CN103422351A - Woolen sweater treating liquid containing abietic acid polyoxyethylene ester - Google Patents
Woolen sweater treating liquid containing abietic acid polyoxyethylene ester Download PDFInfo
- Publication number
- CN103422351A CN103422351A CN2013103343263A CN201310334326A CN103422351A CN 103422351 A CN103422351 A CN 103422351A CN 2013103343263 A CN2013103343263 A CN 2013103343263A CN 201310334326 A CN201310334326 A CN 201310334326A CN 103422351 A CN103422351 A CN 103422351A
- Authority
- CN
- China
- Prior art keywords
- parts
- polyoxyethylene ester
- acid polyoxyethylene
- woollen sweater
- rosin acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- -1 polyoxyethylene Polymers 0.000 title claims abstract description 30
- 229920003171 Poly (ethylene oxide) Polymers 0.000 title claims abstract description 26
- 150000002148 esters Chemical class 0.000 title claims abstract description 26
- 239000007788 liquid Substances 0.000 title abstract 4
- BTXXTMOWISPQSJ-UHFFFAOYSA-N 4,4,4-trifluorobutan-2-one Chemical compound CC(=O)CC(F)(F)F BTXXTMOWISPQSJ-UHFFFAOYSA-N 0.000 title abstract 3
- BQACOLQNOUYJCE-FYZZASKESA-N Abietic acid Natural products CC(C)C1=CC2=CC[C@]3(C)[C@](C)(CCC[C@@]3(C)C(=O)O)[C@H]2CC1 BQACOLQNOUYJCE-FYZZASKESA-N 0.000 title abstract 3
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 title abstract 3
- 239000000284 extract Substances 0.000 claims abstract description 20
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims abstract description 17
- 235000003332 Ilex aquifolium Nutrition 0.000 claims abstract description 12
- 235000002296 Ilex sandwicensis Nutrition 0.000 claims abstract description 12
- 235000002294 Ilex volkensiana Nutrition 0.000 claims abstract description 12
- 229920001817 Agar Polymers 0.000 claims abstract description 8
- 239000008272 agar Substances 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 claims description 15
- 239000012530 fluid Substances 0.000 claims description 15
- 244000007853 Sarothamnus scoparius Species 0.000 claims description 11
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 claims description 7
- 229940070765 laurate Drugs 0.000 claims description 7
- 229940068517 fruit extracts Drugs 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 235000013399 edible fruits Nutrition 0.000 abstract description 10
- 241000222122 Candida albicans Species 0.000 abstract description 6
- 229940095731 candida albicans Drugs 0.000 abstract description 6
- 230000002401 inhibitory effect Effects 0.000 abstract description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 abstract 2
- 239000005639 Lauric acid Substances 0.000 abstract 1
- 241000219871 Ulex Species 0.000 abstract 1
- 235000010730 Ulex europaeus Nutrition 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 6
- 239000006228 supernatant Substances 0.000 description 4
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 210000002268 wool Anatomy 0.000 description 2
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention relates to a woolen sweater treating liquid containing abietic acid polyoxyethylene ester. The woolen sweater treating liquid is prepared from the following ingredients in parts by weight: 2-5 parts of abietic acid polyoxyethylene ester, 2-5 parts of lauric acid polyoxyethylene ester, 3-5 parts of isopropanol, 3-5 parts of agar, 2-5 parts of purpleflower holly fruit extract, 3-5 parts of gorse extract and 80-120 parts of water. The prepared woolen sweater treating liquid has significant functions of inhibiting candida albicans growth and preventing woolen sweaters from pilling.
Description
Technical field
The present invention relates to a kind of woollen sweater treatment fluid, particularly relate to a kind of woollen sweater treatment fluid that contains the rosin acid polyoxyethylene ester.
Background technology
Use the woollen sweater treatment fluid to be processed woollen sweater, can promote the correlated performance of woollen sweater.Wool in use, often can produce the phenomenon of balling-up.If it is improper that the while woollen sweater is preserved, also can be subject to the pollution of mushroom, such as Candida albicans, mould, Escherichia coli, staphylococcus aureus etc.If can solve balling-up and the Browning problem of woollen sweater simultaneously, can widen the scope of application of woollen sweater.
Summary of the invention
The technical problem solved: allow woollen sweater there is the function that suppresses albicans growth and prevent the woollen sweater balling-up after treatment fluid is processed.
Technical scheme: the invention discloses a kind of woollen sweater treatment fluid that contains the rosin acid polyoxyethylene ester, formed according to weight ratio by following composition: 2～5 parts of rosin acid polyoxyethylene ester, 2～5 parts of laurate polyoxyethylene ester, 3～5 parts of isopropyl alcohols, 3～5 parts, agar, 2～5 parts of purpleflower holly fruit extracts, 3～5 parts of broom top extracts, 80～120 parts, water.At first need to prepare purpleflower holly fruit extract and broom top extract, get respectively each 5kg of fresh purpleflower holly fruit and broom top, add the ethanol water 50kg that mass fraction is 20% after smashing to pieces, 60 ℃ of constant temperature stir and extract 3h, obtain respectively supernatant after filtration, again by the supernatant Vacuum Concentration that obtains respectively to 10kg, obtain respectively purpleflower holly fruit extract and broom top extract.Take again rosin acid polyoxyethylene ester 2～5kg, laurate polyoxyethylene ester 2～5kg, isopropyl alcohol 3～5kg, agar 3～5kg, purpleflower holly fruit extract 2～5kg, broom top extract 3～5kg, water 80～120kg, obtain having the antibacterial and treatment fluid ANTIPILLING function after mixing.
Beneficial effect: the woollen sweater treatment fluid prepared by the present invention has good inhibition Candida albicans and prevents woollen sweater balling-up function.After common woollen sweater is processed with this treatment fluid, the inhibiting rate of Candida albicans is more than 95%, has very high bacteriostasis rate.The ANTIPILLING Performance Level of woollen sweater is 4 grades simultaneously, has had the function of good ANTIPILLING.
The specific embodiment
Embodiment 1
Get respectively each 5kg of fresh purpleflower holly fruit and broom top, add the ethanol water 50kg that mass fraction is 20% after smashing to pieces, 60 ℃ of constant temperature stir and extract 3h, obtain respectively supernatant after filtration, again by the supernatant Vacuum Concentration that obtains respectively to 10kg, obtain respectively purpleflower holly fruit extract and broom top extract.Take again rosin acid polyoxyethylene ester 2kg, laurate polyoxyethylene ester 5kg, isopropyl alcohol 3kg, agar 5kg, purpleflower holly fruit extract 2kg, broom top extract 5kg, water 80kg, obtain having the antibacterial and treatment fluid ANTIPILLING function after mixing.
Embodiment 2
The preparation method is with embodiment 1, and concrete component content is as follows: rosin acid polyoxyethylene ester 3kg, laurate polyoxyethylene ester 4kg, isopropyl alcohol 4kg, agar 4kg, purpleflower holly fruit extract 3kg, broom top extract 4kg, water 100kg.
Embodiment 3
The preparation method is with embodiment 1, and concrete component content is as follows: rosin acid polyoxyethylene ester 5kg, laurate polyoxyethylene ester 2kg, isopropyl alcohol 5kg, agar 3kg, purpleflower holly fruit extract 5kg, broom top extract 3kg, water 120kg.
ANTIPILLING and bacteria resistance function test
After under the product normal temperature of embodiment 1, embodiment 2, embodiment 3 for commercially available woollen sweater, soaking 8h, naturally dry.The woollen sweater of not processing through this finishing agent and the wool that process embodiment 1, embodiment 2 and embodiment 3 processed are carried out to the pilling property test, and testing standard is GB/T4802.2-1997.Test result shows, the common woollen sweater grade of unprocessed mistake is 1 grade, and the woollen sweater grade after embodiment 1, embodiment 2 and embodiment 3 process is 4 grades.There is good ANTIPILLING function.
It is Candida albicans that bacteriostatic experiment is selected bacterial classification.Testing standard is AATCC100, and test result shows: the bacteriostasis rate of the Candida albicans of embodiment 1, embodiment 2, embodiment 3 is respectively 95.8%, 96.3%, 97.1%.
Claims (5)
1. a woollen sweater treatment fluid that contains the rosin acid polyoxyethylene ester, is characterized in that being comprised of according to weight ratio following composition: 2～5 parts of rosin acid polyoxyethylene ester, 2～5 parts of laurate polyoxyethylene ester, 3～5 parts of isopropyl alcohols, 3～5 parts, agar, 2～5 parts of purpleflower holly fruit extracts, 3～5 parts of broom top extracts, 80～120 parts, water.
2. a kind of woollen sweater treatment fluid that contains the rosin acid polyoxyethylene ester according to claim 1, is characterized in that into that to be grouped into middle rosin acid polyoxyethylene ester be 2 parts.
3. a kind of woollen sweater treatment fluid that contains the rosin acid polyoxyethylene ester according to claim 1, is characterized in that into that to be grouped into middle laurate polyoxyethylene ester be 5 parts.
4. a kind of woollen sweater treatment fluid that contains the rosin acid polyoxyethylene ester according to claim 1, is characterized in that into that to be grouped into middle isopropyl alcohol be 5 parts.
5. a kind of woollen sweater treatment fluid that contains the rosin acid polyoxyethylene ester according to claim 1, is characterized in that into that to be grouped into middle agar be 3 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310334326.3A CN103422351B (en) | 2013-08-02 | 2013-08-02 | Woolen sweater treating liquid containing abietic acid polyoxyethylene ester |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310334326.3A CN103422351B (en) | 2013-08-02 | 2013-08-02 | Woolen sweater treating liquid containing abietic acid polyoxyethylene ester |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103422351A true CN103422351A (en) | 2013-12-04 |
| CN103422351B CN103422351B (en) | 2015-05-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310334326.3A Expired - Fee Related CN103422351B (en) | 2013-08-02 | 2013-08-02 | Woolen sweater treating liquid containing abietic acid polyoxyethylene ester |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103422351B (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105350315A (en) * | 2015-12-16 | 2016-02-24 | 常熟绣珀纤维有限公司 | Method for preparing ultrahigh molecular weight polyethylene fine fiber |
| CN105780478A (en) * | 2016-04-29 | 2016-07-20 | 江苏苏扬服帽有限公司 | Finishing agent for knitting and preparation method and application of finishing agent for knitting |
| CN105862419A (en) * | 2016-04-29 | 2016-08-17 | 江苏苏扬服帽有限公司 | Anti-pilling agent for knitting and preparing method and application thereof |
| CN105862408A (en) * | 2016-04-29 | 2016-08-17 | 江苏苏扬服帽有限公司 | Treating agent for preventing knitted fabric pilling and preparation method and application thereof |
| CN105887489A (en) * | 2016-04-29 | 2016-08-24 | 江苏苏扬服帽有限公司 | Anti-pilling agent for knitting, and preparation method and application thereof |
| CN105908494A (en) * | 2016-05-19 | 2016-08-31 | 太仓协大申泰羊毛衫有限公司 | Composite anti-microbial finishing agent and application thereof to wool products |
| CN105926298A (en) * | 2016-04-29 | 2016-09-07 | 江苏苏扬服帽有限公司 | Efficient anti-pilling agent for knitted fabric, preparing method and application thereof |
| CN106087385A (en) * | 2016-07-08 | 2016-11-09 | 陆建益 | A kind of Multifunctional woolen sweater finishing agent containing sea mud |
Citations (3)
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|---|---|---|---|---|
| CN101289472A (en) * | 2007-04-18 | 2008-10-22 | 代龙 | Process for separating matrine-like total alkaloids form Chinese medicament extract |
| CN102021825A (en) * | 2010-11-24 | 2011-04-20 | 东华大学 | Method for preparing multifunctional compound preparation of plant source antibacterial pigment for wool product |
| CN102051812A (en) * | 2010-11-24 | 2011-05-11 | 东华大学 | Application of botanical antibacterial mothproof multifunctional composite preparation in wool product |
-
2013
- 2013-08-02 CN CN201310334326.3A patent/CN103422351B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101289472A (en) * | 2007-04-18 | 2008-10-22 | 代龙 | Process for separating matrine-like total alkaloids form Chinese medicament extract |
| CN102021825A (en) * | 2010-11-24 | 2011-04-20 | 东华大学 | Method for preparing multifunctional compound preparation of plant source antibacterial pigment for wool product |
| CN102051812A (en) * | 2010-11-24 | 2011-05-11 | 东华大学 | Application of botanical antibacterial mothproof multifunctional composite preparation in wool product |
Non-Patent Citations (1)
| Title |
|---|
| 余正文等: "贵州金雀花抑菌活性主要成分测定", 《贵州农业科学》, no. 5, 15 October 2006 (2006-10-15) * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105350315A (en) * | 2015-12-16 | 2016-02-24 | 常熟绣珀纤维有限公司 | Method for preparing ultrahigh molecular weight polyethylene fine fiber |
| CN105780478A (en) * | 2016-04-29 | 2016-07-20 | 江苏苏扬服帽有限公司 | Finishing agent for knitting and preparation method and application of finishing agent for knitting |
| CN105862419A (en) * | 2016-04-29 | 2016-08-17 | 江苏苏扬服帽有限公司 | Anti-pilling agent for knitting and preparing method and application thereof |
| CN105862408A (en) * | 2016-04-29 | 2016-08-17 | 江苏苏扬服帽有限公司 | Treating agent for preventing knitted fabric pilling and preparation method and application thereof |
| CN105887489A (en) * | 2016-04-29 | 2016-08-24 | 江苏苏扬服帽有限公司 | Anti-pilling agent for knitting, and preparation method and application thereof |
| CN105926298A (en) * | 2016-04-29 | 2016-09-07 | 江苏苏扬服帽有限公司 | Efficient anti-pilling agent for knitted fabric, preparing method and application thereof |
| CN105908494A (en) * | 2016-05-19 | 2016-08-31 | 太仓协大申泰羊毛衫有限公司 | Composite anti-microbial finishing agent and application thereof to wool products |
| CN106087385A (en) * | 2016-07-08 | 2016-11-09 | 陆建益 | A kind of Multifunctional woolen sweater finishing agent containing sea mud |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103422351B (en) | 2015-05-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| ASS | Succession or assignment of patent right |
Owner name: SUZHOU AILIFANG CLOTHES CO., LTD. Free format text: FORMER OWNER: WUJIANG QIDU MIAOGANG YADI KNITTED CLOTHING FACTORY Effective date: 20150414 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 215232 SUZHOU, JIANGSU PROVINCE TO: 215200 SUZHOU, JIANGSU PROVINCE |
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| TA01 | Transfer of patent application right |
Effective date of registration: 20150414 Address after: Wujiang District of Suzhou City, Jiangsu province 215200 Song Ling Zhen Heng Shan Bridge Road Applicant after: SUZHOU AILIFANG CLOTHING Co.,Ltd. Address before: Wujiang District of Suzhou City, Jiangsu province 215232 seven Zhen Miao gang Kaixiangong 2 group Applicant before: WUJIANG QIDU TOWN MIAOGANG YADI KNITTED CLOTHING FACTORY |
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| C14 | Grant of patent or utility model | ||
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150520 |