[go: up one dir, main page]

CN103243002B - Method for improving quality of smaller lumped koji distilled spirit - Google Patents

Method for improving quality of smaller lumped koji distilled spirit Download PDF

Info

Publication number
CN103243002B
CN103243002B CN201310197665.1A CN201310197665A CN103243002B CN 103243002 B CN103243002 B CN 103243002B CN 201310197665 A CN201310197665 A CN 201310197665A CN 103243002 B CN103243002 B CN 103243002B
Authority
CN
China
Prior art keywords
grain
xiaoqu
baijiu
sweet
fermentation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201310197665.1A
Other languages
Chinese (zh)
Other versions
CN103243002A (en
Inventor
汪江波
蔡凤娇
薛栋升
陈茂彬
方尚玲
镇达
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hubei University of Technology
Original Assignee
Hubei University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hubei University of Technology filed Critical Hubei University of Technology
Priority to CN201310197665.1A priority Critical patent/CN103243002B/en
Publication of CN103243002A publication Critical patent/CN103243002A/en
Application granted granted Critical
Publication of CN103243002B publication Critical patent/CN103243002B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Alcoholic Beverages (AREA)

Abstract

本发明涉及一种提升小曲白酒品质的方法,属于酿酒技术领域。本发明在小曲白酒传统工艺前提下,对曲粉添加量、糖化时间、甜醅糟比例、入罐发酵温度这些工艺进行调整。曲粉添加量为0.2%,培菌糖化22h,甜、醅糟比例为1∶1.5,入罐发酵温度为16℃且控制发酵过程中环境温度为20℃,使小曲白酒的发酵周期由传统的7天左右延长至20天,所酿造出的小曲白酒清亮透明、酒体柔和、醇香清雅、回甜爽口,与传统方法酿造的小曲白酒相比,品质有一定的提升。The invention relates to a method for improving the quality of Xiaoqu Baijiu, which belongs to the technical field of brewing. On the premise of the traditional technology of xiaoqu baijiu, the invention adjusts the processes of koji powder addition, saccharification time, proportion of sweet fermented grains and fermented grains, and tank fermentation temperature. The amount of koji powder added is 0.2%, the saccharification time is 22 hours, the ratio of sweet and fermented grains is 1:1.5, the fermentation temperature in the tank is 16°C, and the ambient temperature during the fermentation process is controlled at 20°C, so that the fermentation cycle of Xiaoqu Baijiu is changed from the traditional one. From about 7 days to 20 days, the brewed Xiaoqu baijiu is clear and transparent, soft in body, mellow and elegant, sweet and refreshing. Compared with Xiaoqu baijiu brewed by traditional methods, the quality has been improved to a certain extent.

Description

一种提升小曲白酒品质的方法A method for improving the quality of Xiaoqu Baijiu

技术领域 technical field

本发明涉及一种提升小曲白酒品质的方法,属于酿酒技术领域。 The invention relates to a method for improving the quality of Xiaoqu Baijiu, which belongs to the technical field of brewing.

背景技术 Background technique

小曲白酒是我国主要的蒸馏酒之一,产量约占我国白酒总量的1/6,其发酵周期短,出酒率高,但与大曲白酒相比,所产的小曲白酒品质一般、口感单一,且带有程度不一的苦涩味,多为中、低档白酒。为了扩大市场,提高小曲白酒的档次,必须提升小曲白酒的品质。 Xiaoqu baijiu is one of the main distilled liquors in my country. Its output accounts for about 1/6 of the total amount of liquor in my country. Its fermentation cycle is short and its yield is high. However, compared with Daqu baijiu, the quality of Xiaoqu baijiu produced is average and the taste is single , and with varying degrees of bitterness, mostly medium and low-grade liquor. In order to expand the market and improve the grade of Xiaoqu liquor, the quality of Xiaoqu liquor must be improved.

小曲白酒传统酿造工艺为:粮食→浸泡→初蒸→闷水→复蒸→摊晾加曲→培菌糖化→出箱摊晾→配糟混合→入池发酵→蒸馏。目前,小曲白酒的发酵周期普遍为7天左右,此时微生物基本已进入衰退期,若继续发酵反而有利于杂菌生长,产生大量的有害物质,影响小曲白酒的品质。但发酵周期的长短是影响酒质的关键因素之一,整个发酵期根据其主产物质的不同可依次分为:产酒精期、产酸期和产酯期,所以适当地延长发酵周期可增长产酯期,有利于有机酸与醇起缓慢的酯化作用生成酯。因此,有必要探索出适宜延长小曲白酒发酵周期的酿造工艺,使得对酿酒有益的微生物在发酵过程中的生命期增长,有利于酯香类物质的生成,以提升小曲白酒的品质。 The traditional brewing process of Xiaoqu baijiu is: grain → soaking → initial steaming → stuffy water → re-steaming → airing and adding koji → culture and saccharification → out of the box and airing → mixing with grains → entering the tank for fermentation → distillation. At present, the fermentation cycle of Xiaoqu baijiu is generally about 7 days. At this time, the microorganisms have basically entered the decline period. If the fermentation continues, it will be conducive to the growth of miscellaneous bacteria and produce a large amount of harmful substances, which will affect the quality of Xiaoqu baijiu. However, the length of the fermentation cycle is one of the key factors affecting the quality of the wine. The entire fermentation period can be divided into: alcohol production period, acid production period and ester production period according to the different main products. During the period of ester production, it is beneficial for the slow esterification of organic acids and alcohols to form esters. Therefore, it is necessary to explore a brewing process suitable for prolonging the fermentation cycle of Xiaoqu Baijiu, so that the life cycle of microorganisms beneficial to winemaking can increase during the fermentation process, which is conducive to the formation of ester aroma substances, so as to improve the quality of Xiaoqu Baijiu.

发明内容 Contents of the invention

本发明所要解决的技术问题在于提供一种提升小曲白酒品质的方法。 The technical problem to be solved by the present invention is to provide a method for improving the quality of Xiaoqu Baijiu.

为了实现上述目的,本发明采用以下技术方案:  In order to achieve the above object, the present invention adopts the following technical solutions:

1)将粮食经过浸泡、初蒸、闷水和复蒸,得到含水量51%~55%的熟粮; 1) The grain is soaked, initially steamed, steamed and re-steamed to obtain cooked grain with a water content of 51% to 55%;

2)将熟粮摊晾至30℃后,添加粮食重量0.2%的小曲粉,翻拌均匀; 2) After spreading the cooked grains to 30°C, add 0.2% of grain weight koji powder, and mix evenly;

3)将添加曲粉后的粮糟做箱糖化,糖化时间为22h; 3) Saccharify the grain grains after adding koji powder, and the saccharification time is 22 hours;

4)糖化结束后,将甜糟摊晾至25℃,加入1.5倍重量的醅糟混合均匀; 4) After the saccharification is completed, spread the sweet grains to 25°C, add 1.5 times the weight of fermented grains and mix evenly;

5)将混合均匀的甜、醅糟摊晾至16℃入发酵罐,密封发酵20天,控制发酵过程中环境温度为20℃。 5) Spread the evenly mixed sweet and fermented grains in the air to 16°C and put them into a fermenter, seal and ferment for 20 days, and control the ambient temperature during the fermentation process to 20°C.

所加入的曲粉为小曲粉,市售或自制均可。 The koji powder added is a small koji powder, which is commercially available or self-made.

所述的粮食为稻谷或小麦或高粱或大麦。 The grain is rice or wheat or sorghum or barley.

上述方法与传统工艺对比主要在以下方面进行调整:                                               加曲方式由多次下曲改为一次下曲,下曲温度由多段温度改为统一采用30℃,曲粉添加量由0.3%~0.5%降为0.2%;培菌糖化时间由24~26h降为22h;甜、醅糟的比例由1:3~1:4改为1:1.5;入池发酵温度为16℃,且发酵过程中控制环境温度为20℃,进行低温缓慢的发酵。 Compared with the traditional process, the above method is mainly adjusted in the following aspects: The method of adding koji was changed from multiple times to one time, the temperature of the next koji was changed from multi-stage temperature to 30°C, and the amount of koji powder added was reduced from 0.3% to 0.5% to 0.2%; The saccharification time of culture culture is reduced from 24 to 26 hours to 22 hours; The ratio of sweet and fermented grains is changed from 1:3 to 1:4 to 1:1.5; The fermentation temperature in the pool is 16°C, and the ambient temperature is controlled at 20°C during the fermentation process, and the fermentation is carried out at low temperature and slowly.

本发明通过减少曲粉添加量、开嫩箱、降低入罐发酵温度以及控制整个发酵过程中环境的温度,使得酒糟中微生物的对数生长期和稳定期得到延长,减缓衰退期的到来,这样有利于有机酸与醇起缓慢的酯化作用生成酯香类物质。 The present invention prolongs the logarithmic growth period and the stable period of microorganisms in the distiller's grains and slows down the coming of the recession period by reducing the amount of koji powder added, opening the tender box, lowering the fermentation temperature in the tank and controlling the temperature of the environment during the entire fermentation process. It is conducive to the slow esterification of organic acids and alcohols to generate ester aroma substances.

本发明方法具有如下有益效果: The inventive method has the following beneficial effects:

与传统小曲白酒酿造工艺相比,采用本发明所提供的方法,可将小曲白酒发酵周期由传统的7天左右延长至20天,明显提升了小曲白酒的酯香味,同时有效的控制了高级醇的生成,所酿造出的小曲白酒总酸含量为:1.48 g/L,总酯含量为:3.01 g/L,高级醇含量为:1.23g/L,酒体柔和,清亮透明,醇香清雅,回甜爽口。 Compared with the traditional brewing process of Xiaoqu Baijiu, the method provided by the present invention can extend the fermentation period of Xiaoqu Baijiu from about 7 days to 20 days, significantly improve the ester aroma of Xiaoqu Baijiu, and effectively control the higher alcohol content. The total acid content of the brewed Xiaoqu Baijiu is 1.48 g/L, the total ester content is 3.01 g/L, and the higher alcohol content is 1.23 g/L. Sweet and refreshing.

具体实施方式 Detailed ways

以下通过具体实施例,对本发明进行更为详细的说明: Below by specific embodiment, the present invention is described in more detail:

(1)称取2Kg稻谷,用72~75℃温水浸泡12h,泡粮水漫过粮面2~3cm,泡粮结束后,进行初蒸20min,闷水60min,再复蒸60min,得到的熟粮柔熟、裂口、收汗,含水量51%~55%; (1) Weigh 2Kg of rice, soak it in warm water at 72-75°C for 12 hours, soak the grain water over the surface of the grain for 2-3cm, after soaking the grain, steam for 20 minutes, steam for 60 minutes, and steam again for 60 minutes to obtain cooked rice The grain is soft and cooked, cracked, and sweated, with a water content of 51% to 55%;

(2)将步骤(1)所得到的熟粮摊晾至30℃左右,加入4g安琪酿酒曲(增香高产),翻拌均匀,摊晾至23℃; (2) Spread the cooked grain obtained in step (1) to about 30°C, add 4g of Angel Brewing Koji (increasing aroma and high yield), mix well, and let it dry to 23°C;

(3)对步骤(2)所得到的粮糟按照10cm的厚度进行做箱,培菌糖化22h; (3) Make a box for the grain grains obtained in step (2) according to the thickness of 10cm, and cultivate and saccharify for 22 hours;

(4)糖化结束后,将步骤(3)所得到的甜糟4.5Kg进行摊晾冷却至25℃,加入6.75Kg摊晾至25℃左右的醅糟,翻拌混合均匀; (4) After the saccharification is completed, spread 4.5Kg of sweet grains obtained in step (3) to cool down to 25°C, add 6.75Kg of fermented grains that are spread to about 25°C, and mix well;

(5)控制步骤(4)所得到的甜、醅混合糟温度在16℃,进入发酵罐,放置于20℃的恒温箱,密封发酵20天; (5) Control the temperature of the sweet and unstrained spirits mixed grains obtained in step (4) at 16°C, enter the fermenter, place in a thermostat at 20°C, and seal and ferment for 20 days;

(6)发酵结束后,对发酵糟进行蒸馏,分段摘酒,取中段酒与按照传统工艺发酵7天后蒸馏得到的中段酒进行感官品评和理化指标检测。 (6) After the fermentation is over, the fermented grains are distilled, the wine is harvested in sections, and the middle wine and the middle wine distilled after 7 days of fermentation according to the traditional process are used for sensory evaluation and physical and chemical index detection.

表1发酵周期为20天的小曲白酒感官品评 Table 1 Sensory evaluation of Xiaoqu Baijiu with a fermentation period of 20 days

色泽color 清亮透明、无悬浮沉淀物Clear and transparent, no suspended sediment 香气aroma 醇香清雅、具有小曲白酒独特的糟香Mellow and elegant, with the unique bad smell of Xiaoqu Baijiu 口味taste 入口绵柔、酒体柔和、醇甜The entrance is soft, the wine is soft and sweet

表2发酵周期为7天的小曲白酒感官品评 Table 2 Sensory evaluation of Xiaoqu Baijiu with a fermentation period of 7 days

色泽color 清亮透明、无悬浮沉淀物Clear and transparent, no suspended sediment 香气aroma 具有小曲白酒独特的糟香Has the unique bad aroma of Xiaoqu Baijiu 口味taste 酒味单调、口味淡薄Monotonous taste, weak taste

表3发酵周期为20天的小曲白酒的理化指标 Table 3 The physical and chemical indicators of Xiaoqu Baijiu with a fermentation period of 20 days

物质substance 总酸(mg/100mL)Total acid (mg/100mL) 总酯(mg/100mL)Total esters (mg/100mL) 高级醇(mg/100mL)Higher Alcohols (mg/100mL) 含量content 148148 301301 123123

表4发酵周期为7天的小曲白酒的理化指标 Table 4 The physical and chemical indicators of Xiaoqu Baijiu with a fermentation period of 7 days

物质substance 总酸(mg/100mL)Total acid (mg/100mL) 总酯(mg/100mL)Total esters (mg/100mL) 高级醇(mg/100mL)Higher Alcohols (mg/100mL) 含量content 139139 205205 128128

从表1、2可以看出,发酵周期为20天的小曲白酒品质明显优于发酵周期为7天的小曲白酒,尤其是口味。 It can be seen from Tables 1 and 2 that the quality of Xiaoqu liquor with a fermentation period of 20 days is obviously better than that of Xiaoqu liquor with a fermentation period of 7 days, especially the taste.

从表3、4可以看出,发酵周期为20天的小曲白酒较发酵周期为7天的小曲白酒的理化指标主要是总酯含量大大增加,总酸含量略升,由于整个发酵过程采用低温缓慢的发酵方式,虽然将发酵周期延长但高级醇的含量反而略降。 It can be seen from Tables 3 and 4 that the physical and chemical indicators of Xiaoqu Baijiu with a fermentation period of 20 days compared with Xiaoqu Baijiu with a fermentation period of 7 days are mainly that the total ester content is greatly increased, and the total acid content is slightly increased. Although the fermentation period is prolonged, the content of higher alcohols decreases slightly.

上述实施例仅为本发明的较佳实施方式之一,并非以此限制本发明的保护范围,故:凡依本发明的方法所做的等效变化,只要在本发明的要旨范围内,均应涵盖于本发明的保护范围之内。 The above-described embodiment is only one of the preferred embodiments of the present invention, and is not intended to limit the protection scope of the present invention, so: all equivalent changes made according to the method of the present invention, as long as they are within the gist of the present invention, are all Should be covered within the protection scope of the present invention.

Claims (4)

1. a method that promotes distilled liquor quality, is characterized in that, comprises the steps:
1), by the immersion of grain process, just steaming, vexed water and multiple steaming, obtain the ripe grain of water content 51%~55%;
2) by after ripe grain airing to 30 DEG C, add the little bent powder of grain weight 0.2%, turn evenly;
3) the grain grain of adding Qu Fenhou is done to case saccharification, saccharification time is 22h;
4), after saccharification finishes, by sweet poor airing to 25 DEG C, add the unstrained spirits grain of 1.5 times of weight to mix;
5) sweet, the unstrained spirits poor airing to 16 DEG C that mix are entered to fermentor tank, sealing and fermenting 20 days, in controlled fermentation process, envrionment temperature is 20 DEG C.
2. method according to claim 1, is characterized in that, the distilled liquor total acid content brewing is 1.48 g/L, and total ester content is 3.01 g/L, and higher alcohols content is 1.23g/L.
3. method according to claim 1, is characterized in that, the commercially available or self-control of the little Qu Fenwei that adds.
4. method according to claim 1, is characterized in that, described grain is paddy or wheat or Chinese sorghum or barley.
CN201310197665.1A 2013-05-24 2013-05-24 Method for improving quality of smaller lumped koji distilled spirit Expired - Fee Related CN103243002B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310197665.1A CN103243002B (en) 2013-05-24 2013-05-24 Method for improving quality of smaller lumped koji distilled spirit

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310197665.1A CN103243002B (en) 2013-05-24 2013-05-24 Method for improving quality of smaller lumped koji distilled spirit

Publications (2)

Publication Number Publication Date
CN103243002A CN103243002A (en) 2013-08-14
CN103243002B true CN103243002B (en) 2014-10-22

Family

ID=48922882

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310197665.1A Expired - Fee Related CN103243002B (en) 2013-05-24 2013-05-24 Method for improving quality of smaller lumped koji distilled spirit

Country Status (1)

Country Link
CN (1) CN103243002B (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103937642A (en) * 2014-05-05 2014-07-23 劲牌有限公司 Method for producing soft-yeast flavored liquor with high acid content and high ester content
CN103952264B (en) * 2014-05-26 2016-05-18 董长河 A kind of Solid Fermentation of Uncooked Material, liquid distillate are prepared the method for white wine
CN105524773A (en) * 2014-09-30 2016-04-27 宁夏鼎夏酒业有限公司 Process for producing Chinese koji baijiu
CN104673610B (en) * 2015-03-20 2017-07-18 云南谷冠生物科技有限公司 A kind of truffle buckwheat health-care wine and preparation method thereof
CN105002063A (en) * 2015-09-10 2015-10-28 郑成宣 Brewing method of ecological rice xiaoqu liquor
CN105039114A (en) * 2015-09-10 2015-11-11 郑成宣 Brewing method of sticky rice ecological Xiaoqu liquor
CN105062792A (en) * 2015-09-10 2015-11-18 郑成宣 Brewage method of wheat ecological Xiaoqu liquor
CN105062796A (en) * 2015-09-10 2015-11-18 郑成宣 Brewing method of rice ecological Xiaoqu wine
CN106085693A (en) * 2016-06-14 2016-11-09 四川凸酒酒业有限公司 The production method of Xiaoqu liquor by solid fermentation without bran
CN106085780A (en) * 2016-08-31 2016-11-09 泰山恒信有限公司 A kind of distilled liquor brewage process and equipment
CN107345184A (en) * 2017-08-02 2017-11-14 合江县白沙镇燕坪酒厂 The brewage process of Yi Zhong Ao arracks
CN110499223A (en) * 2019-06-28 2019-11-26 浙江致中和实业有限公司 Distilled liquor brewage process

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101260352A (en) * 2008-04-17 2008-09-10 广东省蕉岭县一线天酒业有限责任公司 Method for brewing rice-fragrant type Xiaoqu rice wine
CN102978064A (en) * 2012-12-04 2013-03-20 宣汉巴人地窖酒厂 Multi-grain fen-flavor liquor and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101260352A (en) * 2008-04-17 2008-09-10 广东省蕉岭县一线天酒业有限责任公司 Method for brewing rice-fragrant type Xiaoqu rice wine
CN102978064A (en) * 2012-12-04 2013-03-20 宣汉巴人地窖酒厂 Multi-grain fen-flavor liquor and preparation method thereof

Non-Patent Citations (10)

* Cited by examiner, † Cited by third party
Title
小曲清香型燕麦酒的研制;王超凯等;《食品与发酵科技》;20121031;第48卷(第5期);第86-88页 *
小曲白酒的生产工艺及质量控制;易良建;《中国科技信息》;20120430(第7期);第122、130页 *
干红毛樱桃酒酿造工艺研究;高海生等;《中国食品学报》;20020331;第2卷(第1期);第17-21页 *
张宇赤.控制低温缓慢发酵 提高白酒质量.《酿酒》.2003,第30卷(第2期),第1页第2-7段.
张美莉.用糯高粱与小麦酿制小曲白酒.《农产品加工》.2010,(第4期),第16-17页第2、3节.
控制低温缓慢发酵 提高白酒质量;张宇赤;《酿酒》;20030331;第30卷(第2期);第1页第2-7段 *
易良建.小曲白酒的生产工艺及质量控制.《中国科技信息》.2012,(第7期),第122、130页.
王超凯等.小曲清香型燕麦酒的研制.《食品与发酵科技》.2012,第48卷(第5期),第86-88页.
用糯高粱与小麦酿制小曲白酒;张美莉;《农产品加工》;20100430(第4期);第16-17页第2、3节 *
高海生等.干红毛樱桃酒酿造工艺研究.《中国食品学报》.2002,第2卷(第1期),第17-21页.

Also Published As

Publication number Publication date
CN103243002A (en) 2013-08-14

Similar Documents

Publication Publication Date Title
CN103243002B (en) Method for improving quality of smaller lumped koji distilled spirit
CN104450399B (en) A kind of liquid fermentation produces the method for rice spirit
CN103666927B (en) Process for preparing fresh scent strong-flavor Chinese spirit
CN107488602B (en) Abnormal Wickerhamia yeast GJYD15 and application thereof in preparation of low-temperature Daqu
CN107227237B (en) Pure brewing method of white spirit
CN105505721A (en) Production process of fragrant faint scent type liquor
CN108277132A (en) A method of shortening aromatic Chinese spirit fermentation period by storing outer esterification
CN105349400A (en) Cave type pit, pit mud and method of brewing highly flavored type basic liquor by cave type pit and pit mud
CN104987970A (en) Highly-esterified Daqu preparation method
CN107058143A (en) A kind of heat-resisting, acidproof, saccharomyces cerevisiae of resistance to ethanol and brewing fermentation agent
CN101280268A (en) Purebred rose vinegar and preparation method thereof
CN111560304B (en) A kind of wine containing superoxide dismutase SOD activity
CN101735921B (en) High temperature inverted rice wine and preparation method thereof
CN115058345B (en) A kind of Aspergillus flavus strain HJ-3 and brewing method for improving liquor quality
CN110499224A (en) A kind of process preparing strengthening porcelain using monascus
CN104987972A (en) Preparation method of liquid fermentum rubrum for brewing
CN102352287B (en) Method for increasing ester-aroma substances in Fen-flavor liquor by utilizing liquor tailing
CN105176729B (en) A kind of method for producing delicate fragrance type high-ester flavouring wine
CN104762163B (en) A kind of method preparing biological song
CN107083336B (en) A kind of production method of compound nucleoside functional song
CN103205344B (en) Method for preparing red yeast white spirit by vinasse, two yeasts and three segments of large jars
CN103805394B (en) A kind of liquor brewing method
CN107586647B (en) Liquor produced by discarding lees of Xiaoqu Qingxiang liquor and its production method
CN103525682B (en) Vinegar brewing method preventing mycoderm and vinegar flies from being generated
CN103966050B (en) Production method for micro-molecule wine

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20141022

Termination date: 20170524