CN103706691B - Electronic universal tester is utilized to carry out sheet metal bending forming method - Google Patents
Electronic universal tester is utilized to carry out sheet metal bending forming method Download PDFInfo
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- 238000005452 bending Methods 0.000 title claims abstract description 113
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 47
- 239000002184 metal Substances 0.000 title claims abstract description 47
- 238000000034 method Methods 0.000 title claims abstract description 32
- 238000012360 testing method Methods 0.000 claims abstract description 19
- 238000006073 displacement reaction Methods 0.000 claims abstract description 18
- 238000010438 heat treatment Methods 0.000 claims abstract description 5
- 229910001069 Ti alloy Inorganic materials 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 5
- 238000013461 design Methods 0.000 claims description 2
- 238000004826 seaming Methods 0.000 claims 3
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- 238000003825 pressing Methods 0.000 description 8
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- 238000004519 manufacturing process Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000004590 computer program Methods 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
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- 238000005516 engineering process Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
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- 238000003856 thermoforming Methods 0.000 description 1
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Abstract
利用电子万能试验机进行金属板材弯曲成形方法,以解决现有金属板材成形后回弹严重需要校形的问题。装置:定位螺孔中螺纹连接一个定位螺栓,弯曲下模设置在下模通槽中,圆弧通槽对应的弯曲下模两端侧壁上对称设有试样定位槽,弯曲上模的下端设置在下模通槽中。方法:一、将金属板材弯曲成形装置安装在电子万能试验机上;二、加工出适合上模和下模尺寸的试样;三、设置电子试验机的控制程序:设置控制程序包括加载阶段和位移保持阶段;四、对弯曲上模和弯曲下模加热;五、成形试样置于炉内的金属板材弯曲成形装置上;六、利用电子试验机对金属板材弯曲成形装置加载;七、取出试样,即完成一个金属板材弯曲成形。本发明用于金属板材弯曲成形。
A metal plate bending forming method is carried out by using an electronic universal testing machine to solve the problem that the existing metal plate needs to be corrected due to serious springback after forming. Device: a positioning bolt is threaded in the positioning screw hole, the lower bending die is set in the through groove of the lower die, the side walls of both ends of the lower bending die corresponding to the circular arc through groove are symmetrically provided with sample positioning grooves, and the lower end of the bending upper die is set In the lower die through groove. Method: 1. Install the metal plate bending forming device on the electronic universal testing machine; 2. Process samples suitable for the size of the upper and lower dies; 3. Set the control program of the electronic testing machine: set the control program including the loading stage and displacement Holding stage; 4. Heating the bending upper die and bending lower die; 5. Place the formed sample on the sheet metal bending forming device in the furnace; 6. Use the electronic testing machine to load the sheet metal bending forming device; 7. Take out the test piece In this way, a sheet metal bending is completed. The invention is used for bending forming of sheet metal.
Description
技术领域technical field
本发明涉及一种金属板材弯曲成形方法,具体涉及一种利用电子万能试验机进行金属板材弯曲成形方法。The invention relates to a metal plate bending forming method, in particular to a metal plate bending forming method using an electronic universal testing machine.
背景技术Background technique
板材零件广泛应用于航空、航天、舰船及汽车等领域,如飞机的钛合金鳍板、铝合金壁板、汽车钢板覆盖件等,但是这些材料弹性模量低,成形出的零件回弹严重,影响了工件的成形精度,降低了产品质量。为了获得高精度、高质量的板材零部件,传统的方法是在零件的大批量生产之前,在压力机上对零件进行大量的不同成形工艺条件下的研制试验,以获得最佳的成形工艺,包括最佳的热成形参数(成形温度、成形速度等)、热校形参数(保压载荷、保压时间等),以及最佳的冷却方式(空冷、炉冷等)。但是这样直接在压力机上对同尺寸零件进行研制以获得最佳成形工艺存在严重缺点:生产成本高、研制周期长,会浪费大量的人力和物力。另外,板材成形时如果模具内没有合理的定位装置,则成形过程中零件会偏移,造成成形出的零件形状、尺寸与设计要求偏差较大,导致产品报废。急需提出能够大幅度降低生产成本、缩短研制周期和降低废品率的成形装置和成形方法。Plate parts are widely used in the fields of aviation, aerospace, ships and automobiles, such as titanium alloy fins of aircraft, aluminum alloy siding, automobile steel plate coverings, etc., but these materials have low elastic modulus, and the formed parts have serious springback , which affects the forming accuracy of the workpiece and reduces the product quality. In order to obtain high-precision, high-quality plate parts, the traditional method is to carry out a large number of development tests on the parts under different forming process conditions on the press before the mass production of the parts, so as to obtain the best forming process, including The best thermoforming parameters (forming temperature, forming speed, etc.), thermal correction parameters (holding load, holding time, etc.), and the best cooling method (air cooling, furnace cooling, etc.). However, there are serious disadvantages in developing the same size parts directly on the press to obtain the best forming process: high production cost, long development cycle, and a lot of manpower and material resources will be wasted. In addition, if there is no reasonable positioning device in the mold when the sheet is formed, the parts will shift during the forming process, resulting in large deviations in the shape and size of the formed parts from the design requirements, resulting in product scrapping. There is an urgent need to propose a forming device and a forming method that can greatly reduce production costs, shorten the development cycle and reduce the scrap rate.
发明内容Contents of the invention
本发明为解决解决现有金属板材成形成本高、研制周期长,成形后回弹严重需要校形的问题,而提供一种利用电子万能试验机进行金属板材弯曲成形方法。In order to solve the problems of high forming cost, long development cycle and severe springback after forming, the present invention provides a metal sheet bending forming method using an electronic universal testing machine.
装置:利用电子万能试验机进行金属板材弯曲成形装置包括弯曲上模、弯曲下模、下模座、上螺母、下螺母和两个定位螺栓,下模座的下端设有下连接螺栓,下模座的上端设有下模通槽,下模通槽对应的下模座侧壁上对称设有定位螺孔,每个定位螺孔中螺纹连接一个定位螺栓,弯曲下模设置在下模通槽中,弯曲下模的上端面设有圆弧通槽,圆弧通槽对应的弯曲下模两端侧壁上对称设有试样定位槽,弯曲上模的上端设有上连接螺栓,弯曲上模的下端设有圆弧面,上螺母与上连接螺栓螺纹连接,下螺母与下连接螺栓螺纹连接,弯曲上模的下端设置在下模通槽中。Device: The metal plate bending forming device using an electronic universal testing machine includes a bending upper die, a bending lower die, a lower die base, an upper nut, a lower nut and two positioning bolts. The lower end of the lower die base is provided with a lower connecting bolt. The upper end of the seat is provided with a lower mold through groove, and positioning screw holes are symmetrically arranged on the side wall of the lower mold base corresponding to the lower mold through groove, and a positioning bolt is threaded in each positioning screw hole, and the bending lower mold is arranged in the lower mold through groove , the upper end surface of the lower bending die is provided with arc through grooves, and the side walls of both ends of the lower bending die corresponding to the arc through grooves are symmetrically provided with sample positioning grooves, and the upper end of the bending upper die is provided with upper connecting bolts, and the upper end of the bending upper die is provided with upper connecting bolts. The lower end of the curved upper die is provided with an arc surface, the upper nut is threaded with the upper connecting bolt, the lower nut is threaded with the lower connecting bolt, and the lower end of the bending upper die is arranged in the through groove of the lower die.
方法:利用电子万能试验机进行金属板材弯曲成形方法是通过以下步骤实现:Method: The metal plate bending forming method is realized through the following steps by using an electronic universal testing machine:
步骤一、安装金属板材弯曲成形装置:将金属板材弯曲成形装置安装在电子万能试验机上,上连接螺栓旋入上压头中,下连接螺栓旋入下压头中,将弯曲下模水平放置在下模座的下模通槽上,控制横梁缓慢上行,并调节弯曲下模与弯曲上模对正接触,调整接触力为1000N,分别从下模座侧壁的定位螺孔旋入定位螺栓,使弯曲下模固定,向着上压头端面拧紧上螺母将弯曲上模紧固到上压头,朝着下压头端面拧紧下螺母将下模座紧固到下压头,控制横梁使弯曲上模与弯曲下模分开一段距离;Step 1. Install the metal sheet bending forming device: install the metal sheet bending forming device on the electronic universal testing machine, screw the upper connecting bolt into the upper pressing head, screw the lower connecting bolt into the lower pressing head, and place the lower bending die horizontally on the lower pressing head. On the lower mold channel of the mold base, control the beam to move upward slowly, and adjust the bending lower mold and the bending upper mold to align and contact, adjust the contact force to 1000N, and screw the positioning bolts respectively from the positioning screw holes on the side wall of the lower mold base to The lower bending die is fixed, the upper nut is tightened toward the end face of the upper die to fasten the upper die to the upper die, the lower nut is tightened toward the end face of the lower die to fasten the lower die holder to the lower die, and the crossbeam is controlled to make the upper die bend Separate a distance from the bending die;
步骤二、准备成形试样:选定钛合金板料做为成形坯料,并加工出适合上模和下模尺寸的试样;Step 2. Prepare the forming sample: select the titanium alloy sheet as the forming blank, and process a sample suitable for the size of the upper mold and the lower mold;
步骤三、设置电子试验机的控制程序:设置控制程序包括加载阶段和位移保持阶段:Step 3. Set the control program of the electronic testing machine: set the control program including the loading phase and the displacement holding phase:
a、加载阶段横梁的速度设定为5mm/min~15mm/min,设定加载力达到3500N后加载结束;a. The speed of the crossbeam in the loading stage is set at 5mm/min~15mm/min, and the loading ends after the set loading force reaches 3500N;
b、位移保持阶段设定校形持续时间为10min~20min,加载力保持500N恒定,数据采集频率设定为200ms;b. In the displacement maintenance stage, set the duration of the correction to 10min to 20min, keep the loading force constant at 500N, and set the data acquisition frequency to 200ms;
步骤四、对弯曲上模和弯曲下模加热:移动三段式对开电阻炉的电阻炉膛中段位于金属板材弯曲成形装置处,闭合炉门,设定三段式对开电阻炉的温度为600℃~800℃,利用三段式对开电阻炉对弯曲上模和弯曲下模加热;Step 4. Heating the bending upper mold and bending lower mold: move the middle section of the resistance furnace of the three-stage split resistance furnace to the metal plate bending forming device, close the furnace door, and set the temperature of the three-stage split resistance furnace to 600 ℃~800℃, using a three-stage split resistance furnace to heat the bending upper mold and bending lower mold;
步骤五、成形试样置于炉内的金属板材弯曲成形装置上:三段式对开电阻炉内温度达到设定温度后,打开三段式对开电阻炉的炉门,放置钛合金板料,使其置于试样定位槽中,迅速关闭炉门,在计算机的程序控制界面重置载荷清零,手动控制横梁缓慢上升以带动弯曲下模上移,直至试样表面与弯曲下模接触,以观察到载荷传感器有载荷增加为准,通过位移传感器来重置横梁位移清零,继续保温5min;Step 5. The formed sample is placed on the metal plate bending forming device in the furnace: after the temperature in the three-stage split resistance furnace reaches the set temperature, open the furnace door of the three-stage split resistance furnace and place the titanium alloy sheet , put it in the sample positioning groove, quickly close the furnace door, reset the load to zero on the computer program control interface, and manually control the beam to rise slowly to drive the lower bending die upward until the surface of the sample is in contact with the lower bending die , based on the observation that the load of the load sensor has increased, the displacement of the crossbeam is reset to zero through the displacement sensor, and the heat preservation is continued for 5 minutes;
步骤六、利用电子试验机对金属板材弯曲成形装置加载:保温时间到后启动设置好的控制程序并对金属板材弯曲成形装置加载;Step 6. Use the electronic testing machine to load the sheet metal bending forming device: after the holding time is up, start the set control program and load the sheet metal bending forming device;
步骤七、取出试样:成形结束后,打开三段式对开电阻炉的炉门,手动控制横梁下移卸载,迅速取出试样空冷,冷却10min,即完成一个金属板材弯曲成形。Step 7. Take out the sample: After forming, open the furnace door of the three-stage split resistance furnace, manually control the beam to move down and unload, quickly take out the sample and air-cool, cool for 10 minutes, and then complete the bending and forming of a metal sheet.
本发明与传统板材弯曲技术相比具有以下有益效果:Compared with the traditional plate bending technology, the present invention has the following beneficial effects:
一、本发明装置中的试样定位槽可使板料实现快速精确定位,设计的下模座可保证弯曲上模与弯曲下模快速装配及对中,而且成形不同零件时下模座均可使用,从而降低金属板材成形的生产成本和研制周期,并快速确定板材的最佳成形工艺。1. The sample positioning groove in the device of the present invention can realize fast and accurate positioning of the sheet metal, and the designed lower mold base can ensure the fast assembly and alignment of the bending upper mold and the bending lower mold, and the lower mold base can be used when forming different parts , so as to reduce the production cost and development cycle of sheet metal forming, and quickly determine the best forming process of sheet metal.
二、本发明利用定位螺栓调节弯曲下模的左右位置,以使弯曲下模与弯曲上模轴线快速对中,节省了大量装置轴线对中的调节时间。2. The present invention uses positioning bolts to adjust the left and right positions of the lower bending die, so that the axes of the lower bending die and the upper bending die can be quickly centered, saving a lot of adjustment time for the centering of the device axes.
三、利用本发明方法中的工艺参数对金属板材进行加载成形,成形后的工件回弹小,实现了板材零件的精密成形。3. Utilizing the process parameters in the method of the present invention to carry out loading and forming on the metal plate, the workpiece after forming has small rebound, and realizes the precision forming of the plate parts.
附图说明Description of drawings
图1是本发明的整个结构主视图;图2是下模座3的主视图;图3是图2的左视图;图4是图2的俯视图,图5是弯曲上模1的主视图;图6是图5的左视图;图7是弯曲下模2的主视图;图8是图7的左视图;图9是图7的俯视图;图10是具体实施方式三的结构主视图。Fig. 1 is a front view of the entire structure of the present invention; Fig. 2 is a front view of the lower die base 3; Fig. 3 is a left view of Fig. 2; Fig. 4 is a top view of Fig. 2, and Fig. 5 is a front view of a curved upper die 1; Fig. 6 is a left view of Fig. 5; Fig. 7 is a front view of the lower bending die 2; Fig. 8 is a left view of Fig. 7; Fig. 9 is a top view of Fig. 7; Fig. 10 is a structural front view of the third embodiment.
具体实施方式Detailed ways
具体实施方式一:结合图1~图9说明本实施方式,本实施方式包括弯曲上模1、弯曲下模2、下模座3、上螺母4、下螺母5和两个定位螺栓6,下模座3的下端设有下连接螺栓3-1,下模座3的上端设有下模通槽3-2,下模通槽3-2对应的下模座3侧壁上对称设有定位螺孔3-3,每个定位螺孔3-3中螺纹连接一个定位螺栓6,弯曲下模2设置在下模通槽3-2中,弯曲下模2的上端面设有圆弧通槽2-1,圆弧通槽2-1对应的弯曲下模2两端侧壁上对称设有试样定位槽2-2,试样定位槽2-2用于支撑工件,弯曲上模1的上端设有上连接螺栓1-1,弯曲上模1的下端设有圆弧面1-2,上螺母4与上连接螺栓1-1螺纹连接,下螺母5与下连接螺栓3-1螺纹连接,弯曲上模1的下端设置在下模通槽3-2中。Specific embodiment 1: This embodiment is described in conjunction with Fig. 1 to Fig. 9. This embodiment includes a bending upper mold 1, a bending lower mold 2, a lower mold base 3, an upper nut 4, a lower nut 5 and two positioning bolts 6, the lower The lower end of the mold base 3 is provided with a lower connecting bolt 3-1, the upper end of the lower mold base 3 is provided with a lower mold through groove 3-2, and the lower mold base 3 side wall corresponding to the lower mold through groove 3-2 is symmetrically provided with positioning Screw holes 3-3, each positioning screw hole 3-3 is threaded to connect a positioning bolt 6, the bending lower die 2 is arranged in the lower die through groove 3-2, and the upper end surface of the bending lower die 2 is provided with an arc through groove 2 -1, the arc groove 2-1 is symmetrically provided with sample positioning grooves 2-2 on the side walls at both ends of the bending lower die 2, the sample positioning grooves 2-2 are used to support the workpiece, and the upper end of the bending upper die 1 There is an upper connecting bolt 1-1, the lower end of the curved upper die 1 is provided with an arc surface 1-2, the upper nut 4 is threaded with the upper connecting bolt 1-1, the lower nut 5 is threaded with the lower connecting bolt 3-1, The lower end of the bending upper die 1 is arranged in the lower die through groove 3-2.
具体实施方式二:结合图1说明本实施方式,本实施方式的弯曲上模1、弯曲下模2、下模座3、上螺母4、下螺母5和两个定位螺栓6均为4Cr5MoSiV。这种材质耐高温,可以在900℃以下使用。其它组成及连接关系与具体实施方式一相同。Specific Embodiment 2: This embodiment is described in conjunction with FIG. 1 . The bending upper die 1, bending lower die 2, lower die holder 3, upper nut 4, lower nut 5 and two positioning bolts 6 of this embodiment are all 4Cr5MoSiV. This material is resistant to high temperatures and can be used below 900°C. Other components and connections are the same as those in the first embodiment.
具体实施方式三:结合图10说明本实施方式,本实施方式是利用具体实施方式一的装置实现金属材料变截面挤扭成形的方法,其步骤如下:Specific embodiment three: This embodiment is described in conjunction with FIG. 10. This embodiment is a method for realizing variable cross-section extrusion and twisting of metal materials using the device of specific embodiment one. The steps are as follows:
步骤一、安装金属板材弯曲成形装置:将金属板材弯曲成形装置安装在电子万能试验机上,上连接螺栓1-1旋入上压头7中,下连接螺栓3-1旋入下压头8中,将弯曲下模2水平放置在下模座3的下模通槽3-2上,控制横梁9缓慢上行,并调节弯曲下模2与弯曲上模1对正接触,调整接触力为1000N,分别从下模座3侧壁的定位螺孔旋入定位螺栓6,使弯曲下模2固定,向着上压头端面拧紧上螺母4将弯曲上模1紧固到上压头7,朝着下压头端面拧紧下螺母5将下模座3紧固到下压头8,控制横梁9使弯曲上模1与弯曲下模2分开一段距离,该距离以方便放置试件即可;Step 1. Install the sheet metal bending forming device: install the sheet metal bending forming device on the electronic universal testing machine, screw the upper connecting bolt 1-1 into the upper pressing head 7, and screw the lower connecting bolt 3-1 into the lower pressing head 8 , place the bending lower die 2 horizontally on the lower die channel 3-2 of the lower die holder 3, control the beam 9 to move upward slowly, and adjust the bending lower die 2 to be in positive contact with the bending upper die 1, and adjust the contact force to 1000N, respectively Screw in the positioning bolt 6 from the positioning screw hole on the side wall of the lower mold base 3 to fix the curved lower mold 2, tighten the upper nut 4 towards the end face of the upper pressing head to fasten the bending upper mold 1 to the upper pressing head 7, and press down Tighten the lower nut 5 on the end face of the head to fasten the lower mold base 3 to the lower pressing head 8, and control the crossbeam 9 to separate the bending upper mold 1 from the bending lower mold 2 by a certain distance, which is enough for the convenience of placing the test piece;
步骤二、准备成形试样:选定钛合金板料做为成形坯料,并加工出适合上模和下模尺寸的试样;Step 2. Prepare the forming sample: select the titanium alloy sheet as the forming blank, and process a sample suitable for the size of the upper mold and the lower mold;
步骤三、设置电子试验机的控制程序:设置控制程序包括加载阶段和位移保持阶段:Step 3. Set the control program of the electronic testing machine: set the control program including the loading phase and the displacement holding phase:
a、加载阶段横梁9的速度设定为5mm/min~15mm/min,设定加载力达到3500N后加载结束;a. The speed of beam 9 is set at 5 mm/min to 15 mm/min during the loading stage, and the loading ends after the set loading force reaches 3500 N;
b、位移保持阶段设定校形持续时间为10min~20min,加载力保持500N恒定,数据采集频率设定为200ms;b. In the displacement maintenance stage, set the duration of the correction to 10min to 20min, keep the loading force constant at 500N, and set the data acquisition frequency to 200ms;
步骤四、对弯曲上模1和弯曲下模2加热:移动三段式对开电阻炉10的电阻炉膛中段位于金属板材弯曲成形装置处,闭合炉门,设定三段式对开电阻炉10的温度为600℃~800℃,利用三段式对开电阻炉10对弯曲上模1和弯曲下模2加热;Step 4. Heating the upper bending die 1 and the lower bending die 2: move the middle section of the resistance furnace of the three-stage split resistance furnace 10 to the metal plate bending forming device, close the furnace door, and set the three-stage split resistance furnace 10 The temperature is 600°C to 800°C, and the bending upper mold 1 and the bending lower mold 2 are heated by using a three-stage split resistance furnace 10;
步骤五、成形试样置于炉内的金属板材弯曲成形装置上:三段式对开电阻炉10内温度达到设定温度后,打开三段式对开电阻炉10的炉门,放置钛合金板料,使其置于试样定位槽2-2中,迅速关闭炉门,在计算机的程序控制界面重置载荷清零,手动控制横梁9缓慢上升以带动弯曲下模2上移,直至试样表面与弯曲下模2接触,以观察到载荷传感器11有载荷增加为准,通过位移传感器12来重置横梁9位移清零,继续保温5min使试样温度均匀化;Step 5. The formed sample is placed on the metal plate bending forming device in the furnace: after the temperature in the three-stage split resistance furnace 10 reaches the set temperature, open the furnace door of the three-stage split resistance furnace 10, and place the titanium alloy Place the sheet material in the sample positioning groove 2-2, quickly close the furnace door, reset the load to zero on the computer program control interface, manually control the beam 9 to rise slowly to drive the bending lower die 2 to move up until the test The surface of the sample is in contact with the lower bending die 2, subject to the observation that the load of the load sensor 11 increases, the displacement of the crossbeam 9 is reset by the displacement sensor 12, and the displacement of the crossbeam 9 is reset to zero, and the temperature of the sample is uniformed by continuing to keep warm for 5 minutes;
步骤六、利用电子试验机对金属板材弯曲成形装置加载:保温时间到后启动设置好的控制程序并对金属板材弯曲成形装置加载;Step 6. Use the electronic testing machine to load the sheet metal bending forming device: after the holding time is up, start the set control program and load the sheet metal bending forming device;
步骤七、取出试样:成形结束后,打开三段式对开电阻炉10的炉门,手动控制横梁9下移卸载,迅速取出试样空冷,冷却10min,即完成一个金属板材弯曲成形。Step 7. Take out the sample: After forming, open the furnace door of the three-stage split resistance furnace 10, manually control the beam 9 to move down and unload, quickly take out the sample and air-cool it for 10 minutes, and then complete the bending and forming of a metal sheet.
具体实施方式四:结合图10说明本实施方式,本实施方式是步骤三中加载阶段横梁9的速度设定为9mm/min。其它步骤与具体实施方式三相同。Embodiment 4: This embodiment is described with reference to FIG. 10 . In this embodiment, the speed of the crossbeam 9 in the loading stage in step 3 is set to 9 mm/min. Other steps are the same as in the third embodiment.
具体实施方式五:结合图10说明本实施方式,本实施方式是步骤三中加载阶段横梁9的速度设定为12mm/min。其它步骤与具体实施方式三相同。Embodiment 5: This embodiment is described with reference to FIG. 10 . In this embodiment, the speed of the crossbeam 9 in the loading stage in step 3 is set to 12 mm/min. Other steps are the same as in the third embodiment.
具体实施方式六:结合图10说明本实施方式,本实施方式是步骤三中位移保持阶段设定校形持续时间为15min。其它步骤与具体实施方式三、四或五相同。Embodiment 6: This embodiment is described with reference to FIG. 10 . In this embodiment, the duration of the shape correction is set to 15 minutes in the displacement maintenance stage in step 3. Other steps are the same as those in Embodiment 3, 4 or 5.
具体实施方式七:结合图10说明本实施方式,本实施方式是步骤三中位移保持阶段设定校形持续时间为18min。其它步骤与具体实施方式三、四或五相同。Embodiment 7: This embodiment is described with reference to FIG. 10 . In this embodiment, the duration of the shape correction is set to 18 minutes in the displacement maintenance stage in step 3. Other steps are the same as those in Embodiment 3, 4 or 5.
具体实施方式八:结合图10说明本实施方式,本实施方式是步骤四中设定三段式对开电阻炉10的温度为650℃。其它步骤与具体实施方式三相同。Embodiment 8: This embodiment is described with reference to FIG. 10 . In this embodiment, the temperature of the three-stage split resistance furnace 10 is set at 650° C. in step 4. Other steps are the same as in the third embodiment.
具体实施方式九:结合图10说明本实施方式,本实施方式是步骤四中设定三段式对开电阻炉10的温度为700℃。其它步骤与具体实施方式三相同。Ninth specific embodiment: This embodiment is described with reference to FIG. 10 . In this embodiment, the temperature of the three-stage split resistance furnace 10 is set at 700° C. in step four. Other steps are the same as in the third embodiment.
具体实施方式十:结合图10说明本实施方式,本实施方式是步骤四中设定三段式对开电阻炉10的温度为750℃。其它步骤与具体实施方式三相同。Embodiment 10: This embodiment is described with reference to FIG. 10 . In this embodiment, the temperature of the three-stage split resistance furnace 10 is set to 750° C. in step 4. Other steps are the same as in the third embodiment.
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