CN103756771B - A kind of wear-resistant micro emulsion cutting fluid and preparation method thereof - Google Patents
A kind of wear-resistant micro emulsion cutting fluid and preparation method thereof Download PDFInfo
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- CN103756771B CN103756771B CN201310653265.7A CN201310653265A CN103756771B CN 103756771 B CN103756771 B CN 103756771B CN 201310653265 A CN201310653265 A CN 201310653265A CN 103756771 B CN103756771 B CN 103756771B
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- cutting fluid
- sodium
- wear
- water
- micro emulsion
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- 239000002173 cutting fluid Substances 0.000 title claims abstract description 30
- 239000004530 micro-emulsion Substances 0.000 title claims abstract description 12
- 238000002360 preparation method Methods 0.000 title claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 14
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 8
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 8
- 239000011734 sodium Substances 0.000 claims abstract description 8
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000003350 kerosene Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 7
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 7
- 239000000661 sodium alginate Substances 0.000 claims abstract description 7
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 7
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims abstract description 6
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims abstract description 6
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims abstract description 6
- 241001272567 Hominoidea Species 0.000 claims abstract description 6
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000005642 Oleic acid Substances 0.000 claims abstract description 6
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims abstract description 6
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims abstract description 6
- 239000003208 petroleum Substances 0.000 claims abstract description 6
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 6
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 4
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000012964 benzotriazole Substances 0.000 claims abstract description 4
- 229910021538 borax Inorganic materials 0.000 claims abstract description 4
- UQGFMSUEHSUPRD-UHFFFAOYSA-N disodium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Na+].[Na+].O1B([O-])OB2OB([O-])OB1O2 UQGFMSUEHSUPRD-UHFFFAOYSA-N 0.000 claims abstract description 4
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 4
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 14
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims description 12
- 229910001870 ammonium persulfate Inorganic materials 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- OAYXUHPQHDHDDZ-UHFFFAOYSA-N 2-(2-butoxyethoxy)ethanol Chemical compound CCCCOCCOCCO OAYXUHPQHDHDDZ-UHFFFAOYSA-N 0.000 claims description 3
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 3
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 3
- 239000004115 Sodium Silicate Substances 0.000 claims description 3
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 3
- 239000004202 carbamide Substances 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 3
- 235000019795 sodium metasilicate Nutrition 0.000 claims description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 3
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 3
- PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 claims description 2
- 240000006413 Prunus persica var. persica Species 0.000 claims 1
- 238000001816 cooling Methods 0.000 abstract description 6
- 230000015572 biosynthetic process Effects 0.000 abstract description 4
- 238000003786 synthesis reaction Methods 0.000 abstract description 4
- 238000004140 cleaning Methods 0.000 abstract description 3
- 238000005520 cutting process Methods 0.000 abstract description 2
- 239000006185 dispersion Substances 0.000 abstract description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000005555 metalworking Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 244000144730 Amygdalus persica Species 0.000 description 1
- 240000005809 Prunus persica Species 0.000 description 1
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 230000009972 noncorrosive effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000020354 squash Nutrition 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
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- Lubricants (AREA)
Abstract
A kind of wear-resistant micro emulsion cutting fluid, is made up of the raw material of following weight portion: petroleum sodium sulfonate 2-3, oleic acid 3-4, triethanolamine 1-2, APES 3-4, benzotriazole 1-2, sodium tetraborate 2-3, sodium carbonate 1-2, ethanol 30-35, kerosene 10-12, sodium alginate 1-2, auxiliary agent 6-8, water 200; The present invention not only has advantages of that lubricity and synthesis type cutting fluid cleaning that emulsified cutting fluid is good are good, also overcome emulsified cutting fluid perishable smelly, service life is short and the poor shortcoming of synthesis type cutting fluid oiliness greasy property; By using sodium tetraborate, make cutting fluid integrate the performances such as peace and quiet dispersion, the anti-corruption of antioxygen, extreme-pressure anti-wear, greatly improve the service life of machinery and cutting fluid, and cooling performance is good, be applicable to the processing of high-precision workpiece, not only yield rate is high, and cutting speed is fast.
Description
Technical field
The present invention relates to cutting fluid field, relate in particular to a kind of wear-resistant micro emulsion cutting fluid and preparation method thereof.
Background technology
Cutting fluid should possess good cooling performance, greasy property, rustless property, oil removing cleaning function, anticorrosionFunction, easily dilutable feature. Cutting fluid can be divided into two classes, oil-soluble cutting fluid and water-soluble metalworking liquid at present. OneAs oil-soluble cutting fluid lubrication performance good, but poor cooling performance, and contain large amount of organic, contaminated environment. OneAlthough a little water-soluble metalworking liquid cooling performances are good, have again the poor problem of lubricity and rust-proof effect, therefore research and developmentHave lubricity, cooling, rust-preventing characteristic, easy cleaning, nontoxic, tasteless, non-corrosive to human body, to equipment not concurrentlyBurn into just seems very important to the non-staining cutting fluid of environment.
Summary of the invention
The object of the present invention is to provide a kind of wear-resistant micro emulsion cutting fluid and preparation method thereof.
Technical scheme of the present invention is as follows:
A kind of wear-resistant micro emulsion cutting fluid, is characterized in that being made up of the raw material of following weight portion: petroleum sodium sulfonate2-3, oleic acid 3-4, triethanolamine 1-2, APES 3-4, benzotriazole 1-2, four boronAcid sodium 2-3, sodium carbonate 1-2, ethanol 30-35, kerosene 10-12, sodium alginate 1-2, auxiliary agent 6-8, water200; Described auxiliary agent is made up of the raw material of following weight portion: Tween-81 2-3,Nano aluminum nitride 0.1-0.2, carbonic hydroammonium 2-3, monoethanolamine 1-2, CMC 2-3, diethylene glycolButyl ether 1-2, propane diols 5-8, peach gum 2-3, sodium metasilicate 1-2, urea 3-4, ammonium persulfate 1-2, water 20-24;Preparation method be ammonium persulfate is water-soluble after, then add other leftover materials, stir 10-15 minute, heatingTo 70-80 DEG C, stirring reaction 1-2 hour, to obtain final product.
The preparation method of described wear-resistant micro emulsion cutting fluid, is characterized in that comprising the following steps: by water, oilSodium sulfonate, APES, sodium carbonate, sodium alginate mix, and are heated to 40-50 DEG C; Add oilAcid, kerosene, ethanol, auxiliary agent continue to be heated to 70-80 DEG C under 1000-1200 rev/min of stirring, stir10-15 minute; Add other residual components, continue to stir 14-18 minute, to obtain final product.
Beneficial effect of the present invention
The present invention not only has lubricity that emulsified cutting fluid is good and good excellent of synthesis type cutting fluid cleaningPoint, also overcome emulsified cutting fluid perishable smelly, service life is short and synthesis type cutting fluid oiliness lubricityShortcoming that can be poor; By using sodium tetraborate, the peace and quiet dispersion of cutting fluid collection, the anti-corruption of antioxygen, extreme pressure are resistedThe performances such as mill, greatly improved the service life of machinery and cutting fluid, and cooling performance are good, are suitable forIn the processing of high-precision workpiece, not only yield rate is high, and cutting speed is fast.
Detailed description of the invention
A kind of wear-resistant micro emulsion cutting fluid, by following weight portion (kilogram) raw material make: petroleum sodium sulfonate 2.5,Oleic acid 3.5, triethanolamine 1.5, APES 3.5, benzotriazole 1.5, sodium tetraborate2.5, sodium carbonate 1.5, ethanol 33, kerosene 11, sodium alginate 1.5, auxiliary agent 7, water 200; Described helpsAgent by following weight portion (kilogram) raw material make: Tween-81 3, nanometer nitrogenChange aluminium 0.1, carbonic hydroammonium 3, monoethanolamine 1, CMC 2, diethylene glycol butyl ether 1, propane diols 8,Peach gum 3, sodium metasilicate 1, urea 4, ammonium persulfate 2, water 20; Preparation method is that ammonium persulfate is water-solubleAfter, then add other leftover materials, and stir 10-15 minute, be heated to 70-80 DEG C, stirring reaction 1-2 is littleTime, to obtain final product.
The preparation method of described wear-resistant micro emulsion cutting fluid, comprises the following steps: by water, petroleum sodium sulfonate, alkylPhenol polyethenoxy ether, sodium carbonate, sodium alginate mix, and are heated to 45 DEG C; Add oleic acid, kerosene, ethanol,Auxiliary agent continues to be heated to 75 DEG C under 1100 revs/min of stirrings, stirs 13 minutes; Add other residual components,Continue to stir 16 minutes, to obtain final product.
The wear-resistant micro emulsion cutting fluid test data that this embodiment obtains is as follows:
Claims (2)
1. a wear-resistant micro emulsion cutting fluid, is characterized in that being made up of the raw material of following weight portion: petroleum sodium sulfonate 2-3, oleic acid 3-4, triethanolamine 1-2, APES 3-4, benzotriazole 1-2, sodium tetraborate 2-3, sodium carbonate 1-2, ethanol 30-35, kerosene 10-12, sodium alginate 1-2, auxiliary agent 6-8, water 200; Described auxiliary agent is made up of the raw material of following weight portion: Tween-81 2-3, nano aluminum nitride 0.1-0.2, carbonic hydroammonium 2-3, monoethanolamine 1-2, CMC 2-3, diethylene glycol butyl ether 1-2, propane diols 5-8, peach gum 2-3, sodium metasilicate 1-2, urea 3-4, ammonium persulfate 1-2, water 20-24; Preparation method be ammonium persulfate is water-soluble after, then add other leftover materials, stir 10-15 minute, be heated to 70-80 DEG C, stirring reaction 1-2 hour, to obtain final product.
2. the preparation method of wear-resistant micro emulsion cutting fluid according to claim 1, is characterized in that comprising the following steps: water, petroleum sodium sulfonate, APES, sodium carbonate, sodium alginate are mixed, be heated to 40-50 DEG C; Add oleic acid, kerosene, ethanol, auxiliary agent, under 1000-1200 rev/min of stirring, continue to be heated to 70-80 DEG C, stir 10-15 minute; Add other residual components, continue to stir 14-18 minute, to obtain final product.
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| CN201310653265.7A CN103756771B (en) | 2013-12-06 | 2013-12-06 | A kind of wear-resistant micro emulsion cutting fluid and preparation method thereof |
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| CN201310653265.7A CN103756771B (en) | 2013-12-06 | 2013-12-06 | A kind of wear-resistant micro emulsion cutting fluid and preparation method thereof |
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| CN103756771B true CN103756771B (en) | 2016-05-04 |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104120014B (en) * | 2014-06-30 | 2016-05-04 | 安徽铖友汽车零部件制造有限公司 | Environment-friendly water-based cutting fluid of a kind of rust-proof effect excellence and preparation method thereof |
| CN104388172A (en) * | 2014-10-31 | 2015-03-04 | 无锡阳工机械制造有限公司 | Metal cutting fluid |
| CN104560348A (en) * | 2014-12-30 | 2015-04-29 | 繁昌县新科精密模具厂 | Novel cutting fluid with good lubricating and cooling effect and preparation method thereof |
| CN104560331A (en) * | 2014-12-30 | 2015-04-29 | 繁昌县新科精密模具厂 | A kind of multifunctional water-based cutting fluid with wide application range and preparation method thereof |
| CN104560327A (en) * | 2014-12-30 | 2015-04-29 | 芜湖市润雨精密机械有限公司 | High-permeability metal cutting fluid with excellent corrosion resistance and preparation method of metal cutting fluid |
| CN104560329A (en) * | 2014-12-30 | 2015-04-29 | 芜湖市润雨精密机械有限公司 | Metal cutting fluid with good rust prevention and mildewproof effects and preparation method of metal cutting fluid |
| CN105296123A (en) * | 2015-11-25 | 2016-02-03 | 苏州捷德瑞精密机械有限公司 | Rapid cooling cutting fluid and preparation method thereof |
| CN109810769A (en) * | 2017-11-21 | 2019-05-28 | 常州市好利莱光电科技有限公司 | A kind of preparation method of aqueous cutting fluid |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101240217A (en) * | 2008-02-29 | 2008-08-13 | 益田润石（北京）化工有限公司 | Micro-emulsion type metal cutting liquor composition |
| CN102618358A (en) * | 2012-03-06 | 2012-08-01 | 上海应用技术学院 | Green micro-emulsification metal machining liquid and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP5232372B2 (en) * | 2006-09-26 | 2013-07-10 | 株式会社ネオス | Water-soluble metalworking fluid composition |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101240217A (en) * | 2008-02-29 | 2008-08-13 | 益田润石（北京）化工有限公司 | Micro-emulsion type metal cutting liquor composition |
| CN102618358A (en) * | 2012-03-06 | 2012-08-01 | 上海应用技术学院 | Green micro-emulsification metal machining liquid and preparation method thereof |
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Address after: Concentrated area of Taibai town 243181 Anhui city of Ma'anshan province Dangtu County Industrial Applicant after: DANGTU COUNTY JINLONG MACHINERY Co., Ltd. Address before: Concentrated area of Taibai town 243181 Anhui city of Ma'anshan province Dangtu County Industrial Applicant before: DANGTU COUNTY JINLONG MACHINERY PLANT |
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Denomination of invention: The invention relates to an anti-wear Microemulsion Cutting Fluid and a preparation method thereof Effective date of registration: 20210817 Granted publication date: 20160504 Pledgee: Anhui Ma'anshan Rural Commercial Bank Co., Ltd Pledgor: DANTU JINLONG MACHINERY Co.,Ltd. Registration number: Y2021980007815 |
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Address after: 243181 industrial concentration zone, Taibai Town, Dangtu County, Ma'anshan City, Anhui Province Patentee after: Dangtu jinlongfeng Technology Co.,Ltd. Address before: 243181 industrial concentration zone, Taibai Town, Dangtu County, Ma'anshan City, Anhui Province Patentee before: DANTU JINLONG MACHINERY CO.,LTD. |
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