CN103923602A - Manufacturing method for cerium based abrasive material - Google Patents
Manufacturing method for cerium based abrasive material Download PDFInfo
- Publication number
- CN103923602A CN103923602A CN201310014081.6A CN201310014081A CN103923602A CN 103923602 A CN103923602 A CN 103923602A CN 201310014081 A CN201310014081 A CN 201310014081A CN 103923602 A CN103923602 A CN 103923602A
- Authority
- CN
- China
- Prior art keywords
- raw material
- cerium based
- rare earth
- cerium
- abrasive material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229910052684 Cerium Inorganic materials 0.000 title claims abstract description 32
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 title claims abstract description 32
- 239000003082 abrasive agent Substances 0.000 title claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 26
- 238000000034 method Methods 0.000 claims abstract description 14
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 10
- -1 rare earth carbonate Chemical class 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 229910001404 rare earth metal oxide Inorganic materials 0.000 claims abstract description 5
- 239000007864 aqueous solution Substances 0.000 claims description 10
- 238000010298 pulverizing process Methods 0.000 claims description 10
- 150000001875 compounds Chemical class 0.000 claims description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 150000002910 rare earth metals Chemical class 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 238000000227 grinding Methods 0.000 description 6
- 238000013467 fragmentation Methods 0.000 description 3
- 238000006062 fragmentation reaction Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004334 fluoridation Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000000266 injurious effect Effects 0.000 description 1
Landscapes
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
The invention discloses a manufacturing method for a cerium based abrasive material. The method comprises the steps of: 1) soaking a raw material of the cerium based abrasive material in a water solution, and conducting heating and crushing; 2) roasting the crushed raw material; and 3) crushing the roasted raw material. Specifically, the raw material of the cerium based abrasive material adopts a cerium based rare earth carbonate or a mixture of cerium rare earth carbonate and cerium rare earth oxide.
Description
Technical field
The present invention relates to a kind of manufacture method of cerium based abrasive material.
Background technology
Up to now, in the grinding step of implementing corresponding to the magnetic recording medium of high density recording and high-speed read-write, very high to the accuracy requirement of the smoothness of glass baseplate surface, if but the concentration of oversize particle in abrasive substance is high, easily cause being polished the generation of injurious surface mark, thereby can not meet the requirement of smoothness.Based on existing manufacture method, such as the wet processed of being undertaken by use ball mill, masher, and add the fluoridation that fluorine component carries out, can cause the abrasive substance of particulate when grinding easily adhere on the face of being polished and easily residue on the face of being polished, therefore there will be the bad clean problem of the face of being polished.
Summary of the invention
therefore, the object of the present invention is to provide a kind of concentration of oversize particle lower, can guarantee higher abrasive power and be polished the manufacture method of the good cerium based abrasive material of the detergency of face.
in order to solve the problems of the technologies described above, the present invention adopts following technical scheme:
a manufacture method for cerium based abrasive material, comprises the steps:
1) raw material of cerium based abrasive material be impregnated in to the step that under the state of the aqueous solution, heating is pulverized; 2) step of the raw material after pulverizing being carried out to roasting; 3) by the step of the raw material crushing after roasting;
the raw material of wherein said cerium based abrasive material adopts the mixing raw material of cerium based rare earth carbonate or cerium based rare earth carbonate and cerium based rare earth oxide compound.
preferably, the Heating temperature of the aqueous solution of described step 1) is 60 ℃ ~ 100 ℃.
preferably, the Heating temperature of the aqueous solution of described step 1) is 80 ℃.
preferably, in described step 1) ~ 4) between do not comprise the step of case of wet attrition.
owing to having adopted technical scheme as above, the present invention has following beneficial effect:
make the concentration of oversize particle lower; Can guarantee higher abrasive power; Make the detergency of the face that is polished better.
Embodiment
embodiment 1
a manufacture method for cerium based abrasive material, comprises the steps: 1) the raw material 5g of cerium based rare earth carbonate be impregnated under the state of the 10kg aqueous solution and be heated to 60 ℃ of steps of pulverizing; 2) by the step of the raw material roasting 5h at 850 ℃ after pulverizing; 3) step with grinding machine fragmentation by the raw material after roasting.
embodiment 2
a manufacture method for cerium based abrasive material, comprises the steps: 1) the raw material 8g mixing by cerium based rare earth carbonate and cerium based rare earth oxide compound be impregnated under the state of aqueous solution 15kg and be heated to 75 ℃ of steps of pulverizing; 2) by the step of the raw material roasting 5h at 850 ℃ after pulverizing; 3) step with grinding machine fragmentation by the raw material after roasting.
embodiment 3
a manufacture method for cerium based abrasive material, comprises the steps: 1) the raw material 10g of cerium based rare earth carbonate be impregnated under the state of aqueous solution 21kg and be heated to 80 ℃ of steps of pulverizing; 2) by the step of the raw material roasting 5h at 850 ℃ after pulverizing; 3) step with grinding machine fragmentation by the raw material after roasting.
embodiment 4
a manufacture method for cerium based abrasive material, comprises the steps: 1) the raw material 12g mixing by cerium based rare earth carbonate and cerium based rare earth oxide compound be impregnated under the state of aqueous solution 26kg and be heated to 100 ℃ of steps of pulverizing; 2) by the step of the raw material roasting 5h at 850 ℃ after pulverizing; 3) with grinding machine by the step of the raw material crushing after roasting.
obviously, the above embodiment of the present invention is only for example of the present invention is clearly described, and is not the restriction to embodiments of the present invention.For those of ordinary skill in the field, can also make on the basis of the above description other multi-form variation and changes.Here cannot give all embodiments exhaustive.Every still row in protection scope of the present invention of apparent variation that technical scheme of the present invention amplifies out or change that belong to.
Claims (4)
1. a manufacture method for cerium based abrasive material, is characterized in that, comprises the steps: 1) raw material of cerium based abrasive material be impregnated in to the step that under the state of the aqueous solution, heating is pulverized; 2) step of the raw material after pulverizing being carried out to roasting; 3) by the step of the raw material crushing after roasting;
The raw material of wherein said cerium based abrasive material adopts the mixing raw material of cerium based rare earth carbonate or cerium based rare earth carbonate and cerium based rare earth oxide compound.
2. manufacture method according to claim 1, is characterized in that: the Heating temperature of the aqueous solution of described step 1) is 60 ℃ ~ 100 ℃.
3. manufacture method according to claim 1, is characterized in that: the Heating temperature of the aqueous solution of described step 1) is 80 ℃.
4. manufacture method according to claim 1, is characterized in that: in described step 1) ~ 4) between do not comprise the step of case of wet attrition.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201310014081.6A CN103923602A (en) | 2013-01-15 | 2013-01-15 | Manufacturing method for cerium based abrasive material |
Applications Claiming Priority (1)
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CN201310014081.6A CN103923602A (en) | 2013-01-15 | 2013-01-15 | Manufacturing method for cerium based abrasive material |
Publications (1)
Publication Number | Publication Date |
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CN103923602A true CN103923602A (en) | 2014-07-16 |
Family
ID=51142006
Family Applications (1)
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CN201310014081.6A Pending CN103923602A (en) | 2013-01-15 | 2013-01-15 | Manufacturing method for cerium based abrasive material |
Country Status (1)
Country | Link |
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CN (1) | CN103923602A (en) |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001088056A1 (en) * | 2000-05-16 | 2001-11-22 | Mitsui Mining & Smelting Co., Ltd. | Cerium based abrasive material, raw material thereof and method for their preparation |
CN1410502A (en) * | 2001-09-28 | 2003-04-16 | 三井金属鉱业株式会社 | Cerium series abrasive material and analyzing method thereof |
CN1489625A (en) * | 2001-05-29 | 2004-04-14 | ���������kҵ��ʽ���� | Method for producing cerium-based polishing agent |
JP2008013689A (en) * | 2006-07-06 | 2008-01-24 | Mitsui Mining & Smelting Co Ltd | Raw material for cerium-based abrasive, method for producing cerium-based abrasive, and cerium-based abrasive |
-
2013
- 2013-01-15 CN CN201310014081.6A patent/CN103923602A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001088056A1 (en) * | 2000-05-16 | 2001-11-22 | Mitsui Mining & Smelting Co., Ltd. | Cerium based abrasive material, raw material thereof and method for their preparation |
CN1489625A (en) * | 2001-05-29 | 2004-04-14 | ���������kҵ��ʽ���� | Method for producing cerium-based polishing agent |
CN1410502A (en) * | 2001-09-28 | 2003-04-16 | 三井金属鉱业株式会社 | Cerium series abrasive material and analyzing method thereof |
JP2008013689A (en) * | 2006-07-06 | 2008-01-24 | Mitsui Mining & Smelting Co Ltd | Raw material for cerium-based abrasive, method for producing cerium-based abrasive, and cerium-based abrasive |
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PB01 | Publication | ||
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C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20140716 |