CN103496952A - Zirconia toughened alumina ceramic cylinder sleeve - Google Patents
Zirconia toughened alumina ceramic cylinder sleeve Download PDFInfo
- Publication number
- CN103496952A CN103496952A CN201310440880.XA CN201310440880A CN103496952A CN 103496952 A CN103496952 A CN 103496952A CN 201310440880 A CN201310440880 A CN 201310440880A CN 103496952 A CN103496952 A CN 103496952A
- Authority
- CN
- China
- Prior art keywords
- cylinder sleeve
- ceramic cylinder
- alumina ceramic
- zirconia
- toughened alumina
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 title claims abstract description 26
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 title claims abstract description 11
- MRELNEQAGSRDBK-UHFFFAOYSA-N lanthanum(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[La+3].[La+3] MRELNEQAGSRDBK-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000000034 method Methods 0.000 claims abstract description 5
- 238000000498 ball milling Methods 0.000 claims abstract description 4
- 238000005469 granulation Methods 0.000 claims abstract description 4
- 230000003179 granulation Effects 0.000 claims abstract description 4
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229910000021 magnesium carbonate Inorganic materials 0.000 claims abstract description 4
- 239000001095 magnesium carbonate Substances 0.000 claims abstract description 4
- 238000002156 mixing Methods 0.000 claims abstract description 4
- SIWVEOZUMHYXCS-UHFFFAOYSA-N oxo(oxoyttriooxy)yttrium Chemical compound O=[Y]O[Y]=O SIWVEOZUMHYXCS-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000000465 moulding Methods 0.000 claims abstract description 3
- 238000005245 sintering Methods 0.000 claims abstract description 3
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 5
- 229960001708 magnesium carbonate Drugs 0.000 claims description 3
- 235000014380 magnesium carbonate Nutrition 0.000 claims description 3
- 238000005553 drilling Methods 0.000 abstract description 10
- 239000000919 ceramic Substances 0.000 abstract description 9
- 238000005260 corrosion Methods 0.000 abstract description 4
- 230000007797 corrosion Effects 0.000 abstract description 4
- 239000002253 acid Substances 0.000 abstract description 3
- 239000007788 liquid Substances 0.000 abstract description 3
- 239000002245 particle Substances 0.000 abstract description 3
- 239000007790 solid phase Substances 0.000 abstract description 3
- 238000002360 preparation method Methods 0.000 abstract description 2
- 238000000227 grinding Methods 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 4
- 229910000831 Steel Inorganic materials 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 230000003245 working effect Effects 0.000 description 2
- LLJRXVHJOJRCSM-UHFFFAOYSA-N 3-pyridin-4-yl-1H-indole Chemical compound C=1NC2=CC=CC=C2C=1C1=CC=NC=C1 LLJRXVHJOJRCSM-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 230000002706 hydrostatic effect Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- YWYZEGXAUVWDED-UHFFFAOYSA-N triammonium citrate Chemical compound [NH4+].[NH4+].[NH4+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O YWYZEGXAUVWDED-UHFFFAOYSA-N 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention belongs to the technical field of preparation processes of ceramics and specifically relates to a zirconia toughened alumina ceramic cylinder sleeve. The zirconia toughened alumina ceramic cylinder sleeve comprises the following components in percentage by weight: 60-70% of alumina, 20-30% of zirconia, 1.2-1.5% of yttrium oxide, 0.5% of lanthanum oxide and 3-3.3% of magnesium carbonate and is prepared by the process flow comprising the steps of ball milling, mixing, granulation, molding and sintering. The produced ceramic cylinder sleeve has the advantages of corrosion resistance, acid and alkali resistance and high temperature resistance, and can work in drilling mud or other liquid media with strong corrosiveness, and the hardness is sufficient to resist grinding or scoring of various solid-phase particles with sharpness or strong grinding property in the high-pressure mud. The ceramic microstructure is uniform, and the surface gloss is high, so that the zirconia toughened alumina ceramic cylinder sleeve is favorable to prolonging the service life of a piston. The ceramic cylinder sleeve is high in working pressure and can meet the requirements of drilling deep wells and ultra-deep wells.
Description
Technical field
The invention belongs to ceramic fabricating technology field, be specifically related to a kind of Zirconia reinforced alumina ceramic liner.
Background technology
Drill pump is that oil drilling is to carry drilling mud and take bottom rock out of well outer visual plant, therefore, the life-span of cylinder sleeve directly has influence on drilling efficiency and drilling cost and driller's labour intensity, in general, the comprehensive day rate of boring deep-well and ultra deep well is higher, repair pump and can cause very large financial loss, especially offshore drilling, comprehensive day rate of ship unit is higher.
What slush pump used at the latest is generally the metal steel bushing, and according to statistics, its mean lifetime is approximately about tens hours to 200 hours, is improved to afterwards the bimetal steel bushing, and improve a lot work-ing life, and its mean lifetime is greatly about about 300-500 hour.But not wear-resisting, the not corrosion resistant characteristics of its existence, pure zirconia cylinder sleeve life-time service at 100-250 degree temperature there will be powder phenomenon-tion, and wear resisting property reduces, and work-ing life is limited, it is low that the pure alumina cylinder sleeve exists fracture toughness property, and crack performance easily appears in product.
Summary of the invention
Make the drilling mud pump liner to exist the life-span low for solving in above-mentioned prior art, the problem of various bad phenomenon easily appears in product, the invention provides a kind of Zirconia reinforced alumina ceramic liner.
The preparation technology that the present invention adopts is as follows:
A kind of Zirconia reinforced alumina ceramic liner, is characterized in that, weight percent is consisted of: 60 ~ 70% aluminum oxide, 20 ~ 30% zirconium white, 1.2 ~ 1.5% yttrium oxide, 0.5% lanthanum trioxide, 3 ~ 3.3% magnesiumcarbonate, make by the mixing of technical process ball milling, granulation, moulding, sintering.
Beneficial effect of the present invention is: zirconium white is with after aluminum oxide mixes by a certain percentage, by accurate technology controlling and process, realize having complementary advantages, can overcome zirconic powder phenomenon-tion, can overcome the shortcoming that the aluminum oxide fracture toughness property is low again, the ceramic liner of producing is corrosion-resistant, acid and alkali-resistance, high temperature resistant, can meet in drilling mud or the strong liquid and other medium of other corrodibility and work, the various sharp-pointed or solid phase particles that abrasive property is strong that hardness is enough to resist in high-pressure slurry grinds or washes away.The heterogeneous microstructure of pottery is even, and surface gloss is high, is conducive to improve the life-span of piston.The operating pressure of ceramic liner is high, can meet deep-well, the demand of ultra deep well of boring.
Embodiment
100 kilogram weights of per-cents are consisted of: 65% aluminum oxide, 24% zirconium white, 1.5% yttrium oxide, 0.5% lanthanum trioxide, 3% magnesiumcarbonate, after adding ammonium citrate that 50 kg of water and weight percent are 0.4% by the mixing of technical process ball milling, granulation, hydrostatic profile cylinder sleeve, burn till 4 hours at 1650 ℃.The ceramic liner of producing is corrosion-resistant, acid and alkali-resistance, high temperature resistant, can meet in drilling mud or the strong liquid and other medium of other corrodibility and work, and the various sharp-pointed or solid phase particles that abrasive property is strong that hardness is enough to resist in high-pressure slurry grinds or washes away.The heterogeneous microstructure of pottery is even, and surface gloss is high, is conducive to improve the life-span of piston.The operating pressure of ceramic liner is high, can meet deep-well, the demand of ultra deep well of boring.
Claims (1)
1. a Zirconia reinforced alumina ceramic liner, is characterized in that, weight percent is consisted of: 60 ~ 70% aluminum oxide, 20 ~ 30% zirconium white, 1.2 ~ 1.5% yttrium oxide, 0.5% lanthanum trioxide, 3 ~ 3.3% magnesiumcarbonate, make by the mixing of technical process ball milling, granulation, moulding, sintering.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310440880.XA CN103496952A (en) | 2013-09-25 | 2013-09-25 | Zirconia toughened alumina ceramic cylinder sleeve |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310440880.XA CN103496952A (en) | 2013-09-25 | 2013-09-25 | Zirconia toughened alumina ceramic cylinder sleeve |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103496952A true CN103496952A (en) | 2014-01-08 |
Family
ID=49862243
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310440880.XA Pending CN103496952A (en) | 2013-09-25 | 2013-09-25 | Zirconia toughened alumina ceramic cylinder sleeve |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103496952A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104291815A (en) * | 2014-09-25 | 2015-01-21 | 无锡康柏斯机械科技有限公司 | Wear-resistant corrosion-resistant toughened ceramic cylinder liner and preparation method thereof |
| CN104446454A (en) * | 2014-09-17 | 2015-03-25 | 范兴宽 | Research on high-performance ceramic cylinder sleeve preparation process |
| CN104761262A (en) * | 2015-03-23 | 2015-07-08 | 宁夏机械研究院股份有限公司 | Silicon carbide ceramic cylinder sleeve for well-drilling slurry pump and preparation method of silicon carbide ceramic cylinder sleeve |
| CN105036714A (en) * | 2015-07-28 | 2015-11-11 | 湖南大学 | Ceramic piston for air-conditioning compressor and preparation method of ceramic piston |
| CN114560686A (en) * | 2022-03-24 | 2022-05-31 | 东莞市西陶精密陶瓷有限公司 | Ceramic square hole tube and preparation method and application thereof |
| CN114702327A (en) * | 2022-03-24 | 2022-07-05 | 广东工业大学 | A kind of high-strength and tough alumina-based composite ceramic substrate and preparation method thereof |
| CN116197625A (en) * | 2023-04-28 | 2023-06-02 | 安徽巨盛石油钻采配件有限公司 | Preparation process of high-pressure-resistant wear-resistant cylinder sleeve |
| US12209055B2 (en) | 2021-12-28 | 2025-01-28 | Industrial Technology Research Institute | Ceramic material and ceramic object |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1990421A (en) * | 2005-12-29 | 2007-07-04 | 中国核动力研究设计院 | Preparation process of zirconia toughened alumina ceramic composite cylinder sleeve |
| CN103113090A (en) * | 2012-12-12 | 2013-05-22 | 杨益 | Ceramic material and preparation method thereof |
| CN103304222A (en) * | 2013-05-31 | 2013-09-18 | 哈尔滨工业大学 | A method of combustion synthesis melting and casting of Al2O3/ZrO2 eutectic ceramics |
-
2013
- 2013-09-25 CN CN201310440880.XA patent/CN103496952A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1990421A (en) * | 2005-12-29 | 2007-07-04 | 中国核动力研究设计院 | Preparation process of zirconia toughened alumina ceramic composite cylinder sleeve |
| CN103113090A (en) * | 2012-12-12 | 2013-05-22 | 杨益 | Ceramic material and preparation method thereof |
| CN103304222A (en) * | 2013-05-31 | 2013-09-18 | 哈尔滨工业大学 | A method of combustion synthesis melting and casting of Al2O3/ZrO2 eutectic ceramics |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104446454A (en) * | 2014-09-17 | 2015-03-25 | 范兴宽 | Research on high-performance ceramic cylinder sleeve preparation process |
| CN104291815A (en) * | 2014-09-25 | 2015-01-21 | 无锡康柏斯机械科技有限公司 | Wear-resistant corrosion-resistant toughened ceramic cylinder liner and preparation method thereof |
| CN104761262A (en) * | 2015-03-23 | 2015-07-08 | 宁夏机械研究院股份有限公司 | Silicon carbide ceramic cylinder sleeve for well-drilling slurry pump and preparation method of silicon carbide ceramic cylinder sleeve |
| CN105036714A (en) * | 2015-07-28 | 2015-11-11 | 湖南大学 | Ceramic piston for air-conditioning compressor and preparation method of ceramic piston |
| US12209055B2 (en) | 2021-12-28 | 2025-01-28 | Industrial Technology Research Institute | Ceramic material and ceramic object |
| CN114560686A (en) * | 2022-03-24 | 2022-05-31 | 东莞市西陶精密陶瓷有限公司 | Ceramic square hole tube and preparation method and application thereof |
| CN114702327A (en) * | 2022-03-24 | 2022-07-05 | 广东工业大学 | A kind of high-strength and tough alumina-based composite ceramic substrate and preparation method thereof |
| CN114560686B (en) * | 2022-03-24 | 2023-01-17 | 东莞市西陶精密陶瓷有限公司 | Ceramic square hole tube and preparation method and application thereof |
| CN116197625A (en) * | 2023-04-28 | 2023-06-02 | 安徽巨盛石油钻采配件有限公司 | Preparation process of high-pressure-resistant wear-resistant cylinder sleeve |
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Application publication date: 20140108 |