CN103284245A - Method for preparing odorless garlic clarified juice - Google Patents
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Abstract
本发明具体公开了一种制备无臭大蒜澄清汁的方法,目的在于解决大蒜汁的除臭和澄清问题,有利于提供一种供制备大蒜饮料的无臭、澄清无沉淀的原蒜汁。其方法是将脱臭干制大蒜粉碎、过150目筛,得无臭大蒜粉,将大蒜粉与水的质量比为1:10,沸水浴糊化30min,将高温α-淀粉酶加入糊化液中,然后在条件pH4.5、温度90℃、α-淀粉酶用量0.45%、水浴时间55min处理,得酶解液,继续加热至100℃,灭酶煮沸保持15min后,在6000r/min下离心30min得离心液,即为无臭大蒜澄清汁。本发明产品能够较好地解决大蒜饮料原汁的沉淀问题,为提高大蒜饮料制品提供了原料保障。The invention specifically discloses a method for preparing odorless clarified garlic juice, which aims to solve the problems of deodorization and clarification of garlic juice, and is beneficial to provide an odorless, clarified and precipitation-free raw garlic juice for preparing garlic drinks. The method is to crush deodorized dried garlic and pass through a 150-mesh sieve to obtain odorless garlic powder. The mass ratio of garlic powder to water is 1:10, gelatinize in a boiling water bath for 30 minutes, and add high-temperature α-amylase to the gelatinized liquid. Then, under the conditions of pH 4.5, temperature 90°C, α-amylase dosage 0.45%, and water bath time 55 minutes, the enzymolysis solution was obtained, and continued to heat to 100°C, and boiled for 15 minutes to inactivate the enzyme, then centrifuged at 6000r/min After 30 minutes, the centrifugate was obtained, which was odorless garlic clarified juice. The product of the invention can better solve the problem of precipitation of the raw juice of the garlic beverage, and provides raw material guarantee for improving the garlic beverage products.
Description
技术领域 technical field
本发明属于食品加工领域,具体涉及一种制备无臭大蒜澄清汁的方法。 The invention belongs to the field of food processing, and in particular relates to a method for preparing odorless clarified garlic juice.
背景技术 Background technique
大蒜是一种具有滋养功效的保健性食品,我国普遍作为蔬菜和调味品食用。现代药理研究表明大蒜具有很好的生理功能,具有抗菌消炎、抗病毒、降低血脂、降血压、防治糖尿病以及延缓衰老等功效。随着科技发展和人们物质生活提高的需求,随之而来的大蒜加工制品不断涌现,以满足不同人群对大蒜制品需求的选择。目前国内已开发的大蒜制品有大蒜胶囊、软胶囊、大蒜口服液、香脆大蒜米、大蒜口香糖、大蒜饮料以及大蒜果蔬复合饮料等,尤其是以大蒜为有效成分制备的各种饮料,其制备的原料为大蒜汁,由于大蒜具有特殊的刺激性臭味,在制备过程中不能得到很好的祛除,致使产品味道不佳,影响人们的食用;再之就是大蒜原汁液中含有较多的有机质,特别是大蒜中所含的淀粉致使大蒜原汁液很难得到澄清,极易沉淀,因而使后续加工的大蒜饮料制品常常出现混浊、分层、沉淀而影响产品的质量。 Garlic is a health food with nourishing effect, and it is generally eaten as a vegetable and condiment in our country. Modern pharmacological studies have shown that garlic has good physiological functions, such as antibacterial, anti-inflammatory, antiviral, lowering blood fat, lowering blood pressure, preventing and treating diabetes, and delaying aging. With the development of science and technology and the improvement of people's material life, garlic processed products continue to emerge to meet the needs of different groups of people for the choice of garlic products. At present, the garlic products that have been developed in China include garlic capsules, soft capsules, garlic oral liquid, crispy garlic rice, garlic chewing gum, garlic beverages, and garlic fruit and vegetable compound beverages, etc., especially various beverages prepared with garlic as an active ingredient. The raw material is garlic juice. Because garlic has a special pungent odor, it cannot be removed well during the preparation process, resulting in a bad taste of the product and affecting people's consumption; moreover, the raw garlic juice contains more organic matter. , especially the starch contained in the garlic makes the original garlic juice difficult to be clarified and easily precipitated, so that the subsequent processed garlic beverage products often appear turbid, stratified, and precipitated, which affects the quality of the product.
大蒜的化学成分比较复杂,包括常规营养成分如氨基酸、维生素、碳水化合物以及大蒜油等。100g鲜蒜含水70g、蛋白质4.4g、脂肪0.2g、碳水化合物23g、粗纤维0.7g、灰分1.3g,其中钙5mg、磷44mg、铁0.4g、维生素D0.24mg、维生素B20.03mg、烟酸0.9mg、维生素C3mg、大蒜油0.2g。从鲜大蒜所含成分含量中碳水化合物23%,大蒜的碳水化合物有还原糖(以葡萄糖和果糖为主)、蔗糖、多聚糖等。从碳水化合物所含比例来看,以多聚量最高,达到51%,其次为淀粉8.22%,糊精7.69%,蔗糖3.79%,还原糖0.14%(张连富等主编,药食兼用资源与生物活性成分·化学工业出版社,2005年9月第1版,第94页倒数1行至第95页第1-2行)。从上述成分含量比较中可以看出大蒜中淀粉含量占总碳水化合物比例的8.22%,由于淀粉含量不是太高,往往被忽视,使在产品加工加热过程中的糊化淀粉,往往造成大蒜汁产生混浊,继而产生沉淀。现有技术中为了克服大蒜汁制品在贮存期间的沉淀现象,主要采用纤维素酶、果胶酶(如中国专利CN102224955A),木瓜蛋白酶(中国专利CN101664220A)等。 The chemical composition of garlic is relatively complex, including conventional nutrients such as amino acids, vitamins, carbohydrates, and garlic oil. 100g of fresh garlic contains 70g of water, 4.4g of protein, 0.2g of fat, 23g of carbohydrates, 0.7g of crude fiber, and 1.3g of ash, of which 5mg of calcium, 44mg of phosphorus, 0.4g of iron, 0.24mg of vitamin D, 0.03mg of vitamin B2 , smoke Acid 0.9mg, vitamin C 3mg, garlic oil 0.2g. The carbohydrate content of fresh garlic is 23%. The carbohydrates in garlic include reducing sugars (mainly glucose and fructose), sucrose, and polysaccharides. From the perspective of the proportion of carbohydrates, the amount of polysaccharides is the highest, reaching 51%, followed by starch 8.22%, dextrin 7.69%, sucrose 3.79%, reducing sugar 0.14% Composition · Chemical Industry Press, first edition in September 2005, the last line on page 94 to the first and second lines on page 95). From the comparison of the above component contents, it can be seen that the starch content in garlic accounts for 8.22% of the total carbohydrates. Because the starch content is not too high, it is often ignored, so that the gelatinized starch in the product processing and heating process often causes garlic juice to produce Cloudy, followed by precipitation. In the prior art, in order to overcome the precipitation of garlic juice products during storage, cellulase, pectinase (such as Chinese patent CN102224955A), papain (Chinese patent CN101664220A) and the like are mainly used.
本发明的目的所在是研究解决一种无臭大蒜澄清汁的制备方法,目的是解决大蒜汁的除臭和澄清问题,有利于提供一种供制备大蒜饮料的无臭、澄清无沉淀的原蒜汁。 The purpose of the present invention is to study and solve a preparation method of odorless garlic clarified juice, the purpose is to solve the problem of deodorization and clarification of garlic juice, and it is beneficial to provide a kind of raw garlic that is odorless, clarified and free of precipitation for preparing garlic beverage juice.
发明内容 Contents of the invention
本发明所要解决的技术问题是,利用我公司发明专利(申请号:201210249529.8)权利要求1步骤(一)的方法制得的脱臭干制大蒜,经粉碎后,采用高温α-淀粉酶进行酶解处理,制得无臭大蒜澄清汁。 The technical problem to be solved by this invention is to use the method of step (1) of claim 1 of our company's invention patent (application number: 201210249529.8) to crush the deodorized dried garlic and use high-temperature α-amylase for enzymatic hydrolysis processing to produce odorless garlic clarified juice.
本发明所采用的技术方案是: The technical scheme adopted in the present invention is:
一种制备无臭大蒜澄清汁的方法,将脱臭干制大蒜粉碎、过150目筛,得无臭大蒜粉,将无臭大蒜粉与水的质量比为1:10,沸水浴糊化30min,将高温α-淀粉酶加入糊化液中,然后在pH4.5、温度90℃,α-淀粉酶用量0.45%,水浴时间55min的条件处理,得酶解液,酶解液加热至100℃,灭酶煮沸保持15min后,采用6000r/min下离心30min得离心液,即为无臭大蒜澄清汁。 A method for preparing odorless garlic clarified juice. The deodorized dried garlic is crushed and passed through a 150-mesh sieve to obtain odorless garlic powder. The mass ratio of odorless garlic powder to water is 1:10, and gelatinized in a boiling water bath for 30 minutes. Add high-temperature α-amylase into the gelatinization solution, and then treat it at pH 4.5, temperature 90°C, α-amylase dosage 0.45%, and water bath time 55 minutes to obtain an enzymolysis solution, which is heated to 100°C. After boiling for 15 minutes to inactivate the enzyme, centrifuge at 6000 r/min for 30 minutes to obtain the centrifugate, which is odorless garlic clarified juice.
本发明所述的脱臭干制大蒜,是发明专利(申请号:201210249529.8)权利要求1步骤(一)的方法制得,其制备方法是:(1)选料:拣选鳞茎成熟、清洁、干燥、外衣完整、无破损、无霉烂、无虫蛀,剪掉根须的生大蒜头;(2)烘灶干制:在烘房中采用半地下砌灶,下边升火,其上架以横木,再铺以苇席,在苇席上放置大蒜头,物料厚度为15-25厘米,用下边的火力加温,用火力控制温度在80℃-95℃,烘制150-170小时,烘制中每隔18-26小时翻料一次;(3)剥皮:将步骤(2)烘制的大蒜取出,剥去蒜皮,得半干大蒜米;(4)二次烘制:将半干大蒜米再次摊放于苇席上,摊放物料厚度为5-10厘米,用下边的火力加温,用火力控制温度在75℃-90℃,继续烘制24-72小时,使蒜米含水量小于5%时,停止烘制,移出烘房自然降温至室温,即得脱臭干制大蒜成品。 The deodorized dried garlic described in the present invention is obtained by the method of step (1) of claim 1 of the invention patent (application number: 201210249529.8), and its preparation method is: (1) material selection: select mature bulbs, clean, dry, The coat is complete, no damage, no mildew, no moths, and the raw garlic heads with roots and hairs cut off; (2) Drying in a stove: a semi-underground stove is used in the drying room, and a fire is raised below, and a crossbar is placed on it, and then Spread reed mats, place garlic heads on the reed mats, the thickness of the material is 15-25 cm, heat with the lower firepower, control the temperature at 80°C-95°C with firepower, and bake for 150-170 hours. Turn over once every 18-26 hours; (3) peeling: take out the garlic baked in step (2), peel off the garlic skin, and get semi-dried garlic rice; (4) secondary baking: dry the semi-dried garlic rice again Spread on the reed mat, the thickness of the spread material is 5-10 cm, heat with the firepower below, control the temperature at 75°C-90°C with firepower, continue to bake for 24-72 hours, so that the water content of garlic is less than 5 %, stop baking, remove from the drying room and cool down to room temperature naturally, and then the deodorized dried garlic product will be obtained.
无臭大蒜粉糊化时加水量直接影响液化过程和酶解品质,加水量过小,糊化液黏度过大,液化时酶与底物不能很好接触,以至糊化液局部变质。对于酶解成品,加水量越少、浓度越高、黏度越大,相反加水量越大,酶液浓度稀释过低,影响酶解效果。 The amount of water added during gelatinization of odorless garlic powder directly affects the liquefaction process and the quality of enzymatic hydrolysis. If the amount of water added is too small, the viscosity of the gelatinized liquid is too high. For the finished product of enzymatic hydrolysis, the less water is added, the higher the concentration and the greater the viscosity. On the contrary, the more water is added, the concentration of the enzyme solution will be diluted too low, which will affect the effect of enzymatic hydrolysis.
无臭大蒜粉糊化加水比例见表1 See Table 1 for the gelatinization and water ratio of odorless garlic powder
无臭大蒜澄清汁感官口感评分见表2 The sensory taste score of odorless garlic clarified juice is shown in Table 2
本发明的有益效果 Beneficial effects of the present invention
大蒜原汁的加工处理,对延续制备的大蒜饮料的品质影响很大,大蒜饮料在贮藏过程中淀粉的老化是大蒜原汁产生浑浊、沉淀的重要原因,本发明采用α-淀粉酶对无臭蒜粉经过充分的酶解,使糊化液中的直链淀粉水解完全。α-淀粉酶又称液化酶,可随机地作用于淀粉中的α-1,4-糖苷键,生成葡萄糖、麦芽糖、麦芽三糖、糊精等还原糖,同时使淀粉的黏度降低,达到本方法制得的产品澄清透明,无分层和沉淀现象,留样观察6个月,其色泽、外观无变化。本发明方法采用专利技术方法(申请号201210249529.8)制备无臭干制大蒜结合α-淀粉酶酶解方法制得的无臭大蒜澄清汁,一是解决了蒜汁的澄清问题,再就是解决了大蒜除臭问题,使产品具有特殊的烤制大蒜的香味。本发明产品能够较好地解决大蒜饮料原汁的沉淀问题,为提高大蒜饮料制品提供了原料保障。 The processing of raw garlic juice has a great influence on the quality of garlic beverages prepared continuously. The aging of starch in the storage process of garlic beverages is an important reason for the turbidity and precipitation of raw garlic juice. The present invention uses α-amylase to treat odorless The garlic powder is fully enzymatically hydrolyzed to completely hydrolyze the amylose in the gelatinized liquid. α-amylase, also known as liquefying enzyme, can randomly act on α-1,4-glucosidic bonds in starch to generate reducing sugars such as glucose, maltose, maltotriose, and dextrin, and at the same time reduce the viscosity of starch to achieve this The product prepared by the method is clear and transparent, without delamination and precipitation, and the color and appearance of the product remain unchanged for 6 months. The method of the present invention adopts a patented technical method (application number 201210249529.8) to prepare odorless garlic clarified juice obtained by combining odorless dried garlic with α-amylase enzymatic hydrolysis method. Deodorizes the problem, giving the product a special aroma of roasted garlic. The product of the invention can better solve the problem of precipitation of the raw juice of the garlic beverage, and provides raw material guarantee for improving the garlic beverage products.
具体实施方式 Detailed ways
实施例 Example
一种制备无臭大蒜澄清汁的方法:取脱臭干制大蒜成品,经粉碎、过150目筛,得无臭大蒜细粉;称取无臭大蒜细粉10公斤,加水100公斤,充分搅拌均匀,用沸水浴湖化30min后,加入0.495公斤α-淀粉酶搅拌均匀,调整pH值至4.5、温度90℃、水浴保温55min后,得酶解液,将酶解液加热至100℃,灭酶煮沸保持15min后,采用6000r/min下离心30min得离心液,即为无臭大蒜澄清汁。 A method for preparing odorless garlic clarified juice: take deodorized dried garlic finished product, crush and pass through a 150-mesh sieve to obtain odorless garlic fine powder; weigh 10 kg of odorless garlic fine powder, add 100 kg of water, fully stir , after 30 minutes in a boiling water bath, add 0.495 kg of α-amylase and stir evenly, adjust the pH value to 4.5, keep the temperature at 90°C, and keep warm in a water bath for 55 minutes to obtain the enzymatic hydrolysis solution, heat the enzymatic hydrolysis solution to 100°C, and inactivate the enzyme After boiling for 15 minutes, centrifuge at 6000 r/min for 30 minutes to obtain the centrifugate, which is odorless garlic clarified juice.
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CN106690062A (en) * | 2016-12-28 | 2017-05-24 | 江苏千药堂国医研究院有限公司 | Crisp garlic chips and processing method thereof |
CN106722494A (en) * | 2016-12-28 | 2017-05-31 | 江苏千药堂国医研究院有限公司 | Garlic crisp chip and preparation method thereof |
CN108004108A (en) * | 2018-01-21 | 2018-05-08 | 邳州市尕星医药技术服务有限公司 | A kind of garlic health wine and its processing method rich in garlic glycopeptide |
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CN108048291A (en) * | 2018-01-21 | 2018-05-18 | 邳州市尕星医药技术服务有限公司 | A kind of garlic health wine rich in garlic polysaccharide and preparation method thereof |
CN109043532A (en) * | 2018-07-12 | 2018-12-21 | 西安青春康美生物科技有限公司 | A kind of preparation method of Cortex Eucommiae garlic oligopeptide anti-fatigue nutrient powder |
CN109730324A (en) * | 2018-12-28 | 2019-05-10 | 河北肽都生物科技有限公司 | A kind of preparation method of small molecule garlic chelating peptide |
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