CN103284321A - Functional cut stem lowering carbon monoxide release amount in cigarette main stream smoke and preparation method thereof - Google Patents
Functional cut stem lowering carbon monoxide release amount in cigarette main stream smoke and preparation method thereof Download PDFInfo
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- CN103284321A CN103284321A CN201310226471XA CN201310226471A CN103284321A CN 103284321 A CN103284321 A CN 103284321A CN 201310226471X A CN201310226471X A CN 201310226471XA CN 201310226471 A CN201310226471 A CN 201310226471A CN 103284321 A CN103284321 A CN 103284321A
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- stem
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- cigarette
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 57
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 title claims abstract description 23
- 229910002091 carbon monoxide Inorganic materials 0.000 title claims abstract description 19
- 239000000779 smoke Substances 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title claims description 8
- 239000001508 potassium citrate Substances 0.000 claims abstract description 31
- 229960002635 potassium citrate Drugs 0.000 claims abstract description 31
- QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 claims abstract description 31
- 235000011082 potassium citrates Nutrition 0.000 claims abstract description 31
- 241000208125 Nicotiana Species 0.000 claims abstract description 26
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 26
- 239000000654 additive Substances 0.000 claims abstract description 7
- 230000000996 additive effect Effects 0.000 claims abstract description 7
- 238000000034 method Methods 0.000 claims description 18
- 230000008569 process Effects 0.000 claims description 7
- 238000010792 warming Methods 0.000 claims description 7
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 238000003860 storage Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 2
- 238000005520 cutting process Methods 0.000 claims 2
- 239000006193 liquid solution Substances 0.000 claims 2
- 238000003825 pressing Methods 0.000 claims 2
- 239000012527 feed solution Substances 0.000 claims 1
- 238000005507 spraying Methods 0.000 claims 1
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 abstract description 4
- 229960002715 nicotine Drugs 0.000 abstract description 4
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 abstract description 4
- 230000009467 reduction Effects 0.000 description 12
- 238000005516 engineering process Methods 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- 238000002485 combustion reaction Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- NAVWVHRQSDHCHD-UHFFFAOYSA-N 2-hydroxypropane-1,2,3-tricarboxylic acid;potassium Chemical compound [K].OC(=O)CC(O)(C(O)=O)CC(O)=O NAVWVHRQSDHCHD-UHFFFAOYSA-N 0.000 description 4
- 239000003546 flue gas Substances 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000005096 rolling process Methods 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 230000001427 coherent effect Effects 0.000 description 2
- 238000004939 coking Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000008267 milk Substances 0.000 description 2
- 210000004080 milk Anatomy 0.000 description 2
- 235000013336 milk Nutrition 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 208000024896 potassium deficiency disease Diseases 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000007619 statistical method Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 241000675108 Citrus tangerina Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 208000019025 Hypokalemia Diseases 0.000 description 1
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 1
- GPSAAQWVJOVCBK-UHFFFAOYSA-N [K].[K].[K].OC(=O)CC(O)(C(O)=O)CC(O)=O Chemical compound [K].[K].[K].OC(=O)CC(O)(C(O)=O)CC(O)=O GPSAAQWVJOVCBK-UHFFFAOYSA-N 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000000872 buffer Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 235000013351 cheese Nutrition 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 235000021185 dessert Nutrition 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 239000000017 hydrogel Substances 0.000 description 1
- 235000015094 jam Nutrition 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 239000008274 jelly Substances 0.000 description 1
- 238000007726 management method Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
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- Manufacture Of Tobacco Products (AREA)
Abstract
一种降低卷烟主流烟气中的一氧化碳释放量的功能性梗丝,所述的功能性梗丝是在烟梗中加入柠檬酸钾作为添加剂通过后处理获得的。本发明中的获得的功能性烟梗,用于制作成卷烟后,卷烟烟气中烟碱含量与焦油含量降低,一氧化碳的含量也降低,且一氧化碳含量降低的明显。
Disclosed is a functional shredded stem that reduces the amount of carbon monoxide released in cigarette mainstream smoke. The functional shredded stem is obtained by adding potassium citrate as an additive to tobacco stems through post-treatment. After the functional tobacco stem obtained in the present invention is used to make cigarettes, the content of nicotine and tar in cigarette smoke is reduced, and the content of carbon monoxide is also reduced, and the content of carbon monoxide is significantly reduced.
Description
Technical field
The present invention relates to cigarette throwing field, particularly a kind of by adding harmless additive, reduce the method for the carbon monoxide in the stem combustion product gases.
Background technology
2010, State Bureau's establishment " tobacco business " level on the cigarette " overall planning " has been put into effect supporting policy measure file respectively to " level in the brand development ", " raw material ensures the level of going up ", " level in the technological innovation ", " level in the marketing ", " level on the basic management ".Planning clearly proposes: the basic Founder and the strategic task that " level on the cigarette " are defined as an industry job in period at present and in the future.
Along with the proposition of " level on the cigarette " strategic objective, wherein shoulder heavy responsibilities especially as cigarette security and the lowering harm and decreasing coking of mission critical.Wherein in the cigarette burning process, because the carbon monoxide difficulty problem of falling that imperfect combustion causes is everybody research emphasis always, be difficult to effectively reach the reduction effect by existing cigarette processing technology and cigarette composition adjustment.Wherein burning being produced the bigger tobacco material of carbon monoxide contribution amount is offal and reconstituted tobacco etc.Through discovering, the control combustion process is one of a kind of comparatively simple and effective solution with regard to the carbon monoxide that energy better controlled cigarette burning produces so seek a kind of more suitable additive.
Potassium citrate has another name called potassium citrate, citric acid tri potassium.Molecular formula: K
3C
6H
5O
7H
2O, molecular weight: 324.4, proterties: colourless crystallization or white crystalline powder, have and littlely draw moistly, soluble in water, slow be dissolved in glycerine, be insoluble to alcohol, it is salty and cool to distinguish the flavor of.Proportion: 1.98, it is a kind of additive commonly used, main application has and is used as buffer, chelating agent, stabilizing agent, antioxidant, emulsifying agent and flavor enhancement in the food industry.Can be used for milk and milk products, jelly, jam, meat, canned hydrogel dessert, the emulsification of cheese, oranges and tangerines fresh-keeping etc.; Be used for hypokalemia and potassium deficiency disease and alkalized urine in the medical industry.Also can be made into high-efficiency compound fertilizer, also can be used for papermaking, industry such as gold-plated.
Summary of the invention
The shortcoming of prior art in view of the above, purpose of the present invention is intended to overcome the deficiency of existing cigarette lowering harm and decreasing coking technology, by easy process means, do not setting up under the condition that is equipped with, behind the additive that adds a kind of stability and safety, obtain a kind of new type functional stem, make that carbon monoxide content obviously reduces in the cigarette smoke, improve the security of cigarette product.
Reach other relevant purposes for achieving the above object, the invention provides a kind of functional stem that reduces the carbon monoxide burst size in the cigarette mainstream flue gas, described functional stem adds potassium citrate and obtains by post processing as additive in offal.
Preferably, the addition of described potassium citrate is the 6%-10% of tobacco stalk quality.
The preparation technology of described functional stem may further comprise the steps: the feed liquid that contains potassium citrate or the aqueous solution that will prepare, be applied on the offal at the offal charging process, again the offal behind the adding citric acid potassium is carried out a series of processing and obtain the finished product stem, be i.e. functional stem.
Described offal charging process is to utilize compressed air or steam to help spray, and the deployed feed liquid that contains potassium citrate or the aqueous solution are applied on the offal uniformly.
Described a series of being treated to: a series of being treated to: stem, stem warming and humidifying are obstructed, cut to storage stalk, offal warming and humidifying, pressure, stem is reinforced, stem is dry and the stem selection by winnowing.The described step that offal behind the adding citric acid potassium is carried out a series of processing as shown in Figure 1.
A kind of cigarette that reduces the CO burst size contains functional stem described above, is the finished product stem to be mixed according to cigarette join requirement and cigarette shreds is mixed with addition of perfume (or spice), the cigarette finished product pipe tobacco is carried out the storage procedure equilibrium moisture content after, last machine rolling cigarette.
A kind of method that reduces CO burst size in the cigarette smoke, be to adopt in the offal addition step to add potassium citrate feed liquid or the aqueous solution, successively through secondary storage stalk, offal warming and humidifying, press stalk, cut stem, stem warming and humidifying, stem are reinforced, stem warming and humidifying, stem drying, stem selection by winnowing formation finished product stem again, this finished product stem is doped in the cigarette shreds roll through last machine.
The method of CO burst size is in the application in cigarette throwing field in the reduction cigarette smoke described above.
The preparation method of a kind of functional stem that reduces the carbon monoxide burst size in the cigarette mainstream flue gas of the present invention is simple, and to reduce contribution degree little to falling in the cigarette smoke nicotine content and tar content for the functional stem of acquisition; Big to falling the carbon monoxide contribution degree, when the addition of potassium citrate account for whole stem amount ratio 6% the time, with do not add potassium citrate the product contrast of stem, whole cigarette carbon monoxide reduction amount 0.3mg/ props up reduction ratio 2.2%; When the addition of potassium citrate account for whole stem ratio 10% the time, with do not add potassium citrate the product contrast of stem, whole cigarette carbon monoxide reduction amount 1.5mg/ props up reduction ratio 11.0%.This shows that action effect is obvious among the CO of new type functional stem in reducing cigarette smoke.
Description of drawings
Fig. 1 is preparation technology's flow chart of functional stem of the present invention
The specific embodiment
Below by specific instantiation explanation embodiments of the present invention, those skilled in the art can understand other advantages of the present invention and effect easily by the disclosed content of this specification.The present invention can also be implemented or be used by the other different specific embodiment, and the every details in this specification also can be based on different viewpoints and application, carries out various modifications or change under the spirit of the present invention not deviating from.
Embodiment 1
Prepare a certain amount of tobacco stalk raw material, take by weighing offal gross mass 6%, 8% and 10% potassium citrate solid respectively, the potassium citrate solid that takes by weighing is dissolved in the water of equal in quality, obtains the potassium citrate mother liquor.Resulting potassium citrate mother liquor evenly is applied on the offal in offal warming and humidifying operation, makes the new type functional offal.Functional offal is handled through storage stalk and follow-up existing technological process processing, and making moisture content is 12.5% ± 1% stem, obtains functional finished product stem.The finished product stem mixed according to technology join requirement and mix with addition of fragrant operation and finish finished cigarettes pipe tobacco prescription.Join after the finished cut tobacco that finishes carries out storage procedure balance pipe tobacco moisture content mixing, last machine rolls.
The stem (sample in contrast) that makes of the method for adding citric acid potassium not in the finished product stem that makes with said method and the prior art carries out coherent detection through rolling cigarette to its smoke combustion composition respectively, and it is as follows to obtain the result:
The cigarette of table 1 stem preparation of the present invention and contrast cigarette burning flue gas testing result table
Table 2 adds the pure stem sample of sylvite cigarette smoke testing result statistical analysis table
From the result, and to compare in the same old way, the functional stem for preparing among the present invention is made main flume nicotine amount behind the cigarette, tar content, CO content all decline, and is high-positive correlation with the increase of potassium citrate addition.
Embodiment 2
Use the finished product stem of making the potassium citrate that applies 6%, 8%, 10% mass fraction respectively with a kind of tobacco stalk raw material according to technology among the embodiment 1 respectively, the finished product stem (in the same old way) that obtains of the same treatment of adding citric acid potassium not in described finished product stem and the prior art, mix with a kind of leaf silk by 20% mass fraction respectively, through rolling cigarette, and their smoke combustion composition carried out coherent detection, it is as follows to obtain the result:
Two kinds of cigarette smoke testing results of table 3 table
Table 4 applies the cigarette sample cigarette smoke testing result statistical analysis table that the finished product stem of potassium citrate is made
From the result, when the continuous rising of potassium citrate addition in the cigarette offal, the whole fume indication of cigarette changes.Wherein little to nicotine content in the cigarette smoke and tar content reduction contribution degree; It is big that carbon monoxide content is reduced contribution degree, when the addition of potassium citrate account for whole stem mass percent 6% the time, with do not add potassium citrate the product contrast of stem, whole cigarette carbon monoxide reduction amount 0.3mg/ props up reduction ratio 2.2%; When the addition of potassium citrate account for whole stem mass percent 10% the time, with do not add potassium citrate the product of stem compare, whole cigarette carbon monoxide reduction amount 1.5mg/ props up reduction ratio 11.0%.This shows that the CO action effect in the new type functional stem reduction cigarette smoke is obvious.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not is used for restriction the present invention.Any person skilled in the art scholar all can be under spirit of the present invention and category, and above-described embodiment is modified or changed.Therefore, have in the technical field under such as and know that usually the knowledgeable modifies or changes not breaking away from all equivalences of finishing under disclosed spirit and the technological thought, must be contained by claim of the present invention.
Claims (9)
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104382221A (en) * | 2014-10-09 | 2015-03-04 | 红云红河烟草(集团)有限责任公司 | Method for processing tobacco stems into cut stems |
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US4489739A (en) * | 1982-05-24 | 1984-12-25 | Kimberly-Clark Corporation | Smokable tobacco composition and method of making |
CN1350808A (en) * | 2000-10-26 | 2002-05-29 | 昆明卷烟厂 | Technology for dispensing tobacco |
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CN101611923A (en) * | 2008-06-24 | 2009-12-30 | 湖北中烟工业有限责任公司 | Method for processing Burley tobacco stems into expanded shredded stems |
EP2351495A1 (en) * | 2008-11-06 | 2011-08-03 | Japan Tobacco, Inc. | Smoking article and method of manufacturing same, and method for manufacturing carbon monoxide reducing agent |
CN102920004A (en) * | 2012-11-23 | 2013-02-13 | 中国烟草总公司郑州烟草研究院 | Technique for preparing tobacco stalks into stalk slices after threshing |
CN103005693A (en) * | 2012-12-25 | 2013-04-03 | 上海烟草集团有限责任公司 | Functional cut rolled stem for selectively reducing cigarette mainstream smoke carbon monoxide release and application of functional cut rolled stem |
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2013
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Patent Citations (7)
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US4489739A (en) * | 1982-05-24 | 1984-12-25 | Kimberly-Clark Corporation | Smokable tobacco composition and method of making |
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JP2006217820A (en) * | 2005-02-08 | 2006-08-24 | Japan Tobacco Inc | Cigarette |
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EP2351495A1 (en) * | 2008-11-06 | 2011-08-03 | Japan Tobacco, Inc. | Smoking article and method of manufacturing same, and method for manufacturing carbon monoxide reducing agent |
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CN103005693A (en) * | 2012-12-25 | 2013-04-03 | 上海烟草集团有限责任公司 | Functional cut rolled stem for selectively reducing cigarette mainstream smoke carbon monoxide release and application of functional cut rolled stem |
Non-Patent Citations (4)
Title |
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于建军: "《卷烟工艺学 第2版》", 30 October 2009, 中国农业出版社 * |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104382221A (en) * | 2014-10-09 | 2015-03-04 | 红云红河烟草(集团)有限责任公司 | Method for processing tobacco stems into cut stems |
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