CN104122122A - Pressure stabilizing sampling device - Google Patents
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- 238000005070 sampling Methods 0.000 title claims abstract description 42
- 230000000087 stabilizing effect Effects 0.000 title abstract description 13
- 238000012544 monitoring process Methods 0.000 claims abstract description 34
- 230000001105 regulatory effect Effects 0.000 abstract description 14
- 238000002347 injection Methods 0.000 abstract description 10
- 239000007924 injection Substances 0.000 abstract description 10
- 230000006641 stabilisation Effects 0.000 abstract description 10
- 238000011105 stabilization Methods 0.000 abstract description 10
- 238000009423 ventilation Methods 0.000 abstract description 4
- 239000007789 gas Substances 0.000 description 32
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- 210000003437 trachea Anatomy 0.000 description 1
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Abstract
本发明的压力稳定采样装置,包括采样管、压力稳定腔、控制系统及气体监测仪器,采样管连通于压力稳定腔的进气口,压力稳定腔的一路连接多分支管,每支管连通于气体监测仪器,采样管的进气端依次设有第一流量计和限流器,压力稳定腔通过通气管道与真空泵连接,通气管道上安装第二流量计和比例调节阀,本发明的压力稳定采样装置可以使进样压力保持为一个定值,保证进样重复性,通过压力稳定腔和调控装置可以调整仪器内部压力,使仪器内部压强保持为一个定值,航测飞行高度环境须其在低于这个值的情况下,不需要对其进行标定,从而实现飞行器因高度改变带来压力变化造成的不确定性,提高航测时的气体监测仪器的数据精确度。
The pressure stable sampling device of the present invention comprises a sampling tube, a pressure stabilizing chamber, a control system and a gas monitoring instrument, the sampling tube is connected to the air inlet of the pressure stabilizing chamber, one path of the pressure stabilizing chamber is connected to multi-branch pipes, and each branch pipe is connected to the gas monitoring Instrument, the inlet end of the sampling tube is provided with a first flowmeter and a flow restrictor in turn, the pressure stabilization chamber is connected with a vacuum pump through a ventilation pipeline, and a second flowmeter and a proportional regulating valve are installed on the ventilation pipeline. The pressure stabilization sampling device of the present invention The injection pressure can be maintained at a constant value to ensure the repeatability of the injection. The internal pressure of the instrument can be adjusted through the pressure stabilization chamber and the control device to maintain the internal pressure of the instrument at a constant value. The aerial survey flight altitude environment must be lower than this In the case of the value, there is no need to calibrate it, so as to realize the uncertainty caused by the pressure change caused by the altitude change of the aircraft, and improve the data accuracy of the gas monitoring instrument during the aerial survey.
Description
技术领域technical field
本发明涉及了一种稳压采样装置,特别是一种用于航测时的稳压采样装置。The invention relates to a voltage-stabilizing sampling device, in particular to a voltage-stabilizing sampling device used in aerial surveys.
背景技术Background technique
在航测中,通常运用分析仪器对气体样品的浓度进行气体监测,为了能够准确分析和测量气体的浓度,必须保证进样过程具有很好的重复性(即多次采样气体监测结果重复程度),而进样时的稳定压力是确保进样重复性的重要条件,但是在航测中,由于飞行高度的变化,外界压力的实时改变给控制进样压力带来了困难。In aerial surveys, analytical instruments are usually used to monitor the concentration of gas samples. In order to accurately analyze and measure the concentration of gases, it is necessary to ensure that the sampling process has good repeatability (that is, the repeatability of multiple sampling gas monitoring results). The stable pressure during sample injection is an important condition to ensure the repeatability of sample injection, but in the aerial survey, due to the change of flight altitude, the real-time change of external pressure brings difficulties to control the sample injection pressure.
现有的用于地面的大气环境气体监测仪器,可以放置在一个特定环境中(在地面上时一般设定为0.6个大气压),从而保证仪器内部压力始终不变,解决了标定的稳定问题。但是在航测时,随着运输机高度变化时,应用现有的大气环境气体监测仪器还会存在以下问题:The existing atmospheric environment gas monitoring instruments used on the ground can be placed in a specific environment (generally set to 0.6 atmospheric pressure on the ground), so as to ensure that the internal pressure of the instrument remains constant and solve the problem of calibration stability. However, during the aerial survey, as the height of the transport aircraft changes, the following problems still exist in the application of existing atmospheric environment gas monitoring instruments:
1、航测时采样管进风口处的压力随运输机高度变化而变化,外界压力的实时改变给控制进样压力带来了困难,从而导致进样重复性差,这样会对采样测量结果带来误差,从而影响气体监测精度;1. During the aerial survey, the pressure at the air inlet of the sampling pipe changes with the height of the transport aircraft. The real-time change of the external pressure brings difficulties in controlling the injection pressure, which leads to poor repeatability of the injection, which will bring errors to the sampling measurement results. Thus affecting the gas monitoring accuracy;
2、大气环境气体监测仪器需要在一个稳定的气压环境下进行气体监测,而当仪器压力变化不定时,内标定量无法确定,影响气体监测精度。2. Atmospheric environment gas monitoring instruments need to perform gas monitoring in a stable air pressure environment, and when the pressure of the instrument varies, the internal standard quantity cannot be determined, which affects the accuracy of gas monitoring.
发明内容Contents of the invention
本申请的发明目的在于解决目前大气环境气体监测仪器在用于航测时进样压力不稳定,仪器压力变化较大,无法标定的技术问题,而提供一种压力稳定采样装置。The purpose of the invention of this application is to solve the technical problems that the sampling pressure of the current atmospheric environment gas monitoring instrument is unstable when used in aerial surveys, the instrument pressure changes greatly and cannot be calibrated, and to provide a pressure stable sampling device.
为了完成本申请的发明目的,本申请采用以下技术方案:In order to complete the invention purpose of the application, the application adopts the following technical solutions:
本发明的压力稳定采样装置,包括采样管、压力稳定腔和气体监测仪器,所述采样管连通于所述压力稳定腔的进气口,所述压力稳定腔的出气管连通于所述气体监测仪器,所述采样管的进气端依次设有第一流量计和限流器,所述压力稳定腔还具有连接调控装置的端口,所述调控装置包括第二流量计、比例调节阀、真空泵和PC机,所述压力稳定腔通过通气管道与所述真空泵连接,所述通气管道上安装所述第二流量计和所述比例调节阀,所述PC机分别与所述第一流量计、第二流量计、比例调节阀、限流器和真空泵连接。The pressure stable sampling device of the present invention comprises a sampling tube, a pressure stabilizing chamber and a gas monitoring instrument, the sampling tube is connected to the air inlet of the pressure stabilizing chamber, and the gas outlet pipe of the pressure stabilizing chamber is connected to the gas monitoring instrument, the inlet end of the sampling pipe is provided with a first flowmeter and a flow restrictor in turn, and the pressure stabilization chamber also has a port connected to a control device, and the control device includes a second flowmeter, a proportional control valve, a vacuum pump and a PC, the pressure stabilizing chamber is connected to the vacuum pump through a ventilation pipeline, the second flowmeter and the proportional regulating valve are installed on the ventilation pipeline, and the PC is connected to the first flowmeter, the The second flow meter, proportional regulating valve, flow restrictor and vacuum pump are connected.
本发明所述限流器为比例调节阀,所述比例调节阀与所述PC机相连。The current restrictor of the present invention is a proportional regulating valve, and the proportional regulating valve is connected with the PC.
本发明所述气体监测仪器的出气管连通于所述真空泵,所述气体监测仪器和真空泵之间设有第三流量计和调节阀,所述第三流量计和调节阀分别与所述PC机相连。The gas outlet pipe of the gas monitoring instrument of the present invention is communicated with the vacuum pump, and a third flowmeter and a regulating valve are arranged between the gas monitoring instrument and the vacuum pump, and the third flowmeter and the regulating valve are connected with the PC respectively. connected.
本发明所述第一流量计和限流器之间还安装有温度计、湿度计,所述压力稳定腔上也连接有流量计、湿度计和温度计。In the present invention, a thermometer and a hygrometer are also installed between the first flowmeter and the flow restrictor, and a flowmeter, a hygrometer and a thermometer are also connected to the pressure stabilization chamber.
本发明所述第二流量计和比例调节阀可用质量流量控制器替换。The second flow meter and the proportional regulating valve of the present invention can be replaced by a mass flow controller.
本发明所述PC机还连接有报警器。The PC of the present invention is also connected with an alarm.
本发明所述限流器也可以是限流孔或质量流量控制器,所述质量流量控制器与所述PC机相连。The flow restrictor of the present invention may also be a flow restricting hole or a mass flow controller, and the mass flow controller is connected to the PC.
本发明的压力稳定采样装置,通过限流器可以使进样压力保持为一个定值,保证进样重复性,通过压力稳定腔和控制系统可以调整仪器内部压力,使仪器内部压强保持为一个定值,从而实现稳定的标定值,这样航测时气体监测的精度可以大大提高。The pressure stable sampling device of the present invention can keep the sampling pressure at a constant value through the flow limiter to ensure the repeatability of sampling, and can adjust the internal pressure of the instrument through the pressure stabilizing chamber and the control system to maintain the internal pressure of the instrument at a constant value. Value, so as to achieve a stable calibration value, so that the accuracy of gas monitoring during aerial survey can be greatly improved.
此外,气体监测仪器的出气管连通于真空泵,可以通过真空泵来控制气体监测仪器排出的流量,控制气体监测仪器内部气压,同时压力稳定采样装置多处设有流量计、湿度计和温度计,可以起到实时监测内部气压的作用,然后将测得的结果发送给PC机,通过PC机实时控制内部气压。In addition, the outlet pipe of the gas monitoring instrument is connected to the vacuum pump, which can control the discharge flow of the gas monitoring instrument and the internal air pressure of the gas monitoring instrument through the vacuum pump. To monitor the function of the internal air pressure in real time, and then send the measured results to the PC, and control the internal air pressure in real time through the PC.
附图说明Description of drawings
图1为本发明的压力稳定采样装置的整体示意图。FIG. 1 is an overall schematic diagram of a pressure-stabilized sampling device of the present invention.
具体实施方式Detailed ways
如图1所示,本实施例的压力稳定采样装置,包括采样管1、压力稳定腔2和气体监测仪器3,采样管1连通于压力稳定腔2的进气口,压力稳定腔2的出气管通过多分支管连通于气体监测仪器3,每一分支管连通某一种气体监测仪器3,采样管1的进气端依次设有第一流量计4和限流器5,压力稳定腔2还具有连接调控装置6的端口,调控装置6包括第二流量计7、比例调节阀8、真空泵9和PC机10,压力稳定腔2通过通气管道与所述真空泵9连接,通气管道上安装第二流量计7和比例调节阀8,PC机10分别与第一流量计4、第二流量计7、比例调节阀8和真空泵9连接,气体监测仪器3的出气管连通于真空泵9,气体监测仪器3和真空泵9之间设有第三流量计11和调节阀12,所述第三流量计11和调节阀12分别与所述PC机10相连。As shown in Figure 1, the pressure stable sampling device of this embodiment includes a sampling tube 1, a pressure stabilizing chamber 2 and a gas monitoring instrument 3, the sampling tube 1 is connected to the inlet of the pressure stabilizing chamber 2, and the outlet of the pressure stabilizing chamber 2 The trachea is connected to the gas monitoring instrument 3 through a multi-branch pipe, and each branch pipe is connected to a certain gas monitoring instrument 3. The inlet end of the sampling pipe 1 is provided with a first flowmeter 4 and a flow restrictor 5 in turn, and the pressure stabilization chamber 2 is also There is a port connected to the control device 6, the control device 6 includes a second flow meter 7, a proportional control valve 8, a vacuum pump 9 and a PC 10, the pressure stabilization chamber 2 is connected to the vacuum pump 9 through a vent pipe, and the second flow meter is installed on the vent pipe. The flow meter 7 and the proportional regulating valve 8, the PC 10 are respectively connected with the first flow meter 4, the second flow meter 7, the proportional regulating valve 8 and the vacuum pump 9, the gas outlet pipe of the gas monitoring instrument 3 is connected to the vacuum pump 9, and the gas monitoring instrument 3 and the vacuum pump 9 are provided with a third flowmeter 11 and a regulating valve 12, and the third flowmeter 11 and regulating valve 12 are connected to the PC 10 respectively.
本实施例中的限流器5可以是限流孔或质量流量控制器,限流器5与PC机10相连,第一流量计4和限流器5之间还安装有温度计、湿度计,压力稳定腔2上也连接有流量计、湿度计和温度计。The flow limiter 5 in this embodiment can be a flow limiting hole or a mass flow controller, the flow limiter 5 is connected with the PC 10, a thermometer and a hygrometer are also installed between the first flowmeter 4 and the flow limiter 5, A flow meter, a hygrometer and a thermometer are also connected to the pressure stabilization chamber 2 .
本发明所述PC机10还连接有报警器,当第二流量计7测得的压强明显大于第一流量计4的数值时,PC机10会启动报警器,警醒工作人员检修气体监测采样装置。The PC 10 of the present invention is also connected with an alarm. When the pressure measured by the second flowmeter 7 is obviously greater than the value of the first flowmeter 4, the PC 10 will start the alarm to alert the staff to overhaul the gas monitoring and sampling device. .
本实施例的第二流量计7和比例调节阀8可用质量流量控制器替换。The second flow meter 7 and the proportional regulating valve 8 of this embodiment can be replaced by a mass flow controller.
上述压力稳定采样装置的使用方法为:进行航测时,将采样管的进风口正对气流,随着运输机的运行,进样口风速增大,气流流量增大,限流器5处的压力不断提高,但当风速提高到一定程度时,限流器5处的压力会停止上升而处于一个定值,这样进样压力保持不变,在气流通过限流器5后会进入压力稳定腔,可以通过压力稳定腔2减小进样压力变化时对气体监测仪器气体监测精度的影响,保证了进样重复性,提高气体监测精度。此外,可以通过调控装置调整采样装置内部压强,具体方法如下:The method of using the above-mentioned pressure-stabilized sampling device is as follows: during the aerial survey, the air inlet of the sampling pipe is directly facing the air flow. With the operation of the transport plane, the wind speed of the inlet increases, the flow of the air flow increases, and the pressure at the restrictor 5 continues to increase. increase, but when the wind speed increases to a certain level, the pressure at the flow restrictor 5 will stop rising and be at a constant value, so that the sample injection pressure remains unchanged, and the air flow will enter the pressure stabilization chamber after passing through the flow restrictor 5, which can be The pressure stabilizing chamber 2 reduces the impact on the gas monitoring accuracy of the gas monitoring instrument when the sample injection pressure changes, ensures the sample injection repeatability, and improves the gas monitoring accuracy. In addition, the internal pressure of the sampling device can be adjusted through the regulating device, the specific method is as follows:
在运输机运行前,将大气环境气体监测仪器内部气压设定为标定值,一般设定为0.6个大气压,当运输机运行时,随着运输机升高,采样管1进样口风速增大,气流流量增大,限流器处的压力不断提高,但当风速提高到一定程度时,根据文丘里定理可知,限流器5处的压力会停止上升而处于一个定值,同时,采样管进样口处的第一流量计4、温度计和湿度计,第二流量计7、第三流量计11,压力稳定腔2上的流量计、湿度计和温度计将测得的数值时时传输给PC机10,PC机10根据测得的数值控制真空泵9泄压、控制限流器5控制进样口压强,使采样装置内部的压强、采样管1进样口处的压强与标定值相等,从而保证气体监测精确度。Before the operation of the transport plane, set the internal air pressure of the atmospheric environment gas monitoring instrument to the calibration value, generally set to 0.6 atmospheric pressure. As the pressure increases, the pressure at the restrictor continues to increase, but when the wind speed increases to a certain level, according to the Venturi theorem, the pressure at the restrictor 5 will stop rising and remain at a constant value. At the same time, the inlet of the sampling tube The first flowmeter 4, thermometer and hygrometer at the place, the second flowmeter 7, the third flowmeter 11, the flowmeter, hygrometer and thermometer on the pressure stabilization chamber 2 transmit the measured values to the PC 10 from time to time, The PC 10 controls the pressure release of the vacuum pump 9 and the flow limiter 5 to control the pressure of the inlet according to the measured values, so that the pressure inside the sampling device and the pressure at the inlet of the sampling tube 1 are equal to the calibration value, thereby ensuring gas monitoring Accuracy.
以上所述的实施例仅仅是对本发明的优选实施方式进行描述,并非对本发明的范围进行限定,在不脱离本发明设计精神的前提下,本领域普通技术人员对本发明的技术方案作出的各种变形和改进,均应落入本发明权利要求书确定的保护范围内。The above-mentioned embodiments are only descriptions of preferred implementations of the present invention, and are not intended to limit the scope of the present invention. Variations and improvements should fall within the scope of protection defined by the claims of the present invention.
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CN105651854A (en) * | 2016-03-15 | 2016-06-08 | 中国原子能科学研究院 | A system and method for quantitative determination of trace 3 He in tritiated aging samples |
CN105651854B (en) * | 2016-03-15 | 2019-05-24 | 中国原子能科学研究院 | One kind is micro in aged samples containing tritium3The system and method for He quantitative determination |
CN106556676A (en) * | 2016-10-27 | 2017-04-05 | 中法渤海地质服务有限公司 | A kind of detection means and detection method for multi-channel gas |
CN106681383A (en) * | 2017-01-23 | 2017-05-17 | 中国科学院理化技术研究所 | High-precision pressure control device |
CN106681383B (en) * | 2017-01-23 | 2023-07-28 | 中国科学院理化技术研究所 | A high-precision pressure control device |
CN109425514A (en) * | 2017-08-25 | 2019-03-05 | 赛默飞世尔(上海)仪器有限公司 | Fluid sampling device |
CN112114104A (en) * | 2020-08-28 | 2020-12-22 | 山东省地勘局第二水文地质工程地质大队(山东省鲁北地质工程勘察院) | A small flow restrictor for groundwater sample collection |
CN114674622A (en) * | 2022-03-17 | 2022-06-28 | 中国环境科学研究院 | A method for controlling the flow rate of gas in a sampling channel and related products |
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