CN103711004B - A kind of coloring agent not easy to fade - Google Patents
A kind of coloring agent not easy to fade Download PDFInfo
- Publication number
- CN103711004B CN103711004B CN201310748996.XA CN201310748996A CN103711004B CN 103711004 B CN103711004 B CN 103711004B CN 201310748996 A CN201310748996 A CN 201310748996A CN 103711004 B CN103711004 B CN 103711004B
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- CN
- China
- Prior art keywords
- coloring agent
- parts
- easy
- fade
- triethanolamine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000003086 colorant Substances 0.000 title claims abstract description 21
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims abstract description 30
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims abstract description 20
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims abstract description 20
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000004094 surface-active agent Substances 0.000 claims abstract description 12
- SJIXRGNQPBQWMK-UHFFFAOYSA-N 2-(diethylamino)ethyl 2-methylprop-2-enoate Chemical compound CCN(CC)CCOC(=O)C(C)=C SJIXRGNQPBQWMK-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims abstract description 10
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 claims abstract description 10
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims abstract description 10
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 10
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims abstract description 10
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 6
- -1 cetyl naphthalene sulfonic acids amine Chemical class 0.000 claims description 10
- DUXYWXYOBMKGIN-UHFFFAOYSA-N trimyristin Chemical compound CCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCC DUXYWXYOBMKGIN-UHFFFAOYSA-N 0.000 claims description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 3
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 3
- BNCADMBVWNPPIZ-UHFFFAOYSA-N 2-n,2-n,4-n,4-n,6-n,6-n-hexakis(methoxymethyl)-1,3,5-triazine-2,4,6-triamine Chemical compound COCN(COC)C1=NC(N(COC)COC)=NC(N(COC)COC)=N1 BNCADMBVWNPPIZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000002156 mixing Methods 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 239000004744 fabric Substances 0.000 description 3
- 241000322338 Loeseliastrum Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012128 staining reagent Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
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- Coloring (AREA)
Abstract
The invention discloses a kind of coloring agent not easy to fade, comprise the raw material of following parts by weight: dibutyl phthalate 20-30 part, oxydiphthalic 40-50 part, dimethyl formamide 20-30 part, diethyl aminoethyl methacrylate 20-40 part, dibutyl tin laurate 20-50 part, calcium sulfate 10-20 part, triethanolamine 20-50 part, Carboxymethyl Cellulose 50-60 part, barba hispanica 10-20 part, trimethylolpropane 20-30 part, hexamethoxy methyl melamine 20-25 part, initator 10-20 part, surfactant 10-20 part, water 50-80 part.Adopt coloring agent of the present invention, its soaping fastness is in 4.5-5.0 level, and coloring agent combines firmly, and not fugitive color, K/S value is up to 8.215, and dyeability is good.
Description
Technical field
The present invention relates to weaving face fabric colouring art, particularly relate to a kind of coloring agent not easy to fade.
Background technology
Garment material presents colourful, is by after dyeing to calico, just can presents shades of colour, but general staining reagent effect is bad, usually need to carry out fixation to it, but even if general industrial chemicals is after fixation, still easily fade through repeatedly washing.
Summary of the invention
The present invention is directed to the deficiencies in the prior art, provide a kind of coloring agent not easy to fade, coloring agent and fabric combine firmly, not fugitive color.
The present invention is by the following technical solutions:
A kind of coloring agent not easy to fade, comprises the raw material of following parts by weight: dibutyl phthalate 20-30 part, oxydiphthalic 40-50 part, dimethyl formamide 20-30 part, diethyl aminoethyl methacrylate 20-40 part, dibutyl tin laurate 20-50 part, calcium sulfate 10-20 part, triethanolamine 20-50 part, Carboxymethyl Cellulose 50-60 part, barba hispanica 10-20 part, trimethylolpropane 20-30 part, HMMM 20-25 part, initator 10-20 part, surfactant 10-20 part, water 50-80 part.
As preferably, initator is azo-bis-iso-butyl or MEK.
As preferably, surfactant is the one in cetyl naphthalene sulfonic acids amine, triethanolamine myristin or pentaerythrite monoacetate.
The preparation method of coloring agent not easy to fade, dibutyl phthalate, oxydiphthalic, dimethyl formamide, diethyl aminoethyl methacrylate are mixed, add initator, surfactant, water, stir, then dibutyl tin laurate, calcium sulfate, triethanolamine, Carboxymethyl Cellulose, barba hispanica, trimethylolpropane, HMMM is added, mixing.
Beneficial effect of the present invention: adopt coloring agent of the present invention, its soaping fastness is in 4.5-5.0 level, and coloring agent combines firmly, and not fugitive color, K/S value is up to 8.215, and dyeability is good.
Detailed description of the invention
Below by specific embodiment, the present invention is further explained in detail.
Embodiment 1
A kind of coloring agent not easy to fade, comprises the raw material of following parts by weight: dibutyl phthalate 20 parts, oxydiphthalic 40 parts, dimethyl formamide 20 parts, diethyl aminoethyl methacrylate 20 parts, dibutyl tin laurate 20 parts, 10 parts, calcium sulfate, triethanolamine 20 parts, Carboxymethyl Cellulose 50 parts, barba hispanica 10 parts, trimethylolpropane 20 parts, HMMM 20 parts, initator azo-bis-iso-butyl 10 parts, surfactant cetyl naphthalene sulfonic acids amine 10 parts, 50 parts, water.
Preparation method, dibutyl phthalate, oxydiphthalic, dimethyl formamide, diethyl aminoethyl methacrylate are mixed, add initator, surfactant, water, stir, then dibutyl tin laurate, calcium sulfate, triethanolamine, Carboxymethyl Cellulose, barba hispanica, trimethylolpropane, HMMM is added, mixing.
Embodiment 2
A kind of coloring agent not easy to fade, comprises the raw material of following parts by weight: dibutyl phthalate 30 parts, oxydiphthalic 50 parts, dimethyl formamide 30 parts, diethyl aminoethyl methacrylate 40 parts, dibutyl tin laurate 50 parts, 20 parts, calcium sulfate, triethanolamine 50 parts, Carboxymethyl Cellulose 60 parts, barba hispanica 20 parts, trimethylolpropane 30 parts, HMMM 25 parts, initator MEK 20 parts, surfactant triethanolamine myristin 20 parts, 80 parts, water.
Preparation method, dibutyl phthalate, oxydiphthalic, dimethyl formamide, diethyl aminoethyl methacrylate are mixed, add initator, surfactant, water, stir, then dibutyl tin laurate, calcium sulfate, triethanolamine, Carboxymethyl Cellulose, barba hispanica, trimethylolpropane, HMMM is added, mixing.
Embodiment 3
A kind of coloring agent not easy to fade, comprises the raw material of following parts by weight: dibutyl phthalate 25 parts, oxydiphthalic 45 parts, dimethyl formamide 25 parts, diethyl aminoethyl methacrylate 30 parts, dibutyl tin laurate 40 parts, 15 parts, calcium sulfate, triethanolamine 30 parts, Carboxymethyl Cellulose 55 parts, barba hispanica 15 parts, trimethylolpropane 25 parts, HMMM 23 parts, initator azo-bis-iso-butyl 15 parts, surfactant pentaerythrite monoacetate 15 parts, 65 parts, water.
Preparation method, dibutyl phthalate, oxydiphthalic, dimethyl formamide, diethyl aminoethyl methacrylate are mixed, add initator, surfactant, water, stir, then dibutyl tin laurate, calcium sulfate, triethanolamine, Carboxymethyl Cellulose, barba hispanica, trimethylolpropane, HMMM is added, mixing.
Performance parameter of the present invention: three pieces of identical fabrics are put into respectively the coloring agent that embodiment 1-3 makes, be warming up to 90 DEG C of insulation reaction 5h, measure K/S value and soaping fastness after cooling.
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| K/S value | 8.215 | 7.851 | 7.963 |
| Soaping fastness (level) | 4.5-5.0 | 4.5-5.0 | 4.5-5.0 |
As from the foregoing, adopt coloring agent of the present invention, its soaping fastness is in 4.5-5.0 level, and coloring agent combines firmly, and not fugitive color, K/S value is up to 8.215, and dyeability is good.
Claims (3)
1. a coloring agent not easy to fade, is characterized in that: the raw material comprising following parts by weight: dibutyl phthalate 20-30 part, oxydiphthalic 40-50 part, dimethyl formamide 20-30 part, diethyl aminoethyl methacrylate 20-40 part, dibutyl tin laurate 20-50 part, calcium sulfate 10-20 part, triethanolamine 20-50 part, Carboxymethyl Cellulose 50-60 part, barba hispanica 10-20 part, trimethylolpropane 20-30 part, HMMM 20-25 part, initator 10-20 part, surfactant 10-20 part, water 50-80 part.
2. coloring agent not easy to fade according to claim 1, is characterized in that: initator is azo-bis-iso-butyl or MEK.
3. coloring agent not easy to fade according to claim 1, is characterized in that: surfactant is the one in cetyl naphthalene sulfonic acids amine, triethanolamine myristin or pentaerythrite monoacetate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310748996.XA CN103711004B (en) | 2013-12-31 | 2013-12-31 | A kind of coloring agent not easy to fade |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310748996.XA CN103711004B (en) | 2013-12-31 | 2013-12-31 | A kind of coloring agent not easy to fade |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103711004A CN103711004A (en) | 2014-04-09 |
| CN103711004B true CN103711004B (en) | 2015-11-04 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310748996.XA Active CN103711004B (en) | 2013-12-31 | 2013-12-31 | A kind of coloring agent not easy to fade |
Country Status (1)
| Country | Link |
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| CN (1) | CN103711004B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106498771A (en) * | 2016-11-17 | 2017-03-15 | 无锡奔牛生物科技有限公司 | A kind of human body affinity fabric dyeing toner |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104358147A (en) * | 2014-10-20 | 2015-02-18 | 江苏金牛华尔车服饰有限公司 | Fabric coloring agent |
| CN104313909B (en) * | 2014-10-20 | 2016-08-31 | 江苏金牛华尔车服饰有限公司 | Weaving face fabric stain |
| CN106120398A (en) * | 2016-07-18 | 2016-11-16 | 南通富之岛寝具发展有限公司 | Dyeing agent for textile fabrics |
| CN106192476A (en) * | 2016-07-18 | 2016-12-07 | 南通富之岛寝具发展有限公司 | Dyeing agent for textile fabrics |
| CN106120399A (en) * | 2016-07-18 | 2016-11-16 | 南通富之岛寝具发展有限公司 | a fabric dye |
| CN106337301A (en) * | 2016-08-25 | 2017-01-18 | 常熟市华谊织造有限公司 | Wool fabric dyeing method |
| CN108103804A (en) * | 2017-12-25 | 2018-06-01 | 重庆市沁元康虹服饰有限公司 | A kind of dyeing fabric agent prescription and preparation method thereof |
| CN108221411A (en) * | 2018-01-24 | 2018-06-29 | 吴晓丽 | A kind of woven fabric environmental protection dyeing and printing process |
| CN108642917A (en) * | 2018-05-18 | 2018-10-12 | 霍山县佛子岭伟远新型建材厂 | A kind of industrial ground coloring agent and colouring method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2017765A (en) * | 1978-02-21 | 1979-10-10 | Manmade Fibres Res Assoc | Dyeing of textile materials |
| CN1247055A (en) * | 1998-07-17 | 2000-03-15 | 莱雅公司 | Face-care compsns. containing pigment and anti-sweat agent, and application of same composns. |
| CN1687252A (en) * | 2005-05-18 | 2005-10-26 | 江南大学 | Method for preparing Nano dye |
| CN101338523A (en) * | 2007-12-03 | 2009-01-07 | 浙江誉华集团湖州印染有限公司 | Apposition dyeing additive for blended fabric of PTT fibre and cellulose fibre |
| CN102352560A (en) * | 2011-07-28 | 2012-02-15 | 吴江征明纺织有限公司 | Textile flame-retardant finishing agent and preparation method thereof |
-
2013
- 2013-12-31 CN CN201310748996.XA patent/CN103711004B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2017765A (en) * | 1978-02-21 | 1979-10-10 | Manmade Fibres Res Assoc | Dyeing of textile materials |
| CN1247055A (en) * | 1998-07-17 | 2000-03-15 | 莱雅公司 | Face-care compsns. containing pigment and anti-sweat agent, and application of same composns. |
| CN1687252A (en) * | 2005-05-18 | 2005-10-26 | 江南大学 | Method for preparing Nano dye |
| CN101338523A (en) * | 2007-12-03 | 2009-01-07 | 浙江誉华集团湖州印染有限公司 | Apposition dyeing additive for blended fabric of PTT fibre and cellulose fibre |
| CN102352560A (en) * | 2011-07-28 | 2012-02-15 | 吴江征明纺织有限公司 | Textile flame-retardant finishing agent and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106498771A (en) * | 2016-11-17 | 2017-03-15 | 无锡奔牛生物科技有限公司 | A kind of human body affinity fabric dyeing toner |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103711004A (en) | 2014-04-09 |
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