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CN103652540A - Microcapsule formula - Google Patents

Microcapsule formula Download PDF

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Publication number
CN103652540A
CN103652540A CN201210316248.XA CN201210316248A CN103652540A CN 103652540 A CN103652540 A CN 103652540A CN 201210316248 A CN201210316248 A CN 201210316248A CN 103652540 A CN103652540 A CN 103652540A
Authority
CN
China
Prior art keywords
oil
mixture
sodium
fat
microcapsules
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201210316248.XA
Other languages
Chinese (zh)
Inventor
简晓红
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WUHAN SHUTAI TECHNOLOGY Co Ltd
Original Assignee
WUHAN SHUTAI TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WUHAN SHUTAI TECHNOLOGY Co Ltd filed Critical WUHAN SHUTAI TECHNOLOGY Co Ltd
Priority to CN201210316248.XA priority Critical patent/CN103652540A/en
Publication of CN103652540A publication Critical patent/CN103652540A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L29/00Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/30Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/15Vitamins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Mycology (AREA)
  • Molecular Biology (AREA)
  • Medicinal Preparation (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The invention provides a microcapsule formula. A microcapsule contains the following main components in percentage by weight: 35-40% of starch sodium octenylsuccinate, 22.5-30% of nutritive oil, fat soluble nutrients or mixtures of the nutritive oil and the fat soluble nutrients, 8-15% of trehalose, 10-20% of sorbitol, 15-25% of maltodextrin, 5% of glucose, 0.5-1% of sodium tripolyphosphate, 1-1.5% of VC (Vitamin C) sodium, 0.04-0.08% of VE (Vitamin E), 0.1-0.15% of VC palmitate, 0.02-0.07% of rosemary extracts and 0.4-0.6% of tricalcium phosphate. The microcapsule formula has the advantages that all the raw materials conform to the application range of GB2760; meanwhile, the embedding rate of the microcapsule is up to over 99.5%; the oxidation stability of a microcapsule product is better than that of the like product on the market; a good product is provided for the application of the nutritive oil and fat-soluble vitamins to a drink.

Description

A kind of microcapsules formula
Technical field
The present invention relates to a kind of microcapsules formula, relating to specifically with converted starch, trehalose, D-sorbite, maltodextrin, glucose, sodium phosphate trimer, VC sodium, VE, VC palmitate, Rosmarinus officinalis extract, tricalcium phosphate is the formula of raw material embedding nutritional oil, fat-soluble nutrient or its mixture.
Background technology
Along with transformation and the growth in the living standard of people's consumption idea, people's health care consciousness strengthens day by day.In beverage, add various nutritional oil and liposoluble vitamin and will become market focus, but the enforcement along with GB2760, the selection of composite food additive Raw requires stricter, the product quality of microcapsules is most important in beverage, various nutritional oil and liposoluble vitamin, due to self, are easily oxidized, and all have distinctive smell, adopt the stability that can improve product after microcapsule embedded, cover smell.Exploitation is imperative in conjunction with the microcapsule product of microcapsule embedded process characteristic and alimentary codex requirement, the present invention has realized the range of application that whole raw materials all meet GB2760, microcapsule embedded rate reaches more than 99.5% simultaneously, this microcapsule product oxidation stability is better than market like product, for nutritional oil and liposoluble vitamin, applies good product is provided in beverage.
Summary of the invention
(1) [0003]the technical problem solving
The object of the present invention is to provide a kind of microcapsules formula being added in beverage, to meet the needs in market.
(2) summary of the invention
1 a kind of microcapsules formula provided by the invention, is characterized in that the key component of microcapsules and content are as follows: starch sodium octenyl succinate 35-40%; Nutritional oil, fat-soluble nutrient or its mixture 22.5-30%; Trehalose 8-15%; D-sorbite 10-20%; Glucose 5%; Maltodextrin 15-25%; Sodium phosphate trimer 0.5-1%; VC sodium 1-1.5%; VE 0.04-0.08%; VC palmitate 0.1-0.15%; Rosmarinus officinalis extract 0.02-0.07%; Tricalcium phosphate 0.4-0.6%.Production stage is as follows: (1) is heated to 50-60 ℃ by nutritional oil, fat-soluble nutrient or its mixture, and VE, VC palmitate, Rosmarinus officinalis extract are dissolved in wherein and stir, the standby mixture B that obtains;
(2) after starch sodium octenyl succinate, trehalose, D-sorbite, maltodextrin, glucose, sodium phosphate trimer, VC sodium are weighed in proportion, be dissolved in certain water gaging, obtain solution A;
(3) solution A and mixture B emulsification are sheared after 30min, with high pressure homogenizer, carried out homogeneous, homogenization pressure is 10-45MPa, and homogeneous three times makes emulsion droplet diameter be less than 0.5 μ m.
(4) emulsion after homogeneous is sprayed and be dried, on fluid bed, evenly add tricalcium phosphate as anticaking agent, get product.
Described microcapsules heartwood is nutritional oil, fat-soluble nutrient or its mixture.
Described micro-algae DHA(DHA) oil, micro-algae EPA(eicosapentaenoic acid) oil, AA(arachidonic acid) mixture of one or more materials in oil, fish oil, evening primrose oil, borage oil, gamma-Linolenic acid oil, pine-seed oil, soybean oil, grape pip wet goods.
Described fat-soluble nutrient comprises: the mixture of one or more materials in vitamin A, vitamin D, vitamin E, Co-Q10, lutein, Lycopene, beta carotene, lecithin, phytosterol, phytosterin ester.
The invention has the advantages that: the present invention has realized the range of application that whole raw materials all meet GB2760, microcapsule embedded rate reaches more than 99.5% simultaneously, this microcapsule product oxidation stability is better than market like product, for nutritional oil and liposoluble vitamin, applies good product is provided in beverage.
The specific embodiment
embodiment mono-:
Take in proportion starch sodium octenyl succinate 185g; DHA grease 113g; Trehalose 40g; D-sorbite 65g; Glucose 25g; Maltodextrin 60.1g; Sodium phosphate trimer 3g; VC sodium 5g; VE 0.3g; VC palmitate 0.75g; Rosmarinus officinalis extract 0.35g; Tricalcium phosphate 2.5g.DHA grease is heated to 50-60 ℃, and VE, VC palmitate, Rosmarinus officinalis extract are dissolved in wherein and stir, the standby mixture B that obtains.After starch sodium octenyl succinate, trehalose, D-sorbite, maltodextrin, glucose, sodium phosphate trimer, VC sodium are weighed in proportion, be dissolved in certain water gaging, obtain solution A.Solution A and mixture B emulsification are sheared after 30min, with high pressure homogenizer, carried out homogeneous, homogenization pressure is 10-45MPa, and homogeneous three times makes emulsion droplet diameter be less than 0.5 μ m.Emulsion after homogeneous is sprayed dry, on fluid bed, evenly add tricalcium phosphate as anticaking agent, get product.
embodiment bis-:
Take in proportion starch sodium octenyl succinate 185g; Gamma-Linolenic acid oil 113g; Trehalose 40g; D-sorbite 65g; Glucose 25g; Maltodextrin 60.1g; Sodium phosphate trimer 3g; VC sodium 5g; VE 0.3g; VC palmitate 0.75g; Rosmarinus officinalis extract 0.35g; Tricalcium phosphate 2.5g.Gamma-Linolenic acid oil is heated to 50-60 ℃, and VE, VC palmitate, Rosmarinus officinalis extract are dissolved in wherein and stir, the standby mixture B that obtains.After starch sodium octenyl succinate, trehalose, D-sorbite, maltodextrin, glucose, sodium phosphate trimer, VC sodium are weighed in proportion, be dissolved in certain water gaging, obtain solution A.Solution A and mixture B emulsification are sheared after 30min, with high pressure homogenizer, carried out homogeneous, homogenization pressure is 10-45MPa, and homogeneous three times makes emulsion droplet diameter be less than 0.5 μ m.Emulsion after homogeneous is sprayed dry, on fluid bed, evenly add tricalcium phosphate as anticaking agent, get product.

Claims (1)

1. a microcapsules formula, is characterized in that: key component and the content of microcapsules are as follows: starch sodium octenyl succinate 35-40%; Nutritional oil, fat-soluble nutrient or its mixture 22.5-30%; Trehalose 8-15%; D-sorbite 10-20%; Maltodextrin 15-25%; Glucose 5%; Sodium phosphate trimer 0.5-1%; VC sodium 1-1.5%, VE0.04-0.08%, VC palmitate 0.1-0.15%, Rosmarinus officinalis extract 0.02-0.07%, tricalcium phosphate 0.4-0.6%; Production stage is as follows: (1) is heated to 50-60 ℃ by nutritional oil, fat-soluble nutrient or its mixture, and VE, VC palmitate, Rosmarinus officinalis extract are dissolved in wherein and stir, the standby mixture B that obtains;
(2) after starch sodium octenyl succinate, trehalose, D-sorbite, maltodextrin, glucose, sodium phosphate trimer, VC sodium are weighed in proportion, be dissolved in certain water gaging, obtain solution A;
(3) solution A and mixture B emulsification are sheared after 30min, with high pressure homogenizer, carried out homogeneous, homogenization pressure is 10-45MPa, and homogeneous three times makes emulsion droplet diameter be less than 0.5 μ m;
(4) emulsion after homogeneous is sprayed and be dried, on fluid bed, evenly add tricalcium phosphate as anticaking agent, get product.
2.a kind of microcapsules formula according to claim 1, is characterized in that: this microcapsules heartwood is nutritional oil, fat-soluble nutrient or its mixture.
3.a kind of microcapsules formula according to claim 1, is characterized in that: nutritional oil comprises: micro-algae DHA(DHA) oil, micro-algae EPA(eicosapentaenoic acid) oil, AA(arachidonic acid) mixture of one or more materials in oil, fish oil, evening primrose oil, borage oil, gamma-Linolenic acid oil, pine-seed oil, soybean oil, grape pip wet goods.
4.a kind of microcapsules formula according to claim 1 is characterized in that: fat-soluble nutrient comprises: the mixture of one or more materials in vitamin A, vitamin D, vitamin E, Co-Q10, lutein, Lycopene, beta carotene, lecithin, phytosterol, phytosterin ester.
CN201210316248.XA 2012-08-31 2012-08-31 Microcapsule formula Pending CN103652540A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201210316248.XA CN103652540A (en) 2012-08-31 2012-08-31 Microcapsule formula

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201210316248.XA CN103652540A (en) 2012-08-31 2012-08-31 Microcapsule formula

Publications (1)

Publication Number Publication Date
CN103652540A true CN103652540A (en) 2014-03-26

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Country Status (1)

Country Link
CN (1) CN103652540A (en)

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104621570A (en) * 2015-03-11 2015-05-20 杨昭鹏 High-stability algae oil DHA microcapsule powder and preparation method thereof
CN104982933A (en) * 2015-07-06 2015-10-21 中国农业大学 Method for preparing rose hip seed oil microcapsules
CN105076729A (en) * 2015-09-16 2015-11-25 中粮饲料有限公司 Feed additive microcapsule and preparation method thereof
CN105661545A (en) * 2016-01-28 2016-06-15 武汉欧米嘉生物医药有限公司 Alpha-linolenic acid microcapsule capable of being directly used for cooking and preparation method of alpha-linolenic acid microcapsule
WO2017063102A1 (en) * 2015-10-12 2017-04-20 浙江医药股份有限公司新昌制药厂 Method for granulating, forming, and drying fat soluble nutrient microcapsule particles
CN108541772A (en) * 2018-03-15 2018-09-18 东北林业大学 A kind of preparation process of high-content korean pine seed oil powdered oil
CN109418541A (en) * 2017-09-01 2019-03-05 浙江医药股份有限公司新昌制药厂 A kind of preparation method of novel hydrophobic type liposoluble vitamin microcapsules
CN109567169A (en) * 2018-12-29 2019-04-05 北京金康普食品科技有限公司 Microencapsulation nanometer formulation of micronutrient premix and preparation method thereof
CN112075630A (en) * 2020-08-24 2020-12-15 武汉星辰现代生物工程有限公司 Natural carotene microcapsule and preparation method thereof
CN112274494A (en) * 2019-07-24 2021-01-29 重庆桑禾动物药业有限公司 Preparation of novel high-stability vitamin D3 microcapsule dispersing agent

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104621570A (en) * 2015-03-11 2015-05-20 杨昭鹏 High-stability algae oil DHA microcapsule powder and preparation method thereof
CN104982933A (en) * 2015-07-06 2015-10-21 中国农业大学 Method for preparing rose hip seed oil microcapsules
CN105076729A (en) * 2015-09-16 2015-11-25 中粮饲料有限公司 Feed additive microcapsule and preparation method thereof
WO2017063102A1 (en) * 2015-10-12 2017-04-20 浙江医药股份有限公司新昌制药厂 Method for granulating, forming, and drying fat soluble nutrient microcapsule particles
CN105661545A (en) * 2016-01-28 2016-06-15 武汉欧米嘉生物医药有限公司 Alpha-linolenic acid microcapsule capable of being directly used for cooking and preparation method of alpha-linolenic acid microcapsule
CN109418541A (en) * 2017-09-01 2019-03-05 浙江医药股份有限公司新昌制药厂 A kind of preparation method of novel hydrophobic type liposoluble vitamin microcapsules
CN109418541B (en) * 2017-09-01 2022-08-19 浙江医药股份有限公司新昌制药厂 Preparation method of hydrophobic fat-soluble vitamin microcapsule
CN108541772A (en) * 2018-03-15 2018-09-18 东北林业大学 A kind of preparation process of high-content korean pine seed oil powdered oil
CN109567169A (en) * 2018-12-29 2019-04-05 北京金康普食品科技有限公司 Microencapsulation nanometer formulation of micronutrient premix and preparation method thereof
CN112274494A (en) * 2019-07-24 2021-01-29 重庆桑禾动物药业有限公司 Preparation of novel high-stability vitamin D3 microcapsule dispersing agent
CN112075630A (en) * 2020-08-24 2020-12-15 武汉星辰现代生物工程有限公司 Natural carotene microcapsule and preparation method thereof

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Application publication date: 20140326