB frost is the abbreviation of Blemish Balm, the earliest for medical cosmetology, is to after peeling or whitening (brightening), impaired and the skin care of damage and the regeneration frost that maintenance is used, and because it can improve and make up the shortcoming of skin, and the BB frost of gaining the name.Traditional BB frost, easily causes skinfeel thick and heavy dry, allows skin water content of stratum corneum reduce, and by the dry stricture of vagina of rear easy appearance and floating adornment phenomenon, destroys the balance of nature of skin.
Summary of the invention
An object of the present invention is the problem that will solve for above, the not BB frost of floating adornment of fine and smooth, frivolous ventilative, the long-time moisturizing of a kind of skinfeel is provided.
Another object of the present invention is to provide the preparation method of above-mentioned BB frost.
For this reason, the invention provides a kind of BB frost with long-acting moisture-keeping functions, its component by following percentage by weight forms:
Encircle five polydimethylsiloxane 8.5%~12%, the different pelargonate 3% of different tridecanol, ultra-fine silicon is processed titanium dioxide 3%, nano-silicon is processed titanium dioxide 3%, KF-6028 1.5~2%, phenyl gathers trimethicone 2%, polydimethylsiloxane 2~3%, KF6017 1~1.5%, encircle five polydimethylsiloxane (with) polydimethylsiloxane/vinyl dimethione cross linked polymer (with) polydimethylsiloxane 2~5%, encircle five polydimethylsiloxane/distearyl dimethylammonium Strese Hofmann's hectorite ./propylene glycol carbonate 3~5%, encircle five polydimethylsiloxane/acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer 0.5~2.0%, methyl methacrylate cross linked polymer 1~2%, dimetylsilyl SiClx stone 0.2~0.3%, glycerol 5~7%, propylene glycol 5~7%, stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide black 0.05~0.1%, stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide red 0.1~0.15%, stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide yellow 0.23~0.4%, antifreeze 1.0%, antiseptic 0.3~0.4%, antibacterial 0.1%, water/soluble collagen 1~2%, essence 0.02~0.05%, dipentaerythritol three-poly-hydroxy stearic acid ester 2~4%, water surplus.
Preferably, described antifreeze includes but not limited to sodium chloride.
Preferably, described antiseptic includes but not limited to phenoxyethanol/Sensiva SC50.
Preferably, described antibacterial includes but not limited to o-p-Cymene-5-alcohol.
The present invention also provides the preparation method of described BB frost, and its step is as follows:
(1) quantitatively take each component;
(2) stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide black, stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide red, stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide yellow, ultra-fine silicon being processed to titanium dioxide, nano-silicon processing titanium dioxide and the different pelargonate of different tridecanol grinds;
(3) component in step (2) is added to KF-6028, KF6017, dimetylsilyl SiClx stone, methyl methacrylate cross linked polymer, encircle five polydimethylsiloxane (with) polydimethylsiloxane/vinyl dimethione cross linked polymer (with) polydimethylsiloxane, encircle five polydimethylsiloxane/distearyl dimethylammonium Strese Hofmann's hectorite ./propylene glycol carbonate, encircle five polydimethylsiloxane/acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer, phenyl gathers trimethicone, polydimethylsiloxane, encircle five polydimethylsiloxane, dipentaerythritol three-poly-hydroxy stearic acid ester, antibacterial, mix homogeneously, and be warming up to 70 ℃,
(4) by propylene glycol, glycerol, antifreeze and water mix homogeneously and be warming up to 70 ℃;
(5) under middling speed (600~900r/min) stirring, the mixture in step (4) is evenly added to the mixture in step (3), and homogenizing;
(6) stir and to be cooled to 45 ℃ when following, add essence, water/soluble collagen and antiseptic, homogenizing also stirs; Obtain finished product.
After tested, BB frost skinfeel of the present invention is fine and smooth, frivolous ventilative, and moistening effect reaches eight hours, can significantly increase skin water content of stratum corneum, realizes the not floating adornment of long-time moisturizing.
Accompanying drawing explanation
Fig. 1 is the keratodermatitis water content test result of the BB frost of embodiment 1.
Fig. 2 is the keratodermatitis water content test result of the BB frost of embodiment 2.
Fig. 3 is the keratodermatitis water content test result of the BB frost of embodiment 3.
Fig. 4 is the keratodermatitis water content test result of commercially available common BB frost.
The specific embodiment
Below in conjunction with specific embodiment, technical scheme of the present invention is described in further detail, but protection scope of the present invention is not limited in following examples.In embodiment, various raw material components used all can be buied by commercial channel.Wherein, encircle five polydimethylsiloxane (with) polydimethylsiloxane/vinyl dimethione cross linked polymer (with) polydimethylsiloxane is for purchased from the FB-9586SILICONE ELASTOMER BLEND of Dow Corning, encircle five polydimethylsiloxane/distearyl dimethylammonium Strese Hofmann's hectorite ./propylene glycol carbonate for the BENTONE GEL VS-5PCV purchased from ELEMENTIS company, encircling five polydimethylsiloxane/acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer (ring five polydimethylsiloxane and acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer mass ratio are 7:3) is the KP-545 purchased from Shin Etsu company, iron oxide yellow/stearoyl-glutamic acid disodium/aluminium hydroxide (NAI-C33134-10), iron oxide red/stearoyl-glutamic acid disodium/aluminium hydroxide (NAI-C33-8075-10), iron oxide black/stearoyl-glutamic acid disodium/aluminium hydroxide (NAI-C33-8073-10) is purchased from MIYOSHI KASEI company, water/soluble collagen (mass ratio is 99:1) is the Maricol CLR purchased from CLR-Chemisches Laboratorium, phenoxyethanol/Sensiva SC50 (Euxyl PE 9010) is purchased from Schulke company.
BB according to the following step difference Preparation Example 1~3 is white:
1. quantitatively take each component;
2.A component is crossed three-roller and is ground 2 times;
3. A component is added to B component mix homogeneously, and be warming up to 70 ℃;
4. by C component mix homogeneously and be warming up to 70 ℃;
5. under middling speed (600~900r/min) stirring, C component is evenly added to A, B blending ingredients, and homogenizing;
6. stir and be cooled to 45 ℃ when following, add D component, homogenizing also stirs;
7. be up to the standards, discharging fill.
BB frost and commercially available common BB frost to above-described embodiment 1~3 carry out respectively keratodermatitis water content test comparison.Testing result demonstration, the BB frost of embodiment 1~3 is significantly higher than commercially available common BB frost by rear keratodermatitis water content.Concrete method of testing and data analysis are as follows:
The test of keratodermatitis water content
1. white, the commercially available common BB of the BB of tested material: embodiment 1~3 is white
2. experimental basis: QB/T 4256-2011 < < cosmetics moisture-keeping efficacy evaluation guide > >
3. test method:
3.1 each BB frost are respectively looked for 9 experimenters, experimenter's feature: women, 38.5 ± 11.2 years old mean age.
3.2 tested positions: two forearms inner side, labelling is tested position everywhere, random assortment Wei Tuyang district 1, Tu Yang district 2, Tu Yang district 3 and check plot, Tu Yang smears tested material in district, and any product is not smeared in check plot.
3.3 products are smeared dosage: application area: 3cm * 3cm, smears dosage: 2mg/cm2.
3.4 test indexs: keratodermatitis water content.
Test environment: temperature: 20-22 ℃, relative humidity: 40-60%.
3.5 test procedures: experimenter sits quietly after 20min, (T0) keratodermatitis water content before testing tested position sample and smearing, then dosage is smeared tested material in accordance with regulations, Tu Yang district 1, Tu Yang district 2, Tu Yang district 3 are respectively at smearing 1 hour (T1) after tested material, and 4 hours (T2) and 8 hours (T3) tests tested position keratodermatitis water content.Before test, with dry napkin wiping, remove the residual product of skin surface (also using twice of dry napkin wiping skin before smearing sample and before the skin test of blank position).In process of the test, experimenter's forearm exposes, and is test mode and places, and keeps loosening.
Statistical method: if test data is normal distribution, adopt t check; If test data is nonnormal distribution, adopt rank test, two-tailed test, inspection level α=0.05.
4. result of the test:
As shown in Figure 1, as shown in Figure 2, as shown in Figure 3, reference examples test result as shown in Figure 4 for embodiment 3 test results for embodiment 2 test results for embodiment 1 test result.
Result of the test shows, compares with commercially available common BB frost, and the BB frost of embodiment 1~3, after smearing 1 hour, 4 hours, 8 hours, all has good moistening effect.In addition, observe as seen in process of the test, compare with commercially available common BB frost, the white ductility of BB of embodiment 1~3 is better, and skinfeel is more fine and smooth, and more frivolous ventilative non-greasy.
In addition, embodiment 1~3 is all by heat-resisting (40 ± 1 ℃, after 24 hours recovery room temperatures, sample is normal), cold-resistant (15 ± 1 ℃, after 24 hours recovery room temperatures, sample is normal), and sanitary index meets cosmetics health standard.
Claims (5)
1. a BB with long-acting moisture-keeping functions is white, is further characterized in that the component by following percentage by weight forms:
Encircle five polydimethylsiloxane 8.5%~12%, the different pelargonate 3% of different tridecanol, ultra-fine silicon is processed titanium dioxide 3%, nano-silicon is processed titanium dioxide 3%, KF-6028 1.5~2%, phenyl gathers trimethicone 2%, polydimethylsiloxane 2~3%, KF6017 1~1.5%, encircle five polydimethylsiloxane (with) polydimethylsiloxane/vinyl dimethione cross linked polymer (with) polydimethylsiloxane 2~5%, encircle five polydimethylsiloxane/distearyl dimethylammonium Strese Hofmann's hectorite ./propylene glycol carbonate 3~5%, encircle five polydimethylsiloxane/acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer 0.5~2.0%, methyl methacrylate cross linked polymer 1~2%, dimetylsilyl SiClx stone 0.2~0.3%, glycerol 5~7%, propylene glycol 5~7%, stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide black 0.05~0.1%, stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide red 0.1~0.15%, stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide yellow 0.23~0.4%, antifreeze 1.0%, antiseptic 0.3~0.4%, antibacterial 0.1%, water/soluble collagen 1~2%, essence 0.02~0.05%, dipentaerythritol three-poly-hydroxy stearic acid ester 2~4%, water surplus.
2. BB frost according to claim 1, is characterized in that: described antifreeze is sodium chloride.
3. BB frost according to claim 1, is characterized in that: described antiseptic is phenoxyethanol/Sensiva SC50.
4. BB frost according to claim 1, is characterized in that: described antibacterial is o-p-Cymene-5-alcohol.
5. the preparation method of BB frost described in claim 1 to 4 any one, its step is as follows:
(1) quantitatively take each component;
(2) stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide black, stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide red, stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide yellow, ultra-fine silicon being processed to titanium dioxide, nano-silicon processing titanium dioxide and the different pelargonate of different tridecanol grinds;
(3) component in step (2) is added to KF-6028, KF6017, dimetylsilyl SiClx stone, methyl methacrylate cross linked polymer, encircle five polydimethylsiloxane (with) polydimethylsiloxane/vinyl dimethione cross linked polymer (with) polydimethylsiloxane, encircle five polydimethylsiloxane/distearyl dimethylammonium Strese Hofmann's hectorite ./propylene glycol carbonate, encircle five polydimethylsiloxane/acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer, phenyl gathers trimethicone, polydimethylsiloxane, encircle five polydimethylsiloxane, dipentaerythritol three-poly-hydroxy stearic acid ester, antibacterial, mix homogeneously, and be warming up to 70 ℃,
(4) by propylene glycol, glycerol, antifreeze and water mix homogeneously and be warming up to 70 ℃;
(5) under stirring, the mixture in step (4) is evenly added to the mixture in step (3), and homogenizing;
(6) stir and to be cooled to 45 ℃ when following, add essence, water/soluble collagen and antiseptic, homogenizing also stirs; Obtain finished product.
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CN102327196A (en) * | 2011-08-19 | 2012-01-25 | 广州市白云联佳精细化工厂 | Sun-proof BB (Blemish Balm) cream and preparation method thereof |
CN103735461A (en) * | 2014-01-13 | 2014-04-23 | 广东幸美化妆品股份有限公司 | Blemish balm (BB) cream capable of preventing makeup meltdown for seven hours and preparation method thereof |
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