CN103938493B - A kind of Waterproofing/oilproofing oil filter filter paper and preparation method thereof - Google Patents
A kind of Waterproofing/oilproofing oil filter filter paper and preparation method thereof Download PDFInfo
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- CN103938493B CN103938493B CN201410099718.0A CN201410099718A CN103938493B CN 103938493 B CN103938493 B CN 103938493B CN 201410099718 A CN201410099718 A CN 201410099718A CN 103938493 B CN103938493 B CN 103938493B
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- zirconium english
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- 239000002939 oilproofing Substances 0.000 title claims abstract description 11
- 238000004078 waterproofing Methods 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title claims description 7
- 239000000843 powder Substances 0.000 claims abstract description 37
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229910052726 zirconium Inorganic materials 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000000839 emulsion Substances 0.000 claims abstract description 11
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 10
- 241000609240 Ambelania acida Species 0.000 claims abstract description 7
- 239000010905 bagasse Substances 0.000 claims abstract description 7
- 229960002233 benzalkonium bromide Drugs 0.000 claims abstract description 7
- KHSLHYAUZSPBIU-UHFFFAOYSA-M benzododecinium bromide Chemical compound [Br-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 KHSLHYAUZSPBIU-UHFFFAOYSA-M 0.000 claims abstract description 7
- SCPWMSBAGXEGPW-UHFFFAOYSA-N dodecyl(trimethoxy)silane Chemical compound CCCCCCCCCCCC[Si](OC)(OC)OC SCPWMSBAGXEGPW-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000010433 feldspar Substances 0.000 claims abstract description 7
- 229920001289 polyvinyl ether Polymers 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 4
- WQZGKKKJIJFFOK-QTVWNMPRSA-N D-mannopyranose Chemical compound OC[C@H]1OC(O)[C@@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-QTVWNMPRSA-N 0.000 claims abstract description 4
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229920002689 polyvinyl acetate Polymers 0.000 claims abstract description 4
- 239000011118 polyvinyl acetate Substances 0.000 claims abstract description 4
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 4
- 239000000661 sodium alginate Substances 0.000 claims abstract description 4
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- 239000002002 slurry Substances 0.000 claims description 9
- 239000005995 Aluminium silicate Substances 0.000 claims description 6
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 6
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 6
- 235000012211 aluminium silicate Nutrition 0.000 claims description 6
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Inorganic materials [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 claims description 6
- CSSYLTMKCUORDA-UHFFFAOYSA-N barium(2+);oxygen(2-) Chemical compound [O-2].[Ba+2] CSSYLTMKCUORDA-UHFFFAOYSA-N 0.000 claims description 6
- 239000004927 clay Substances 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 6
- 239000011236 particulate material Substances 0.000 claims description 6
- 238000007493 shaping process Methods 0.000 claims description 6
- 238000007598 dipping method Methods 0.000 claims description 4
- JHWNWJKBPDFINM-UHFFFAOYSA-N Laurolactam Chemical compound O=C1CCCCCCCCCCCN1 JHWNWJKBPDFINM-UHFFFAOYSA-N 0.000 claims description 3
- 239000004677 Nylon Substances 0.000 claims description 3
- 229920000299 Nylon 12 Polymers 0.000 claims description 3
- DOOTYTYQINUNNV-UHFFFAOYSA-N Triethyl citrate Chemical compound CCOC(=O)CC(O)(C(=O)OCC)CC(=O)OCC DOOTYTYQINUNNV-UHFFFAOYSA-N 0.000 claims description 3
- 238000010009 beating Methods 0.000 claims description 3
- 230000015556 catabolic process Effects 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 3
- 238000006731 degradation reaction Methods 0.000 claims description 3
- 230000018044 dehydration Effects 0.000 claims description 3
- 238000006297 dehydration reaction Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 235000013312 flour Nutrition 0.000 claims description 3
- 238000005469 granulation Methods 0.000 claims description 3
- 230000003179 granulation Effects 0.000 claims description 3
- 238000005470 impregnation Methods 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- 239000011812 mixed powder Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 229920001778 nylon Polymers 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 239000001069 triethyl citrate Substances 0.000 claims description 3
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 claims description 3
- 235000013769 triethyl citrate Nutrition 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 239000003921 oil Substances 0.000 abstract description 17
- 239000010721 machine oil Substances 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- 239000012535 impurity Substances 0.000 abstract description 3
- 229910010293 ceramic material Inorganic materials 0.000 abstract description 2
- 239000000084 colloidal system Substances 0.000 abstract description 2
- 238000002485 combustion reaction Methods 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 229910052751 metal Inorganic materials 0.000 abstract description 2
- 239000002184 metal Substances 0.000 abstract description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 abstract description 2
- 238000001179 sorption measurement Methods 0.000 abstract description 2
- 229920001131 Pulp (paper) Polymers 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000009172 bursting Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 239000013528 metallic particle Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000004071 soot Substances 0.000 description 1
Landscapes
- Filtering Materials (AREA)
- Paper (AREA)
Abstract
The invention discloses a kind of Waterproofing/oilproofing oil filter filter paper, it is characterized in that, be made up of the raw material of following weight portion: bagasse pulp 50-56, manila pulp 46-49, zirconium English powder 2-4, feldspar powder 2-3, magnet powder 1-2, dodecyl trimethoxy silane 0.5-0.9, sodium alginate 0.5-0.7, poly-galactolipin mannose 0.2-0.3, polyvinyl acetate emulsion 6-8, butyl acrylate 2-3, benzalkonium bromide 0.5-0.7, polyvinylether 0.4-0.6, auxiliary agent 1-2; The present invention is by the combination of ceramic material and filter paper, durable, filters effective, advantages of good adsorption effect, and add auxiliary agent, safety and environmental protection, has good resistance to water and oil resistivity; Interpolation zirconium English powder, magnet powder can filter out engine well and produce in combustion and be mixed into the impurity such as the colloid of metal filings, carbon granules and the machine oil generation in machine oil, reduce exhaust emissions.
Description
Technical field
The present invention relates to automobile filter field, particularly a kind of Waterproofing/oilproofing oil filter filter paper and preparation method thereof.
Background technology
Oil filter is the one of cleaner, can remove the impurity such as the dust in machine oil, metallic particles, carbon precipitates and coal soot, protection engine.Oil filter paper is the key building block in oil filter, decide the performance of oil strainer, oil filter paper he to generally include with common wood pulp be a kind of INVENTIONPaper filter layer that main component is made, because normal wood pulp fibres is comparatively thin, hold the shortcomings such as ash quantity is low, the life-span is short, and oil filter paper made of paper also ubiquity resistance to water and oil resistivity is poor, the non-refractory characteristic such as not environmentally, when fuel oil soaks easy distortion for a long time, and then affects filter effect.
Summary of the invention
The object of this invention is to provide a kind of Waterproofing/oilproofing oil filter filter paper and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of Waterproofing/oilproofing oil filter filter paper, is made up of the raw material of following weight portion: bagasse pulp 50-56, manila pulp 46-49, zirconium English powder 2-4, feldspar powder 2-3, magnet powder 1-2, dodecyl trimethoxy silane 0.5-0.9, sodium alginate 0.5-0.7, poly-galactolipin mannose 0.2-0.3, polyvinyl acetate emulsion 6-8, butyl acrylate 2-3, benzalkonium bromide 0.5-0.7, polyvinylether 0.4-0.6, auxiliary agent 1-2;
Described auxiliary agent is made up of the raw material of following weight portion: kaolin 7-9, clay 5-8, zirconium English powder 4-6, barium monoxide 2-3, aluminium hydroxide 2-3, nylon 1214-16, triethyl citrate 2-3, acetic acid 1-2; First kaolin, clay, zirconium English powder, barium monoxide, aluminium hydroxide are put into ball mill by preparation method, wear into 100-140 object powder, mix; Then nylon 12 is heated to soften, adds the stirring of all the other residual componentss and add mixed-powder after 15-25 minute, send into double screw extruder granulation, obtain particulate material; Finally particulate material is put into flour mill to pulverize, to obtain final product.
A kind of Waterproofing/oilproofing oil filter filter paper of the present invention, be made up of following concrete steps:
(1) zirconium English powder, feldspar powder, magnet powder are mixed, grind to form 50-100 object powder, add dodecyl trimethoxy silane, with the speed of 850-950 rev/min, stir 25-30 minute, then 110-120 DEG C dry 1.5-2.5 hour stand-by;
(2) bagasse pulp, manila pulp are put into hydrabrusher size degradation, then through beater, beating consistency controls at 5.8-6.2%, obtained slurry;
(3) compound of step (1) is added in slurry, add benzalkonium bromide, polyvinylether, be heated to 65-75 DEG C, stir, add appropriate water size mixing to solid content be 2-3%, the slurry mixed up, after forming web is shaping, carries out suction dehydration to the l Water Paper after shaping under the vacuum condition of 0.05-0.08Mpa;
(4) all the other residual componentss mixed, dilute with water, then heat, temperature controls, at 60-70 DEG C, to boil 50-60 minute, and insulation 25-30 minute, is warming up to 70-75 DEG C, stirs and make dipping emulsion; (5) the paper homogeneous impregnation emulsion after step (3) being dewatered with spreader, then dries 4-5min by the paper electric drying oven with forced convection flooded, finally dry 5-10min on polisher, after taking-up and get final product.
The invention has the beneficial effects as follows: the present invention is by the combination of ceramic material and filter paper, durable, filters effective, advantages of good adsorption effect, add auxiliary agent, safety and environmental protection, has good resistance to water and oil resistivity; Add zirconium English powder, magnet powder can filter out engine well and produce in combustion and be mixed into the impurity such as the colloid that metal filings, carbon granules and machine oil in machine oil produces gradually, reduce exhaust emissions.
Specific embodiments
Below by instantiation, the present invention is described in detail.
A kind of Waterproofing/oilproofing oil filter filter paper, is made up of the raw material of following weight portion (kilogram): bagasse pulp 50, manila pulp 46, zirconium English powder 2, feldspar powder 2, magnet powder 1, dodecyl trimethoxy silane 0.5, sodium alginate 0.5, poly-galactolipin mannose 0.2, polyvinyl acetate emulsion 6, butyl acrylate 2, benzalkonium bromide 0.5, polyvinylether 0.4, auxiliary agent 1;
Described auxiliary agent is made up of the raw material of following weight portion (kilogram): kaolin 7, clay 5, zirconium English powder 4, barium monoxide 2, aluminium hydroxide 2, nylon 1214, triethyl citrate 2, acetic acid 1; First kaolin, clay, zirconium English powder, barium monoxide, aluminium hydroxide are put into ball mill by preparation method, wear into 100-140 object powder, mix; Then nylon 12 is heated to soften, adds the stirring of all the other residual componentss and add mixed-powder after 15-25 minute, send into double screw extruder granulation, obtain particulate material; Finally particulate material is put into flour mill to pulverize, to obtain final product.
A kind of Waterproofing/oilproofing oil filter filter paper of the present invention, be made up of following concrete steps:
(1) zirconium English powder, feldspar powder, magnet powder are mixed, grind to form 50-100 object powder, add dodecyl trimethoxy silane, with the speed of 850-950 rev/min, stir 25-30 minute, then 110-120 DEG C dry 1.5-2.5 hour stand-by;
(2) bagasse pulp, manila pulp are put into hydrabrusher size degradation, then through beater, beating consistency controls at 5.8-6.2%, obtained slurry;
(3) compound of step (1) is added in slurry, add benzalkonium bromide, polyvinylether, be heated to 65-75 DEG C, stir, add appropriate water size mixing to solid content be 2-3%, the slurry mixed up, after forming web is shaping, carries out suction dehydration to the l Water Paper after shaping under the vacuum condition of 0.05-0.08Mpa;
(4) all the other residual componentss mixed, dilute with water, then heat, temperature controls, at 60-70 DEG C, to boil 50-60 minute, and insulation 25-30 minute, is warming up to 70-75 DEG C, stirs and make dipping emulsion; (5) the paper homogeneous impregnation emulsion after step (3) being dewatered with spreader, repeated multiple times, use up to dipping emulsion, then dry 4-5min by the paper electric drying oven with forced convection flooded, finally dry 5-10min on polisher, after taking-up and get final product.
After testing, the bursting strength 350KPa of the filter paper that the present invention obtains, Air permenbility 85-88L/m
2between s, maximum diameter of hole is 75 μm, and average pore size is 55 μm, filter efficiency 92.4%.
Claims (1)
1. a Waterproofing/oilproofing oil filter filter paper, it is characterized in that, be made up of the raw material of following weight portion: bagasse pulp 50-56, manila pulp 46-49, zirconium English powder 2-4, feldspar powder 2-3, magnet powder 1-2, dodecyl trimethoxy silane 0.5-0.9, sodium alginate 0.5-0.7, poly-galactolipin mannose 0.2-0.3, polyvinyl acetate emulsion 6-8, butyl acrylate 2-3, benzalkonium bromide 0.5-0.7, polyvinylether 0.4-0.6, auxiliary agent 1-2;
Described auxiliary agent is made up of the raw material of following weight portion: kaolin 7-9, clay 5-8, zirconium English powder 4-6, barium monoxide 2-3, aluminium hydroxide 2-3, nylon 1214-16, triethyl citrate 2-3, acetic acid 1-2; First kaolin, clay, zirconium English powder, barium monoxide, aluminium hydroxide are put into ball mill by the preparation method of described auxiliary agent, wear into 100-140 object powder, mix; Then nylon 12 is heated to soften, adds the stirring of all the other residual componentss and add mixed-powder after 15-25 minute, send into double screw extruder granulation, obtain particulate material; Finally particulate material is put into flour mill to pulverize, to obtain final product;
Described a kind of Waterproofing/oilproofing oil filter filter paper, be made up of following concrete steps:
(1) zirconium English powder, feldspar powder, magnet powder are mixed, grind to form 50-100 object powder, add dodecyl trimethoxy silane, with the speed of 850-950 rev/min, stir 25-30 minute, then 110-120 DEG C dry 1.5-2.5 hour stand-by;
(2) bagasse pulp, manila pulp are put into hydrabrusher size degradation, then through beater, beating consistency controls at 5.8-6.2%, obtained slurry;
(3) compound of step (1) is added in slurry, add benzalkonium bromide, polyvinylether, be heated to 65-75 DEG C, stir, add appropriate water size mixing to solid content be 2-3%, the slurry mixed up, after forming web is shaping, carries out suction dehydration to the l Water Paper after shaping under the vacuum condition of 0.05-0.08Mpa;
(4) all the other residual componentss mixed, dilute with water, then heat, temperature controls, at 60-70 DEG C, to boil 50-60 minute, and insulation 25-30 minute, is warming up to 70-75 DEG C, stirs and make dipping emulsion;
(5) the paper homogeneous impregnation emulsion after step (3) being dewatered with spreader, then dries 4-5min by the paper electric drying oven with forced convection flooded, finally dry 5-10min on polisher, after taking-up and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410099718.0A CN103938493B (en) | 2014-03-18 | 2014-03-18 | A kind of Waterproofing/oilproofing oil filter filter paper and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410099718.0A CN103938493B (en) | 2014-03-18 | 2014-03-18 | A kind of Waterproofing/oilproofing oil filter filter paper and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN103938493A CN103938493A (en) | 2014-07-23 |
| CN103938493B true CN103938493B (en) | 2016-04-06 |
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|---|---|---|---|
| CN201410099718.0A Expired - Fee Related CN103938493B (en) | 2014-03-18 | 2014-03-18 | A kind of Waterproofing/oilproofing oil filter filter paper and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004035173A1 (en) * | 2002-10-16 | 2004-04-29 | Hokuetsu Paper Mills, Ltd. | Air purification filter and process for producing the same |
| CN102912680A (en) * | 2012-09-20 | 2013-02-06 | 蚌埠凤凰滤清器有限责任公司 | High-temperature resistant fiber filter paper for engine oil filter and preparation method of high-temperature resistant fiber filter paper |
| CN102952485A (en) * | 2012-10-27 | 2013-03-06 | 蚌埠凤凰滤清器有限责任公司 | Adhesive film containing modified nano potassium feldspar powder for filter |
| CN103382684A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠首创滤清器有限公司 | Filter paper with high filtration efficiency and preparation method thereof |
-
2014
- 2014-03-18 CN CN201410099718.0A patent/CN103938493B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004035173A1 (en) * | 2002-10-16 | 2004-04-29 | Hokuetsu Paper Mills, Ltd. | Air purification filter and process for producing the same |
| CN102912680A (en) * | 2012-09-20 | 2013-02-06 | 蚌埠凤凰滤清器有限责任公司 | High-temperature resistant fiber filter paper for engine oil filter and preparation method of high-temperature resistant fiber filter paper |
| CN102952485A (en) * | 2012-10-27 | 2013-03-06 | 蚌埠凤凰滤清器有限责任公司 | Adhesive film containing modified nano potassium feldspar powder for filter |
| CN103382684A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠首创滤清器有限公司 | Filter paper with high filtration efficiency and preparation method thereof |
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| Publication number | Publication date |
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| CN103938493A (en) | 2014-07-23 |
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Denomination of invention: Water and oil resistant oil filter paper and preparation method thereof Effective date of registration: 20170512 Granted publication date: 20160406 Pledgee: Bengbu financing guarantee Group Co., Ltd. Pledgor: Bengbu Feng Chi cleaner Co., Ltd Registration number: 2017340000060 |
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