CN103340818B - Massage tea oil - Google Patents
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- CN103340818B CN103340818B CN201310334112.6A CN201310334112A CN103340818B CN 103340818 B CN103340818 B CN 103340818B CN 201310334112 A CN201310334112 A CN 201310334112A CN 103340818 B CN103340818 B CN 103340818B
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Abstract
The invention discloses massage tea oil, and relates to the technical field of medicine health care product manufacture. The massage tea oil is prepared from the following raw materials in parts by weight: 2-5 parts of glycerol distearates, 20-30 parts of pure tea seed oil, 10-15 parts of red flower essential oil, 5-10 parts of trogopterus dung extracting solution, 5-10 parts of cucumber juice, 5-10 parts of algin, 10-15 parts of arabian jasmine flower essential oil, 2-6 parts of linseed oil, 5-10 parts of collagen, and 2-6 parts of pollen typhae extracting solution. The massage tea oil has the characteristics of being low in cost, having good skin moistening effect, and the like, is suitable for women and men of different ages to use in massage, and can be used as a skin care product.
Description
Technical field
The present invention relates to medicines and health protection product processing technique field, particularly a kind of massage Oleum Camelliae.
Background technology
Massage oil is a kind of liquid or semisolid ointment that adopts plants essential oil or mineral oil to make, and has promotion skin moisturizing, the function of lubricated skin.At present, the massage oil kind of selling is on the market more, mixes the genuine with the fictitious, and quality is uneven, and measured its price of matter is generally higher; Some evil mind businessman adopt industry glycerol allotment spice to make massage oil, and people's health is had to certain injury.Chinese patent (number of patent application 201210596525.7) " a kind of massage oil ", by Ungula Cervi grass juice factor, Herba Rosmarini Officinalis juice, Aloe juice, the water of crowing, Eucalyptus oil, retinal, Oleum menthae, Herba Lysimachiae foenum-graeci quintessence oil, tea tree oil, Oleum Camphora, vitamin A etc. mix, and have the skin of releiving and alleviate pain and reduce wrinkle and eliminate acne functions, are a kind of top grade and low cost massage oil.And for example Chinese patent (number of patent application 200610044639.5) " health-care massage oil ", is made up of natural tea tree quintessence oil and two kinds of material allocations of Oleum menthae, has that hand-held cost is low, effect good, refrigerant pleasant and easy to carry, safe and reliable.Also just like Chinese patent (number of patent application 201110346721.4) " beauty care Oleum Camelliae and preparation method thereof ", comprise the raw material composition of following weight part ratio: hard fat compound: 10-15 part, fusing point >=25 ℃ of described hard fat compound, are selected from any one or more the mixture in fatty alcohol, fatty acid, fatty alcohol derivative, derivative of fatty acid; Oleum Camelliae: 20-30 part; Linolenic acid: 5-10 part; Nutrient: 3-5 part, described nutrient is one of vitamin E acetas, seaweed extracted liquor or its mixture; This invention adds in Camellia oil has bioactive material to reach enhancing skin protection, skin-protecting function, and beauty care Oleum Camelliae of the present invention protective effect is strong, makes simply, safe and reliable, is convenient to produce in enormous quantities reasonable component formula, beauty care successful.
Summary of the invention
The object of the present invention is to provide a kind of production cost lower, to the good massage oil of skin moisturizing effect.
For achieving the above object, the technical measures that the present invention takes are a kind of massage Oleum Camelliae of invention, are to be prepared from by following raw material by weight:
The pure Oleum Camelliae 20-30 of glycerol distearate 2-5 Flos Carthami quintessence oil 10-15
Oletum Trogopterori extracting solution 5-10 Sucus Cucumidis sativi 5-10 seaweeds 5-10
Flos Jasmini Sambac quintessence oil 10-15 Semen Lini oil 2-6 collagen protein 5-10
Pollen typhae 2-6;
Its preparation method is as follows:
A, Sucus Cucumidis sativi, collagen protein, seaweeds, glycerol distearate, Oletum Trogopterori extracting solution, Pollen typhae are dropped in mixer, rotating speed is turn/min of 40-100, first counterclockwise rotates 40-100min, then rotates clockwise 30-70min; Then dropped in oscillator, homogenize, obtains mixed material, for subsequent use;
B, Semen Lini oil, Flos Jasmini Sambac quintessence oil, Flos Carthami quintessence oil are added respectively in mixed material for subsequent use in order, again add lower a kind of raw material after first stirring 5-15min at every turn, finally add pure Oleum Camelliae, stir, mix, obtain total mixture material, for subsequent use;
C, by total mixture material through subpackage, sterilizing, can obtain massage Oleum Camelliae;
Described Oletum Trogopterori extracting solution is to extract by following method:
A, get Oletum Trogopterori by above-mentioned weight portion, be placed in container, then to adding 2-4 times of weight, ethyl acetate by weight in container: the mixed solution of normal hexane=1-3:0.4 preparation, at 40-80 ℃ of remove impurity 1.2-1.8 hour, filter, stay slag, obtain remove impurity Oletum Trogopterori, for subsequent use;
B, to the clear water that adds 3-7 times of weight in remove impurity Oletum Trogopterori for subsequent use, boil and extract 0.8-1.2 hour, filter; To the clear water that adds equivalent weight in recrement, boil and extract 0.3-0.7 hour again, filter, merges twice filtrate, obtain extract at the beginning of Oletum Trogopterori, for subsequent use;
C, by Oletum Trogopterori for subsequent use just extract keep 30-50 ℃ of temperature, cross by thin river sand: the mixed column that kieselguhr: clay=1:1:0.2 form, the flow velocity of controlling upper prop is 20-40L/h, the filtrate after collection upper prop is for subsequent use;
D, filtrate for subsequent use is concentrated into 1/4 to 1/2 of original volume through rising membrane concentrator at 40-80 ℃, obtains concentrated solution, for subsequent use;
E, by concentrated solution for subsequent use under 0.5-2.2Mpa pressure cross reverse osmosis membrane apparatus, membrane aperture is 5～15nm, collect filtrate, obtain Oletum Trogopterori extracting solution;
Described Pollen typhae is to extract by following method:
A`, get Pollen Typhae by above-mentioned weight portion, be placed in container, then to adding 1-3 times of weight, petroleum ether by weight in container: the mixed liquor of water=1-4:1 preparation, at 35-65 ℃, carry out lixiviate remove impurity, the time is 0.5-2.0 hour, filters, stays slag, obtain remove impurity Pollen Typhae, for subsequent use;
B`, to adding equivalent weight, ethyl acetate by weight in remove impurity Pollen Typhae for subsequent use: the mixed liquor of water=2-6:1 preparation, at temperature 30-70 ℃, soak, the time is 1.0-2.0 hour, filters, and must soak Pollen Typhae afterwards; After soaking, 30-55 ℃ of warm water washing 1-4 time for Pollen Typhae, filters, stays slag again, obtains water treatment Pollen Typhae, for subsequent use;
C`, add to water treatment Pollen Typhae for subsequent use the ethanol that 2-6 times of weight, volumetric concentration are 70-90%, boil and extract 0.5-3.0 hour, filter, collect filtrate; In recrement, add the ethanol that 1-2 times of weight, volumetric concentration are 50-70% again, boil and extract 0.5-1.5 hour, filter, merge extracted twice liquid, obtain just extract of Pollen Typhae, for subsequent use;
D`, by Pollen Typhae for subsequent use just extract at 55-90 ℃, be concentrated into 1/5 to 1/3 of original volume, obtain the preliminary concentrated solution of Pollen Typhae, for subsequent use;
E`, the Ph value of the preliminary concentrated solution of Pollen Typhae is adjusted to 7.5-8.5 with the aqueous alkali of weight concentration 1.5-3.0%, obtains Pollen Typhae provisional value and adjust concentrated solution, for subsequent use; Aqueous alkali used is one or more in sodium carbonate, sodium bicarbonate, sodium hydroxide, potassium hydroxide, in the time being multiple, the ratio of each component is equal portions or other ratio;
F`, Pollen Typhae provisional value for subsequent use is adjusted to concentrated solution, drop in falling film condenser, at 45-70 ℃, be concentrated into 1/2 of original volume, filter, obtain Pollen Typhae concentrated solution, for subsequent use;
G`, by Pollen Typhae concentrated solution for subsequent use under 1.0-1.5Mpa pressure, through flame filter press filter, obtain Pollen typhae.
The technical scheme one of its optimization is to be prepared from by following raw material by weight:
The pure Oleum Camelliae 30 Flos Carthami quintessence oils 13 of glycerol distearate 5
Oletum Trogopterori extracting solution 5 Sucus Cucumidis sativi 10 seaweeds 10
Flos Jasmini Sambac quintessence oil 10 Semen Lini oil 2 collagen protein 10
Pollen typhae 5.
The technical scheme two of its optimization is to be prepared from by following raw material by weight:
The pure Oleum Camelliae 20 Flos Carthami quintessence oils 15 of glycerol distearate 2
Oletum Trogopterori extracting solution 10 Sucus Cucumidis sativi 10 seaweeds 10
Flos Jasmini Sambac quintessence oil 15 Semen Lini oil 6 collagen protein 10
Pollen typhae 2.
The technical scheme three of its optimization is to be prepared from by following raw material by weight:
The pure Oleum Camelliae 25 Flos Carthami quintessence oils 10 of glycerol distearate 3
Oletum Trogopterori extracting solution 10 Sucus Cucumidis sativi 10 seaweeds 10
Flos Jasmini Sambac quintessence oil 15 Semen Lini oil 4 collagen protein 10
Pollen typhae 3.
The technical scheme four of its optimization is to be prepared from by following raw material by weight:
The pure Oleum Camelliae 30 Flos Carthami quintessence oils 15 of glycerol distearate 5
Oletum Trogopterori extracting solution 8 Sucus Cucumidis sativi 5 seaweeds 5
Flos Jasmini Sambac quintessence oil 15 Semen Lini oil 6 collagen protein 5
Pollen typhae 6.
The technical scheme five of its optimization is to be prepared from by following raw material by weight:
The pure Oleum Camelliae 28 Flos Carthami quintessence oils 13 of glycerol distearate 4
Oletum Trogopterori extracting solution 8 Sucus Cucumidis sativi 8 seaweeds 8
Flos Jasmini Sambac quintessence oil 12 Semen Lini oil 5 collagen protein 8
Pollen typhae 6.
Massage Oleum Camelliae of the present invention, adopt pure Oleum Camelliae (Camellia oleifera Abel) as primary raw material, auxiliary material includes Flos Jasmini Sambac quintessence oil (Jasminum officinale), Flos Carthami quintessence oil (Carthamus tinctorius L.), Semen Lini oil (Linseed), collagen protein (Collagen), Sucus Cucumidis sativi (Cucumis sativus), seaweeds, glycerol distearate, Pollen typhae (Typha angustifolia L. or Typha latifolia L or Typha orientalis Preel or Typha angustata Bory et Chaub.), Oletum Trogopterori extracting solution (Trogopterus xanthipes Milne-Edwards).
Modern study shows, Oleum Camelliae contains the compositions such as abundant oleic acid, linoleic acid, linolenic acid, vitamin E, theasaponin, Squalene and trace element, and its nutrition and health care function even exceedes olive oil; The oleic acid of Oleum Camelliae is easy to be absorbed by the skin, energy nourishes rough skin cell; Meanwhile, in Oleum Camelliae, contain the active substance to skin beneficiating such as vitamin E, D, K and carotene and camellin, and there is certain sterilization, absorption ultraviolet effect; And Oleum Camelliae difficulty is evaporated, moisture retention is good, and antioxygenic property is good, is difficult for becoming sour.Flos Jasmini Sambac quintessence oil can be nursed one's health dry and responsive skin, and desalination striae gravidarum and cicatrix increase skin elasticity and draw, and are called as " king of quintessence oil ".Flos Carthami quintessence oil is warm in nature, acrid in the mouth, has effect of promoting blood circulation to restore menstrual flow, eliminating stasis to stop pain.Pollen Typhae (Pollen typhae used, adopts special extracting method, has removed harmful substance, has strengthened its effect) has effect of cooling blood for hemostasis, activating blood circulation and dissipating blood stasis.Oletum Trogopterori (Oletum Trogopterori extracting solution used, adopts special extracting method, has removed harmful substance, has strengthened its effect) has effect of promoting blood circulation and stopping pain, removing stasis to stop bleeding, removing food stagnancy removing toxic substances.Semen Lini oil can improve skin fat content, makes the younger cunning of skin, moist, soft flexible, normal with seasonal dermal respiration and perspire, alleviates all skin problems; Can consume health superabundant fats, contained Ω-3 unsaturated fatty acid can reduce the impact of the harmful biochemical material producing when health is stressed, and stabilizing the emotions keeps tranquil phychology, reduces melancholia and insomnia; Help and alleviate anaphylaxis; To treating and preventing that arthritis from having very big effect; Improve moisture content and the elasticity of cell membrane, increase Cellular respiration and nutrition function of exchange, and strengthen soma and repair and healing ability, make cell health; Balance and improve health blood glucose amount, makes you more have vigor.Also can increase the endurance of muscle, more can make Fatique after Sports muscle recover sooner.Collagen protein has very strong stretch capability, is the Main Ingredients and Appearance of ligament and flesh key, the chief component composition of collagen protein or extracellular matrix, and it makes skin keep elasticity.In Sucus Cucumidis sativi, contain hydroxymalonic acid, its existing inhibition saccharide is converted into fatty effect, also has a kind of special cosmetology function, wherein contains abundant potassium salt and carotene, can eliminate freckle, skin whitening.Seaweeds can promote cell division, slow down aging.Glycerol distearate is nonionic emulsifier, can be by even being integrated of above-mentioned plurality of raw materials emulsifying.Meanwhile, above-mentioned various raw material sources are extensive, and price is not high.Thereby massage Oleum Camelliae of the present invention, has gathered many effects of above-mentioned various raw materials, is applied to massage, better to the moisturizing effect of skin, and its production cost is also lower.
Table 1 is below that the active ingredient of massage Oleum Camelliae of the present invention detects data:
The active ingredient of table 1 massage Oleum Camelliae of the present invention detects table (100 grams of content)
Massage Oleum Camelliae of the present invention, once did skin massaging controlled trial:
(i), definite principle of testing crew
(1), the age is between 30-40 year;
(2), life style and family's condition and working environment are close;
(3), body constitution and health are close.
(ii), physical data
According to mentioned above principle, determine testing crew 100 people, then, be divided at random massage test group (50 people), massage matched group (30 people) and matched group (20 people).
(iii), test method
(1), massage test group: at duration of test, daily life and diet are all the same when normal, and its difference is to adopt weekly massage Oleum Camelliae of the present invention, and massage once;
(2), massage matched group: during experimental control, daily life and diet are all the same when normal, and its difference is to adopt weekly the massage oil of selling quite, on the market with massage Oleum Camelliae price of the present invention, and massage once;
(3), matched group: during experimental control, daily life and diet are all the same when normal, and its difference is never to carry out massage.
(iv), criterion
(1), skin health standard
1., the elasticity of skin: skin is rich in certain elasticity, the brilliance that seems, smooth;
2., skin is moistening: skin moisturizing is glossy, moist, does not occur wrinkle;
3., color and luster and the texture of skin: the color of skin meets color race's normal color, clean mark;
4., the clean and vigor of skin: skin does not have dirt, stain, is maintained in the clean condition;
5., normally also ability is old for skin: skin is insensitive, non-greasy and moist.
(2), the good and bad criterion of skin
1., above-mentioned 5 standards all meet, and are skin fine;
2. 1, in above-mentioned 5 standards does not meet, is skin better;
3. the 2-3 point, in above-mentioned 5 standards does not meet, and is skin poor;
4. the 4-5 point, in above-mentioned 5 standards does not meet, and is skin very poor.
(v), result of the test
Through the tests of six months (on April 30th, 1 2013 on November 1st, 2012), statistical data, forms following form:
Shown by above-mentioned statistical data, in massage test group skin better above ratio reach 86%, the ratio 70%, 70% than skin in massage matched group and matched group more than better, has improved 16 percentage points.
Therefore, massage Oleum Camelliae of the present invention, has good moisturizing effect to skin.
The specific embodiment
Below in conjunction with embodiment, the present invention is further illustrated.Explanation is below the mode exemplifying, but protection scope of the present invention is not limited to this.
Embodiment mono-:
The massage Oleum Camelliae of the present embodiment, its procedure of processing is as follows:
A, get the raw materials ready: get respectively by weight 30 parts of pure Oleum Camelliae, 10 parts of Flos Jasmini Sambac quintessence oils, 13 parts of Flos Carthami quintessence oils, 2 parts of Semen Lini oil, 10 parts of collagen protein, the Sucus Cucumidis sativi (Sucus Cucumidis sativi that new fresh cucumbers is extracted after pulverizing, coarse filtration, fine straining, its riboflavin >=0.1mg/ml, lower with) 10 parts, 10 parts of seaweeds, 5 parts of glycerol distearate, 5 parts of Pollen typhaes, 5 parts of Oletum Trogopterori extracting solution, for subsequent use;
Wherein:
Oletum Trogopterori extracting solution is to extract by following method:
A, Oletum Trogopterori raw material is placed in to container, then to adding 2-4 times of weight, ethyl acetate by weight in container: the mixed solution of normal hexane=1-3:0.4 preparation, at 40-80 ℃ of remove impurity 1.2-1.8 hour, filter, stay slag, obtain remove impurity Oletum Trogopterori, for subsequent use;
B, to the clear water that adds 3-7 times of weight in remove impurity Oletum Trogopterori for subsequent use, boil and extract 0.8-1.2 hour, filter; To the clear water that adds equivalent weight in recrement, boil and extract 0.3-0.7 hour again, filter, merges twice filtrate, obtain extract at the beginning of Oletum Trogopterori, for subsequent use;
C, by Oletum Trogopterori for subsequent use just extract keep 30-50 ℃ of temperature, cross by thin river sand: the mixed column that kieselguhr: clay=1:1:0.2 form, the flow velocity of controlling upper prop is 20-40L/h, the filtrate after collection upper prop is for subsequent use;
D, filtrate for subsequent use is concentrated into 1/4 to 1/2 of original volume through rising membrane concentrator at 40-80 ℃, obtains concentrated solution, for subsequent use;
E, by concentrated solution for subsequent use under 0.5-2.2Mpa pressure cross reverse osmosis membrane apparatus, membrane aperture is 5～15nm, collect filtrate, obtain Oletum Trogopterori extracting solution, its vitamin A content is 56.24mg/ml.
Pollen typhae is to extract by following method:
A`, Pollen Typhae raw material is placed in to container, to adding 1-3 times of weight, petroleum ether by weight in container: the mixed liquor of water=1-4:1 preparation, at 35-65 ℃, carry out lixiviate remove impurity, the time is 0.5-2.0 hour, filters, stays slag, obtains remove impurity Pollen Typhae, for subsequent use;
B`, to adding equivalent weight, ethyl acetate by weight in remove impurity Pollen Typhae for subsequent use: the mixed liquor of water=2-6:1 preparation, at temperature 30-70 ℃, soak, the time is 1.0-2.0 hour, filters, and must soak Pollen Typhae afterwards; After soaking, 30-55 ℃ of warm water washing 1-4 time for Pollen Typhae, filters, stays slag again, obtains water treatment Pollen Typhae, for subsequent use;
C`, add to water treatment Pollen Typhae for subsequent use the ethanol that 2-6 times of weight, volumetric concentration are 70-90%, boil and extract 0.5-3.0 hour, filter, collect filtrate; In recrement, add the ethanol that 1-2 times of weight, volumetric concentration are 50-70% again, boil and extract 0.5-1.5 hour, filter, merge extracted twice liquid, obtain just extract of Pollen Typhae, for subsequent use;
D`, by Pollen Typhae for subsequent use just extract at 55-90 ℃, be concentrated into 1/5 to 1/3 of original volume, obtain the preliminary concentrated solution of Pollen Typhae, for subsequent use;
E`, the Ph value of the preliminary concentrated solution of Pollen Typhae is adjusted to 7.5-8.5 with the aqueous alkali of weight concentration 1.5-3.0%, obtains Pollen Typhae provisional value and adjust concentrated solution, for subsequent use; Aqueous alkali used is one or more in sodium carbonate, sodium bicarbonate, sodium hydroxide, potassium hydroxide, in the time being multiple, the ratio of each component is equal portions or other ratio;
F`, Pollen Typhae provisional value for subsequent use is adjusted to concentrated solution, drop in falling film condenser, at 45-70 ℃, be concentrated into 1/2 of original volume, filter, obtain Pollen Typhae concentrated solution, for subsequent use;
G`, by Pollen Typhae concentrated solution for subsequent use under 1.0-1.5Mpa pressure, through flame filter press filter, obtain Pollen typhae, its flavone (that is: naringenin) content is 43.12mg/ml.
B, mixed material preparation:
Sucus Cucumidis sativi for subsequent use, collagen protein, seaweeds, glycerol distearate, Oletum Trogopterori extracting solution, Pollen typhae are dropped into mixer, and (model that this example adopts is VH50, lower same) in, rotating speed is 100 turn/min, first counterclockwise rotates 100min, then rotates clockwise 30min; Then dropped in oscillator, homogenize, obtains mixed material, for subsequent use;
C, Semen Lini oil for subsequent use, Flos Jasmini Sambac quintessence oil, Flos Carthami quintessence oil are added respectively in mixed material for subsequent use in order, again add lower a kind of raw material after first stirring 15min at every turn, finally add pure Oleum Camelliae, stir, mix, obtain total mixture material, for subsequent use;
D, by total mixture material through subpackage, sterilizing, can obtain massage Oleum Camelliae.
Embodiment bis-:
The massage Oleum Camelliae of the present embodiment, its procedure of processing is as follows:
A, get the raw materials ready: get respectively by weight 20 parts of pure Oleum Camelliae, 15 parts of Flos Jasmini Sambac quintessence oils, 15 parts of Flos Carthami quintessence oils, 6 parts of Semen Lini oil, 10 parts of collagen protein, 10 parts of Sucus Cucumidis sativis, 10 parts of seaweeds, 2 parts of glycerol distearate, 2 parts of Pollen typhaes, 10 parts of Oletum Trogopterori extracting solution, for subsequent use;
Other step is identical with embodiment mono-, repeats no more.
Embodiment tri-:
The massage Oleum Camelliae of the present embodiment, its procedure of processing is as follows:
A, get the raw materials ready: get respectively by weight 25 parts of pure Oleum Camelliae, 15 parts of Flos Jasmini Sambac quintessence oils, 10 parts of Flos Carthami quintessence oils, 4 parts of Semen Lini oil, 10 parts of collagen protein, 10 parts of Sucus Cucumidis sativis, 10 parts of seaweeds, 3 parts of glycerol distearate, 3 parts of Pollen typhaes, 10 parts of Oletum Trogopterori extracting solution, for subsequent use;
Other step is identical with embodiment mono-, repeats no more.
Embodiment tetra-:
The massage Oleum Camelliae of the present embodiment, its procedure of processing is as follows:
A, get the raw materials ready: get respectively by weight 30 parts of pure Oleum Camelliae, 15 parts of Flos Jasmini Sambac quintessence oils, 15 parts of Flos Carthami quintessence oils, 6 parts of Semen Lini oil, 5 parts of collagen protein, 5 parts of Sucus Cucumidis sativis, 5 parts of seaweeds, 5 parts of glycerol distearate, 6 parts of Pollen typhaes, 8 parts of Oletum Trogopterori extracting solution, for subsequent use;
Other step is identical with embodiment mono-, repeats no more.
Embodiment five:
The massage Oleum Camelliae of the present embodiment, its procedure of processing is as follows:
A, get the raw materials ready: get respectively by weight 28 parts of pure Oleum Camelliae, 12 parts of Flos Jasmini Sambac quintessence oils, 13 parts of Flos Carthami quintessence oils, 5 parts of Semen Lini oil, 8 parts of collagen protein, 8 parts of Sucus Cucumidis sativis, 8 parts of seaweeds, 4 parts of glycerol distearate, 6 parts of Pollen typhaes, 8 parts of Oletum Trogopterori extracting solution, for subsequent use;
Other step is identical with embodiment mono-, repeats no more.
Massage Oleum Camelliae of the present invention, uses while being applicable to men and women's massage of each ages, also can be used as skin care item.
Claims (6)
1. a massage Oleum Camelliae, it is characterized in that being prepared from by following raw material by weight:
Its preparation method is as follows:
A, Sucus Cucumidis sativi, collagen protein, seaweeds, glycerol distearate, Oletum Trogopterori extracting solution, Pollen typhae are dropped in mixer, rotating speed is turn/min of 40-100, first counterclockwise rotates 40-100min, then rotates clockwise 30-70min; Then dropped in oscillator, homogenize, obtains mixed material, for subsequent use;
B, Semen Lini oil, Flos Jasmini Sambac quintessence oil, Flos Carthami quintessence oil are added respectively in mixed material for subsequent use in order, again add lower a kind of raw material after first stirring 5-15min at every turn, finally add pure Oleum Camelliae, stir, mix, obtain total mixture material, for subsequent use;
C, by total mixture material through subpackage, sterilizing, can obtain massage Oleum Camelliae;
Described Oletum Trogopterori extracting solution is to extract by following method:
A, Oletum Trogopterori raw material is placed in to container, then to adding 2-4 times of weight, ethyl acetate by weight in container: the mixed solution of normal hexane=1-3:0.4 preparation, at 40-80 ℃ of remove impurity 1.2-1.8 hour, filter, stay slag, obtain remove impurity Oletum Trogopterori, for subsequent use;
B, to the clear water that adds 3-7 times of weight in remove impurity Oletum Trogopterori for subsequent use, boil and extract 0.8-1.2 hour, filter; To the clear water that adds equivalent weight in recrement, boil and extract 0.3-0.7 hour again, filter, merges twice filtrate, obtain extract at the beginning of Oletum Trogopterori, for subsequent use;
C, by Oletum Trogopterori for subsequent use just extract keep 30-50 ℃ of temperature, cross by thin river sand: the mixed column that kieselguhr: clay=1:1:0.2 form, the flow velocity of controlling upper prop is 20-40L/h, the filtrate after collection upper prop is for subsequent use;
D, filtrate for subsequent use is concentrated into 1/4 to 1/2 of original volume through rising membrane concentrator at 40-80 ℃, obtains concentrated solution, for subsequent use;
E, by concentrated solution for subsequent use under 0.5-2.2MPa pressure cross reverse osmosis membrane apparatus, membrane aperture is 5～15nm, collect filtrate, obtain Oletum Trogopterori extracting solution;
Described Pollen typhae is to extract by following method:
A`, Pollen Typhae raw material is placed in to container, then to adding 1-3 times of weight, petroleum ether by weight in container: the mixed liquor of water=1-4:1 preparation, at 35-65 ℃, carry out lixiviate remove impurity, the time is 0.5-2.0 hour, filters, stays slag, obtains remove impurity Pollen Typhae, for subsequent use;
B`, to adding equivalent weight, ethyl acetate by weight in remove impurity Pollen Typhae for subsequent use: the mixed liquor of water=2-6:1 preparation, at temperature 30-70 ℃, soak, the time is 1.0-2.0 hour, filters, and must soak Pollen Typhae afterwards; After soaking, 30-55 ℃ of warm water washing 1-4 time for Pollen Typhae, filters, stays slag again, obtains water treatment Pollen Typhae, for subsequent use;
C`, add to water treatment Pollen Typhae for subsequent use the ethanol that 2-6 times of weight, volumetric concentration are 70-90%, boil and extract 0.5-3.0 hour, filter, collect filtrate; In recrement, add the ethanol that 1-2 times of weight, volumetric concentration are 50-70% again, boil and extract 0.5-1.5 hour, filter, merge extracted twice liquid, obtain just extract of Pollen Typhae, for subsequent use;
D`, by Pollen Typhae for subsequent use just extract at 55-90 ℃, be concentrated into 1/5 to 1/3 of original volume, obtain the preliminary concentrated solution of Pollen Typhae, for subsequent use;
E`, the pH value of the preliminary concentrated solution of Pollen Typhae is adjusted to 7.5-8.5 with the aqueous alkali of weight concentration 1.5-3.0%, obtains Pollen Typhae provisional value and adjust concentrated solution, for subsequent use;
F`, Pollen Typhae provisional value for subsequent use is adjusted to concentrated solution, drop in falling film condenser, at 45-70 ℃, be concentrated into 1/2 of original volume, filter, obtain Pollen Typhae concentrated solution, for subsequent use;
G`, by Pollen Typhae concentrated solution for subsequent use under 1.0-1.5MPa pressure, through flame filter press filter, obtain Pollen typhae.
2. massage Oleum Camelliae according to claim 1, it is characterized in that being prepared from by following raw material by weight:
3. massage Oleum Camelliae according to claim 1, it is characterized in that being prepared from by following raw material by weight:
4. massage Oleum Camelliae according to claim 1, it is characterized in that being prepared from by following raw material by weight:
5. massage Oleum Camelliae according to claim 1, it is characterized in that being prepared from by following raw material by weight:
6. massage Oleum Camelliae according to claim 1, it is characterized in that being prepared from by following raw material by weight:
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310334112.6A CN103340818B (en) | 2013-08-03 | 2013-08-03 | Massage tea oil |
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| CN201310334112.6A CN103340818B (en) | 2013-08-03 | 2013-08-03 | Massage tea oil |
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| CN103340818A CN103340818A (en) | 2013-10-09 |
| CN103340818B true CN103340818B (en) | 2014-07-02 |
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| CN105687237A (en) * | 2016-01-27 | 2016-06-22 | 屈良军 | Cancer treatment medicine and preparation method of external massage oil |
| CN108403542A (en) * | 2018-03-20 | 2018-08-17 | 王新会 | One kind is compacted massage oil and preparation method thereof |
| CN112316094A (en) * | 2020-12-30 | 2021-02-05 | 李桥梁 | Male lymph health-care essential oil and preparation method thereof |
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| CN101268995A (en) * | 2008-05-12 | 2008-09-24 | 谭长明 | Tea seed oil skin-protection cheirapsis cream and preparation method thereof |
| CN102885749B (en) * | 2012-10-15 | 2014-03-12 | 管天球 | Oil tea cosmetic |
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