CN103331029B

CN103331029B - Distiller

Info

Publication number: CN103331029B
Application number: CN201310288941.5A
Authority: CN
Inventors: 曹瑾
Original assignee: HUZHOU XIN DING SEMICONDUCTOR MATERIALS Co Ltd
Current assignee: HUZHOU XIN DING SEMICONDUCTOR MATERIALS Co Ltd
Priority date: 2013-07-10
Filing date: 2013-07-10
Publication date: 2015-06-17
Anticipated expiration: 2033-07-10
Also published as: CN103331029A

Abstract

A distiller belongs to distillation equipment and comprises a collection chamber for collecting a gas, the upper portion of the collection chamber is communicated with a distillation chamber through a communication port, a helical tube used for condensing the gas is arranged in the distillation chamber, the helical tube is communicated with a water storage chamber arranged in the periphery of the distillation chamber, the water storage chamber is provided with an inlet, and the helical tube is communicated with an outlet; a downward purification tube is arranged at one side of the connection port of the collection chamber and the distillation chamber at the bottom of the distillation chamber; and the purification tube is communicated with a shunting chamber, a magnet offset device for changing the flow track of a liquid is arranged in the shunting chamber, the bottom of the shunting chamber is communicated with a shunting tube and a refluxing tube respectively, and the refluxing tube is communicated with the collection chamber. The distiller can synchronously detect the purity of a purified product, and can instantly automatically returns the undistilled and inadequately-distilled liquid to the distillation chamber for afresh distillation, so the purification quality is guarantees, and the work efficiency is accelerated.

Description

A kind of distiller

Technical field

The present invention relates to equipment for purifying, particularly a kind of distilation device.

Background technology

By heating liquid to boiling, make liquid become steam, then make steam cool and be condensed into liquid again, the joint operation of these two processes is called distillation.Distiller is exactly the utensil utilizing way of distillation separate substance.Clearly, volatile and not volatile separating substances can come by distillation, also liquid mixtures different for boiling point can be separated.Its advantage is not need to use other solvent beyond system components, thus ensures to introduce new impurity.

But existing a lot of distiller is all be divided into a lot of distilation steps, sometimes also need multiple tracks still-process, which improves equipment cost, and the efficiency reduced, and be not easy to form circulation distillation, can not test be carried out for the distillating liquid after distillation immediately and effectively recycle distillation.

Summary of the invention

Object of the present invention solves the problems of the technologies described above, and provides a kind of circulation distillation, test in time to liquid after distillation, and walk around to redistillation process to not distilling part fully.

Technical solution of the present invention is: a kind of distiller, comprise the collecting chamber for collecting gas, described collecting chamber top is communicated with distillery by connected entrance, the helix tube being used for condensed gas is set in described distillery, described helix tube communicates with the water storage cavity being arranged on distillery periphery, water storage cavity arranges an import, and helix tube connects an outlet; In the bottom of distillery, the connected entrance side setting direction purification pipe down of collecting chamber and distillery; Described purification pipe is communicated with diffluence room, and arrange the magnetite offset assembly for changing liquid flow track in diffluence room, the bottom of diffluence room is communicated with isocon and return duct respectively, and described return duct is communicated with collecting chamber.

The gas collected imports in distillery by this distiller, and gas, after the helix tube that cold water is equipped with in inside, is condensed into liquid, fall back to again bottom distillery, flow in purification pipe, then flow in diffluence room, the magnetite offset assembly of diffluence room, the flow track of liquid is changed by magnetic force, make it to drop in amesiality isocon, and it is larger not distill sufficient liquid gravity, direct vertical drop is in return duct, then enter in collecting chamber, through again distilling.

As preferably, in diffluence room, between described isocon and return duct, baffle plate is set.Because magnetite offset assembly utilizes the effect of magnetite, liquid is made to offset flow track, but the not all liquid of the caliber reason that is different and isocon of the flow velocity because of liquid can drop in isocon accurately, so arrange baffle plate between isocon and return duct, for preventing from entering the liquid of isocon and having flow in return duct.

As preferably, described isocon one end is communicated with diffluence room, and the other end arranges S shape bend.Liquid in isocon is hotter, and S shape bend by a part of fluid storage in bend, can reach certain cooling effect.

As preferably, the top of described distillery is communicated with relief tube.Because the pressure ratio in distillery is comparatively large, if the airtight setting of distillery, be easy to set off an explosion.

As preferably, described relief tube comprises extension, and described extension is connected with isocon.Relief tube arranges extension and is conducive to cooling and pressurize.

As preferably, described distillery is provided with seal closure outside the connected entrance of collecting chamber, and passage is offered in the both sides of seal closure.Seal closure is directly entered in distillery for the gas cut off in collecting chamber, can only be entered in distillery by the passage on seal closure.To prevent the liquid in distillery from entering in collecting chamber like this.

As preferably, the distance of described passage and distillery bottom surface is more than or equal to 5mm.Because liquid cooled in distillery likely can not enter in purification pipe at once, certain extruding can be had bottom distillery, so passage can not be arranged on the bottom surface of distillery, certain distance will be had with bottom surface.

As preferably, described collecting chamber integrally connects temperature tube, temperature tube one end open, opening direction is towards outside collecting chamber.

As preferred further, described distiller is quartz still.Quartz is the mineral resources that a kind of physical property and chemical property are all very stable, and crystal belongs to the oxide mineral of trigonal system.All reaction can not be produced with a lot of chemical substance.

Beneficial effect of the present invention is:

1. this distiller synchronously can detect the purity of purification, and automatically immediately turns back to redistillation again in distillery by not distilling insufficient liquid, ensure that purification quality, and accelerates operating efficiency.

2. this apparatus structure is simple, easy to operate, and integral type connects, and good airproof performance, purification efficiency is high.

Accompanying drawing explanation

Fig. 1 is embodiment of the present invention structure chart;

Fig. 2 is the enlarged drawing in the A portion of Fig. 1.

In figure: 1-collecting chamber, 11-temperature tube, 12-passage, 13-connected entrance, 2-distillery, 21-seal closure, 3-helix tube, 4-water storage cavity, 41-import, 42-exports, 5-relief tube, 51-extension, 6-isocon, 61-bend, 7-return duct, 8-diffluence room, 81-baffle plate, 9-magnetite offset assembly, 10-purifies pipe.

Detailed description of the invention

Below in conjunction with accompanying drawing, with embodiment, the invention will be further described.

This specific embodiment is only explanation of the invention; it is not limitation of the present invention; those skilled in the art can make to the present embodiment the amendment not having creative contribution as required after reading this description, as long as but be all subject to the protection of Patent Law in right of the present invention.

Embodiment 1, as shown in Figure 1, a kind of distiller, all material is all make with quartz, comprises the collecting chamber 1 for collecting gas, and described collecting chamber 1 top is communicated with distillery 2 by connected entrance 13, and collecting chamber 1 and distillery 2 are that one is connected.Also integrally be connected to temperature tube 11 in collecting chamber 1, temperature tube 11 one end open, opening direction is towards outside collecting chamber 1.Such user just can measure inner temperature outside distiller.The top of distillery 2 has been communicated with relief tube 5.In described distillery 2, the helix tube 3 being used for condensed gas is set, described helix tube 3 communicates with the water storage cavity 4 being arranged on distillery 2 periphery, water storage cavity 4 and distillery 2 are also that one is connected, and the top of water storage cavity 4 arranges an import 41, and the bottom of helix tube 3 connects an outlet 42; Such benefit is the gravity utilizing water, and cold water can automatically from import to outlet.In the bottom of distillery 2, the connected entrance 13 side setting direction purification pipe 10 down of collecting chamber 1 and distillery 2; The gas that collecting chamber 1 is collected enters into distillery 2, is condensed into liquid, then drops to the bottom of distillery 2, enter into purification pipe 10 after running into helix tube 3.Described purification pipe 10 is communicated in diffluence room 8, magnetite offset assembly 9 for changing liquid flow track is set in diffluence room 8, the bottom of diffluence room 8 is communicated with isocon 6 and return duct 7 respectively, magnetite offset assembly 9 can change the flow track of liquid in purification pipe 10 by the effect of magnetic force, distillation is made partly to flow in isocon 6 fully, not distilling part fully can because magnetic force is inadequate, and directly drop in return duct 7, and described return duct 7 is communicated with collecting chamber 1.Do not distill part fully like this to come back in collecting chamber 1, again distill.Due to the flow rate of liquid problem in the pipe diameter size of isocon 8 and purification pipe, be not can drop in isocon 8, so be provided with baffle plate 81 between isocon 8 and return duct 7.One end of isocon 6 is communicated with diffluence room 8, and the other end arranges the bend 61 of S shape, and the height of bend 61 will connect one end of diffluence room 8 lower than isocon 6, like this can anti-backflow.Bend 61 can play the function of cooling liquid in addition, prevents overheated liquid to be directly received.The relief tube 5 that distillery 2 top is communicated with has extension 51, and extension 51 and whole distiller phase co-altitude, the bend 61 of isocon 6 is communicated with extension 51.Whole extension 51 can play the function of pressurize and cooling.

As shown in Figure 2, distillery 2 is provided with seal closure 21 outside the connected entrance 13 of collecting chamber 1, and the passage 12 of many rows has been offered in the both sides of seal closure 21.Seal closure 21 can prevent the liquid of cooling in distillery 2 to be back in collecting chamber 1 again, and passage 12 ensure that the gas in collecting chamber 1 can enter in distillery 2.Because purification pipe 10 is the bottoms being arranged on distillery 2, and can not at once enter in purification pipe 10 completely due to cooled liquid, the bottom at distillery 2 may be overstock, so passage 12 is more than or equal to 5mm with the distance of distillery 2 bottom surface, be preferably 8mm or 10mm.

Claims

1. a distiller, comprise the collecting chamber (1) for collecting gas, described collecting chamber (1) top is communicated with distillery (2) by connected entrance (13), it is characterized in that: the helix tube (3) being used for condensed gas is set in described distillery (2), described helix tube (3) communicates with the water storage cavity (4) being arranged on distillery (2) periphery, water storage cavity (4) arranges an import (41), and helix tube (3) connects an outlet (42); In the bottom of distillery (2), connected entrance (13) the side setting direction purification pipe (10) down of collecting chamber (1) and distillery (2); Described purification pipe (10) is communicated with diffluence room (8), magnetite offset assembly (9) for changing liquid flow track is set in diffluence room (8), the bottom of diffluence room (8) is communicated with isocon (6) and return duct (7) respectively, and described return duct (7) is communicated with collecting chamber (1); In diffluence room (8), baffle plate (81) is set between described isocon (6) and return duct (7); Described distillery (2) is provided with seal closure (21) outside the connected entrance (13) of collecting chamber (1), and passage (12) is offered in the both sides of seal closure (21).

2. by a kind of distiller according to claim 1, it is characterized in that: described isocon (6) one end is communicated with diffluence room (8), and the other end arranges S shape bend (61).

3. by a kind of distiller according to claim 2, it is characterized in that: the top of described distillery (2) is communicated with relief tube (5).

4., by a kind of distiller according to claim 3, it is characterized in that: described relief tube (5) comprises extension (51), described extension (51) is connected with isocon (6).

5. by a kind of distiller according to claim 1, it is characterized in that: described passage (12) is more than or equal to 5mm with the distance of distillery (2) bottom surface.

6., by a kind of distiller according to claim 1, it is characterized in that: described collecting chamber (1) integrally connects temperature tube (11), temperature tube (11) one end open, opening direction towards collecting chamber (1) outward.

7., by a kind of distiller described in claim 4 or 5 or 6, it is characterized in that: described distiller is quartz still.