CN104126861B - Applications of Coconut Juice Concentrate - Google Patents
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- 235000020415 coconut juice Nutrition 0.000 title claims description 37
- 239000012141 concentrate Substances 0.000 title claims description 37
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 28
- 244000060011 Cocos nucifera Species 0.000 claims abstract description 27
- 235000013162 Cocos nucifera Nutrition 0.000 claims abstract description 27
- 241000208125 Nicotiana Species 0.000 claims abstract description 16
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 16
- 235000021579 juice concentrates Nutrition 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims abstract description 5
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 4
- 239000007787 solid Substances 0.000 claims description 9
- 238000005507 spraying Methods 0.000 claims description 8
- 230000003020 moisturizing effect Effects 0.000 claims description 4
- 238000007738 vacuum evaporation Methods 0.000 claims 2
- 239000000779 smoke Substances 0.000 abstract description 25
- 239000007789 gas Substances 0.000 abstract description 16
- 230000000694 effects Effects 0.000 abstract description 9
- 235000009508 confectionery Nutrition 0.000 abstract description 4
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 abstract description 2
- 229960002715 nicotine Drugs 0.000 abstract description 2
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 abstract description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract 2
- 239000003546 flue gas Substances 0.000 abstract 2
- 238000011156 evaluation Methods 0.000 description 17
- 239000003205 fragrance Substances 0.000 description 12
- 238000000034 method Methods 0.000 description 10
- 230000000391 smoking effect Effects 0.000 description 9
- 206010013911 Dysgeusia Diseases 0.000 description 8
- 239000012496 blank sample Substances 0.000 description 8
- 230000007794 irritation Effects 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 6
- 238000001704 evaporation Methods 0.000 description 5
- 230000008020 evaporation Effects 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 239000000571 coke Substances 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 235000013372 meat Nutrition 0.000 description 3
- 235000013336 milk Nutrition 0.000 description 3
- 239000008267 milk Substances 0.000 description 3
- 210000004080 milk Anatomy 0.000 description 3
- 208000005577 Gastroenteritis Diseases 0.000 description 2
- 208000004880 Polyuria Diseases 0.000 description 2
- 230000035619 diuresis Effects 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 239000001963 growth medium Substances 0.000 description 2
- 238000009629 microbiological culture Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 201000006082 Chickenpox Diseases 0.000 description 1
- 206010008631 Cholera Diseases 0.000 description 1
- 241000737241 Cocos Species 0.000 description 1
- 208000010201 Exanthema Diseases 0.000 description 1
- 201000005505 Measles Diseases 0.000 description 1
- 241000244206 Nematoda Species 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- 206010046980 Varicella Diseases 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000011712 cell development Effects 0.000 description 1
- 230000010261 cell growth Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 229940105039 coconut extract Drugs 0.000 description 1
- 235000020197 coconut milk Nutrition 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 201000005884 exanthem Diseases 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 235000019264 food flavour enhancer Nutrition 0.000 description 1
- 208000006454 hepatitis Diseases 0.000 description 1
- 231100000283 hepatitis Toxicity 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
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- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
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- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 238000004161 plant tissue culture Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
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- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 206010037844 rash Diseases 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- 230000001256 tonic effect Effects 0.000 description 1
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Abstract
Description
技术领域technical field
本发明涉及一种椰子原汁浓缩物的应用,属于烟草增香领域。The invention relates to the application of coconut raw juice concentrate and belongs to the field of tobacco flavoring.
背景技术Background technique
椰子属于棕榈科椰子属,是热带地区主要油料作物和食品能源作物,其综合利用经济价值高,故享有“宝树”的美誉。椰子主要分布在南北纬20°间的热带地区,全世界有90多个国家和地区种植,种植面积达1100万m2,年产椰果570亿个。我国椰子种植已有2000多年的历史,主要种植于海南省,在广东、广西、云南和台湾有少量种植。目前我国椰子种植面积为4.6万m2,年产椰果2.43亿个。椰子水是椰子坚果腔内的液体胚乳,是一种营养丰富的天然饮料。椰子水对增强肾脏血液循环和利尿均有良好的作用,临床上可用于辅助治疗肝炎和肠胃炎;微生物学上可作为微生物培养基;在食品工业上可利用研制多种食品,如椰果、椰子酒、椰子水饮料等。其主要成分是还原糖、矿物质、蛋白质、氨基酸及其它微量成分。椰子水特别是嫩椰子水具有促消化、利尿、抗菌消炎等药用价值。在民间,嫩椰子水常被用于治疗婴儿肠胃炎、降暑、杀蛔虫,也被用于治疗皮疹水痘和麻疹等引起的发热,还可作为霍乱病人的饮料和老弱病人的滋补品等。由于养分全面并且富含多种可促进细胞生长发育的激素,椰子水可作为培养液应用于微生物培养和植物组织培养,还可应用于鲜花保鲜。Coconut belongs to the genus Cocos palmaceae and is the main oil crop and food energy crop in the tropics. Its comprehensive utilization has high economic value, so it enjoys the reputation of "treasure tree". Coconuts are mainly distributed in tropical regions between north and south latitudes of 20°. They are planted in more than 90 countries and regions around the world, with a planting area of 11 million m2 and an annual output of 57 billion coconuts. Coconut cultivation in my country has a history of more than 2,000 years, mainly in Hainan Province, and a small amount in Guangdong, Guangxi, Yunnan and Taiwan. At present, my country's coconut planting area is 46,000 m2, with an annual output of 243 million coconuts. Coconut water, the liquid endosperm inside the coconut nut cavity, is a nutrient-dense natural beverage. Coconut water has a good effect on enhancing kidney blood circulation and diuresis. It can be used clinically as an auxiliary treatment for hepatitis and gastroenteritis; in microbiology it can be used as a microbial culture medium; in the food industry it can be used to develop a variety of foods, such as coconut, Coconut wine, coconut water drinks, etc. Its main components are reducing sugars, minerals, proteins, amino acids and other trace components. Coconut water, especially tender coconut water, has medicinal value such as promoting digestion, diuresis, antibacterial and anti-inflammatory. In the folk, tender coconut water is often used to treat infant gastroenteritis, reduce heat, kill roundworms, and also be used to treat fever caused by rashes, chickenpox, and measles. It can also be used as a drink for cholera patients and a tonic for the elderly and weak. . Because of its comprehensive nutrition and rich in a variety of hormones that can promote cell growth and development, coconut water can be used as a culture medium for microbial culture and plant tissue culture, and can also be used for fresh flowers.
发明内容Contents of the invention
本发明的目的是在于提供椰子原汁浓缩物在卷烟中的应用,将椰子原汁浓缩物添加在卷烟叶丝、梗丝等中,不但能起到保润作用,而且和卷烟烟气产生很好的烟气协同增香作用,能降低烟碱刺激性,增强甜润感,柔和烟气,掩盖杂气,提高卷烟的抽吸品质。The purpose of the present invention is to provide the application of coconut juice concentrate in cigarettes. Adding coconut juice concentrate to shredded cigarette leaves and cut stems can not only play a moisturizing role, but also produce a lot of moisture with cigarette smoke. Good smoke synergizes with flavor enhancement, which can reduce the irritation of nicotine, enhance the sweetness, soften the smoke, cover up miscellaneous gases, and improve the smoking quality of cigarettes.
本发明提供了椰子原汁浓缩物的应用,该应用是将椰子原汁浓缩物添加在卷烟叶丝、梗丝、烟草薄片或它们的混合物中应用于卷烟增香和保润;所述的椰子原汁浓缩物由椰子原汁在压强为65~85mmHg,温度为40~60℃的条件下减压浓缩到固含量≥90%制得。The present invention provides the application of the concentrated coconut juice, which is to add the concentrated coconut juice to shredded cigarette leaves, shredded stems, tobacco flakes or their mixtures for flavoring and moisturizing of cigarettes; the coconut The raw juice concentrate is prepared by concentrating coconut raw juice under reduced pressure to a solid content ≥ 90% under the conditions of a pressure of 65-85 mmHg and a temperature of 40-60°C.
本发明的椰子原汁浓缩物的应用方法还包括以下优选方案。The application method of the coconut juice concentrate of the present invention also includes the following preferred options.
优选的应用方法中椰子原汁在压强为70~80mmHg,温度为43~47℃的条件下进行减压蒸发浓缩;最优选为在压强为76mmHg,温度为45℃的条件下进行减压蒸发浓缩。In the preferred application method, the raw coconut juice is evaporated and concentrated under reduced pressure at a pressure of 70 to 80 mmHg and a temperature of 43 to 47 °C; the most preferred method is to evaporate and concentrate under reduced pressure at a pressure of 76 mmHg and a temperature of 45 °C .
优选的应用方法中减压蒸发浓缩直到浓缩物固含量≥99%。The preferred application method is to concentrate by evaporation under reduced pressure until the solid content of the concentrate is ≥ 99%.
优选的应用方法中椰子原汁浓缩物在卷烟叶丝、梗丝、烟草薄片或它们的混合物中的添加量为5ppm~50ppm;最优选为10ppm~30ppm。In the preferred application method, the amount of coconut juice concentrate added to shredded cigarette leaves, shredded stems, tobacco flakes or their mixture is 5ppm-50ppm; most preferably 10ppm-30ppm.
优选的应用方法中椰子原汁浓缩物通过大曲酒稀释后采用喷雾方式添加。In the preferred application method, the coconut juice concentrate is added by spraying after being diluted with Daqu wine.
本发明的有益效果:本发明首次将椰子原汁在适当压强和温度范围内进行浓缩,发现以该方法获得的椰子浓缩物具有自然、浓郁、舒适的果甜香味,将其作为增香剂添加在卷烟的叶丝、薄片等中,不但能增强烟气甜润感,而且和卷烟烟气产生很好的协同增香作用,能和烟气融合成一种具有果甜香味和烟草本香的复合香味,能细腻、柔和烟气,掩盖杂气,降低刺激性,大大提升了卷烟抽吸品质。此外,本发明的制备方法操作简单,不使用任何化学试剂,对环境无污染,能耗少、原料来源广,生产成本低。Beneficial effects of the present invention: the present invention concentrates the raw coconut juice in a suitable pressure and temperature range for the first time, and finds that the coconut concentrate obtained by this method has a natural, rich and comfortable fruity sweet fragrance, which is added as a flavor enhancer In the shredded leaves and thin slices of cigarettes, it can not only enhance the sweetness of the smoke, but also produce a good synergistic aroma-enhancing effect with the cigarette smoke, and can be integrated with the smoke to form a compound aroma with fruity aroma and tobacco aroma , can delicate and soft the smoke, cover up miscellaneous gas, reduce irritation, and greatly improve the smoking quality of cigarettes. In addition, the preparation method of the present invention is simple to operate, does not use any chemical reagents, has no pollution to the environment, has low energy consumption, wide source of raw materials, and low production cost.
具体实施方式detailed description
以下实施例旨在进一步说明本发明内容,而非限制本发明的保护范围。The following examples are intended to further illustrate the content of the present invention, but not to limit the protection scope of the present invention.
实施例1Example 1
取新鲜椰子原汁在压强为76mmHg,温度为45℃的条件下进行减压蒸发,浓缩到浓缩物的固含量≥99%,即得椰子原汁浓缩物。Get the fresh coconut juice and evaporate it under reduced pressure under the condition that the pressure is 76mmHg and the temperature is 45° C., and concentrate until the solid content of the concentrate is ≥ 99%, so as to obtain the coconut juice concentrate.
取椰子原汁浓缩物若干,用52°的大曲酒稀释成浓度为2.0g/L溶液,取上述溶液5mL,采用喷雾方式加香,使上述溶液均匀喷洒在1000g烟丝上,于22℃和相对湿度60%的条件下平衡48h,取出做成卷烟,进行评吸,与空白样对比(不加香),进行评价,其评价效果主要表现为:与烟草本香协调较好,具有烟草本香和果甜香的复合香味,烟气细腻、柔和,湿润感增强,烟气较飘逸,杂气被掩盖,刺激性降低,余味舒适,提升了卷烟抽吸品质。Take some coconut juice concentrate, dilute it with 52° Daqu wine to a solution with a concentration of 2.0g/L, take 5mL of the above solution, and use the spray method to add flavor, so that the above solution is evenly sprayed on 1000g of shredded tobacco. Equilibrate for 48 hours under the condition of 60% humidity, take out and make cigarettes, smoke them for evaluation, compare with the blank sample (without flavoring), and evaluate the evaluation results. The compound aroma of wagashi and fruit, the smoke is delicate and soft, the moist feeling is enhanced, the smoke is more elegant, the miscellaneous gas is covered, the irritation is reduced, and the aftertaste is comfortable, which improves the smoking quality of cigarettes.
取椰子原汁浓缩物若干,用52°的大曲酒稀释成浓度为6.0g/L溶液,取上述溶液5mL,采用喷雾方式加香,使上述溶液均匀喷洒在1000g烟丝上,于22℃和相对湿度60%的条件下平衡48h,取出做成卷烟,进行评吸,与空白样对比(不加香),进行评价,其评价效果主要表现为:与烟草本香协调较好,具有烟草本香和浓郁的果甜香的复合香味,烟气细腻、柔和,湿润感增强,烟气较飘逸,无杂气,刺激性降低,余味舒适,提升了卷烟抽吸品质。Take some coconut juice concentrate, dilute it with 52° Daqu wine to a solution with a concentration of 6.0g/L, take 5mL of the above solution, and use the spray method to add flavor, so that the above solution is evenly sprayed on 1000g of shredded tobacco. Equilibrate for 48 hours under the condition of 60% humidity, take out and make cigarettes, smoke them for evaluation, compare with the blank sample (without flavoring), and evaluate the evaluation results. It has a compound fragrance with strong fruity sweetness, the smoke is delicate and soft, the moist feeling is enhanced, the smoke is more elegant, no miscellaneous gas, the irritation is reduced, and the aftertaste is comfortable, which improves the smoking quality of cigarettes.
取椰子原汁浓缩物若干,用52°的大曲酒稀释成浓度为4.0g/L溶液,取上述溶液5mL,采用喷雾方式加香,使上述溶液均匀喷洒在1000g薄片上,于22℃和相对湿度60%的条件下平衡48h,取出做成卷烟,进行评吸,与空白样对比(不加香),进行评价,其评价效果主要表现为:香气量增加明显,椰子果甜香表现突出,木质气和枯焦气被掩盖,烟气湿润感增强,烟气较飘逸,刺激性降低,余味舒适,提升了薄片抽吸品质。Take some coconut juice concentrate, dilute it with 52° Daqu liquor to a solution with a concentration of 4.0g/L, take 5mL of the above solution, and add fragrance by spraying, so that the above solution is evenly sprayed on 1000g of thin slices. Balanced for 48 hours under the condition of 60% humidity, took out and made into cigarettes, evaluated and smoked, compared with the blank sample (without flavoring), and evaluated, the evaluation effect was mainly as follows: the amount of aroma increased significantly, the sweetness of coconut fruit was outstanding, The woody gas and coke gas are covered up, the moistness of the smoke is enhanced, the smoke is more elegant, the irritation is reduced, the aftertaste is comfortable, and the smoking quality of the flakes is improved.
实施例2Example 2
取新鲜椰子原汁在在压强为85mmHg,温度为40℃的条件下进行减压蒸发,浓缩到浓缩物的固含量≥95%,即得椰子原汁浓缩物。Get the fresh coconut juice and evaporate it under reduced pressure under the condition that the pressure is 85mmHg and the temperature is 40° C., and concentrate until the solid content of the concentrate is ≥ 95%, so as to obtain the coconut juice concentrate.
取椰子原汁浓缩物若干,用52°的大曲酒稀释成浓度为1g/L溶液,取上述溶液5mL,采用喷雾方式加香,使上述溶液均匀喷洒在1000g薄片上,于22℃和相对湿度60%的条件下平衡48h,取出做成卷烟,进行评吸,与空白样对比(不加香),进行评价,其评价效果:细腻、柔和烟气,木质气和枯焦气等杂气减弱,烟气湿润感增强,刺激性略有降低,余味略有涩感,总的来说提升了薄片抽吸品质。Take some coconut juice concentrate, dilute it with 52° Daqu liquor to a solution with a concentration of 1g/L, take 5mL of the above solution, and use spraying method to add fragrance, so that the above solution is evenly sprayed on 1000g of flakes, and placed at 22°C and relative humidity Equilibrate for 48 hours under the condition of 60%, take it out to make cigarettes, and conduct evaluation and smoking, and compare with the blank sample (without flavoring) for evaluation, and the evaluation effect: delicate and soft smoke, woody gas and coke gas and other miscellaneous gases are weakened, The moistness of the smoke is enhanced, the irritation is slightly reduced, and the aftertaste is slightly astringent, which generally improves the smoking quality of the flakes.
实施例3Example 3
取新鲜椰子原汁在压强为65mmHg,温度为60℃的条件下进行减压蒸发,浓缩到浓缩物的固含量≥90%,即得椰子原汁浓缩物。Fresh coconut juice is taken and evaporated under reduced pressure at a pressure of 65mmHg and a temperature of 60°C until the solid content of the concentrate is greater than or equal to 90%, to obtain the coconut juice concentrate.
取椰子原汁浓缩物若干,用52°的大曲酒稀释成浓度为10g/L溶液,取上述溶液5mL,采用喷雾方式加香,使上述溶液均匀喷洒在1000g薄片上,于22℃和相对湿度60%的条件下平衡48h,取出做成卷烟,进行评吸,与空白样对比(不加香),进行评价,其评价效果:细腻、柔和烟气,木质气和枯焦气等杂气消失,椰子果甜香较浓,烟气湿润感增强,烟气较飘逸,刺激性降低,余味舒适,总的来说提升了薄片抽吸品质。Take some coconut juice concentrate, dilute it with 52° Daqu wine to a solution with a concentration of 10g/L, take 5mL of the above solution, and use spraying method to add fragrance, so that the above solution is evenly sprayed on 1000g flakes, at 22°C and relative humidity Equilibrate for 48 hours under the condition of 60%, take it out to make cigarettes, and conduct evaluation and smoking, compare with the blank sample (without flavoring), and evaluate the evaluation effect: delicate and soft smoke, woody gas and coke gas and other miscellaneous gases disappear, The sweetness of coconut fruit is stronger, the moistness of the smoke is enhanced, the smoke is more elegant, the irritation is reduced, and the aftertaste is comfortable. Generally speaking, the smoking quality of the flakes is improved.
对比实施例1Comparative Example 1
取新鲜椰子原汁在压强为60mmHg,温度为70℃的条件下进行减压蒸发,浓缩到浓缩物的固含量≥99%,即得椰子原汁浓缩物。Fresh coconut juice is taken and evaporated under reduced pressure at a pressure of 60mmHg and a temperature of 70°C until the solid content of the concentrate is greater than or equal to 99%, thereby obtaining the coconut juice concentrate.
取椰子原汁浓缩物若干,用52℃的大曲酒稀释成浓度为2.0g/L溶液,取上述溶液5mL,采用喷雾方式加香,使上述溶液均匀喷洒在1000g烟丝上,于22℃和相对湿度60%的条件下平衡48h,取出做成卷烟,进行评吸,与空白样(不加香)对比进行评价,其评价效果:香气量有所增加,甜感增强,但与烟草本香协调性不好。主要表现为焦甜,且有点过焦的味道,余味略苦,舒适感下降。Take some coconut juice concentrate, dilute it with Daqu liquor at 52°C to a solution with a concentration of 2.0g/L, take 5mL of the above solution, and add fragrance by spraying, so that the above solution is evenly sprayed on 1000g of shredded tobacco, at 22°C and relative Equilibrate for 48 hours under the condition of humidity 60%, take it out and make cigarettes, smoke them for evaluation, compare with the blank sample (without flavoring) for evaluation, the evaluation effect: the amount of aroma is increased, the sweetness is enhanced, but it is in harmony with the original aroma of tobacco Sex is not good. The main performance is burnt sweet, with a slightly burnt taste, slightly bitter aftertaste, and decreased comfort.
对比实施例2Comparative Example 2
取新鲜椰子原汁在压强为90mmHg,温度为30℃的条件下进行减压蒸发,浓缩到浓缩物的固含量≥99%,即得椰子原汁浓缩物。Fresh coconut juice is taken under reduced pressure evaporation at a pressure of 90 mmHg and a temperature of 30° C., concentrated until the solid content of the concentrate is ≥ 99%, and the coconut juice concentrate is obtained.
取椰子浓缩物若干,用52℃的大曲酒稀释成浓度为2.0g/L溶液,取上述溶液5mL,采用喷雾方式加香,使上述溶液均匀喷洒在1000g烟丝上,于22℃和相对湿度60%的条件下平衡48h,取出做成卷烟,进行评吸,与空白样进行(不加香)相对评价,其评价效果:香气量有所增加,烟气细腻、柔和,甜润感增强,但杂气增加,与烟草本香不协调。具体表现为:鼻腔杂气有所增加,余味发涩,椰子的香气(奶香)明显。Take some coconut concentrate, dilute it with Daqu wine at 52°C to a solution with a concentration of 2.0g/L, take 5mL of the above solution, and add fragrance by spraying, so that the above solution is evenly sprayed on 1000g of cut tobacco, at 22°C and a relative humidity of 60 % under the condition of 48h, take out and make cigarettes, smoke them, and make a relative evaluation with the blank sample (without flavoring). The gas is increased, which is not in harmony with the original aroma of tobacco. The specific manifestations are: nasal miscellaneous gas has increased, the aftertaste is astringent, and the aroma of coconut (milk fragrance) is obvious.
对比实施例3Comparative Example 3
以新鲜椰肉作为原料,将椰肉进行机械绞碎,加入其重量的2倍的70%的酒精,陈化6小时,然后过滤、乙醇洗滤渣,滤液在45℃下进行减压蒸发,除去99%的溶剂和其它物质即得。With fresh coconut meat as raw material, the coconut meat is mechanically minced, add 70% alcohol twice its weight, age for 6 hours, then filter and wash the filter residue with ethanol, and the filtrate is evaporated under reduced pressure at 45°C to remove 99% of solvents and other substances are available.
取椰子肉浓缩物若干,用52℃的大曲酒稀释成浓度为2.0g/L溶液,取上述溶液5mL,采用喷雾方式加香,使上述溶液均匀喷洒在1000g烟丝上,于22℃和相对湿度60%的条件下平衡48h,取出做成卷烟,进行评吸,与空白样(不加香)比进行评价,其评价效果具体表现为:香气量有所增加,烟气细腻、柔和,甜润感增强,但杂气增加,与烟草本香不协调,余味发涩,椰子的香气(奶香)明显。Take some coconut meat concentrate, dilute it with Daqu wine at 52°C to a solution with a concentration of 2.0g/L, take 5mL of the above solution, and add fragrance by spraying, so that the above solution is evenly sprayed on 1000g of shredded tobacco, at 22°C and relative humidity Equilibrate for 48 hours under the condition of 60%, take out and make cigarettes, smoke them for evaluation, and compare with the blank sample (without flavoring) for evaluation. The evaluation effect is as follows: the amount of aroma has increased, the smoke is delicate, soft, and sweet. Enhanced, but the mixed gas is increased, which is not in harmony with the original aroma of tobacco, the aftertaste is astringent, and the aroma of coconut (milk aroma) is obvious.
从对比实施例1和对比实施例2来看,只有在适当的蒸发压强和温度下才能保证椰子提取物中具有增香保润作用的活性组分的最大保留量,若蒸发浓缩真空度过高和温度过高,活性组分挥发过多,同时发生焦糖化反应,产生过焦的焦甜味道,舒适感下降;而若蒸发浓缩真空度过低和温度过低,过多的低沸点杂质保留下来,其杂气较明显,主要是椰奶香味残留较重,而奶香是一般卷烟制品所避及的。从对比实施例3可以看出,以不同的溶剂提取的化合物浓缩获得的浓缩物成分完全不同,具有的香味也完全不同。Judging from Comparative Example 1 and Comparative Example 2, only under appropriate evaporation pressure and temperature can the maximum retention of the active components with aroma-enhancing and moisturizing effects in the coconut extract be guaranteed. If the evaporation concentration vacuum is too high If the temperature and temperature are too high, the active components will volatilize too much, and the caramelization reaction will occur at the same time, resulting in a burnt sweet taste, and the comfort will decrease; and if the evaporation and concentration vacuum is too low and the temperature is too low, too many low-boiling impurities will remain. When it comes down, its miscellaneous smell is more obvious, mainly because the coconut milk fragrance is relatively strong, and the milk fragrance is avoided by ordinary cigarette products. It can be seen from Comparative Example 3 that the concentrates obtained by concentrating the compounds extracted with different solvents have completely different components and completely different fragrances.
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