CN103555151A - Temperature-resistant corrosion-preventing mixed resin powder coating - Google Patents
Temperature-resistant corrosion-preventing mixed resin powder coating Download PDFInfo
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- CN103555151A CN103555151A CN201310516012.5A CN201310516012A CN103555151A CN 103555151 A CN103555151 A CN 103555151A CN 201310516012 A CN201310516012 A CN 201310516012A CN 103555151 A CN103555151 A CN 103555151A
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- 239000000843 powder Substances 0.000 title claims abstract description 35
- 239000011248 coating agent Substances 0.000 title claims abstract description 27
- 238000000576 coating method Methods 0.000 title claims abstract description 27
- 229920005989 resin Polymers 0.000 title claims abstract description 15
- 239000011347 resin Substances 0.000 title claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 13
- LZCLXQDLBQLTDK-UHFFFAOYSA-N ethyl 2-hydroxypropanoate Chemical compound CCOC(=O)C(C)O LZCLXQDLBQLTDK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000003822 epoxy resin Substances 0.000 claims abstract description 5
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 4
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 claims abstract description 4
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004793 Polystyrene Substances 0.000 claims abstract description 4
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims abstract description 4
- IUNMPGNGSSIWFP-UHFFFAOYSA-N dimethylaminopropylamine Chemical compound CN(C)CCCN IUNMPGNGSSIWFP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229940116333 ethyl lactate Drugs 0.000 claims abstract description 4
- 229920002223 polystyrene Polymers 0.000 claims abstract description 4
- 229910052902 vermiculite Inorganic materials 0.000 claims abstract description 4
- 239000010455 vermiculite Substances 0.000 claims abstract description 4
- 235000019354 vermiculite Nutrition 0.000 claims abstract description 4
- ZYUVGYBAPZYKSA-UHFFFAOYSA-N 5-(3-hydroxybutan-2-yl)-4-methylbenzene-1,3-diol Chemical compound CC(O)C(C)C1=CC(O)=CC(O)=C1C ZYUVGYBAPZYKSA-UHFFFAOYSA-N 0.000 claims description 6
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 6
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 claims description 6
- 238000000498 ball milling Methods 0.000 claims description 6
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 6
- 239000011575 calcium Substances 0.000 claims description 6
- 229910052791 calcium Inorganic materials 0.000 claims description 6
- 239000000919 ceramic Substances 0.000 claims description 6
- NHADDZMCASKINP-HTRCEHHLSA-N decarboxydihydrocitrinin Natural products C1=C(O)C(C)=C2[C@H](C)[C@@H](C)OCC2=C1O NHADDZMCASKINP-HTRCEHHLSA-N 0.000 claims description 6
- 229910001710 laterite Inorganic materials 0.000 claims description 6
- 239000011504 laterite Substances 0.000 claims description 6
- 229920005610 lignin Polymers 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 239000004417 polycarbonate Substances 0.000 claims description 6
- 229920000515 polycarbonate Polymers 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 3
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 claims description 3
- 239000000853 adhesive Substances 0.000 claims description 3
- 230000001070 adhesive effect Effects 0.000 claims description 3
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000000428 dust Substances 0.000 claims description 3
- RKISUIUJZGSLEV-UHFFFAOYSA-N n-[2-(octadecanoylamino)ethyl]octadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(=O)NCCNC(=O)CCCCCCCCCCCCCCCCC RKISUIUJZGSLEV-UHFFFAOYSA-N 0.000 claims description 3
- 239000004843 novolac epoxy resin Substances 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 230000000630 rising effect Effects 0.000 claims description 3
- 239000010802 sludge Substances 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 239000002131 composite material Substances 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract description 2
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 abstract 2
- 239000004593 Epoxy Substances 0.000 abstract 1
- 239000004841 bisphenol A epoxy resin Substances 0.000 abstract 1
- 238000013329 compounding Methods 0.000 abstract 1
- 239000000945 filler Substances 0.000 abstract 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 abstract 1
- 235000010299 hexamethylene tetramine Nutrition 0.000 abstract 1
- 239000004312 hexamethylene tetramine Substances 0.000 abstract 1
- 229920003986 novolac Polymers 0.000 abstract 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 abstract 1
- 230000002335 preservative effect Effects 0.000 abstract 1
- 229910001928 zirconium oxide Inorganic materials 0.000 abstract 1
- 239000002904 solvent Substances 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 2
- 238000005452 bending Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000004811 fluoropolymer Substances 0.000 description 1
- 229920002313 fluoropolymer Polymers 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
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- Paints Or Removers (AREA)
Abstract
The invention discloses a temperature-resistant corrosion-preventing mixed resin powder coating which consists of the following raw materials in parts by weight: 40-55 parts of phenol novolac epoxy, 20-30 parts of bisphenol A epoxy resin, 6-10 parts of hexamethylenetetramine, 3-4 parts of ethyl lactate, 0.7-1 part of 2, 4, 5-sodium trichlorobenzenesulfonate, 0.8-1 part of cetyl trimethyl ammonium bromide, 2-3 parts of glitter powder, 3-4 parts of aluminum hydroxide, 1-2 parts of dimethylaminopropylamine, 2-4 parts of zirconium oxide, 10-13 parts of graphite powder, 1-2 parts of polystyrene, 4-6 parts of vermiculite powder and 5-10 parts of composite filler. The powder coating disclosed by the invention is prepared from mixing and compounding two epoxy resins, so that the temperature-resistant effect is improved, and the powder coating is simple to apply and can be directly sprayed on base materials. The powder coating is good in preservative effect, low in cost and good in protectiveness.
Description
Technical field
The present invention relates generally to a kind of coating, relates in particular to the anticorrosion hybrid resin powder coating of a kind of heatproof.
Background technology
Powder coating is a kind of novel not containing solvent 100% solid powdery coating.Have without solvent, pollution-free, save the energy and resource, physical strength high reduces labor intensity and films.The kind of powder coating has two large classes: thermoplastic powder coating and thermosetting powder coating(s).Although the kind of powder coating is not various as solvent based coating, can be also a lot of as the fluoropolymer resin of powder coating.
Summary of the invention
The object of the invention is exactly in order to provide a kind of heatproof anticorrosion hybrid resin powder coating.
The present invention is achieved by the following technical solutions:
An anticorrosion hybrid resin powder coating, is characterized in that what it was comprised of the raw material of following weight parts:
Phenol novolac epoxy resins 40-55, bisphenol A epoxide resin 20-30, vulkacit H 6-10, ethyl lactate 3-4,2,4,5-trichlorobenzene sodium sulfonate 0.7-1, cetyl trimethylammonium bromide 0.8-1, glitter powder 2-3, aluminium hydroxide 3-4, dimethylaminopropylamine 1-2, zirconium white 2-4, Graphite Powder 99 10-13, polystyrene 1-2, vermiculite power 4-6, compounded mix 5-10;
Described compounded mix is comprised of the raw material of following weight parts:
Laterite 35-40, breeze 5-7, ceramics powder 4-6, phenol A polycarbonate 2-3, ethylene bis stearamide 1-2, calcium lignin sulphonate 0.6-1, antioxidant 1010 0.1-0.2;
Above-mentioned calcium lignin sulphonate is joined in 10-15 times of water, add ceramics powder, breeze after being uniformly mixed, at 100-120 ℃, insulated and stirred is dry to water, add phenol A polycarbonate, rising temperature is 180-200 ℃, and 200-300 rev/min of dispersed with stirring 4-6 minute, obtains Preblend; Above-mentioned laterite is calcined after 2-3 hour and mixed with above-mentioned Preblend at 700-800 ℃, and ball milling 1-2 hour, adds each raw material of residue, and fully ball milling, obtains described adhesive aid.
A preparation method for the anticorrosion hybrid resin powder coating of heatproof, comprises the following steps:
Above-mentioned each raw material is mixed, by melt extruding in forcing machine, compressing tablet, air-cooled, add sludge ice agent, abrasive dust, sieves, and obtains the anticorrosion hybrid resin powder coating of described heatproof.
Advantage of the present invention is:
Powder coating of the present invention mixes two kinds of epoxy resin composite, has improved heatproof effect, use simple, can direct spraying in base material, favorable anti-corrosion effect, cost is low, protectiveness is good.
Embodiment
Embodiment 1,
An anticorrosion hybrid resin powder coating, it by following weight parts (kilogram) raw material form:
Phenol novolac epoxy resins 55, bisphenol A epoxide resin 30, vulkacit H 10, ethyl lactate 4,2,4,5-trichlorobenzene sodium sulfonate 0.7, cetyl trimethylammonium bromide 0.8, glitter powder 3, aluminium hydroxide 3, dimethylaminopropylamine 1, zirconium white 4, Graphite Powder 99 13, polystyrene 1-2, vermiculite power 4, compounded mix 10;
Described compounded mix is comprised of the raw material of following weight parts:
Laterite 40, breeze 7, ceramics powder 6, phenol A polycarbonate 3, ethylene bis stearamide 1, calcium lignin sulphonate 0.6, antioxidant 1010 0.2;
Above-mentioned calcium lignin sulphonate is joined in 15 times of water, add ceramics powder, breeze after being uniformly mixed, at 120 ℃, insulated and stirred is dry to water, adds phenol A polycarbonate, and rising temperature is 200 ℃, and 300 revs/min of dispersed with stirring 6 minutes, obtain Preblend; Above-mentioned laterite is calcined after 2 hours and mixed with above-mentioned Preblend at 700 ℃, and ball milling 2 hours, adds each raw material of residue, and fully ball milling, obtains described adhesive aid.
A preparation method for the anticorrosion hybrid resin powder coating of heatproof, comprises the following steps:
Above-mentioned each raw material is mixed, by melt extruding in forcing machine, compressing tablet, air-cooled, add sludge ice agent, abrasive dust, sieves, and obtains the anticorrosion hybrid resin powder coating of described heatproof.
Performance test:
Pencil hardness test: 2H is without scuffing;
Bending hardness test: 0T is curved to be passed through;
Salt spray resistance test: corrosion strength was not more than 1 grade in 1000 hours.
Claims (2)
1. the anticorrosion hybrid resin powder coating of heatproof, is characterized in that what it was comprised of the raw material of following weight parts:
Phenol novolac epoxy resins 40-55, bisphenol A epoxide resin 20-30, vulkacit H 6-10, ethyl lactate 3-4,2,4,5-trichlorobenzene sodium sulfonate 0.7-1, cetyl trimethylammonium bromide 0.8-1, glitter powder 2-3, aluminium hydroxide 3-4, dimethylaminopropylamine 1-2, zirconium white 2-4, Graphite Powder 99 10-13, polystyrene 1-2, vermiculite power 4-6, compounded mix 5-10;
Described compounded mix is comprised of the raw material of following weight parts:
Laterite 35-40, breeze 5-7, ceramics powder 4-6, phenol A polycarbonate 2-3, ethylene bis stearamide 1-2, calcium lignin sulphonate 0.6-1, antioxidant 1010 0.1-0.2;
Above-mentioned calcium lignin sulphonate is joined in 10-15 times of water, add ceramics powder, breeze after being uniformly mixed, at 100-120 ℃, insulated and stirred is dry to water, add phenol A polycarbonate, rising temperature is 180-200 ℃, and 200-300 rev/min of dispersed with stirring 4-6 minute, obtains Preblend; Above-mentioned laterite is calcined after 2-3 hour and mixed with above-mentioned Preblend at 700-800 ℃, and ball milling 1-2 hour, adds each raw material of residue, and fully ball milling, obtains described adhesive aid.
2. a preparation method for the anticorrosion hybrid resin powder coating of heatproof as claimed in claim 1, is characterized in that comprising the following steps:
Above-mentioned each raw material is mixed, by melt extruding in forcing machine, compressing tablet, air-cooled, add sludge ice agent, abrasive dust, sieves, and obtains the anticorrosion hybrid resin powder coating of described heatproof.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310516012.5A CN103555151A (en) | 2013-10-28 | 2013-10-28 | Temperature-resistant corrosion-preventing mixed resin powder coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310516012.5A CN103555151A (en) | 2013-10-28 | 2013-10-28 | Temperature-resistant corrosion-preventing mixed resin powder coating |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103555151A true CN103555151A (en) | 2014-02-05 |
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| CN201310516012.5A Pending CN103555151A (en) | 2013-10-28 | 2013-10-28 | Temperature-resistant corrosion-preventing mixed resin powder coating |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104119776A (en) * | 2014-06-25 | 2014-10-29 | 蚌埠凯盛工程技术有限公司 | Corrosion-resistant wear-resistant powder paint for illumination instruments |
| CN104292759A (en) * | 2014-10-31 | 2015-01-21 | 合肥鼎雅家具有限责任公司 | Novel epoxy resin composite added with vermiculite and manufacturing method thereof |
| CN104312386A (en) * | 2014-09-23 | 2015-01-28 | 尤明 | Anti-corrosion powder coating material for wind power plant engineering instrument |
| CN105419140A (en) * | 2016-01-25 | 2016-03-23 | 深圳市摩天氟碳科技有限公司 | Building heat preservation material with excellent fireproof performance |
| CN108676460A (en) * | 2018-05-03 | 2018-10-19 | 广州挚业化工有限公司 | A kind of brilliant color terrace decorative paint and preparation method thereof |
| CN110002496A (en) * | 2019-02-25 | 2019-07-12 | 王召惠 | A kind of anti-preparation method for peeling off zirconia coating Zirconium oxide powder |
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| CN102161859A (en) * | 2011-05-27 | 2011-08-24 | 常州市飞扬粉末涂料有限公司 | Modified epoxy heavy-duty anticorrosion powder paint and preparation method thereof |
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| CN103073972A (en) * | 2012-11-19 | 2013-05-01 | 山西中天新技术开发有限公司 | Heatproof anticorrosion wear resistant powdery paint, preparation method and application |
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2013
- 2013-10-28 CN CN201310516012.5A patent/CN103555151A/en active Pending
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| CN101560355A (en) * | 2008-04-14 | 2009-10-21 | 徐州正菱涂装工程技术研究中心 | Heavy anti-corrosion antirust powder paint |
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| CN101724331A (en) * | 2008-10-29 | 2010-06-09 | 中国科学院金属研究所 | Anticorrosion epoxy powder paint used outside marine steel pipe pile |
| CN102161859A (en) * | 2011-05-27 | 2011-08-24 | 常州市飞扬粉末涂料有限公司 | Modified epoxy heavy-duty anticorrosion powder paint and preparation method thereof |
| CN102492353A (en) * | 2011-11-28 | 2012-06-13 | 江苏兰陵高分子材料有限公司 | Novel fast-set anticorrosion and wear-resistant epoxy powder coating and preparation process thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104119776A (en) * | 2014-06-25 | 2014-10-29 | 蚌埠凯盛工程技术有限公司 | Corrosion-resistant wear-resistant powder paint for illumination instruments |
| CN104312386A (en) * | 2014-09-23 | 2015-01-28 | 尤明 | Anti-corrosion powder coating material for wind power plant engineering instrument |
| CN104292759A (en) * | 2014-10-31 | 2015-01-21 | 合肥鼎雅家具有限责任公司 | Novel epoxy resin composite added with vermiculite and manufacturing method thereof |
| CN105419140A (en) * | 2016-01-25 | 2016-03-23 | 深圳市摩天氟碳科技有限公司 | Building heat preservation material with excellent fireproof performance |
| CN108676460A (en) * | 2018-05-03 | 2018-10-19 | 广州挚业化工有限公司 | A kind of brilliant color terrace decorative paint and preparation method thereof |
| CN108676460B (en) * | 2018-05-03 | 2020-06-30 | 广州挚业化工有限公司 | A kind of crystal color floor decoration coating and preparation method thereof |
| CN110002496A (en) * | 2019-02-25 | 2019-07-12 | 王召惠 | A kind of anti-preparation method for peeling off zirconia coating Zirconium oxide powder |
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Application publication date: 20140205 |