CN103652930B - Moringa calcium total nutrient and preparation method thereof - Google Patents
Moringa calcium total nutrient and preparation method thereof Download PDFInfo
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- CN103652930B CN103652930B CN201310752607.0A CN201310752607A CN103652930B CN 103652930 B CN103652930 B CN 103652930B CN 201310752607 A CN201310752607 A CN 201310752607A CN 103652930 B CN103652930 B CN 103652930B
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- moringa
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- stevia rebaudiana
- total nutrient
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- 241000220215 Moringa Species 0.000 title claims abstract description 192
- 235000011347 Moringa oleifera Nutrition 0.000 title claims abstract description 192
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title claims abstract description 39
- 239000011575 calcium Substances 0.000 title claims abstract description 39
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 39
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 235000015097 nutrients Nutrition 0.000 title claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 52
- 244000228451 Stevia rebaudiana Species 0.000 claims abstract description 51
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- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 2
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- 206010006956 Calcium deficiency Diseases 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 244000000626 Daucus carota Species 0.000 description 1
- 235000002767 Daucus carota Nutrition 0.000 description 1
- 108010082495 Dietary Plant Proteins Proteins 0.000 description 1
- 240000008790 Musa x paradisiaca Species 0.000 description 1
- 235000018290 Musa x paradisiaca Nutrition 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
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- 229930003268 Vitamin C Natural products 0.000 description 1
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- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000003613 bile acid Substances 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
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- 150000001720 carbohydrates Chemical class 0.000 description 1
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- 208000016097 disease of metabolism Diseases 0.000 description 1
- 235000006694 eating habits Nutrition 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 210000003743 erythrocyte Anatomy 0.000 description 1
- 238000002481 ethanol extraction Methods 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 230000002641 glycemic effect Effects 0.000 description 1
- 230000003054 hormonal effect Effects 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 230000001077 hypotensive effect Effects 0.000 description 1
- 208000033065 inborn errors of immunity Diseases 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 230000006651 lactation Effects 0.000 description 1
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- 208000028529 primary immunodeficiency disease Diseases 0.000 description 1
- 239000000047 product Substances 0.000 description 1
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- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a moringa calcium total nutrient and a preparation method thereof. The invention has the core that biomass enzymatic hydrolysis, nanometer dual wall breaking and the whole-course low-temperature extraction new technology are adopted. The moringa calcium total nutrient comprises the following components in percentage by weight: 50-70% of moringa leaf, 10-30% of moringa seed, 10-20% of moringa root and 5-10% of stevia rebaudiana. In the preparation process, the whole-course constant low-temperature ethyl alcohol extraction and the neutral protease, cellulose and pectinase enzymolysis wall breaking technology are adopted, the new technology of distilled water repeated pressure reduction and repeated recycling extraction is adopted, and the effective nutrition ingredient and the bioactivity of the natural original ecology moringa are prevented from being damaged by high temperature and chemical solvent; the new technology of nanometer physics wall breaking and nanometer tower spray drying is adopted to obtain the moringa powder of 100-200 nanometers; the effective ingredient activity of the moringa can be directly adsorbed by the human body tissue cell; the bioavailability of the moringa calcium total nutrient ingredient by the human body can be effectively improved; the moringa calcium total nutrient is suitable for the children growth period, middle and old age calcium supplement and the effective conditioning of people suffering from hyperglycemia, hyperlipidemia, hypertension, heart and cerebral vessel diseases and tumor as well as the sub-health crowd.
Description
Technical field
The present invention relates to a kind of calcium nutrient, specifically a kind of moringa calcium total nutrient and preparation method thereof.
Background technology
Along with the change of compatriots' life style and customs, dietary structure irrationality is on the rise, and overbalance nutrition threatens people ' s health.Metabolic disease raises year by year, sub-health population is up to 70%, the famous expert of China, Chinese Academy of Sciences Yang Jia steps academician points out: calcium deficiency is the source of ten thousand diseases, and calcium participates in the metabolic process of all functions of human body, and adult takes in required 1000mg calcium every day, and the eating habit of people only can take in 500mg calcium, therefore everyone replenishes the calcium needing more or less, healthy to guarantee, prevents and cures diseases.
Although the calcium supplementing product a multitude of names of selling in the market, chemical synthesis mostly, animal is extracted, and containing cholesterol, the high worn-out end of saturated fatty acid, and the absorption of calcium and function must have the participation of vitamin d and P elements, simple replenishing the calcium not easily absorbs, and Moringa is rich in the vitamin D and phosphorus that participate in calcium uptake while that calcic being the highest in plant, it is the complete nutrition ingredients that the most natural a kind of calcium content is high, Calcium in Plants is better than synthesizing calcium, animal calcium, current pure plant high calcium fully nutrient is almost blank market at present, good market prospects, demand is very large.
Summary of the invention
For the problem existing for above-mentioned prior art, the object of this invention is to provide a kind ofly be suitable for that crowd is wide, comprehensive nutrition and moringa calcium total nutrient easily absorbed and preparation method thereof.
For achieving the above object, the technical solution adopted in the present invention is: a kind of moringa calcium total nutrient, be characterized in comprising and adopt low temperature and organic solvents solution to repeat to reduce pressure and reclaim the obtained leaf of Moringa powder of the biological technique method of extraction, because leaf of Moringa has the feature of high calcium, high protein and homovitamin, its calcium content is the plant that on the earth, calcic is the highest, and its health is worth the important minerals of mainly bone and tooth: child growth, anti-osteomalacia, control senile osteoporosis, pregnant woman's lactation are special procured supplementary; Its healthy value of vegetable protein supplements eight kinds of necessary high-quality eggs of health, is the important substance of human body cell health, lacks high-quality protein and hypoimmunity, function can be caused to decline, and then produce various disease.So the balance of leaf of Moringa powder energy conditioning subhealthy state colony, supplement the seven major nutrient of natural needed by human body.
Wherein, there is certain sweet taste mouthfeel in order to make the present invention and do not affect glycemic index, the present invention can be the powder comprising leaf of Moringa that the biological technique method that adopts low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains and STEVIA REBAUDIANA mixing, wherein the content of leaf of Moringa is 85-95%, the content of STEVIA REBAUDIANA is 5-15%, described STEVIA REBAUDIANA has low-yield, not participate in metabolism feature, therefore be applicable to diabetic's use, and STEVIA REBAUDIANA has hypoglycemic and hypotensive effect, treatment diabetes are had certain effect.
Further, the present invention can be the powder comprising leaf of Moringa, moringa seeds and the STEVIA REBAUDIANA mixing that the biological technique method that adopts low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains, wherein the content of leaf of Moringa is 65-85%, the content of moringa seeds is 10-30%, and the content of STEVIA REBAUDIANA is 5-15%., because this moringa seeds has the feature of high ferro, several amino acids, multiple unrighted acid, wherein iron is red blood cell Main Ingredients and Appearance, is to prevent and treat anaemia important element, is also the important substance of children's heart and brain intelligence muscle health; And unrighted acid is the important substance of conditioning internal organ function especially cardiovascular and cerebrovascular diseases, or transmit and absorb the medium of vitamin A. D. E, K, be also manufacture bile acid and hormonal primary raw material simultaneously.Therefore moringa seeds have promote bone and tooth, the effect such as children become a useful person, anti-osteomalacia, senile osteoporosis.
Further, the present invention can be the powder comprising leaf of Moringa, moringa seeds, Moringa root and the STEVIA REBAUDIANA mixing that the biological technique method that adopts low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains, wherein the content of leaf of Moringa is 50-70%, the content of moringa seeds is 10-30%, the content of Moringa root is 10-20%, the content of STEVIA REBAUDIANA is 5-10%, because this Moringa root is rich in the feature of flavones and saponin(e, therefore can regulate internal organ function especially cardiovascular and cerebrovascular and anaemia.
The optimum proportioning of instant component is: the content of leaf of Moringa is 60%, and the content of moringa seeds is 20%, the content of Moringa root be 10% and the content of STEVIA REBAUDIANA be 10%.
The preparation method of moringa calcium total nutrient of the present invention, its preparation process is as follows:
1., the Moringa root of the moringa seeds of the leaf of Moringa of 50-70%, 10-30%, 10-20% is put into clear water together with the STEVIA REBAUDIANA of 5-10% and clean dedusting;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 2-3 hour;
3., with 6 times of 75% alcohol immersion component 8-15 hour to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 35 DEG C-55 DEG C distilled water immersion steps residue 8-15 hour 3. to group component, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 5 DEG C-15 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 5 DEG C-15 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 100-200 millimicron.
Measure according to quality of vegetable supervision and inspection center of the Ministry of Agriculture and prove, containing 27.1 grams, protein in the leaf of Moringa of every 100g, be about 2 times of milk; Containing vitamin C 200 milligrams, be about 7 times of orange; Containing vitamin A 16.3 milligrams, be about 4 times of carrot; Iron content 28.2 milligrams, is about 3 times of spinach; Calcic 2003 milligrams, is about 4 times of milk; Containing 1324 milligrams, potassium, be about 3 times of banana.Leaf of Moringa is rich in the large nutrition of whole seven needed for health: quality plant albumen, unsaturated matter aliphatic acid, vitamin, carbohydrate, mineral matter, trace element, dietary fiber and water.Therefore, there is the feature of high calcium, high protein and homovitamin according to leaf of Moringa, utilize leaf of Moringa to extract Calcium in Plants for main component, it is not containing cholesterol, the high worn-out end of saturated fatty acid, be better than synthesizing calcium, animal calcium, and itself is containing vitamin and P elements, is conducive to the absorption of calcium.In preparation process, adopt omnidistance permanent cold ethanol to extract and adopt distilled water to repeat decompression and repeat to reclaim novel extraction technology, guarantee effective nutrition of the natural Moringa of ecosystem and biologically active not by high temperature and chemical solvent destroy; Also add neutral proteinase broken wall simultaneously, utilize the cellulose in neutral protease enzymolysis component, increase its permeability, thus by effective ingredient breakdown out, make the nutrient of cell become Small molecular from large molecule; The new technology of applying nano tower spraying dry and nanometer physical wall breaking makes Moringa powder reach 100-200 millimicron again, realize Moringa effective ingredient activity directly to be absorbed by human tissue cell, effectively improve human body to the bioavilability of the full nutrition of Moringa calcium.Moringa calcium total nutrient of the present invention is adapted to the child growth phase, person in middle and old age replenish the calcium and effective conditioning of hyperglycaemia, high fat of blood, hypertension, cardiovascular and cerebrovascular, tumour and sub-health population thereof.
Detailed description of the invention
The core technology of this invention uses modern biological project preparation, and new and high technology carries out extracting effective elite composition, perfect retentive activity.This invention has significant characteristic sum progress compared with existing Moringa crushing technology, and has significant effect.
embodiment one:
Choose the leaf of Moringa of 100%, the leaf of Moringa powder that the biological technique method adopting low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains, concrete preparation process is as follows:
1., leaf of Moringa is put into clear water and clean dedusting;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 2 hours;
3., by 6 times of 75% alcohol immersion components 8 hours to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 55 DEG C of distilled water immersion steps to group component residue 3. 8 hours, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 5 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 15 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 150 millimicrons.
This ultra micro leaf of Moringa powder can add maltodextrin hybrid process and make capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
embodiment two:
Choose the leaf of Moringa of 85% and the STEVIA REBAUDIANA of 15%, the biological technique method adopting low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains the powder of leaf of Moringa and STEVIA REBAUDIANA mixing, and concrete preparation process is as follows:
1., the leaf of Moringa of 85% is put into clear water together with the STEVIA REBAUDIANA of 15% and clean dedusting;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 2 hours;
3., by 6 times of 75% alcohol immersion components 10 hours to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 40 DEG C of distilled water immersion steps to group component residue 3. 12 hours, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 10 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 10 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 120 millimicrons.
The powder of this ultra micro leaf of Moringa and STEVIA REBAUDIANA mixing can add maltodextrin hybrid process and make capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
embodiment three:
Choose the leaf of Moringa of 95% and the STEVIA REBAUDIANA of 5%, the biological technique method adopting low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains the powder of leaf of Moringa and STEVIA REBAUDIANA mixing, and concrete preparation process is as follows:
1., the leaf of Moringa of 95% is put into clear water together with the STEVIA REBAUDIANA of 5% and clean dedusting;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 2.5 hours;
3., by 6 times of 75% alcohol immersion components 10 hours to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 45 DEG C of distilled water immersion steps to group component residue 3. 10 hours, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 15 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 15 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 120 millimicrons.
The powder of this ultra micro leaf of Moringa and STEVIA REBAUDIANA mixing can add maltodextrin hybrid process and make capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
embodiment four:
Choose the leaf of Moringa of 65%, the moringa seeds of 30% and 5% STEVIA REBAUDIANA, the biological technique method adopting low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains the powder of leaf of Moringa, moringa seeds and STEVIA REBAUDIANA mixing, and concrete preparation process is as follows:
1., by the leaf of Moringa of 65%, 30% moringa seeds put into clear water clean dedusting together with the STEVIA REBAUDIANA of 5%;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 2.5 hours;
3., by 6 times of 75% alcohol immersion components 12 hours to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 35 DEG C of distilled water immersion steps to group component residue 3. 15 hours, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 15 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 15 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 130 millimicrons.
The powder of this ultra micro leaf of Moringa, moringa seeds and STEVIA REBAUDIANA mixing can add maltodextrin hybrid process and make capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
embodiment five:
Choose the leaf of Moringa of 75%, the moringa seeds of 15% and 10% STEVIA REBAUDIANA, the biological technique method adopting low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains the powder of leaf of Moringa, moringa seeds and STEVIA REBAUDIANA mixing, and concrete preparation process is as follows:
1., by the leaf of Moringa of 75%, 15% moringa seeds put into clear water clean dedusting together with the STEVIA REBAUDIANA of 10%;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 3 hours;
3., by 6 times of 75% alcohol immersion components 10 hours to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 50 DEG C of distilled water immersion steps to group component residue 3. 10 hours, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 10 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 15 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 110 millimicrons.
The powder of this ultra micro leaf of Moringa, moringa seeds and STEVIA REBAUDIANA mixing can add maltodextrin hybrid process and make capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
embodiment six:
Choose the leaf of Moringa of 85%, the moringa seeds of 10% and 5% STEVIA REBAUDIANA, the biological technique method adopting low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains the powder of leaf of Moringa, moringa seeds and STEVIA REBAUDIANA mixing, and concrete preparation process is as follows:
1., by the leaf of Moringa of 85%, 10% moringa seeds put into clear water clean dedusting together with the STEVIA REBAUDIANA of 5%;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 3 hours;
3., by 6 times of 75% alcohol immersion components 12 hours to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 40 DEG C of distilled water immersion steps to group component residue 3. 12 hours, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 10 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 10 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 140 millimicrons.
The powder of this ultra micro leaf of Moringa, moringa seeds and STEVIA REBAUDIANA mixing can add maltodextrin hybrid process and make capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
embodiment seven:
Choose the leaf of Moringa of 50%, the moringa seeds of 30%, the Moringa root of 10% and 10% STEVIA REBAUDIANA, the biological technique method adopting low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains the powder of leaf of Moringa, moringa seeds, Moringa root and STEVIA REBAUDIANA mixing, and concrete preparation process is as follows:
1., the leaf of Moringa of 50%, the moringa seeds of 30%, the Moringa root of 10% are put into clear water and cleaned dedusting together with the STEVIA REBAUDIANA of 10%;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 2 hours;
3., by 6 times of 75% alcohol immersion components 15 hours to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 45 DEG C of distilled water immersion steps to group component residue 3. 8 hours, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 15 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 10 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 160 millimicrons.
The powder of this ultra micro leaf of Moringa, moringa seeds, Moringa root and STEVIA REBAUDIANA mixing can add maltodextrin hybrid process and make capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
embodiment eight:
Choose the leaf of Moringa of 60%, the moringa seeds of 20%, the Moringa root of 10% and 10% STEVIA REBAUDIANA, the biological technique method adopting low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains the powder of leaf of Moringa, moringa seeds, Moringa root and STEVIA REBAUDIANA mixing, and concrete preparation process is as follows:
1., the leaf of Moringa of 60%, the moringa seeds of 20%, the Moringa root of 10% are put into clear water and cleaned dedusting together with the STEVIA REBAUDIANA of 10%;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 3 hours;
3., by 6 times of 75% alcohol immersion components 15 hours to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 50 DEG C of distilled water immersion steps to group component residue 3. 15 hours, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 10 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 10 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 100 millimicrons.
The powder of this ultra micro leaf of Moringa, moringa seeds, Moringa root and STEVIA REBAUDIANA mixing can add maltodextrin hybrid process and make capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
embodiment nine:
Choose the leaf of Moringa of 65%, the moringa seeds of 10%, the Moringa root of 20% and 5% STEVIA REBAUDIANA, the biological technique method adopting low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains the powder of leaf of Moringa, moringa seeds, Moringa root and STEVIA REBAUDIANA mixing, and concrete preparation process is as follows:
1., the leaf of Moringa of 65%, the moringa seeds of 10%, the Moringa root of 20% are put into clear water and cleaned dedusting together with the STEVIA REBAUDIANA of 5%;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 2.5 hours;
3., by 6 times of 75% alcohol immersion components 15 hours to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 55 DEG C of distilled water immersion steps to group component residue 3. 8 hours, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 5 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 10 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 110 millimicrons.
The powder of this ultra micro leaf of Moringa, moringa seeds, Moringa root and STEVIA REBAUDIANA mixing can add maltodextrin hybrid process and make capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
embodiment ten:
Choose the leaf of Moringa of 70%, the moringa seeds of 15%, the Moringa root of 10% and 5% STEVIA REBAUDIANA, the biological technique method adopting low temperature and organic solvents solution to repeat to reduce pressure and reclaim extraction obtains the powder of leaf of Moringa, moringa seeds, Moringa root and STEVIA REBAUDIANA mixing, and concrete preparation process is as follows:
1., the leaf of Moringa of 70%, the moringa seeds of 15%, the Moringa root of 10% are put into clear water and cleaned dedusting together with the STEVIA REBAUDIANA of 5%;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 2 hours;
3., by 6 times of 75% alcohol immersion components 8 hours to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 35 DEG C of distilled water immersion steps to group component residue 3. 12 hours, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 15 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 10 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 120 millimicrons.
The powder of this ultra micro leaf of Moringa, moringa seeds, Moringa root and STEVIA REBAUDIANA mixing can add maltodextrin hybrid process and make capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
The Moringa powder prepared by above-mentioned ten embodiments and method thereof can reach 100 millimicrons, can directly be absorbed by human tissue cell fully, and adopt omnidistance permanent cold ethanol extraction and distilled water repeatedly to add the extraction of neutral proteinase repetition recovered under reduced pressure, meet the feature that Moringa herbaceous plant avoids high temperature and chemical solvent destruction effective ingredient activity completely, ensure that the nutritional labeling of Moringa itself is complete, effectively improve human body to the bioavilability of the full nutrition of Moringa calcium.This Moringa powder can add other batchings and make soft capsule, tablet, oral liquid, aaerosol solution or Moringa food etc., is adapted to the child growth phase, person in middle and old age replenish the calcium and effective conditioning of hyperglycaemia, high fat of blood, hypertension, cardiovascular and cerebrovascular, tumour and sub-health population thereof.
Although the present invention describes with reference to specific embodiment, this description not meaning that is construed as limiting the present invention.With reference to description of the invention, other changes of the disclosed embodiments, all can expect for those skilled in the art, this change should belong in appended claims limited range.
Claims (4)
1. a preparation method for moringa calcium total nutrient, is characterized in that its preparation process is as follows:
1., Moringa raw material is put into clear water clean dedusting, wherein said Moringa raw material is: I leaf of Moringa; Or the mixture of the leaf of Moringa of II 85 ~ 95% and the STEVIA REBAUDIANA of 5 ~ 15%; Or the leaf of Moringa of III 65 ~ 85% and the moringa seeds of 10 ~ 30% and 5 ~ 15% the mixture of STEVIA REBAUDIANA; Or the mixture of the leaf of Moringa of IV 50 ~ 70% and the moringa seeds of 10 ~ 30% and the Moringa root of 10 ~ 20% and the STEVIA REBAUDIANA of 5 ~ 10%;
2., the component after cleaning is put into vacuum refrigeration device and carry out freeze drying 2-3 hour;
3., with 6 times of 75% alcohol immersion component 8-15 hour to group component, filtered and recycled residue also extracts and forms first time extract;
4., with 6 times of 35 DEG C-55 DEG C distilled water immersion steps residue 8-15 hour 3. to group component, add the neutral proteinase of each 1%, cellulase and pectase in immersion process and carry out enzymolysis broken wall, then filter to extract and form second time extract;
5., by step residue 4. undertaken forming third time extract as step enzymolysis broken wall 4. also filters to extract, wherein the temperature of distilled water is than front once lifting 5 DEG C-15 DEG C;
6., by step residue 5. undertaken extracting formation No. the 4th extract as step enzymolysis broken wall 4. also filters, wherein the temperature of distilled water once promotes 5 DEG C-15 DEG C than front;
7., by above-mentioned first time extract, second time extract, third time extract and No. the 4th extract mixing after tubulation put into the extractor of extracter, be uniformly mixed after adding extract, then start compressor to carry out reduction vaporization to extractor and start vavuum pump carrying out negative pressure evaporation to extractor, control temperature repeatedly extracts again, until extracted;
8., by the extract after extraction through tubulation negative pressure concentrate drying, then the standard of 1000 object physical wall breaking is reached through nanometer tower ultramicro grinding, and simultaneous spray drying, finally form the ultra micro Moringa powder of 100-200 millimicron.
2. the moringa calcium total nutrient that obtains of a preparation method according to claim 1.
3. moringa calcium total nutrient according to claim 2, is characterized in that: the content of leaf of Moringa is 60%, and the content of moringa seeds is 20%, the content of Moringa root be 10% and the content of STEVIA REBAUDIANA be 10%.
4. a purposes for the moringa calcium total nutrient of preparation method's acquisition according to claim 1, is characterized in that: above-mentioned ultra micro Moringa powder adds maltodextrin hybrid process and makes capsule, tablet, oral liquid, aaerosol solution, electuary, Moringa food or Moringa beverage.
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| CN104664366A (en) * | 2014-12-18 | 2015-06-03 | 云南龙润茶业集团有限公司 | Moringa oleifera and starch composition capable of regulating insulin secretion |
| CN104432075B (en) * | 2014-12-25 | 2016-08-17 | 福州嘉佑化学科技有限公司 | A kind of leaf of Moringa oral liquid and preparation method thereof |
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| CN105211998A (en) * | 2015-08-24 | 2016-01-06 | 李奕鸿 | A kind of Moringa beverage and preparation method thereof |
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| CN106306936A (en) * | 2016-08-17 | 2017-01-11 | 深圳百绿盛农业科技发展有限公司 | Preparation method of moringa oleifera enzymolyzed drink |
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| CN108244656A (en) * | 2018-03-28 | 2018-07-06 | 顾文宏 | A kind of method that Calcium in Plants is extracted from leaf of Moringa |
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