CN103989244A - Chinese style flue-cured tobacco odor type electronic cigarette tobacco juice capable of improving smoking satisfaction sense - Google Patents
Chinese style flue-cured tobacco odor type electronic cigarette tobacco juice capable of improving smoking satisfaction sense Download PDFInfo
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- CN103989244A CN103989244A CN201410249859.6A CN201410249859A CN103989244A CN 103989244 A CN103989244 A CN 103989244A CN 201410249859 A CN201410249859 A CN 201410249859A CN 103989244 A CN103989244 A CN 103989244A
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- 241000208125 Nicotiana Species 0.000 title claims abstract description 163
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 163
- 235000011389 fruit/vegetable juice Nutrition 0.000 title claims abstract description 45
- 239000003571 electronic cigarette Substances 0.000 title abstract description 13
- 230000000391 smoking effect Effects 0.000 title abstract description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 93
- 238000000605 extraction Methods 0.000 claims abstract description 56
- 239000000284 extract Substances 0.000 claims abstract description 49
- 238000002360 preparation method Methods 0.000 claims abstract description 29
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 27
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims abstract description 25
- 229960002715 nicotine Drugs 0.000 claims abstract description 25
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims abstract description 25
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 13
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000011187 glycerol Nutrition 0.000 claims description 45
- 239000000779 smoke Substances 0.000 claims description 39
- 241000196324 Embryophyta Species 0.000 claims description 34
- OEYQBKYISMRWQB-UHFFFAOYSA-N Santal Chemical compound C=1C(OC)=CC(O)=C(C2=O)C=1OC=C2C1=CC=C(O)C(O)=C1 OEYQBKYISMRWQB-UHFFFAOYSA-N 0.000 claims description 32
- 241000271309 Aquilaria crassna Species 0.000 claims description 16
- 241000563988 Turpinia Species 0.000 claims description 16
- 244000248021 Vitex negundo Species 0.000 claims description 16
- 235000013427 Vitex negundo var incisa Nutrition 0.000 claims description 16
- 235000014961 Vitex negundo var negundo Nutrition 0.000 claims description 16
- 230000001154 acute effect Effects 0.000 claims description 16
- 235000014956 negundo chastetree Nutrition 0.000 claims description 16
- 241001647745 Banksia Species 0.000 claims description 15
- 241000220317 Rosa Species 0.000 claims description 15
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 9
- 230000006837 decompression Effects 0.000 claims description 7
- 239000000706 filtrate Substances 0.000 claims description 7
- 238000002137 ultrasound extraction Methods 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 2
- 235000019504 cigarettes Nutrition 0.000 abstract description 6
- 238000002156 mixing Methods 0.000 abstract description 6
- 239000000796 flavoring agent Substances 0.000 abstract description 5
- 235000019634 flavors Nutrition 0.000 abstract description 4
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 abstract 3
- GPLRAVKSCUXZTP-UHFFFAOYSA-N diglycerol Chemical compound OCC(O)COCC(O)CO GPLRAVKSCUXZTP-UHFFFAOYSA-N 0.000 abstract 2
- 241000256844 Apis mellifera Species 0.000 abstract 1
- 244000116484 Inula helenium Species 0.000 abstract 1
- 235000002598 Inula helenium Nutrition 0.000 abstract 1
- 240000000513 Santalum album Species 0.000 abstract 1
- 235000008632 Santalum album Nutrition 0.000 abstract 1
- 241001331775 Sauropus spatulifolius Species 0.000 abstract 1
- 244000063464 Vitex agnus-castus Species 0.000 abstract 1
- 235000009347 chasteberry Nutrition 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 235000002020 sage Nutrition 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 6
- 239000003205 fragrance Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 238000001303 quality assessment method Methods 0.000 description 5
- 230000001953 sensory effect Effects 0.000 description 5
- 235000009508 confectionery Nutrition 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 206010011224 Cough Diseases 0.000 description 3
- 208000006673 asthma Diseases 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 239000002304 perfume Substances 0.000 description 3
- 230000001737 promoting effect Effects 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 206010062717 Increased upper airway secretion Diseases 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 210000004072 lung Anatomy 0.000 description 2
- 210000000214 mouth Anatomy 0.000 description 2
- 208000026435 phlegm Diseases 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- 206010047700 Vomiting Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000013530 defoamer Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
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- Cosmetics (AREA)
Abstract
The invention discloses application of diglycerol in electronic cigarette tobacco juice preparation, and discloses electronic cigarette tobacco juice prepared through the application. The electronic cigarette tobacco juice is made of the raw materials, by mass, five percent to ten percent of tobacco extracts, two percent to four percent of tobacco flavor, one percent to three percent of tobacco essence, two percent to six percent of edible essence, one percent to two percent of natural nicotine, one percent to four percent of natural phytoextraction essence, 30 percent to 85 percent of the diglycerol, and the balance one or more kind of propylene glycol, glycerol, ethyl alcohol, butanediol and triethylene glycol. The natural phytoextraction essence is formed by mixing agilawood, sandalwood, elecampane, bee sage roundleaves, sauropus spatulifolius and vitex leaves according to the mass ratio of (1-3):(1-2):(1-2):(1-2):(1-2):(1-2), and is obtained through supercritical CO2 extraction. The invention further discloses a method for preparing the electronic cigarette tobacco juice. The Chinese style flue-cured tobacco extractive and tobacco flavor and essence ingredients are included in the electronic cigarette tobacco juice, the odor and taste are close to those of traditional Chinese style flue-cured tobacco odor type cigarettes, and the smoking satisfaction sense is improved.
Description
Technical field
The present invention relates to a kind of Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke that improves suction satisfaction, belong to electronic cigarette technical field.
Background technology
Progressively enforcement, the development of global Tobacco Control campaign and carrying forward vigorously of State Bureau's lowering harm and decreasing coking along with < < Framework Convention on Tobacco Control > >, people improve day by day to healthy degree of concern, make cigarette living environment just increasingly serious.In order to meet different consumer demands, the product of various simulation cigarette continues to bring out, wherein general with electronic cigarette, and particularly American-European countries obtains and extensively to approve and to have obtained great development in the world, people have generally had science and objectively judgement more to electronic cigarette, and this industry is being accelerated and promoted to the progress of electronic cigarette product self also towards optimum and healthy direction progress.But, on market, now sell tobacco juice for electronic smoke, mostly have that to suck in rear oral cavity sweet soapy feeling overweight, give a kind of very uncomfortable sensation of people, and tobacco flavor too a little less than, can not meet the domestic consumer who has been accustomed to suction Chinese style flue-cured tobacco odor type cigarette, seriously restricted the development of electronic cigarette.
Two glycerine have another name called contracting two glycerine, are a kind of yellow thick liquids, the easy moisture absorption, and water-soluble and ethanol, is insoluble to ether, and main emulsifying agent, defoamer and the replacement glycerine of being used as is used for stamp at present, but not yet has the report that is applied to tobacco juice for electronic smoke.
Summary of the invention
The object of the present invention is to provide the application of two glycerine in tobacco juice for electronic smoke preparation.
Another object of the present invention is to provide a kind of tobacco juice for electronic smoke that utilizes two glycerine to prepare.
For achieving the above object, the present invention adopts following technical scheme:
The application of two glycerine in tobacco juice for electronic smoke preparation, in tobacco juice for electronic smoke, the mass percent of two glycerine is 30-85%;
A tobacco juice for electronic smoke that utilizes two glycerine to prepare, by the raw material of following mass percent, made:
Tobacco extract 5-10%, tobacco aromatics using 2-4%, flavouring essence for tobacco 1-3%, flavoring essence 2-6%, natural nicotine 1-2%, natural plant extraction elite 1-4%, two glycerine 30-85%, surplus is one or more in propane diols, glycerine, alcohol, butanediol, triethylene glycol;
Wherein, tobacco extract is selected from Yunnan tobacco extract, Tobacco In Guangxi extract or Hubei tobacco extract;
Natural plant extraction elite is agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Folium Sauropi, leaf of negundo chastetree (1～3) in mass ratio: (1～2): (1～2): (1～2): (1～2): mix (1～2), through supercritical CO
2the extract that extraction obtains;
Agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Folium Sauropi, leaf of negundo chastetree are the kind that < < Chinese pharmacopoeia > > (version in 2010) records, and its quality all meets the requirement under each kind item.
Preferably, this tobacco juice for electronic smoke is made by the raw material of following mass percent:
Tobacco extract 6-8%, tobacco aromatics using 2-4%, flavouring essence for tobacco 1-3%, flavoring essence 3-5%, natural nicotine 1-2%, natural plant extraction elite 2-4%, two glycerine 50-80%, surplus is one or more in propane diols, glycerine, alcohol, butanediol, triethylene glycol;
The preparation method of this tobacco juice for electronic smoke, comprises the following steps:
(1) preparation of tobacco extract: by drying tobacco, pulverize, the water that adds 8-10 doubly to measure, ultrasonic extraction 30-60 minute, filters, and it is 1.05-1.10 (50 ℃ of surveys) that filtrate decompression is concentrated into relative density, obtains tobacco extract;
(2) preparation of natural plant extraction elite: take agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Folium Sauropi and leaf of negundo chastetree by mass parts, pulverize, cross 80-100 mesh sieve, through supercritical CO
2extraction, extracting pressure is 20-25MPa, CO
2flow is 20-30L/h, and extraction time is 1-2h, and entrainer is 95% ethanol;
(3) by tobacco extract, tobacco aromatics using, flavouring essence for tobacco, flavoring essence, natural nicotine, natural plant extraction elite, two glycerine, and one or more in propane diols, glycerine, alcohol, butanediol, triethylene glycol, add in mass ratio, mixes, and obtains.
Beneficial effect of the present invention is:
(1) tobacco juice for electronic smoke of the present invention is usingd two glycerine as solvent, and during suction, in oral cavity, sweet soapy feeling obviously reduces, and comfort is better;
(2) tobacco juice for electronic smoke of the present invention contains Chinese style flue-cured tobacco extract and essence spice for cigarette composition, comparatively approaching with traditional Chinese flue-cured tobacco flavor types cigarette aspect fragrance, mouthfeel, has improved suction satisfaction.
(3) tobacco juice for electronic smoke of the present invention contains natural plant extraction elite, wherein, and agalloch eaglewood: fragrant odour, has promoting qi circulation and relieving pain, warming middle energizer to arrest vomiting, the effect of promoting inspiration to relieve asthma; Santal: smell delicate fragrance; In promoting the circulation of qi temperature, for cold obstruction causing qi stagnation, chest diaphragm does not relax; Bee saage: fragrant odour; Acute turpinia leaf: fragrant odour, have clearing heat and detoxicating, the effect of reducing pharyngeal swelling; Folium Sauropi: gas is micro-, has the effect moistening the lung and relieve the cough; Leaf of negundo chastetree: fragrant odour, has and eliminate the phlegm, cough-relieving, the effect of relievining asthma; Above-mentioned 6 taste medicines have the smell of natural aromatic mostly, have increased fragrance matter and the perfume quantity of tobacco juice, but also have moisten the lung and relieve the cough, the effect of eliminating phlegm and relieving asthma, reducing pharyngeal swelling, in smoking, also played certain medical care effect.
The specific embodiment
The present invention is further illustrated in conjunction with the embodiments, should be noted that following explanation is only in order to explain the present invention, not limits its content.
Embodiment 1:
A tobacco juice for electronic smoke that utilizes two glycerine to prepare, by the raw material of following mass percent, made:
Yunnan tobacco extract 8%, tobacco aromatics using 3%, flavouring essence for tobacco 2%, flavoring essence 4%, natural nicotine 1.5%, natural plant extraction elite 3%, two glycerine 50%, surplus is that propane diols, glycerine, alcohol, butanediol, triethylene glycol are with the miscible mixed liquor of equal-volume;
Wherein, natural plant extraction elite is the 2:1.5:1.5:1.5:1.5:1.5 mixing in mass ratio of agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Folium Sauropi, leaf of negundo chastetree, through supercritical CO
2the extract that extraction obtains;
The fragrance-enhancing tobacco material (QY021) that tobacco aromatics using provides for Shanghai Qi Yuan essence and flavoring agent Co., Ltd;
Flavouring essence for tobacco is the fragrance-enhancing tobacco material (BD010) that Shenzhen BoDun spice Co., Ltd produces;
Flavoring essence is the heterocyclic material that Tengzhou City Wu Tong spices Co., Ltd produces;
The purity of natural nicotine is greater than 98%.
The preparation method of this tobacco juice for electronic smoke is:
(1) preparation of tobacco extract: Yunnan tobacco be dry, pulverize, get 30g Yunnan tobacco powder, add the water of 240ml, ultrasonic extraction 40 minutes, filters, and it is 1.05-1.10 (50 ℃ of surveys) that filtrate decompression is concentrated into relative density, obtains tobacco extract;
(2) preparation of natural plant extraction elite: take agalloch eaglewood 20g, santal 15g, banksia rose 15g, acute turpinia leaf 15g, Folium Sauropi 15g and leaf of negundo chastetree 15g, pulverize, cross 100 mesh sieves, through supercritical CO
2extraction, extracting pressure is 25MPa, CO
2flow is 20L/h, and extraction time is 1.5h, and entrainer is 95% ethanol;
(3) by tobacco extract, natural plant extraction elite, tobacco aromatics using, flavouring essence for tobacco, flavoring essence, natural nicotine, two glycerine and propane diols, glycerine, alcohol, butanediol, triethylene glycol mixed liquor, add in mass ratio, mix, obtain.
Embodiment 2:
A tobacco juice for electronic smoke that utilizes two glycerine to prepare, by the raw material of following mass percent, made:
Tobacco In Guangxi extract 5%, tobacco aromatics using 4%, flavouring essence for tobacco 1%, flavoring essence 6%, natural nicotine 1%, natural plant extraction elite 4%, two glycerine 30%, surplus is the mixed liquor of propane diols, triethylene glycol;
Wherein, natural plant extraction elite is the 3:1:2:1:2:1 mixing in mass ratio of agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Folium Sauropi, leaf of negundo chastetree, through supercritical CO
2the extract that extraction obtains;
The source of tobacco aromatics using, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.
The preparation method of this tobacco juice for electronic smoke is:
(1) preparation of tobacco extract: Yunnan tobacco be dry, pulverize, get 30g Guangxi tobacco leaf powder, add the water of 270ml, ultrasonic extraction 30 minutes, filters, and it is 1.05-1.10 (50 ℃ of surveys) that filtrate decompression is concentrated into relative density, obtains tobacco extract;
(2) preparation of natural plant extraction elite: take agalloch eaglewood 30g, santal 10g, banksia rose 20g, acute turpinia leaf 10g, Folium Sauropi 20g and leaf of negundo chastetree 10g and pulverize, cross 80 mesh sieves, through supercritical CO
2extraction, extracting pressure is 20MPa, CO
2flow is 30L/h, and extraction time is 2h, and entrainer is 95% ethanol;
(3) by the mixed liquor of tobacco extract, natural plant extraction elite, tobacco aromatics using, flavouring essence for tobacco, flavoring essence, natural nicotine, two glycerine and propane diols, triethylene glycol, add in mass ratio, mix, obtain.
Embodiment 3:
A tobacco juice for electronic smoke that utilizes two glycerine to prepare, by the raw material of following mass percent, made:
Hubei tobacco extract 10%, tobacco aromatics using 2%, flavouring essence for tobacco 3%, flavoring essence 2%, natural nicotine 2%, natural plant extraction elite 1%, two glycerine 65%, surplus is triethylene glycol;
Wherein, natural plant extraction elite is the 2:2:1:2:1:2 mixing in mass ratio of agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Folium Sauropi, leaf of negundo chastetree, through supercritical CO
2the extract that extraction obtains;
The source of tobacco aromatics using, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.
The preparation method of this tobacco juice for electronic smoke is:
(1) preparation of tobacco extract: Hubei tobacco leaf be dry, pulverize, get 30g Yunnan tobacco powder, add the water of 300ml, ultrasonic extraction 45 minutes, filters, and it is 1.05-1.10 (50 ℃ of surveys) that filtrate decompression is concentrated into relative density, obtains tobacco extract;
(2) preparation of natural plant extraction elite: take agalloch eaglewood 20g, santal 20g, banksia rose 10g, acute turpinia leaf 20g, Folium Sauropi 10g and leaf of negundo chastetree 20g, pulverize, cross 100 mesh sieves, through supercritical CO
2extraction, extracting pressure is 25MPa, CO
2flow is 25L/h, and extraction time is 1h, and entrainer is 95% ethanol;
(3) by tobacco extract, natural plant extraction elite, tobacco aromatics using, flavouring essence for tobacco, flavoring essence, natural nicotine, two glycerine and triethylene glycol, add in mass ratio, mix, obtain.
Embodiment 4:
A tobacco juice for electronic smoke that utilizes two glycerine to prepare, by the raw material of following mass percent, made:
Yunnan tobacco extract 5%, tobacco aromatics using 2%, flavouring essence for tobacco 1%, flavoring essence 2%, natural nicotine 1%, natural plant extraction elite 1%, two glycerine 85%, surplus is propane diols;
Wherein, natural plant extraction elite is the 2:1:1:1:1:1 mixing in mass ratio of agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Folium Sauropi, leaf of negundo chastetree, through supercritical CO
2the extract that extraction obtains;
The source of tobacco aromatics using, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.
The preparation method of this tobacco juice for electronic smoke is:
(1) preparation of tobacco extract: Yunnan tobacco be dry, pulverize, get 30g Yunnan tobacco powder, add the water of 300ml, ultrasonic extraction 45 minutes, filters, and it is 1.05-1.10 (50 ℃ of surveys) that filtrate decompression is concentrated into relative density, obtains tobacco extract;
(2) preparation of natural plant extraction elite: take agalloch eaglewood 20g, santal 10g, banksia rose 10g, acute turpinia leaf 10g, Folium Sauropi 10g and leaf of negundo chastetree 10g, pulverize, cross 100 mesh sieves, through supercritical CO
2extraction, extracting pressure is 25MPa, CO
2flow is 25L/h, and extraction time is 1h, and entrainer is 95% ethanol;
(3) by tobacco extract, natural plant extraction elite, tobacco aromatics using, flavouring essence for tobacco, flavoring essence, natural nicotine, two glycerine and propane diols, add in mass ratio, mix, obtain.
Embodiment 5:
A tobacco juice for electronic smoke that utilizes two glycerine to prepare, by the raw material of following mass percent, made:
Yunnan tobacco extract 6%, tobacco aromatics using 3%, flavouring essence for tobacco 1%, flavoring essence 2%, natural nicotine 1.5%, natural plant extraction elite 3%, two glycerine 80%, surplus is butanediol;
Wherein, natural plant extraction elite is the 2:1.5:2:1.5:2:1.5 mixing in mass ratio of agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Folium Sauropi, leaf of negundo chastetree, through supercritical CO
2the extract that extraction obtains;
The source of tobacco aromatics using, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.
The preparation method of this tobacco juice for electronic smoke is:
(1) preparation of tobacco extract: Yunnan tobacco be dry, pulverize, get 30g Yunnan tobacco powder, add the water of 300ml, ultrasonic extraction 45 minutes, filters, and it is 1.05-1.10 (50 ℃ of surveys) that filtrate decompression is concentrated into relative density, obtains tobacco extract;
(2) preparation of natural plant extraction elite: take agalloch eaglewood 20g, santal 15g, banksia rose 20g, acute turpinia leaf 15g, Folium Sauropi 20g and leaf of negundo chastetree 15g, pulverize, cross 100 mesh sieves, through supercritical CO
2extraction, extracting pressure is 25MPa, CO
2flow is 25L/h, and extraction time is 1h, and entrainer is 95% ethanol;
(3) by tobacco extract, natural plant extraction elite, tobacco aromatics using, flavouring essence for tobacco, flavoring essence, natural nicotine, two glycerine and butanediol, add in mass ratio, mix, obtain.
Embodiment 6:
Sensory quality assessment experiment:
(1) experiment material: the tobacco juice for electronic smoke of the embodiment of the present invention 1,2,3,4,5 preparations is as sample.
(2) electronic cigarette sensory quality assessment standard:
With reference to patent " a kind of tobacco juice for electronic smoke that utilizes Luzhou-flavor tobacco leaf to prepare " (number of patent application: 201310030063.7) 7 assessment items are set, the maximum scale of each assessment item is 9 minutes, each assessment item is all divided into score unit with 1, specifically in Table 1.
Table 1 electronic cigarette sensory quality assessment standard
| Score value | Fragrance matter | Perfume quantity | Sweet soapy feeling | Excitant | Assorted gas | Strength | Pleasant impression |
| 9 | Fine | Sufficient | Very light | Very little | Very light | Very large | Fine |
| 8 | Good | Foot | Light | Little | Gently | Greatly | Good |
| 7 | Better | More sufficient | Lighter | Less | Lighter | Larger | Better |
| 6 | Slightly good | Still sufficient | Slightly light | Slightly little | Still light | Slightly large | Slightly good |
| 5 | In | In | In | In | In | In | In |
| 4 | Slightly poor | Slightly | Slightly dense | Slightly large | Slightly heavy | Slightly little | Slightly poor |
| 3 | Poor | Lighter | Denseer | Larger | Heavier | Less | Poor |
| 2 | Poor | Flat | Dense | Greatly | Heavy | Little | Poor |
| 1 | Very poor | Very light | Dense | Very large | Very heavy | Very little | Very poor |
(3) evaluation method: provide sample and sensory quality assessment standard scale to the expert that smokes panel test, by form requirement, indices is smoked panel test.
(4) result statistics: all experts' that smoke panel test smoking result is all effective, and the expert's that respectively smokes panel test individual event smoking result is asked to arithmetic mean of instantaneous value, and result remains to 1 decimal, and the arithmetic mean of instantaneous value of each individual event is added and, obtain total points, the results are shown in Table 2.
Table 2 sensory quality assessment result
| Sample | Fragrance matter | Perfume quantity | Sweet soapy feeling | Excitant | Assorted gas | Strength | Pleasant impression | Add up to |
| Embodiment 1 | 7.6 | 7.5 | 7.7 | 7.8 | 7.6 | 7.9 | 7.6 | 53.7 |
| Embodiment 2 | 7.4 | 7.6 | 7.4 | 7.4 | 7.8 | 7.6 | 7.5 | 52.7 |
| Embodiment 3 | 7.5 | 7.4 | 7.6 | 7.6 | 7.5 | 8.0 | 7.6 | 53.2 |
| Embodiment 4 | 7.3 | 7.2 | 7.4 | 7.6 | 7.6 | 7.2 | 7.2 | 51.5 |
| Embodiment 5 | 7.4 | 7.2 | 7.5 | 7.4 | 7.3 | 7.8 | 7.6 | 52.2 |
Above-described embodiment is preferably embodiment of the present invention; but embodiments of the present invention are not restricted to the described embodiments; one of ordinary skill in the art should be understood that; on the basis of technical scheme of the present invention, those skilled in the art do not need to pay various modifications that creative work can make or distortion still in protection scope of the present invention.
Claims (10)
1. the application of two glycerine in tobacco juice for electronic smoke preparation, is characterized in that, in tobacco juice for electronic smoke, the mass percent of two glycerine is 30-85%.
2. the application of two glycerine as claimed in claim 1 in tobacco juice for electronic smoke preparation, is characterized in that the tobacco juice for electronic smoke of preparing during application.
3. a tobacco juice for electronic smoke, is characterized in that, by the raw material of following mass percent, is made:
Tobacco extract 5-10%, tobacco aromatics using 2-4%, flavouring essence for tobacco 1-3%, flavoring essence 2-6%, natural nicotine 1-2%, natural plant extraction elite 1-4%, two glycerine 30-85%, surplus is one or more in propane diols, glycerine, alcohol, butanediol, triethylene glycol;
Wherein, tobacco extract is selected from Yunnan tobacco extract, Tobacco In Guangxi extract or Hubei tobacco extract;
Natural plant extraction elite is agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Folium Sauropi, leaf of negundo chastetree (1～3) in mass ratio: (1～2): (1～2): (1～2): (1～2): mix (1～2), through supercritical CO
2the extract that extraction obtains.
4. tobacco juice for electronic smoke as claimed in claim 3, it is characterized in that, raw material by following mass percent is made: tobacco extract 6-8%, tobacco aromatics using 2-4%, flavouring essence for tobacco 1-3%, flavoring essence 3-5%, natural nicotine 1-2%, natural plant extraction elite 2-4%, two glycerine 50-80%, surplus is one or more in propane diols, glycerine, alcohol, butanediol, triethylene glycol.
5. tobacco juice for electronic smoke as claimed in claim 3, it is characterized in that, raw material by following mass percent is made: Yunnan tobacco extract 8%, tobacco aromatics using 3%, flavouring essence for tobacco 2%, flavoring essence 4%, natural nicotine 1.5%, natural plant extraction elite 3%, two glycerine 50%, surplus is that propane diols, glycerine, alcohol, butanediol, triethylene glycol are with the miscible mixed liquor of equal-volume.
6. tobacco juice for electronic smoke as claimed in claim 3, it is characterized in that, raw material by following mass percent is made: Tobacco In Guangxi extract 5%, tobacco aromatics using 4%, flavouring essence for tobacco 1%, flavoring essence 6%, natural nicotine 1%, natural plant extraction elite 4%, two glycerine 30%, surplus is the mixed liquor of propane diols, triethylene glycol.
7. tobacco juice for electronic smoke as claimed in claim 3, it is characterized in that, raw material by following mass percent is made: Hubei tobacco extract 10%, tobacco aromatics using 2%, flavouring essence for tobacco 3%, flavoring essence 2%, natural nicotine 2%, natural plant extraction elite 1%, two glycerine 65%, surplus is triethylene glycol.
8. the preparation method of tobacco juice for electronic smoke claimed in claim 3, it is characterized in that, by one or more in tobacco extract, natural plant extraction elite, tobacco aromatics using, flavouring essence for tobacco, flavoring essence, natural nicotine, two glycerine and propane diols, glycerine, alcohol, butanediol, triethylene glycol, add by mass percentage, mix, obtain.
9. the preparation method of tobacco juice for electronic smoke as claimed in claim 8, is characterized in that, the preparation method of tobacco extract is: by drying tobacco, pulverize the water that adds 8-10 doubly to measure, ultrasonic extraction 30-60 minute, filter, it is 1.05-1.10 that filtrate decompression is concentrated into relative density, obtains.
10. the preparation method of tobacco juice for electronic smoke as claimed in claim 8, it is characterized in that, the preparation method of natural plant extraction elite is: by mass parts, take agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Folium Sauropi, leaf of negundo chastetree, pulverize, cross 80-100 mesh sieve, through supercritical CO
2extraction, extracting pressure is 20-25MPa, CO
2flow is 20-30L/h, and extraction time is 1-2h, and entrainer is 95% ethanol, obtains.
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