CN103668954B - The antibiotic finishing method of antibacterial finishing agent, fabric and antibiotic fabric - Google Patents
The antibiotic finishing method of antibacterial finishing agent, fabric and antibiotic fabric Download PDFInfo
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- CN103668954B CN103668954B CN201210356393.0A CN201210356393A CN103668954B CN 103668954 B CN103668954 B CN 103668954B CN 201210356393 A CN201210356393 A CN 201210356393A CN 103668954 B CN103668954 B CN 103668954B
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Abstract
The invention discloses a kind of antibacterial finishing agent, the antibiotic finishing method of fabric and antibiotic fabric, described antibacterial finishing agent, comprise the component of following weight parts: MIT 10-30 part, poly-Hydroxypropyldimonium Chloride 15-25 part, dodecyl carboxymethyl sodium form imidazoline acetate 30-50 part.Antibiotic fabric of the present invention can be obtained by dipping or padding finishing method.Use antibacterial finishing agent of the present invention through dipping or pad the obtained antibiotic fabric of Final finishing; there is the performance such as deodorization, anticorrosion; high to the bacteriostasis rate of Escherichia coli and staphylococcus aureus; still higher level is remained on through 30 washing bacteriostasis rates; thus protection health, that improves clothing wears performance.
Description
Technical field
The present invention relates to a kind of antibacterial finishing agent, the antibiotic finishing method of fabric and antibiotic fabric.
Background technology
As everyone knows, survive various microorganism in the environment of human lives, on the skin of only upper half of human body, every square metre just has 50-5000 microorganism, wherein some is useful to human body, or even it is indispensable, but also there are many microorganisms to impair health, they can survive in people's fabric used in everyday, as socks, underwear, underpants, cotton-wadded quilt, sheet, towel etc., at warm tide. in wet environment, these microorganisms are with the sweat of human secretory, grease, the decomposed substance of scurf or fabric itself is bred rapidly as nutriment, form a large amount of harmful bacterium, they can go out the volatile compounds frowzy such as various lower fatty acid and amine by catalyze metabolic decomposition product, add the smell that the secretion of bacterium itself rots with its dead bones of the body, discharge nauseating bad odor, more seriously they also can produce abnormal stimulation to human body skin, bring out various disease of skin, even can propagate various disease as venereal disease, skin disease etc., unhealthful.In addition, the existence of microorganism also can cause fabric fibre macromolecules degradation, the phenomenon such as make fabric occur tendering, variable color, to go mouldy, and affects the outward appearance of clothes and ornament, color and luster; For some militarias, as parachute, gun cover, tent etc., then entail dangers to safety, affects fighting capacity, and consequence is hardly imaginable, therefore people always by every means kill harmful microorganism.
In fact, the mankind use the historical origin of antiseptic for a long time, and before several thousand, spices has just been used for anticorrosion by the China of country that ancient civilization is the most flourishing in the world, Egypt, India and Babylon; Ancient Egyptian just knows cover silver strip to prevent bacteriological infection on wound; Greeks have just known by copper sheet nail alow, can reduce the corrosion caused by microorganism; Mongolia herdsman just uses silver-colored bowl splendid attire goat milk to make milk fresh-keeping; Shang dynasty has just been understood by skin diseases such as the insane diseases of mercury medical treatment; In the historical relic be unearthed in Western Han Dynastry's Han tomb at Mawangdui, many fabrics also all have passed through mildew-resistant process.Long ago visible, sterilization, sterilization, mildew-resistant, aseptic technic are just applied in practice by first people.
Antibacterial fabric process refers to use to kill and processes fabric or fiber to the medicament of the microorganism that human body and clothing are harmful to.
But the antibacterial treatment of existing fabric, unsatisfactory.
Summary of the invention
For the deficiencies in the prior art, one of technical problem to be solved by this invention is to provide a kind of antibacterial finishing agent.
Two of technical problem to be solved by this invention is to provide a kind of antibiotic finishing method of fabric.
Three of technical problem to be solved by this invention is to provide the antibiotic finishing method of another fabric
Four of technical problem to be solved by this invention is to provide a kind of antibiotic fabric.
For solving the problems of the technologies described above, the present invention is achieved through the following technical solutions:
A kind of antibacterial finishing agent, comprises the component of following weight parts: MIT 10-30 part, poly-Hydroxypropyldimonium Chloride 15-25 part, dodecyl carboxymethyl sodium form imidazoline acetate 30-50 part.
Preferably, also comprise: ethylenediamine two salicyl large acetic acid ferrisodium 0.5-1.5 part, decamethylene biguanides dihydrochloride 4-6 part.
Above-mentioned each component is uniformly mixed, described antibacterial finishing agent can be obtained.
MIT, 2-Methyl-4-Isothiazolin-3-one, No. CAS: 2682-20-4.
Poly-Hydroxypropyldimonium Chloride, poly (dimethylamine-co-epichlorohydrin), No. CAS: 25988-97-0.
Dodecyl carboxymethyl sodium form imidazoline acetate, sodiumlaulylcarboxymethylimidazolineacetate, No. CAS: 64041-76-5.
The large acetic acid ferrisodium of ethylenediamine two salicyl, SodiumferricEDDHA, No. CAS: 16455-61-1.
Decamethylene biguanides dihydrochloride, Decamethylenediguanidinedihydrochloride, No. CAS: 301-15-5.
An antibiotic finishing method for fabric, comprise and pad, dewater and baking step, described step of padding comprises:
(1) prepare antibiotic finishing solution: be dissolved in the water by described antibacterial finishing agent, be mixed with antibiotic finishing solution, the mass concentration controlling antibacterial finishing agent is 15 ~ 50g/l,
(2) fabric is padded by antibiotic finishing solution, pick-up 70-80%.
Described baking step is: by fabric drying at 90-110 DEG C of temperature.
An antibiotic finishing method for fabric, comprise dipping, dehydration and baking step, described impregnation steps comprises:
By fabric normal temperature dipping 15-20 minute, described antibacterial finishing agent consumption is 1.0-3.0%o.w.f, and bath raio is 1:15-1:30.
Described baking step is: by fabric drying at 90-110 DEG C of temperature.
A kind of antibiotic fabric, adopts above-mentioned method for sorting to be prepared from.
The advantage major embodiment of technical solution of the present invention is: use antibacterial finishing agent of the present invention through dipping or pad the obtained fabric of Final finishing; there is the performance such as deodorization, anticorrosion; high to the bacteriostasis rate of Escherichia coli and staphylococcus aureus; still higher level is remained on through 30 washing bacteriostasis rates; thus protection health, that improves clothing wears performance.
Detailed description of the invention
Embodiment 1
Each raw material is taken by embodiment corresponding to table 11 data.MIT, poly-Hydroxypropyldimonium Chloride and dodecyl carboxymethyl sodium form imidazoline acetate are uniformly mixed, antibacterial finishing agent of the present invention can be obtained.
Embodiment 2
Each raw material is taken by embodiment corresponding to table 12 data.By method described in embodiment 1, antibacterial finishing agent of the present invention can be obtained.
Embodiment 3
Each raw material is taken by embodiment corresponding to table 13 data.By method described in embodiment 1, antibacterial finishing agent of the present invention can be obtained.
Embodiment 4
Each raw material is taken by embodiment corresponding to table 14 data.MIT, poly-Hydroxypropyldimonium Chloride, dodecyl carboxymethyl sodium form imidazoline acetate, the large acetic acid ferrisodium of ethylenediamine two salicyl and decamethylene biguanides dihydrochloride are uniformly mixed, antibacterial finishing agent of the present invention can be obtained.
Embodiment 5
Each raw material is taken by embodiment corresponding to table 15 data.By method described in embodiment 4, antibacterial finishing agent of the present invention can be obtained.
Table 1: antibacterial finishing agent formula table unit: kilogram
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| MIT | 10 | 30 | 26 | 25 | 20 |
| Poly-Hydroxypropyldimonium Chloride | 25 | 15 | 20 | 15 | 20 |
| Dodecyl carboxymethyl sodium form imidazoline acetate | 50 | 30 | 40 | 35 | 40 |
| The large acetic acid ferrisodium of ethylenediamine two salicyl | / | / | / | 1.5 | 1 |
| Decamethylene biguanides dihydrochloride | / | / | / | 4 | 5 |
Embodiment 6
The antibiotic finish of fabric:
(1) prepare antibiotic finishing solution: be dissolved in the water by the antibacterial finishing agent prepared by embodiment 3, be mixed with antibiotic finishing solution, the mass concentration controlling antibacterial finishing agent is 30g/l.
(2) fabric is padded by antibiotic finishing solution, pick-up 80%.
(3) dewater, by fabric drying at 100 DEG C of temperature, antibiotic fabric of the present invention can be obtained.
Embodiment 7
The antibiotic finish of fabric:
(1) prepare antibiotic finishing solution: be dissolved in the water by the antibacterial finishing agent prepared by embodiment 5, be mixed with antibiotic finishing solution, the mass concentration controlling antibacterial finishing agent is 30g/l.
(2) fabric is padded by antibiotic finishing solution, pick-up 80%.
(3) dewater, by fabric drying at 100 DEG C of temperature, antibiotic fabric of the present invention can be obtained.
Embodiment 8
The antibiotic finish of fabric:
(1) antibacterial finishing agent prepared by embodiment 3 is dissolved in the water, is mixed with antibiotic finishing solution.
(2) by fabric normal temperature dipping antibiotic finishing solution 20 minutes, controlling antibacterial finishing agent consumption is 2.0%o.w.f, and bath raio is 1:20.
(3) dewater, by fabric drying at 100 DEG C of temperature, antibiotic fabric of the present invention can be obtained.
Embodiment 9
The antibiotic finish of fabric:
(1) antibacterial finishing agent prepared by embodiment 5 is dissolved in the water, is mixed with antibiotic finishing solution.
(2) by fabric normal temperature dipping antibiotic finishing solution 20 minutes, controlling antibacterial finishing agent consumption is 2.0%o.w.f, and bath raio is 1:20.
(3) dewater, by fabric drying at 100 DEG C of temperature, antibiotic fabric of the present invention can be obtained.
Embodiment 6-9, fabric used is COTTON FABRIC, and its specification is: the textile poplin cloth in 15tex × 15tex523 × 283 (40s × 40s/133 × 72 piece/inch).
Test case 1
Adopt evaluation the 3rd part of standard GB/T/T20944.3-2008 antibacterial textile performance: succusion carries out antibiotic property quantitative test, and test result is in table 2.
Use antibacterial finishing agent of the present invention through dipping or pad the obtained fabric of Final finishing; there is the performance such as deodorization, anticorrosion; high to the bacteriostasis rate of Escherichia coli and staphylococcus aureus; still higher level is remained on through 30 washing bacteriostasis rates; thus protection health, that improves clothing wears performance.
Claims (4)
1. an antibacterial finishing agent, it is characterized in that, comprise the component of following weight parts: MIT 10-30 part, poly-Hydroxypropyldimonium Chloride 15-25 part, dodecyl carboxymethyl sodium form imidazoline acetate 30-50 part, ethylenediamine two salicyl large acetic acid ferrisodium 0.5-1.5 part, decamethylene biguanides dihydrochloride 4-6 part.
2. an antibiotic finishing method for fabric, comprise and pad, dewater and baking step, it is characterized in that, described step of padding comprises:
(1) prepare antibiotic finishing solution: be dissolved in the water by antibacterial finishing agent described in claim 1, be mixed with antibiotic finishing solution, the mass concentration controlling antibacterial finishing agent is 15 ~ 50g/l,
(2) fabric is padded by antibiotic finishing solution, pick-up 70-80%.
3. the antibiotic finishing method of fabric as claimed in claim 2, it is characterized in that, described baking step is: by fabric drying at 90-110 DEG C of temperature.
4. an antibiotic fabric, is characterized in that: adopt the antibiotic finishing method of the fabric described in Claims 2 or 3 to be prepared from.
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| CN201210356393.0A CN103668954B (en) | 2012-09-21 | 2012-09-21 | The antibiotic finishing method of antibacterial finishing agent, fabric and antibiotic fabric |
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| CN201210356393.0A CN103668954B (en) | 2012-09-21 | 2012-09-21 | The antibiotic finishing method of antibacterial finishing agent, fabric and antibiotic fabric |
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| CN103668954B true CN103668954B (en) | 2015-11-25 |
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| CN104452266B (en) * | 2014-12-03 | 2016-05-11 | 山东新丝丽织造技术有限公司 | A kind of antibacterial modified method of towel |
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| CN105696344A (en) * | 2016-03-11 | 2016-06-22 | 湖州宏鑫绸厂 | Antibacterial finishing method of silk fabric |
| CN105648776A (en) * | 2016-04-01 | 2016-06-08 | 吴江市林旺纺织厂 | Antibacterial and anti-ultraviolet finishing agent and method for preparing same |
| CN106049038A (en) * | 2016-05-30 | 2016-10-26 | 太仓红桥服饰有限公司 | Antibacterial finishing agent for apparel fabrics and finishing process thereof |
| CN106049040A (en) * | 2016-07-29 | 2016-10-26 | 桐乡市素丝五祁服饰有限公司 | Bacteriostatic and antibacterial fabric finishing agent and finishing technology |
| CN106758139A (en) * | 2016-12-16 | 2017-05-31 | 吴江市北厍盛源纺织品助剂厂 | A kind of textile auxiliary with anti-microbial property and preparation method thereof |
| CN107853758A (en) * | 2017-10-11 | 2018-03-30 | 江苏拓福服装有限公司 | Antibacterial shirt fabric |
| CN108651450A (en) * | 2018-05-02 | 2018-10-16 | 合肥市晨雷思建筑材料科技有限公司 | A kind of composition for the processing of hearing aid surface long-acting bacteriostatic |
| CN109295711B (en) * | 2018-09-07 | 2021-07-13 | 深圳市康源新材料科技有限公司 | Preparation method of washable antiviral and antibacterial fiber and fiber product |
| CN109468844B (en) * | 2018-11-15 | 2021-06-01 | 旷达汽车饰件系统有限公司 | Antibacterial fabric and production process thereof |
| CN109322153A (en) * | 2018-11-16 | 2019-02-12 | 无锡环中科技服务有限公司 | Mosquito proof camouflage facing material |
| CN109554926A (en) * | 2018-11-16 | 2019-04-02 | 无锡环中科技服务有限公司 | Permanent inflaming retarding fabric |
| CN116263031B (en) * | 2022-12-08 | 2024-10-25 | 杭州华利实业集团有限公司 | Antivirus finishing method for bedding fabric of train |
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| DE10206759A1 (en) * | 2002-02-19 | 2003-08-28 | Dragoco Gerberding Co Ag | Use of 1,2-alkanediol mixture as an antimicrobial agent, e.g. for treating body odor, acne or mycoses or preserving perishable products |
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| CN101189971A (en) * | 2006-11-20 | 2008-06-04 | 北京崇高纳米科技有限公司 | A kind of inorganic/organic nanocomposite antibacterial agent and its fiber product application |
| CN102558064A (en) * | 2012-01-29 | 2012-07-11 | 安润医药科技（苏州）有限公司 | Antihypertensive compound, and its preparation method, application and pharmaceutically acceptable salts and solvates |
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Effective date of registration: 20180830 Address after: 223600 Jiangsu Suqian Shuyang County Economic Development Zone Taipei Avenue East, Ruian Road South Patentee after: JIANGSU CHENSHI WEIYE TEXTILE TECHNOLOGY CO., LTD. Address before: 200137 1F79 14, 528 Yang Gao Bei Road, Pudong New Area, Shanghai. Patentee before: Shanghai Taohong Chemical Technology Co., Ltd. |
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Granted publication date: 20151125 Termination date: 20190921 |