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CN103989622A - Tea saponin shampoo and production method thereof - Google Patents

Tea saponin shampoo and production method thereof Download PDF

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CN103989622A
CN103989622A CN201410264849.XA CN201410264849A CN103989622A CN 103989622 A CN103989622 A CN 103989622A CN 201410264849 A CN201410264849 A CN 201410264849A CN 103989622 A CN103989622 A CN 103989622A
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tea saponin
essential oil
shampoo
essence
distilled water
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CN103989622B (en
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刘明新
兰时乐
刘思远
周芳如
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Hunan Agricultural University
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Hunan Agricultural University
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Abstract

The invention provides tea saponin shampoo and a production method thereof. The shampoo is mainly prepared from the effective components refined tea saponin, aloe essence, seaweed extract, green tea essence and glycerinum. The production method comprises the following steps: adding the refined tea saponin into distilled water which is heated to 45-50 DEG C, and stirring to completely dissolve the tea saponin; sequentially adding the aloe extract, green tea essence, seaweed extract and glycerinum, and uniformly stirring while adding to completely dissolve the components; adding plant essential oil and bacteriostatic agent, and uniformly stirring; adding uniformly mixed thickening agent and NaCl, uniformly stirring, and standing. The shampoo is all-natural, has the functions of washing and nourishing hair and improving the hair quality, enables smooth, black, bright and elegant hair after the hair is washed, and has the characteristics of safety, no residues, low cost, simple production process and the like.

Description

茶皂素洗发液及其生产方法Tea saponin shampoo and production method thereof

技术领域 technical field

本发明属于日用化工的洗涤剂,具体涉及一种茶皂素洗发液及其生产方法。 The invention belongs to daily-use chemical detergents, in particular to a tea saponin shampoo and a production method thereof.

背景技术 Background technique

洗发液又称洗发水、洗发精或洗发香波,是应用最为广泛的头发和头皮基础护理化妆用品,是人们日常生活中必不可少的生活用品之一。一般采用硫酸脂肪醇的三乙醇胺与氢氧化胺的混合盐、十二酸异丙醇酰胺、甲醛、聚氧乙烯、羊毛脂、香料、色料和水作为原料。目前主要种类,按透明度可分为透明型、珠光型和乳浊型;按功能可分为调理香波、中性香波、油性香波、干性香波,去头皮屑香波、染发香波等。市场上的洗发液大多加入了一定的添加剂以及化学合成洗净剂,使用不当会使头皮过分脱脂,引发发根瘙痒、发炎,使发质受损。 Shampoo, also known as shampoo, shampoo or shampoo, is the most widely used hair and scalp basic care cosmetics, and is one of the requisite daily necessities in people's daily life. Generally, the mixed salt of triethanolamine of fatty alcohol sulfate and ammonium hydroxide, isopropanolamide of lauric acid, formaldehyde, polyoxyethylene, lanolin, spices, colorants and water are used as raw materials. At present, the main types can be divided into transparent type, pearl type and opacity type according to transparency; according to function, they can be divided into conditioning shampoo, neutral shampoo, oily shampoo, dry shampoo, anti-dandruff shampoo, hair coloring shampoo, etc. Most of the shampoos on the market have added certain additives and chemical synthetic detergents. Improper use will cause excessive degreasing of the scalp, cause itching and inflammation of the hair roots, and damage the hair quality.

茶皂素是由茶树种子中提取出来的一类醣甙化合物,是一种性能良好的天然表面活性剂,具有良好的乳化、分散、发泡、湿润等功能,并且具有消炎、镇痛,抗渗透等药理作用。我国从古至今就有利用茶籽饼洗头的习惯。茶粕中含有茶皂素、蛋白质、天然茶油等,长期使用有止屑、止痒、去油、杀菌、修复受损发质的功效,还有明显的乌发生发作用。实践证明,茶皂素洗头发不仅具有发松、光滑、去头屑、止痒等优点,有洁发护发之功效,而且对皮肤无刺激、过敏作用,使用安全。随着人们生活水平的提高和对环保、绿色生活方式的追求,一些天然植物原料被逐渐引入到洗发用品中。经检索,中国专利CN101129310A、CN102836097A、CN101390816A等均公开了含茶皂素洗发液或茶皂素洗发露配方及生产工艺等,以及文献[茶皂素及其在化妆品中的应用,北京工商大学学报,2009,27(3)]公开了高档洗发香波和天然草本洗发露配方。虽然这些技术产品中都含有茶皂素,同时也含有常规洗发液(露)所含有的各种合成化学物质,尽管具有一定的护发、美发作用,但也存在污染环境、生产工艺复杂等问题。 Tea saponin is a kind of glycoside compound extracted from tea tree seeds. It is a kind of natural surfactant with good performance. Penetration and other pharmacological effects. Our country has the habit of using tea seed cake to wash hair since ancient times. Tea meal contains tea saponin, protein, natural tea oil, etc. Long-term use has the effects of anti-dandruff, anti-itch, oil removal, sterilization, and repair of damaged hair, as well as obvious black hair growth effect. Practice has proved that tea saponin shampoo not only has the advantages of loosening, smoothing, anti-dandruff, anti-itching, etc., but also has the effect of cleansing and hair care, and has no irritation and allergies to the skin, so it is safe to use. With the improvement of people's living standards and the pursuit of environmental protection and green lifestyles, some natural plant materials are gradually introduced into shampoo products. After searching, Chinese patents CN101129310A, CN102836097A, CN101390816A, etc. all disclose the formula and production process of tea saponin shampoo or tea saponin shampoo, etc., as well as the literature [tea saponin and its application in cosmetics, Beijing Industrial and Commercial University Journal, 2009, 27 (3)] disclosed high-grade shampoo and natural herbal shampoo formulations. Although these technical products all contain tea saponin and various synthetic chemical substances contained in conventional shampoos (dews), although they have certain hair care and hair beautification effects, they also have environmental pollution and complicated production processes. question.

发明内容 Contents of the invention

本发明所要解决的技术问题是:针对现有技术产品的不足以及人们对绿色生态环保产品的需要,提供一种茶皂素洗发液及其生产方法,本发明产品采用的原料对人体无任何毒副作用,具有生产工艺简单且易于控制、成本和能耗低、易于批量生产的特点。 The technical problem to be solved by the present invention is to provide a tea saponin shampoo and a production method thereof for the deficiencies of prior art products and people's needs for green ecological products. Toxic and side effects, it has the characteristics of simple and easy-to-control production process, low cost and energy consumption, and easy mass production.

为了解决上述技术问题,本发明所采用的技术方案是:一种茶皂素洗发液,该洗发液由下述重量百分比的组分组成:精制茶皂素8-10%、芦荟精华液3-5%、海藻提取物5-8%、绿茶精华液3-5%、甘油5-8%、NaCl4-6%、抑菌剂0.1-0.2%、植物香精油0.01-0.1%、增稠剂1.5-2.2%及蒸馏水60-70%。 In order to solve the above-mentioned technical problems, the technical solution adopted in the present invention is: a tea saponin shampoo, which is composed of the following components in percentage by weight: refined tea saponin 8-10%, aloe essence 3-5%, seaweed extract 5-8%, green tea essence 3-5%, glycerin 5-8%, NaCl4-6%, antibacterial agent 0.1-0.2%, plant essential oil 0.01-0.1%, thickening Agent 1.5-2.2% and distilled water 60-70%.

本发明还提供上述茶皂素洗发液的生产方法,该方法步骤如下: The present invention also provides the production method of above-mentioned tea saponin shampoo, and the method steps are as follows:

(1)按上述重量配比取蒸馏水加入搅拌罐中,开动搅拌,将蒸馏水加热至45-50℃; (1) Take distilled water according to the above weight ratio and add it to the mixing tank, start stirring, and heat the distilled water to 45-50°C;

(2)将精制茶皂素慢慢加入加热后的蒸馏水中,80-100r/min搅拌10-20min,使精制茶皂素完全溶解,得到澄清溶液; (2) Slowly add the refined tea saponin into the heated distilled water, stir at 80-100r/min for 10-20min, completely dissolve the refined tea saponin, and obtain a clear solution;

(3)依次加入所需的芦荟精华液、绿茶精华液、海藻提取物、甘油,80-100r/min条件下边加边搅拌,使之完全溶解; (3) Add the required aloe essence, green tea essence, seaweed extract, and glycerin in sequence, and stir while adding at 80-100r/min to make them completely dissolve;

(4)加入所需香精和抑菌剂,搅拌均匀; (4) Add the required essence and antibacterial agent, and stir evenly;

(5)将所需的增稠剂和NaCl充分混合均匀后,缓慢加入步骤(4)中,80-100r/min搅拌20-30min,使增稠剂完全溶解,静置10-12h,即可。 (5) After fully mixing the required thickener and NaCl, slowly add it to step (4), stir at 80-100r/min for 20-30min to completely dissolve the thickener, and let it stand for 10-12h. .

上述抑菌剂为双乙酸钠或脱氢乙酸钠中的一种或两种。 Above-mentioned antibacterial agent is one or both in sodium diacetate or sodium dehydroacetate.

上述植物香精油为迷迪香精油、百里香酚精油、薰衣草精油或葡萄柚精油中的一种或几种。 The above-mentioned plant essential oils are one or more of middling essential oil, thymol essential oil, lavender essential oil or grapefruit essential oil.

上述增稠剂为黄原胶或阿拉伯树胶中的一种或两种。 Above-mentioned thickening agent is one or both in xanthan gum or gum arabic.

本发明中用到的精制茶皂素(也可采用茶皂素按现有技术精制而成)、芦荟精华液、海藻提取物、绿茶精华液等,均为公众可以得到的常规产品,市场有售。其中,芦荟精华液中含有多种天然营养成分,可增强头发光泽、抑制头屑的形成、减少脱发、防治头皮瘙痒、消灭头虱等,起到护发美容的作用;精制茶皂素是一种天然非离子型表面活性剂,具有良好的乳化、分散、发泡、湿润等功能,并且具有消炎、镇痛,抗渗透等药理作用;绿茶精华液具有抗菌、抑制黑色素细胞的活动、促进血液循环、滋润皮肤等作用;海藻提取物可以刺激纤维细胞生成胶原蛋白和弹性蛋白,促进皮肤的新陈代谢,抗皱和抗衰老,增进表面皮肤造血功能,对体外皮肤具有抑菌作用。如此,本发明的洗发液为全天然洗发液,具有洗发、养发和改善发质的功能,洗后头发光润亮泽、乌黑发亮、柔顺飘逸,具有安全无残留的特点。 The refined tea saponin used in the present invention (also can adopt tea saponin to refine by prior art), aloe essence, seaweed extract, green tea essence etc., all are conventional products that the public can obtain, and the market has sale. Among them, aloe essence contains a variety of natural nutrients, which can enhance hair luster, inhibit the formation of dandruff, reduce hair loss, prevent and treat scalp itching, eliminate head lice, etc., and play the role of hair care and beauty; refined tea saponin is a A natural non-ionic surfactant with good emulsifying, dispersing, foaming, moisturizing and other functions, and has anti-inflammatory, analgesic, anti-osmotic and other pharmacological effects; green tea essence has antibacterial, inhibits the activity of melanocytes, promotes blood circulation Circulation, moisturizing the skin, etc. Seaweed extract can stimulate fibroblasts to produce collagen and elastin, promote skin metabolism, anti-wrinkle and anti-aging, improve the hematopoietic function of the surface skin, and have antibacterial effects on the skin in vitro. In this way, the shampoo of the present invention is an all-natural shampoo, which has the functions of shampooing, nourishing and improving hair quality. After washing, the hair is smooth and shiny, black and shiny, soft and elegant, and has the characteristics of safety and no residue.

与现有技术相比,本发明具有以下优点: Compared with the prior art, the present invention has the following advantages:

1、本发明使用的茶皂素为精制茶皂素,避免了直接使用茶籽粉或低纯度茶皂素中所含有的蛋白质、有机酸等杂质对杀菌去屑的影响。 1. The tea saponin used in the present invention is refined tea saponin, which avoids the influence of impurities such as proteins and organic acids contained in tea seed powder or low-purity tea saponin on sterilization and dandruff removal.

2、本发明所使用的原材料对人体无任何毒副作用,且具有护发、洗发、杀菌、止痒等多重功效,避免了化学洗发剂对头发的损伤和对皮肤的刺激以及对环境的污染。 2. The raw materials used in the present invention have no toxic and side effects on the human body, and have multiple effects such as hair care, shampoo, sterilization, and antipruritic, avoiding the damage of chemical shampoos to the hair, the stimulation to the skin, and the impact on the environment. pollute.

3、本发明生产工艺简单,能耗低,成本低廉,投资小,无三废和易于规模化生产等特点。 3. The invention has the characteristics of simple production process, low energy consumption, low cost, small investment, no three wastes and easy large-scale production.

具体实施方式 Detailed ways

以下结合实施例对本发明作进一步说明。 The present invention will be further described below in conjunction with embodiment.

实施例1 Example 1

取60kg蒸馏水加入搅拌罐中,开动搅拌,通过夹层将蒸馏水加热至45℃,将10kg精制茶皂素慢慢加入加热后的蒸馏水中,100r/min搅拌10min,使精制茶皂素完全溶解,得到澄清溶液;依次加入3kg芦荟精华液、5kg绿茶精华液、8kg海藻提取物及8kg甘油,100r/min下边加边搅拌,使之完全溶解;再加入0.07kg迷迪香精油、0.03kg薰衣草精油和0.1kg脱氢乙酸钠,搅拌均匀;最后缓慢加入充分混合均匀的1.8kg黄原胶和4kgNaCl,以80r/min搅拌30min,使黄原胶完全溶解,静置10h,即可。 Take 60kg of distilled water and put it into the mixing tank, start stirring, heat the distilled water to 45°C through the interlayer, slowly add 10kg of refined tea saponin into the heated distilled water, stir at 100r/min for 10min, completely dissolve the refined tea saponin, and obtain Clarify the solution; add 3kg aloe essence, 5kg green tea essence, 8kg seaweed extract and 8kg glycerin successively, add while stirring at 100r/min, make it dissolve completely; add 0.07kg Midixiang essential oil, 0.03kg lavender essential oil and 0.1kg sodium dehydroacetate, stir evenly; finally slowly add 1.8kg xanthan gum and 4kgNaCl, which are fully mixed evenly, stir at 80r/min for 30min to completely dissolve the xanthan gum, and let it stand for 10h.

实施例2 Example 2

取70kg蒸馏水加入搅拌罐中,开动搅拌,通过夹层将蒸馏水加热至50℃,将8kg精制茶皂素慢慢加入加热后的蒸馏水中,80r/min搅拌20min,使精制茶皂素完全溶解,得到澄清溶液;依次加入3kg芦荟精华液、3kg绿茶精华液、5kg海藻提取物及5kg甘油,80r/min下边加边搅拌,使之完全溶解;再加入0.01kg百里香酚精油、0.02kg薰衣草精油、0.02kg葡萄柚精油、0.05kg脱氢乙酸钠和0.05kg双乙酸钠,搅拌均匀;最后缓慢加入充分混合均匀的0.8kg黄原胶、0.7kg阿拉伯树胶和4.35kgNaCl,以100r/min搅拌20min,使黄原胶和阿拉伯树胶完全溶解,静置12h,即可。 Take 70kg of distilled water and put it into the mixing tank, start stirring, heat the distilled water to 50°C through the interlayer, slowly add 8kg of refined tea saponin into the heated distilled water, stir at 80r/min for 20min, completely dissolve the refined tea saponin, and obtain Clarify the solution; add 3kg aloe essence, 3kg green tea essence, 5kg seaweed extract and 5kg glycerin successively, add while stirring at 80r/min, make it dissolve completely; add 0.01kg thymol essential oil, 0.02kg lavender essential oil, 0.02 kg of grapefruit essential oil, 0.05kg of sodium dehydroacetate and 0.05kg of sodium diacetate, and stir evenly; finally, slowly add 0.8kg of xanthan gum, 0.7kg of gum arabic, and 4.35kg of NaCl, and stir at 100r/min for 20min to make The xanthan gum and gum arabic are completely dissolved and left to stand for 12 hours.

实施例3 Example 3

取63.29kg蒸馏水加入搅拌罐中,开动搅拌,通过夹层将蒸馏水加热至48℃,将8.5kg精制茶皂素慢慢加入加热后的蒸馏水中,90r/min搅拌15min,使精制茶皂素完全溶解,得到澄清溶液;依次加入5kg芦荟精华液、3.5kg绿茶精华液、5.5kg海藻提取物及5.8kg甘油,90r/min下边加边搅拌,使之完全溶解;再加入0.006kg迷迪香精油、0.004kg葡萄柚精油和0.2kg双乙酸钠,搅拌均匀;最后缓慢加入充分混合均匀的2.2kg阿拉伯树胶和6kgNaCl,以90r/min搅拌25min,使阿拉伯树胶完全溶解,静置11h,即可。 Take 63.29kg of distilled water into the mixing tank, start stirring, heat the distilled water to 48°C through the interlayer, slowly add 8.5kg of refined tea saponin into the heated distilled water, stir at 90r/min for 15min, and completely dissolve the refined tea saponin , to obtain a clarified solution; add 5kg aloe essence, 3.5kg green tea essence, 5.5kg seaweed extract and 5.8kg glycerin successively, stir while adding at 90r/min, make it dissolve completely; add 0.006kg Midixiang essential oil, Stir 0.004kg grapefruit essential oil and 0.2kg sodium diacetate; finally add 2.2kg gum arabic and 6kgNaCl which are well mixed and mix well, stir at 90r/min for 25min to completely dissolve the gum arabic, and let stand for 11h.

Claims (8)

1.一种茶皂素洗发液,其特征在于,该洗发液由下述重量百分比的组分组成:精制茶皂素8-10%、芦荟精华液3-5%、海藻提取物5-8%、绿茶精华液3-5%、甘油5-8%、NaCl4-6%、抑菌剂0.1-0.2%、植物香精油0.01-0.1%、增稠剂1.5-2.2%及蒸馏水60-70%。 1. a tea saponin shampoo, is characterized in that, this shampoo is made up of the component of following percentage by weight: refined tea saponin 8-10%, aloe essence 3-5%, seaweed extract 5% -8%, green tea essence 3-5%, glycerin 5-8%, NaCl4-6%, antibacterial agent 0.1-0.2%, plant essential oil 0.01-0.1%, thickener 1.5-2.2% and distilled water 60- 70%. 2.如权利要求1所述的茶皂素洗发液,其特征在于,所述抑菌剂为双乙酸钠或脱氢乙酸钠中的一种或两种。 2. tea saponin shampoo as claimed in claim 1, is characterized in that, described antibacterial agent is one or both in sodium diacetate or sodium dehydroacetate. 3.如权利要求1所述的茶皂素洗发液,其特征在于,所述植物香精油为迷迪香精油、百里香酚精油、薰衣草精油或葡萄柚精油中的一种或几种混合。 3. tea saponin shampoo as claimed in claim 1, is characterized in that, described plant essential oil is one or more mixes in Midi essential oil, thymol essential oil, lavender essential oil or grapefruit essential oil. 4.如权利要求1所述的茶皂素洗发液,其特征在于,所述增稠剂为黄原胶或阿拉伯树胶中的一种或两种。 4. tea saponin shampoo as claimed in claim 1, is characterized in that, described thickener is one or both in xanthan gum or gum arabic. 5.生产权利要求1所述的茶皂素洗发液的方法,其特征在于,该方法步骤如下: 5. produce the method for the described tea saponin shampoo of claim 1, it is characterized in that, the method step is as follows: (1)按重量配比取蒸馏水加入搅拌罐中,开动搅拌,将蒸馏水加热至45-50℃; (1) Add distilled water into the mixing tank according to the weight ratio, start stirring, and heat the distilled water to 45-50°C; (2)将精制茶皂素慢慢加入加热后的蒸馏水中,80-100r/min搅拌10-20min,使精制茶皂素完全溶解,得到澄清溶液; (2) Slowly add the refined tea saponin into the heated distilled water, stir at 80-100r/min for 10-20min, completely dissolve the refined tea saponin, and obtain a clear solution; (3)依次加入所需的芦荟精华液、绿茶精华液、海藻提取物、甘油,80-100r/min条件下边加边搅拌,使之完全溶解; (3) Add the required aloe essence, green tea essence, seaweed extract, and glycerin in sequence, and stir while adding at 80-100r/min to make them completely dissolve; (4)加入所需香精和抑菌剂,搅拌均匀; (4) Add the required essence and antibacterial agent, and stir evenly; (5)将所需的增稠剂和NaCl充分混合均匀后,缓慢加入步骤(4)中,80-100r/min搅拌20-30min,使增稠剂完全溶解,静置10-12h,即可。 (5) After fully mixing the required thickener and NaCl, slowly add it to step (4), stir at 80-100r/min for 20-30min to completely dissolve the thickener, and let it stand for 10-12h. . 6.如权利要求5所述的方法,其特征在于,所述抑菌剂为双乙酸钠或脱氢乙酸钠中的一种或两种。 6. The method according to claim 5, wherein the bacteriostatic agent is one or both of sodium diacetate or sodium dehydroacetate. 7.如权利要求5所述的方法,其特征在于,所述植物香精油为迷迪香精油、百里香酚精油、薰衣草精油或葡萄柚精油中的一种或几种。 7. The method according to claim 5, wherein the plant essential oil is one or more of Midi essential oil, thymol essential oil, lavender essential oil or grapefruit essential oil. 8.如权利要求5所述的方法,其特征在于,所述增稠剂为黄原胶或阿拉伯树胶中的一种或两种。 8. The method according to claim 5, characterized in that, the thickener is one or both of xanthan gum or gum arabic.
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Cited By (4)

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Publication number Priority date Publication date Assignee Title
CN105012206A (en) * 2015-09-03 2015-11-04 哈尔滨泉兴科技有限公司 Green tea shampoo formula
CN105616292A (en) * 2016-02-03 2016-06-01 九沪(上海)生物科技有限公司 Tea saponin shampoo containing traditional Chinese medicine extracts and preparation method thereof
CN106333876A (en) * 2016-09-19 2017-01-18 拉芳家化股份有限公司 Plant essential oil liquid soap for increasing volume of hair and preparation method of plant essential oil liquid soap
CN108403541A (en) * 2018-03-16 2018-08-17 柳州市奥康眼镜有限公司 A kind of antibacterial shampoo of plant source

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CN103385831A (en) * 2013-07-19 2013-11-13 泉州市新益日用化妆品有限公司 Novel oil tea shampoo and preparation method thereof
CN103520036A (en) * 2013-10-12 2014-01-22 湖南金浩茶油股份有限公司 An anti-hair loss shampoo
CN103565690A (en) * 2013-03-01 2014-02-12 云南云道茶业有限公司 Healthcare shampoo

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CN102836097A (en) * 2012-08-21 2012-12-26 伊国群 Liquid shampoo containing tea saponin
CN103565690A (en) * 2013-03-01 2014-02-12 云南云道茶业有限公司 Healthcare shampoo
CN103385831A (en) * 2013-07-19 2013-11-13 泉州市新益日用化妆品有限公司 Novel oil tea shampoo and preparation method thereof
CN103520036A (en) * 2013-10-12 2014-01-22 湖南金浩茶油股份有限公司 An anti-hair loss shampoo

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105012206A (en) * 2015-09-03 2015-11-04 哈尔滨泉兴科技有限公司 Green tea shampoo formula
CN105616292A (en) * 2016-02-03 2016-06-01 九沪(上海)生物科技有限公司 Tea saponin shampoo containing traditional Chinese medicine extracts and preparation method thereof
CN105616292B (en) * 2016-02-03 2019-03-12 九沪(上海)生物科技有限公司 Tea Saponin shampoo containing Chinese medical extract and preparation method thereof
CN106333876A (en) * 2016-09-19 2017-01-18 拉芳家化股份有限公司 Plant essential oil liquid soap for increasing volume of hair and preparation method of plant essential oil liquid soap
CN106333876B (en) * 2016-09-19 2019-09-24 拉芳家化股份有限公司 A kind of plants essential oil soap lye and preparation method increasing hair volume sense
CN108403541A (en) * 2018-03-16 2018-08-17 柳州市奥康眼镜有限公司 A kind of antibacterial shampoo of plant source

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