CN103471953A - Automatic test system and test method for testing surface capillary water absorption of concrete - Google Patents
Automatic test system and test method for testing surface capillary water absorption of concrete Download PDFInfo
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Abstract
Description
技术领域technical field
本发明涉及一种测试系统及其测试方法,特别是混凝土表面毛细吸水率自动测试系统及其测试方法。The invention relates to a test system and a test method thereof, in particular to an automatic test system and a test method for capillary water absorption of concrete surface.
背景技术Background technique
混凝土材料的耐久性对于混凝土结构全寿命周期的安全性、经济性具有重要意义。如何正确评估、检测混凝土材料的耐久性,对于混凝土材料的工程应用非常重要。混凝土的耐久性与侵蚀性介质通过材料内部的孔隙、裂纹往内部迁移的快慢密切相关。毛细吸水率能定量刻画在毛细作用下混凝土材料吸入水分的容易程度或快慢,且与水分扩散率、渗透率之间存在明确、严格的理论关系,是一个定量表征混凝土材料耐久性优劣的重要指标。相比于混凝土气体、水分及氯离子渗透率等指标的测试来说,表面毛细吸水率通过测量混凝土试件单位面积吸水质量随时间的变化快慢来评价混凝土材料物质传输性能、耐久性能的好坏,测试原理简单且尤其适合于表征与耐久性直接、密切相关的表层混凝土的质量优劣,在学术界与工程界广泛应用。The durability of concrete materials is of great significance to the safety and economy of the whole life cycle of concrete structures. How to correctly evaluate and detect the durability of concrete materials is very important for the engineering application of concrete materials. The durability of concrete is closely related to the speed at which aggressive media migrate through the pores and cracks inside the material. Capillary water absorption can quantitatively describe the ease or speed of water absorption by concrete materials under capillary action, and there is a clear and strict theoretical relationship with water diffusivity and permeability. It is an important indicator for quantitatively characterizing the durability of concrete materials. index. Compared with the test of concrete gas, moisture and chloride ion permeability and other indicators, the surface capillary water absorption rate is used to evaluate the material transmission performance and durability of concrete materials by measuring the speed of water absorption per unit area of concrete specimens over time. , the test principle is simple and is especially suitable for characterizing the quality of surface concrete, which is directly and closely related to durability, and is widely used in academia and engineering.
表面毛细吸水率测试要求监测侧面密封的试件在表面与水接触过程中的质量变化,实际测量时往往直接通过手工测量混凝土试件的质量变化来计算。此时随着表面毛细吸水的进行,在整个测量过程中难以保证混凝土试件浸没在水中的深度始终恒定为一较小值。其次,由于混凝土试件密度、质量均较大而吸水质量相对很小,直接测试吸水混凝土试件的质量时还要求用湿布擦干试件与水接触表面上的自由水,这使得吸水质量的测量精度低且容易受到人工操作误差的影响。此外,手工测量吸水混凝土试件的质量必然需要花费一定的时间,测试质量期间不能停止计时而此期间混凝土试件表面的水力边界条件被改变,这会使得表面接触自由水并在毛细驱动力作用下将水吸入材料内部的整个过程受到干扰。上述多方面的影响因素使得表面毛细吸水率的测量结果可能引入较大误差,且难以长时间连续进行监测。Sabir于1998年提出采用悬挂式的电子天平直接测量吸水混凝土试件的质量变化来换算毛细吸水率,尽管可以避免手工擦干试件与水的接触面导致的人工操作误差,但该系统测试时仍不能保证试件浸没于水中的深度始终恒定为一较小值。Cerny等于2006年提出采用马氏瓶装置来维持水位恒定,他在Sabir的测试装置的基础上有些改进,但它与Sabir所提装置一样通过测量密度、质量较大的混凝土试件的质量变化来计算吸水质量,由于毛细吸水产生的质量变化非常微小而传统马氏瓶的灵敏度(待测水位变化的灵敏度约为0.5mm)不能满足要求,使得混凝土毛细吸水质量的测量精度难以保证,对测试长期吸水质量变化尤其不利。The surface capillary water absorption test requires monitoring the mass change of the side-sealed specimen when the surface is in contact with water, and the actual measurement is often directly calculated by manually measuring the mass change of the concrete specimen. At this time, with the progress of capillary water absorption on the surface, it is difficult to ensure that the depth of the concrete specimen immersed in water is always a small value during the entire measurement process. Secondly, due to the high density and mass of concrete specimens and the relatively small water absorption mass, when directly testing the quality of water-absorbing concrete specimens, it is also required to dry the free water on the surface of the specimens in contact with water with a damp cloth, which makes the water absorption quality difficult to determine. The measurement accuracy is low and it is easily affected by manual operation error. In addition, manual measurement of the mass of water-absorbing concrete specimens will inevitably take a certain amount of time, and the timing cannot be stopped during the quality test. During this period, the hydraulic boundary conditions on the surface of the concrete specimens are changed, which will make the surface contact with free water and act on the capillary driving force. The entire process of drawing water into the interior of the material is disturbed. The above-mentioned various influencing factors make the measurement results of surface capillary water absorption may introduce large errors, and it is difficult to monitor continuously for a long time. In 1998, Sabir proposed to use a suspended electronic balance to directly measure the mass change of the water-absorbing concrete specimen to convert the capillary water absorption rate. Although the manual operation error caused by manually drying the contact surface between the specimen and water can be avoided, the system is tested. It still cannot guarantee that the depth of the test piece submerged in water is always constant to a small value. In 2006, Cerny proposed to use a Martens bottle device to maintain a constant water level. He made some improvements on the basis of Sabir's test device, but it is the same as the device proposed by Sabir by measuring the mass change of a concrete specimen with a large density and mass. Calculating the water absorption quality, because the mass change caused by capillary water absorption is very small and the sensitivity of the traditional Malovich bottle (the sensitivity of the water level change to be measured is about 0.5mm) cannot meet the requirements, making it difficult to guarantee the measurement accuracy of the concrete capillary water absorption quality, which is very important for long-term testing. Changes in the quality of water absorption are particularly disadvantageous.
发明内容Contents of the invention
本发明的目的是为了解决现有表面毛细吸水率测试系统难以保证混凝土试件浸没在水中的有效深度始终恒定为一较小值,不能对混凝土试件的吸水质量进行实时、自动化连续测量并且存在手工操作等引入的偶然误差、测试灵敏度低、精度低的问题,提供一种混凝土表面毛细吸水率自动测试系统及其测试方法。The purpose of the present invention is to solve the problem that the existing surface capillary water absorption test system is difficult to ensure that the effective depth of the concrete specimen immersed in water is always a small value, and the water absorption quality of the concrete specimen cannot be measured in real time, automatically and continuously, and there are In order to solve the problems of accidental error, low test sensitivity and low precision introduced by manual operation, an automatic test system and test method for concrete surface capillary water absorption are provided.
本发明的一种混凝土表面毛细吸水率自动测试系统,由恒压给水单元、电子天平和试件吸水单元构成,恒压给水单元与试件吸水单元通过出水管、硅胶软管和进水管连通;A concrete surface capillary water absorption automatic testing system of the present invention is composed of a constant pressure water supply unit, an electronic balance and a test piece water absorption unit, and the constant pressure water supply unit and the test piece water absorption unit are connected through a water outlet pipe, a silicone hose and a water inlet pipe;
所述的恒压给水单元由恒压给水密封瓶、气体连通管、平衡进气管和出水管构成;所述的电子天平设置在恒压给水密封瓶底端并用来测量恒压给水单元的重量;其中,气体连通管与平衡进气管均设置在恒压给水密封瓶的上端,气体连通管在恒压给水密封瓶内部的一端设置在靠近恒压给水密封瓶的上端,平衡进气管在恒压给水密封瓶内部的一端设置在靠近恒压给水密封瓶的下端;气体连通管上部设置有一个气体阀门;平衡进气管上部设置有一个气体阀门;平衡进气管底部设置有一个针管;带阀门的出水管一端与恒压给水密封瓶底部侧端连通,另一端通过硅胶软管与进水管连通,所述的进水管与试样密封室底部侧面连通;The constant pressure water supply unit is composed of a constant pressure water supply sealed bottle, a gas connecting pipe, a balance inlet pipe and a water outlet pipe; the electronic balance is arranged at the bottom of the constant pressure water supply sealed bottle and is used to measure the weight of the constant pressure water supply unit; Among them, the gas connecting pipe and the balanced air inlet pipe are both arranged on the upper end of the constant pressure water supply sealed bottle, and the end of the gas connected pipe inside the constant pressure water sealed bottle is arranged near the upper end of the constant pressure water fed sealed bottle, and the balanced air inlet pipe is placed on the constant pressure water supply sealed bottle. One end inside the sealed bottle is set near the lower end of the constant pressure water supply sealed bottle; a gas valve is arranged on the upper part of the gas communication pipe; a gas valve is arranged on the upper part of the balanced air inlet pipe; a needle tube is arranged at the bottom of the balanced air inlet pipe; the outlet pipe with valve One end communicates with the bottom side end of the constant pressure water supply seal bottle, and the other end communicates with the water inlet pipe through a silicone hose, and the water inlet pipe communicates with the bottom side of the sample sealing chamber;
所述的试件吸水单元由试样密封室、进水管、排水阀、调节阀、L型水位计和试样支撑件构成;其中,试样密封室上部设置有一个水平仪,在下端设置有进水管,在密封室右侧下端设置有L型水位计,L型水位计另一端朝上设置;试样密封室右侧上端设置有调节阀;排水阀设置在试样密封室的底部;试样密封室底部内侧设置有三个等高的试样支撑件。The sample water absorption unit is composed of a sample sealing chamber, a water inlet pipe, a drain valve, a regulating valve, an L-shaped water level gauge and a sample support; wherein, a level is arranged on the upper part of the sample sealing chamber, and an inlet is arranged on the lower end. For the water pipe, an L-shaped water level gauge is installed at the lower end of the right side of the sealed chamber, and the other end of the L-shaped water level gauge is set upward; a regulating valve is installed at the upper right end of the sample sealed chamber; Three equal-height sample supports are arranged on the inner side of the bottom of the sealed chamber.
本发明的一种混凝土表面毛细吸水率自动测试系统的测试方法如下:The test method of a kind of concrete surface capillary water absorption automatic test system of the present invention is as follows:
一、关闭出水管上的阀门,往恒压给水密封瓶装水至恰不淹没气体连通管的下端;打开气体连通管上的气体阀门和平衡进气管上的气体阀门并密封好恒压给水密封瓶,之后关闭气体连通管上部的气体阀门;打开出水管上的阀门,恒压给水密封瓶内部的水通过出水管流出,恒压给水密封瓶内的水位微降、内部空腔气压稍降且平衡进气管内的水位较快下降,待其水位下降到平衡进气管的下端且气体开始通过平衡进气管进入恒压给水密封瓶时,关闭出水管上的阀门,排空平衡进气管内液体完成,恒压给水密封瓶内部液体处于平衡状态;1. Close the valve on the water outlet pipe, seal the bottled water to the constant pressure water supply until it does not submerge the lower end of the gas connection pipe; open the gas valve on the gas connection pipe and the gas valve on the balance inlet pipe and seal the constant pressure water supply seal bottle , and then close the gas valve on the upper part of the gas communication pipe; open the valve on the water outlet pipe, the water inside the constant pressure water supply sealed bottle flows out through the water outlet pipe, the water level in the constant pressure water supply sealed bottle drops slightly, and the air pressure in the internal cavity drops slightly and balances The water level in the intake pipe drops rapidly. When the water level drops to the lower end of the balanced intake pipe and the gas begins to enter the constant pressure water supply seal bottle through the balanced intake pipe, close the valve on the water outlet pipe to empty the liquid in the balanced intake pipe. The liquid inside the constant pressure water supply sealed bottle is in a balanced state;
二、用硅胶软管将出水管与进水管相连通,关闭排水阀,打开调节阀,往试样密封室内加水至淹没进水管和L形水位计与试样密封室的联通孔,同时要求水位淹没试样支撑件的顶端3mm,盖好试样密封室的顶盖并密封好;调整高度调节脚使试件密封瓶的高度变化至使内部液面低于平衡进气管的针尖水平高度10~15mm,打开出水管上的阀门,恒压给水密封瓶内的水开始向试样密封室内补充并排空硅胶软管内可能存在的气体,关闭调节阀,试样密封室内水位保持不变,L形水位计内的水位继续上升并可能发生溢出;调整高度调节脚使气体不再通过平衡进气管进入恒压给水密封瓶内并且L形水位计内的相应平衡水位低于L形水位计的顶端1mm,同时通过水平仪控制试件吸水单元水平;试件吸水单元高度及水位调整完毕,整个系统处于水位平衡状态;此时若从L形水位计顶端吸走微量水分,气体将通过平衡进气管进入恒压给水密封瓶,并使整个系统重新处于平衡状态;2. Use a silicone hose to connect the outlet pipe with the water inlet pipe, close the drain valve, open the regulating valve, add water to the sample sealing chamber to submerge the water inlet pipe and the communication hole between the L-shaped water level gauge and the sample sealing chamber, and at the same time require the water level Submerge the top of the sample support by 3mm, cover and seal the top cover of the sample sealing chamber; adjust the height adjustment feet to change the height of the sample sealing bottle to make the
三、关闭出水管上的阀门,打开调节阀,打开试样密封室的上盖,通过排水阀降低试样密封室的水位并使试样支撑件的尖端露出水面;将所有侧面密封的混凝土试件置于试件支撑件上部且暂时不与水接触,盖上试样密封室的上盖并密封好;打开出水管上的阀门,水开始从恒压给水密封瓶内向试样密封室内补充,气体通过平衡进气管进入恒压给水密封瓶内且试样密封室内的水位逐渐升高,待其内部水位淹没试件的高度为3mm时关闭调节阀,试样密封室内水位不变而L形水位计内水位继续上升至离顶端1mm时达平衡状态,让计算机开始按事先设置好的时间间隔采集恒压给水单元的质量数据。随着混凝土试件吸水,试样密封室内的气压微降,水继续从恒压给水密封瓶向试样密封室内补充,恒压给水密封瓶上部气体空腔压力下降,外部大气通过平衡进气管向恒压给水密封瓶内部补充并达到新的平衡状态。平衡后,L形水位计内的液位不变,对应试件底面淹没于水中的有效深度恒定,试件吸入水的质量等于恒压给水单元质量的减少量并能够被电子天平测出,计算机采集电子天平的质量减少量即等于混凝土试件质量的增加量,通过质量变化量可计算混凝土试件的表面毛细吸水率。3. Close the valve on the water outlet pipe, open the regulating valve, open the upper cover of the sample sealing chamber, lower the water level of the sample sealing chamber through the drain valve and make the tip of the sample support part exposed to the water surface; Put the test piece on the upper part of the support piece of the test piece and temporarily do not contact with water, cover the upper cover of the sample sealing chamber and seal it well; open the valve on the water outlet pipe, water starts to replenish from the constant pressure water supply sealing bottle to the sample sealing chamber, The gas enters the constant pressure water supply sealed bottle through the balance inlet pipe, and the water level in the sample sealed chamber gradually rises. When the internal water level submerges the test piece to a height of 3mm, close the regulating valve, and the water level in the sample sealed chamber remains unchanged and the L-shaped water level The water level in the meter continues to rise until it is 1mm from the top and reaches a balanced state, allowing the computer to start collecting quality data of the constant pressure water supply unit at a preset time interval. As the concrete specimen absorbs water, the air pressure in the sample sealing chamber drops slightly, water continues to be replenished from the constant pressure water supply sealing bottle to the sample sealing chamber, the pressure of the gas cavity in the upper part of the constant pressure water supply sealing bottle drops, and the external atmosphere flows into the sample sealing chamber through the balanced air inlet pipe. Constant pressure feeds water to the inside of the sealed bottle to replenish and reach a new equilibrium state. After balancing, the liquid level in the L-shaped water level gauge remains unchanged, and the effective depth corresponding to the bottom surface of the test piece submerged in water is constant. The mass of water absorbed by the test piece is equal to the reduction in the mass of the constant pressure water supply unit and can be measured by the electronic balance. Computer The mass decrease of the collection electronic balance is equal to the increase of the concrete specimen mass, and the surface capillary water absorption of the concrete specimen can be calculated through the mass change.
本发明包含以下有益效果:The present invention comprises following beneficial effect:
1、由于恒压给水单元与试件吸水单元之间通过硅胶软管相连通,恒压给水单元能够严格保证L形水位计的液面恒定不变,从而保证混凝土试件底面浸没于水中的有效深度为一恒定较小值,严格满足表面毛细吸水率测试所要求的水力边界条件,同时可以避免长时间测试时试样密封室内水分蒸发影响测量精度;1. Since the constant pressure water supply unit and the specimen water absorption unit are connected through a silicone hose, the constant pressure water supply unit can strictly ensure that the liquid level of the L-shaped water level gauge is constant, thereby ensuring that the bottom of the concrete specimen is immersed in water effectively. The depth is a constant minimum value, which strictly meets the hydraulic boundary conditions required by the surface capillary water absorption test, and can avoid affecting the measurement accuracy due to the evaporation of water in the sample sealing chamber during long-term testing;
本发明采用试样密封室搭配调节阀,不但可以保证试件底面浸没于水中的有效深度恒定为一较小数值,同时可以避免长时间测试时试样密封室内水分蒸发影响测量精度,采用L型水位计搭配试样密封室能大幅提升测试系统的灵敏度,本发明试样吸水约0.5g时平衡进气管即开始补气,对应密封室内水位变化约为0.02mm,由于平衡进气管底端弯液面的存在并能自适应调整液面的弯曲程度,实际吸水质量测量精度更高;而传统马氏瓶对待测水位变化的灵敏度约为0.5mm;The present invention adopts a sample sealing chamber with a regulating valve, which can not only ensure that the effective depth of the bottom surface of the test piece immersed in water is constant at a small value, but also avoid the impact of water evaporation in the sample sealing chamber on the measurement accuracy during long-term testing. The L-type The water level gauge and the sample sealing chamber can greatly improve the sensitivity of the test system. When the sample absorbs about 0.5g of water in the present invention, the balance inlet pipe will start to replenish air, and the water level in the corresponding sealing chamber will change by about 0.02mm. The existence of the liquid surface can adaptively adjust the curvature of the liquid surface, and the measurement accuracy of the actual water absorption quality is higher; while the sensitivity of the traditional Martens bottle to the change of the measured water level is about 0.5mm;
2、由于恒压给水单元与试件吸水单元之间通过硅胶软管相连通,混凝土试件所吸收的水分能够实时、连续地从恒压给水单元得到补充,混凝土试件的吸水量恒等于恒压给水单元质量的减少量,通过间接测量恒压给水单元质量的减少量可以实时测量混凝土试件的吸水量,具有较高测试精度且能满足对各种不同大小、不同质量混凝土试件表面毛细吸水率的测试要求;2. Since the constant pressure water supply unit and the specimen water absorption unit are connected through a silicone hose, the moisture absorbed by the concrete specimen can be replenished from the constant pressure water supply unit in real time and continuously, and the water absorption of the concrete specimen is equal to constant The reduction of the mass of the pressure water supply unit, through the indirect measurement of the reduction of the mass of the constant pressure water supply unit, can measure the water absorption of the concrete specimen in real time. Water absorption test requirements;
3、由于通过间接测量恒压给水单元的质量变化来监测混凝土试件的吸水质量,可以减小由于手工擦干混凝土试件底面自由水、试件底面脱离自由水一段时间等因素而引入的偶然误差;3. Since the water absorption quality of the concrete specimen is monitored by indirect measurement of the quality change of the constant pressure water supply unit, it can reduce the accidental water caused by manual drying of the free water at the bottom of the concrete specimen, and the free water at the bottom of the specimen for a period of time. error;
4、由于采用电子天平测量恒压给水单元的质量变化来间接测量混凝土试件的吸水质量,可以做到实时、连续、全自动且长时间的跟踪测量,可以用于测量、研究混凝土材料长时间表面吸水的质量变化及其表面毛细吸水率。本发明能严格满足表面毛细吸水率测试所要求的混凝土试件浸没于水中的有效深度恒定为一较小数值的水力边界条件,能实时、全自动、长时间地连续测试且精度高、试验结果重现性好,试验操作方便,可以应用于混凝土材料孔隙(裂纹)结构、表面毛细吸水率的试验研究及实际工程耐久性检测领域。4. Because the electronic balance is used to measure the quality change of the constant pressure water supply unit to indirectly measure the water absorption quality of the concrete specimen, real-time, continuous, fully automatic and long-term tracking measurement can be achieved, and it can be used to measure and study concrete materials for a long time Mass change of surface water absorption and its surface capillary water absorption. The invention can strictly meet the hydraulic boundary condition that the effective depth of the concrete specimen submerged in water is constant to a small value required by the surface capillary water absorption test, and can perform real-time, fully automatic and long-term continuous testing with high precision and excellent test results. With good reproducibility and convenient test operation, it can be applied to the experimental research of concrete material pore (crack) structure, surface capillary water absorption and actual engineering durability testing.
附图说明Description of drawings
图1为表面毛细吸水率自动化测量系统结构示意图;Fig. 1 is the structure schematic diagram of automatic measurement system of surface capillary water absorption;
图2为实施例一中混凝土表面毛细吸水率测试结果图,其中·表示实测数据,——表示拟合曲线。Fig. 2 is a test result graph of concrete surface capillary water absorption in Example 1, wherein · represents the measured data, — represents the fitting curve.
具体实施方式Detailed ways
本发明技术方案不局限于以下所列举具体实施方式,还包括各具体实施方式间的任意组合。The technical solution of the present invention is not limited to the specific embodiments listed below, but also includes any combination of the specific embodiments.
具体实施方式一:本实施方式的一种混凝土表面毛细吸水率自动测试系统由恒压给水单元、电子天平2和试件吸水单元构成,恒压给水单元与试件吸水单元通过出水管7、硅胶软管8和进水管9连通;Specific embodiment one: a kind of concrete surface capillary water absorption automatic test system of this embodiment is made up of constant pressure water supply unit,
所述的恒压给水单元由恒压给水密封瓶1、气体连通管5、平衡进气管6和出水管7构成;所述的电子天平2设置在恒压给水密封瓶1底端并用来测量恒压给水单元的重量;其中,气体连通管5与平衡进气管6均设置在恒压给水密封瓶1的上端,气体连通管5在恒压给水密封瓶1内部的一端设置在靠近恒压给水密封瓶1的上端,平衡进气管6在恒压给水密封瓶1内部的一端设置在靠近恒压给水密封瓶1的下端;气体连通管5上部设置有一个气体阀门14;平衡进气管6上部设置有一个气体阀门15;平衡进气管6底部设置有一个针管;带阀门16的出水管7一端与恒压给水密封瓶1底部侧端连通,另一端通过硅胶软管8与进水管9连通,所述的进水管9与试样密封室3底部侧面连通;The constant pressure water supply unit is composed of a constant pressure water supply sealed bottle 1, a gas communication pipe 5, a balance inlet pipe 6 and a water outlet pipe 7; the electronic balance 2 is arranged at the bottom of the constant pressure water supply sealed bottle 1 and is used to measure the The weight of the pressure water supply unit; wherein, the gas communication pipe 5 and the balance air intake pipe 6 are all arranged on the upper end of the constant pressure water supply sealed bottle 1, and the end of the gas communication pipe 5 inside the constant pressure water supply sealed bottle 1 is arranged near the constant pressure water supply seal On the upper end of the bottle 1, one end of the balanced air intake pipe 6 inside the constant pressure water supply sealed bottle 1 is arranged near the lower end of the constant pressure water supply sealed bottle 1; the upper part of the gas communication pipe 5 is provided with a gas valve 14; the upper part of the balanced air intake pipe 6 is provided with A gas valve 15; a needle tube is arranged at the bottom of the balance inlet pipe 6; one end of the water outlet pipe 7 with the valve 16 communicates with the side end of the bottom of the constant pressure water supply sealing bottle 1, and the other end communicates with the water inlet pipe 9 through the silicone hose 8. The
所述的试件吸水单元由试样密封室3、进水管9、排水阀10、调节阀11、L型水位计12和试样支撑件13构成;其中,试样密封室3上部设置有一个水平仪18,在下端设置有进水管9,在密封室3右侧下端设置有L型水位计12,L型水位计12另一端朝上设置;试样密封室3右侧上端设置有调节阀11;排水阀10设置在试样密封室3的底部;试样密封室3底部内侧设置有三个等高的试样支撑件13。The sample water absorption unit is composed of a
本实施方式的有益效果:The beneficial effect of this implementation mode:
1、由于恒压给水单元与试件吸水单元之间通过硅胶软管相连通,恒压给水单元能够严格保证L形水位计的液面恒定不变,从而保证混凝土试件底面浸没于水中的有效深度为一恒定较小值,严格满足表面毛细吸水率测试所要求的水力边界条件,同时可以避免长时间测试时试样密封室内水分蒸发影响测量精度;1. Since the constant pressure water supply unit and the specimen water absorption unit are connected through a silicone hose, the constant pressure water supply unit can strictly ensure that the liquid level of the L-shaped water level gauge is constant, thereby ensuring that the bottom of the concrete specimen is immersed in water effectively. The depth is a constant minimum value, which strictly meets the hydraulic boundary conditions required by the surface capillary water absorption test, and can avoid affecting the measurement accuracy due to the evaporation of water in the sample sealing chamber during long-term testing;
本实施方式采用试样密封室搭配调节阀,不但可以保证试件底面浸没于水中的有效深度恒定为一较小数值,同时可以避免长时间测试时试样密封室内水分蒸发影响测量精度,采用L型水位计搭配试样密封室能大幅提升测试系统的灵敏度,本实施方式试样吸水约0.5g时平衡进气管即开始补气,对应密封室内水位变化约为0.02mm,由于平衡进气管底端弯液面的存在并能自适应调整液面的弯曲程度,实际吸水质量测量精度更高;而传统马氏瓶对待测水位变化的灵敏度约为0.5mm;In this embodiment, the sample sealing chamber is used with a regulating valve, which not only ensures that the effective depth of the bottom surface of the test piece immersed in water is kept at a small value, but also avoids the influence of water evaporation in the sample sealing chamber on the measurement accuracy during long-term testing. The combination of a water level gauge with a sample sealing chamber can greatly improve the sensitivity of the test system. In this embodiment, when the sample absorbs about 0.5g of water, the balance inlet pipe will start to replenish air, and the water level in the corresponding sealing chamber will change by about 0.02mm. The existence of the meniscus can adaptively adjust the curvature of the liquid surface, and the measurement accuracy of the actual water absorption quality is higher; while the sensitivity of the traditional Martens bottle to the change of the measured water level is about 0.5mm;
2、由于恒压给水单元与试件吸水单元之间通过硅胶软管相连通,混凝土试件所吸收的水分能够实时、连续地从恒压给水单元得到补充,混凝土试件的吸水量恒等于恒压给水单元质量的减少量,通过间接测量恒压给水单元质量的减少量可以实时测量混凝土试件的吸水量,具有较高测试精度且能满足对各种不同大小、不同质量混凝土试件表面毛细吸水率的测试要求。2. Since the constant pressure water supply unit and the specimen water absorption unit are connected through a silicone hose, the moisture absorbed by the concrete specimen can be replenished from the constant pressure water supply unit in real time and continuously, and the water absorption of the concrete specimen is equal to constant The reduction of the mass of the pressure water supply unit, through the indirect measurement of the reduction of the mass of the constant pressure water supply unit, can measure the water absorption of the concrete specimen in real time. Water absorption test requirements.
具体实施方式二:本实施方式与具体实施方式一不同的是:所述的试件吸水单元还包括高度调节脚17和水平仪18。其它与具体实施方式一相同。Embodiment 2: This embodiment differs from Embodiment 1 in that: the specimen water absorption unit also includes
具体实施方式三:本实施方式与具体实施方式一或二不同的是:所述的试样密封室3外侧设置有三个等高的高度调节脚17,并坐落于水平操作台19上。其它与具体实施方式一或二相同。Embodiment 3: This embodiment differs from Embodiment 1 or
具体实施方式四:本实施方式与具体实施方式一至三之一不同的是:所述的电子天平2的量程为1000g,精度为0.001g。其它与具体实施方式一至三之一相同。Embodiment 4: This embodiment differs from Embodiments 1 to 3 in that: the
具体实施方式五:本实施方式与具体实施方式一至四之一不同的是:所述的气体连通管5、平衡进气管6、出水管7、进水管9和L形水位计12材质为有机玻璃。其它与具体实施方式一至四之一相同。Embodiment 5: This embodiment is different from Embodiment 1 to
具体实施方式六:本实施方式与具体实施方式一至五之一不同的是:所述的L形水位计12的顶端高于试样支撑件13的顶端的铅垂方向距离为5mm。其它与具体实施方式一至五之一相同。Embodiment 6: This embodiment differs from Embodiment 1 to
具体实施方式七:本实施方式一种混凝土表面毛细吸水率自动测试系统的测试方法,其测试方法包括如下步骤:Specific implementation mode seven: the present embodiment is a test method of a concrete surface capillary water absorption automatic test system, and its test method comprises the following steps:
一、关闭出水管7上的阀门16,往恒压给水密封瓶1装水至恰不淹没气体连通管5的下端;打开气体连通管5上的气体阀门14和平衡进气管6上的气体阀门15并密封好恒压给水密封瓶1,之后关闭气体连通管5上部的气体阀门14;打开出水管7上的阀门16,恒压给水密封瓶1内部的水通过出水管7流出,恒压给水密封瓶1内的水位微降、内部空腔气压稍降且平衡进气管6内的水位较快下降,待其水位下降到平衡进气管6的下端且气体开始通过平衡进气管6进入恒压给水密封瓶1时,关闭出水管7上的阀门16,排空平衡进气管内液体完成,恒压给水密封瓶1内部液体处于平衡状态;1. Close the
二、用硅胶软管8将出水管7与进水管9相连通,关闭排水阀10,打开调节阀11,往试样密封室3内加水至淹没进水管9和L形水位计12与试样密封室3的联通孔,同时要求水位淹没试样支撑件13的顶端3mm,盖好试样密封室3的顶盖并密封好;调整高度调节脚17使试件密封瓶3的高度变化至使内部液面低于平衡进气管6的针尖水平高度10~15mm,打开出水管7上的阀门16,恒压给水密封瓶1内的水开始向试样密封室3内补充并排空硅胶软管8内可能存在的气体,关闭调节阀11,试样密封室3内水位保持不变,L形水位计12内的水位继续上升并可能发生溢出;调整高度调节脚17使气体不再通过平衡进气管6进入恒压给水密封瓶1内并且L形水位计12内的相应平衡水位低于L形水位计的顶端1mm,同时通过水平仪18控制试件吸水单元水平;试件吸水单元高度及水位调整完毕,整个系统处于水位平衡状态;此时若从L形水位计顶端吸走微量水分,气体将通过平衡进气管6进入恒压给水密封瓶1,并使整个系统重新处于平衡状态;2. Use a
三、关闭出水管7上的阀门16,打开调节阀11,打开试样密封室3的上盖,通过排水阀10降低试样密封室3的水位并使试样支撑件13的尖端露出水面;将所有侧面密封的混凝土试件4置于试件支撑件13上部且暂时不与水接触,盖上试样密封室3的上盖并密封好;打开出水管7上的阀门16,水开始从恒压给水密封瓶1内向试样密封室3内补充,气体通过平衡进气管6进入恒压给水密封瓶1内且试样密封室3内的水位逐渐升高,待其内部水位淹没试件4的高度为3mm时关闭调节阀11,试样密封室3内水位不变而L形水位计12内水位继续上升至离顶端1mm时达平衡状态,让计算机开始按事先设置好的时间间隔采集恒压给水单元的质量数据。随着混凝土试件4吸水,试样密封室3内的气压微降,水继续从恒压给水密封瓶1向试样密封室3内补充,恒压给水密封瓶1上部气体空腔压力下降,外部大气通过平衡进气管6向恒压给水密封瓶1内部补充并达到新的平衡状态。平衡后,L形水位计12内的液位不变,对应试件底面淹没于水中的有效深度恒定,试件吸入水的质量等于恒压给水单元质量的减少量并能够被电子天平2测出,计算机采集电子天平2的质量减少量即等于混凝土试件4质量的增加量,通过质量变化量可计算混凝土试件的表面毛细吸水率。3. Close the
本实施方式的有益效果:The beneficial effect of this implementation mode:
1、由于通过间接测量恒压给水单元的质量变化来监测混凝土试件的吸水质量,可以减小由于手工擦干混凝土试件底面自由水、试件底面脱离自由水一段时间等因素而引入的偶然误差;1. Since the water absorption quality of the concrete specimen is monitored by indirect measurement of the quality change of the constant pressure water supply unit, it can reduce the accidents caused by factors such as manually drying the free water on the bottom surface of the concrete specimen, and the bottom surface of the specimen being separated from free water for a period of time. error;
2、由于采用电子天平测量恒压给水单元的质量变化来间接测量混凝土试件的吸水质量,可以做到实时、连续、全自动且长时间的跟踪测量,可以用于测量、研究混凝土材料长时间表面吸水的质量变化及其表面毛细吸水率。本实施方式能严格满足表面毛细吸水率测试所要求的混凝土试件浸没于水中的有效深度恒定为一较小数值的水力边界条件,能实时、全自动、长时间地连续测试且精度高、试验结果重现性好,试验操作方便,可以应用于混凝土材料孔隙(裂纹)结构、表面毛细吸水率的试验研究及实际工程耐久性检测领域。2. Because the electronic balance is used to measure the quality change of the constant pressure water supply unit to indirectly measure the water absorption quality of the concrete specimen, real-time, continuous, fully automatic and long-term tracking measurement can be achieved, and it can be used to measure and study concrete materials for a long time Mass change of surface water absorption and its surface capillary water absorption. This embodiment can strictly meet the hydraulic boundary condition that the effective depth of the concrete specimen submerged in water is constant to a small value required by the surface capillary water absorption test, and can perform real-time, fully automatic, and long-term continuous testing with high precision. The reproducibility of the results is good, the test operation is convenient, and it can be applied to the experimental research of the pore (crack) structure of concrete materials, surface capillary water absorption and actual engineering durability testing.
通过以下实施例证明本发明的有益效果:Prove beneficial effect of the present invention by following examples:
实施例一:Embodiment one:
本实施例一种混凝土表面毛细吸水率自动测试系统,由恒压给水单元、电子天平2和试件吸水单元构成,恒压给水单元与试件吸水单元通过出水管7、硅胶软管8和进水管9连通;In this embodiment, a concrete surface capillary water absorption automatic testing system is composed of a constant pressure water supply unit, an
所述的恒压给水单元由恒压给水密封瓶1、气体连通管5、平衡进气管6和出水管7构成;所述的电子天平2设置在恒压给水密封瓶1底端并用来测量恒压给水单元的重量;其中,气体连通管5与平衡进气管6均设置在恒压给水密封瓶1的上端,气体连通管5在恒压给水密封瓶1内部的一端设置在靠近恒压给水密封瓶1的上端,平衡进气管6在恒压给水密封瓶1内部的一端设置在靠近恒压给水密封瓶1的下端;气体连通管5上部设置有一个气体阀门14;平衡进气管6上部设置有一个气体阀门15;平衡进气管6底部设置有一个针管;带阀门16的出水管7一端与恒压给水密封瓶1底部侧端连通,另一端通过硅胶软管8与进水管9连通,所述的进水管9与试样密封室3底部侧面连通;The constant pressure water supply unit is composed of a constant pressure water supply sealed bottle 1, a gas communication pipe 5, a balance inlet pipe 6 and a water outlet pipe 7; the electronic balance 2 is arranged at the bottom of the constant pressure water supply sealed bottle 1 and is used to measure the The weight of the pressure water supply unit; wherein, the gas communication pipe 5 and the balance air intake pipe 6 are all arranged on the upper end of the constant pressure water supply sealed bottle 1, and the end of the gas communication pipe 5 inside the constant pressure water supply sealed bottle 1 is arranged near the constant pressure water supply seal On the upper end of the bottle 1, one end of the balanced air intake pipe 6 inside the constant pressure water supply sealed bottle 1 is arranged near the lower end of the constant pressure water supply sealed bottle 1; the upper part of the gas communication pipe 5 is provided with a gas valve 14; the upper part of the balanced air intake pipe 6 is provided with A gas valve 15; a needle tube is arranged at the bottom of the balance inlet pipe 6; one end of the water outlet pipe 7 with the valve 16 communicates with the side end of the bottom of the constant pressure water supply sealed bottle 1, and the other end communicates with the water inlet pipe 9 through the silicone hose 8. The
所述的试件吸水单元由试样密封室3、进水管9、排水阀10、调节阀11、L型水位计12和试样支撑件13构成;其中,试样密封室3上部设置有一个水平仪18,在下端设置有进水管9,在密封室3右侧下端设置有L型水位计12,L型水位计12另一端朝上设置;试样密封室3右侧上端设置有调节阀11;排水阀10设置在试样密封室3的底部;试样密封室3底部内侧设置有三个等高的试样支撑件13。The sample water absorption unit is composed of a
混凝土试件4常用的制作方法为:将在实验室养护好(养护一定龄期)的混凝土试件或现场取芯所得的混凝土试件在60℃温度下烘干至恒重,然后在混凝土试件的所有侧面上涂刷上环氧树脂或石蜡材料作防水密封处理,最后将干燥好的试件置于干燥环境中冷却至室温。The common production method of
混凝土试件4的形状可以为圆柱体或棱柱体。The shape of the
本实施实例中,电子天平2用来实时测量恒压给水单元的质量随时间的变化过程;平衡进气管6底部设置有一个针管以控制进气量;混凝土试件4采用直径为100mm、高度为50mm的圆柱体(高度不限,但须采用高度与试件长度相匹配的试样密封室3),4个侧面采用环氧树脂进行防水密封;气体连通管5、平衡进气管6、出水管7、进水管9和L形水位计12均采用外径为6mm、壁厚1mm的有机玻璃管;平衡进气管6底端连接的针管(其内径为0.5~1.5mm,针管内径可以调整以适应不同材料的测量)本实施例中为内径1mm的注射用针管;试样支撑件13的高度为10mm。In this implementation example, the
本实施例一种混凝土表面毛细吸水率自动测试系统的测试方法如下:The test method of a kind of concrete surface capillary water absorption automatic test system of the present embodiment is as follows:
一、关闭出水管7上的阀门16,往恒压给水密封瓶1装水至恰不淹没气体连通管5的下端;打开气体连通管5上的气体阀门14和平衡进气管6上的气体阀门15并密封好恒压给水密封瓶1,之后关闭气体连通管5上部的气体阀门14;打开出水管7上的阀门16,恒压给水密封瓶1内部的水通过出水管7流出,恒压给水密封瓶1内的水位微降、内部空腔气压稍降且平衡进气管6内的水位较快下降,待其水位下降到平衡进气管6的下端且气体开始通过平衡进气管6进入恒压给水密封瓶1时,关闭出水管7上的阀门16,排空平衡进气管内液体完成,恒压给水密封瓶1内部液体处于平衡状态;1. Close the
二、用硅胶软管8将出水管7与进水管9相连通,关闭排水阀10,打开调节阀11,往试样密封室3内加水至淹没进水管9和L形水位计12与试样密封室3的联通孔,同时要求水位淹没试样支撑件13的顶端3mm,盖好试样密封室3的顶盖并密封好;调整高度调节脚17使试件密封瓶3的高度变化至使内部液面低于平衡进气管6的针尖水平高度15mm,打开出水管7上的阀门16,恒压给水密封瓶1内的水开始向试样密封室3内补充并排空硅胶软管8内可能存在的气体,关闭调节阀11,试样密封室3内水位保持不变,L形水位计12内的水位继续上升并可能发生溢出;调整高度调节脚17使气体不再通过平衡进气管6进入恒压给水密封瓶1内并且L形水位计12内的相应平衡水位低于L形水位计的顶端1mm,同时通过水平仪18控制试件吸水单元水平;试件吸水单元高度及水位调整完毕,整个系统处于水位平衡状态;此时若从L形水位计顶端吸走微量水分,气体将通过平衡进气管6进入恒压给水密封瓶1,并使整个系统重新处于平衡状态;2. Use a silicone hose 8 to connect the outlet pipe 7 with the water inlet pipe 9, close the drain valve 10, open the regulating valve 11, add water to the sample sealing chamber 3 until the water inlet pipe 9 and the L-shaped water level gauge 12 and the sample are submerged The connecting hole of the sealing chamber 3 requires the water level to submerge the top 3mm of the sample support member 13, cover the top cover of the sample sealing chamber 3 and seal it well; adjust the height adjustment foot 17 to change the height of the test piece sealing bottle 3 to The internal liquid level is 15mm lower than the needle tip level of the balance inlet pipe 6, and the valve 16 on the outlet pipe 7 is opened, and the water in the constant pressure water supply sealing bottle 1 starts to replenish into the sample sealing chamber 3 and empty the silicone hose 8 If the gas that may exist, close the regulating valve 11, the water level in the sample sealing chamber 3 remains unchanged, and the water level in the L-shaped water level gauge 12 continues to rise and overflow may occur; adjust the height regulating foot 17 so that the gas no longer passes through the balance intake pipe 6 Enter the constant pressure water supply seal bottle 1 and the corresponding equilibrium water level in the L-shaped water level gauge 12 is lower than the top 1mm of the L-shaped water level gauge, and at the same time control the level of the water absorption unit of the test piece through the level gauge 18; the height and water level of the water absorption unit of the test piece have been adjusted. The whole system is in a state of water level balance; at this time, if a small amount of water is sucked from the top of the L-shaped water level gauge, the gas will enter the constant pressure water supply seal bottle 1 through the
三、关闭出水管7上的阀门16,打开调节阀11,打开试样密封室3的上盖,通过排水阀10降低试样密封室3的水位并使试样支撑件13的尖端露出水面;将所有侧面密封的混凝土试件4置于试件支撑件13上部且暂时不与水接触,盖上试样密封室3的上盖并密封好;打开出水管7上的阀门16,水开始从恒压给水密封瓶1内向试样密封室3内补充,气体通过平衡进气管6进入恒压给水密封瓶1内且试样密封室3内的水位逐渐升高,待其内部水位淹没试件4的高度为3mm时关闭调节阀11,试样密封室3内水位不变而L形水位计12内水位继续上升至离顶端1mm时达平衡状态,让计算机开始按事先设置好的时间间隔采集恒压给水单元的质量数据。随着混凝土试件4吸水,试样密封室3内的气压微降,水继续从恒压给水密封瓶1向试样密封室3内补充,恒压给水密封瓶1上部气体空腔压力下降,外部大气通过平衡进气管6向恒压给水密封瓶1内部补充并达到新的平衡状态。平衡后,L形水位计12内的液位不变,对应试件底面淹没于水中的有效深度恒定,试件吸入水的质量等于恒压给水单元质量的减少量并能够被电子天平2测出,计算机按时间间隔2min采集电子天平2的质量减少量即等于混凝土试件4质量的增加量,通过质量变化量可计算混凝土试件的表面毛细吸水率。3. Close the
通过数据线将电子天平连接到计算机上,通过计算机按一定时间间隔自动采集质量数据,实时连续监测给水单元的质量变化量,即恒压给水密封瓶1内水的质量变化量。The electronic balance is connected to the computer through the data line, and the quality data is automatically collected by the computer at a certain time interval, and the quality change of the water supply unit is continuously monitored in real time, that is, the quality change of the water in the constant pressure water supply sealed bottle 1 .
采集数据的间隔时间在测试前期可以短一些,后期质量变化趋慢之后可以将采集数据的时间间隔设置相对较长一些。The data collection interval can be shorter in the early stage of the test, and the data collection interval can be set relatively longer after the quality change slows down in the later stage.
对上述的混凝土试件计算其表面毛细吸水率,步骤如下:To calculate the surface capillary water absorption of the above-mentioned concrete specimens, the steps are as follows:
一、计电子天平2的初始质量测试数据为M0(kg),之后ti(min)时间的第i次质量测量数据为Mi,则ti时间内混凝土试件的实际吸水质量为M0-Mi,此时可依据下式计算ti时间内单位面积的吸水体积Vi(m)为:1. The initial mass test data of
Vi=(M0-Mi)/ρA ①V i =(M 0 -M i )/ρA ①
其中A(m2)为混凝土试件与水接触的底面面积,ρ为水的密度(kg/m3);Among them, A (m 2 ) is the area of the bottom surface of the concrete specimen in contact with water, and ρ is the density of water (kg/m 3 );
二、将不同时刻ti与对应单位面积吸水体积Vi(m)按下式进行线性拟合:2. Carry out linear fitting between different time t i and the corresponding unit area water absorption volume V i (m) according to the following formula:
所得斜率S(m/min0.5)即为所测试件的表面毛细吸水率。The obtained slope S (m/min 0.5 ) is the surface capillary water absorption of the tested piece.
三、当混凝土试件测试完成时,依次关闭出水管7的阀门16、打开调节阀11,打开试样密封室3的顶盖并将试件取出(重复上述步骤即可继续测试下一个混凝土试件的表面毛细吸水率)。3. When the test of the concrete specimen is completed, close the
采用直径为100mm、高度为50mm的圆柱体试件,在对试件进行侧面密封并干燥预处理之后,按照上述步骤每隔2min采集电子天平2的质量数据,按公式①计算单位面积的吸水质量mi之后按公式②进行线性回归,求得回归之后的斜率即为混凝土试件的毛细吸水率S,测试结果如图2所示,其中·表示实测数据,——表示拟合曲线。Use a cylindrical specimen with a diameter of 100 mm and a height of 50 mm. After sealing the side of the specimen and pre-drying, follow the above steps to collect the mass data of the
最小二乘法所得拟合曲线的函数表达式为:The function expression of the fitted curve obtained by the least square method is:
拟合函数与实测数据的相关度R达0.9948,由上式③可知,该试件的表面毛细吸水率S为0.039m/min0.5。The correlation R between the fitting function and the measured data is 0.9948. It can be seen from the
上述各实施实例中,各部件的结构、设置位置及其连接都是可以有所变化的,在本发明技术方案的基础上,对个别部件进行的改进和等同代换,不应排除在本发明的保护范围之外。In each above-mentioned embodiment example, the structure of each component, setting position and connection thereof all can be changed to some extent, on the basis of the technical solution of the present invention, the improvement and equivalent replacement of individual components should not be excluded from the scope of the present invention. outside the scope of protection.
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