CN103243002B - Method for improving quality of smaller lumped koji distilled spirit - Google Patents
Method for improving quality of smaller lumped koji distilled spirit Download PDFInfo
- Publication number
- CN103243002B CN103243002B CN201310197665.1A CN201310197665A CN103243002B CN 103243002 B CN103243002 B CN 103243002B CN 201310197665 A CN201310197665 A CN 201310197665A CN 103243002 B CN103243002 B CN 103243002B
- Authority
- CN
- China
- Prior art keywords
- grain
- xiaoqu
- baijiu
- sweet
- fermentation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000034 method Methods 0.000 title claims abstract description 19
- 238000000855 fermentation Methods 0.000 claims abstract description 31
- 230000004151 fermentation Effects 0.000 claims abstract description 31
- 235000009508 confectionery Nutrition 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 9
- 235000013339 cereals Nutrition 0.000 claims description 33
- 150000002148 esters Chemical class 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 6
- 150000001298 alcohols Chemical class 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 238000010025 steaming Methods 0.000 claims description 4
- 235000015096 spirit Nutrition 0.000 claims description 3
- 240000005979 Hordeum vulgare Species 0.000 claims description 2
- 235000007340 Hordeum vulgare Nutrition 0.000 claims description 2
- 235000021307 Triticum Nutrition 0.000 claims description 2
- 244000046109 Sorghum vulgare var. nervosum Species 0.000 claims 1
- 241000209140 Triticum Species 0.000 claims 1
- 238000007654 immersion Methods 0.000 claims 1
- 238000007789 sealing Methods 0.000 claims 1
- 235000019996 baijiu Nutrition 0.000 abstract description 27
- 239000000126 substance Substances 0.000 description 9
- 235000019640 taste Nutrition 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 240000007594 Oryza sativa Species 0.000 description 3
- 235000007164 Oryza sativa Nutrition 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 3
- 238000013124 brewing process Methods 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- 235000009566 rice Nutrition 0.000 description 3
- 230000001953 sensory effect Effects 0.000 description 3
- 230000007423 decrease Effects 0.000 description 2
- 230000032050 esterification Effects 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 235000005985 organic acids Nutrition 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 240000006394 Sorghum bicolor Species 0.000 description 1
- 235000011684 Sorghum saccharatum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000011514 vinification Methods 0.000 description 1
Landscapes
- Alcoholic Beverages (AREA)
Abstract
本发明涉及一种提升小曲白酒品质的方法,属于酿酒技术领域。本发明在小曲白酒传统工艺前提下,对曲粉添加量、糖化时间、甜醅糟比例、入罐发酵温度这些工艺进行调整。曲粉添加量为0.2%,培菌糖化22h,甜、醅糟比例为1∶1.5,入罐发酵温度为16℃且控制发酵过程中环境温度为20℃,使小曲白酒的发酵周期由传统的7天左右延长至20天,所酿造出的小曲白酒清亮透明、酒体柔和、醇香清雅、回甜爽口,与传统方法酿造的小曲白酒相比,品质有一定的提升。The invention relates to a method for improving the quality of Xiaoqu Baijiu, which belongs to the technical field of brewing. On the premise of the traditional technology of xiaoqu baijiu, the invention adjusts the processes of koji powder addition, saccharification time, proportion of sweet fermented grains and fermented grains, and tank fermentation temperature. The amount of koji powder added is 0.2%, the saccharification time is 22 hours, the ratio of sweet and fermented grains is 1:1.5, the fermentation temperature in the tank is 16°C, and the ambient temperature during the fermentation process is controlled at 20°C, so that the fermentation cycle of Xiaoqu Baijiu is changed from the traditional one. From about 7 days to 20 days, the brewed Xiaoqu baijiu is clear and transparent, soft in body, mellow and elegant, sweet and refreshing. Compared with Xiaoqu baijiu brewed by traditional methods, the quality has been improved to a certain extent.
Description
技术领域 technical field
本发明涉及一种提升小曲白酒品质的方法,属于酿酒技术领域。 The invention relates to a method for improving the quality of Xiaoqu Baijiu, which belongs to the technical field of brewing.
背景技术 Background technique
小曲白酒是我国主要的蒸馏酒之一,产量约占我国白酒总量的1/6,其发酵周期短,出酒率高,但与大曲白酒相比,所产的小曲白酒品质一般、口感单一,且带有程度不一的苦涩味,多为中、低档白酒。为了扩大市场,提高小曲白酒的档次,必须提升小曲白酒的品质。 Xiaoqu baijiu is one of the main distilled liquors in my country. Its output accounts for about 1/6 of the total amount of liquor in my country. Its fermentation cycle is short and its yield is high. However, compared with Daqu baijiu, the quality of Xiaoqu baijiu produced is average and the taste is single , and with varying degrees of bitterness, mostly medium and low-grade liquor. In order to expand the market and improve the grade of Xiaoqu liquor, the quality of Xiaoqu liquor must be improved.
小曲白酒传统酿造工艺为:粮食→浸泡→初蒸→闷水→复蒸→摊晾加曲→培菌糖化→出箱摊晾→配糟混合→入池发酵→蒸馏。目前,小曲白酒的发酵周期普遍为7天左右,此时微生物基本已进入衰退期,若继续发酵反而有利于杂菌生长,产生大量的有害物质,影响小曲白酒的品质。但发酵周期的长短是影响酒质的关键因素之一,整个发酵期根据其主产物质的不同可依次分为:产酒精期、产酸期和产酯期,所以适当地延长发酵周期可增长产酯期,有利于有机酸与醇起缓慢的酯化作用生成酯。因此,有必要探索出适宜延长小曲白酒发酵周期的酿造工艺,使得对酿酒有益的微生物在发酵过程中的生命期增长,有利于酯香类物质的生成,以提升小曲白酒的品质。 The traditional brewing process of Xiaoqu baijiu is: grain → soaking → initial steaming → stuffy water → re-steaming → airing and adding koji → culture and saccharification → out of the box and airing → mixing with grains → entering the tank for fermentation → distillation. At present, the fermentation cycle of Xiaoqu baijiu is generally about 7 days. At this time, the microorganisms have basically entered the decline period. If the fermentation continues, it will be conducive to the growth of miscellaneous bacteria and produce a large amount of harmful substances, which will affect the quality of Xiaoqu baijiu. However, the length of the fermentation cycle is one of the key factors affecting the quality of the wine. The entire fermentation period can be divided into: alcohol production period, acid production period and ester production period according to the different main products. During the period of ester production, it is beneficial for the slow esterification of organic acids and alcohols to form esters. Therefore, it is necessary to explore a brewing process suitable for prolonging the fermentation cycle of Xiaoqu Baijiu, so that the life cycle of microorganisms beneficial to winemaking can increase during the fermentation process, which is conducive to the formation of ester aroma substances, so as to improve the quality of Xiaoqu Baijiu.
发明内容 Contents of the invention
本发明所要解决的技术问题在于提供一种提升小曲白酒品质的方法。 The technical problem to be solved by the present invention is to provide a method for improving the quality of Xiaoqu Baijiu.
为了实现上述目的,本发明采用以下技术方案: In order to achieve the above object, the present invention adopts the following technical solutions:
1)将粮食经过浸泡、初蒸、闷水和复蒸,得到含水量51%~55%的熟粮; 1) The grain is soaked, initially steamed, steamed and re-steamed to obtain cooked grain with a water content of 51% to 55%;
2)将熟粮摊晾至30℃后,添加粮食重量0.2%的小曲粉,翻拌均匀; 2) After spreading the cooked grains to 30°C, add 0.2% of grain weight koji powder, and mix evenly;
3)将添加曲粉后的粮糟做箱糖化,糖化时间为22h; 3) Saccharify the grain grains after adding koji powder, and the saccharification time is 22 hours;
4)糖化结束后,将甜糟摊晾至25℃,加入1.5倍重量的醅糟混合均匀; 4) After the saccharification is completed, spread the sweet grains to 25°C, add 1.5 times the weight of fermented grains and mix evenly;
5)将混合均匀的甜、醅糟摊晾至16℃入发酵罐,密封发酵20天,控制发酵过程中环境温度为20℃。 5) Spread the evenly mixed sweet and fermented grains in the air to 16°C and put them into a fermenter, seal and ferment for 20 days, and control the ambient temperature during the fermentation process to 20°C.
所加入的曲粉为小曲粉,市售或自制均可。 The koji powder added is a small koji powder, which is commercially available or self-made.
所述的粮食为稻谷或小麦或高粱或大麦。 The grain is rice or wheat or sorghum or barley.
上述方法与传统工艺对比主要在以下方面进行调整: 加曲方式由多次下曲改为一次下曲,下曲温度由多段温度改为统一采用30℃,曲粉添加量由0.3%~0.5%降为0.2%;培菌糖化时间由24~26h降为22h;甜、醅糟的比例由1:3~1:4改为1:1.5;入池发酵温度为16℃,且发酵过程中控制环境温度为20℃,进行低温缓慢的发酵。 Compared with the traditional process, the above method is mainly adjusted in the following aspects: The method of adding koji was changed from multiple times to one time, the temperature of the next koji was changed from multi-stage temperature to 30°C, and the amount of koji powder added was reduced from 0.3% to 0.5% to 0.2%; The saccharification time of culture culture is reduced from 24 to 26 hours to 22 hours; The ratio of sweet and fermented grains is changed from 1:3 to 1:4 to 1:1.5; The fermentation temperature in the pool is 16°C, and the ambient temperature is controlled at 20°C during the fermentation process, and the fermentation is carried out at low temperature and slowly.
本发明通过减少曲粉添加量、开嫩箱、降低入罐发酵温度以及控制整个发酵过程中环境的温度,使得酒糟中微生物的对数生长期和稳定期得到延长,减缓衰退期的到来,这样有利于有机酸与醇起缓慢的酯化作用生成酯香类物质。 The present invention prolongs the logarithmic growth period and the stable period of microorganisms in the distiller's grains and slows down the coming of the recession period by reducing the amount of koji powder added, opening the tender box, lowering the fermentation temperature in the tank and controlling the temperature of the environment during the entire fermentation process. It is conducive to the slow esterification of organic acids and alcohols to generate ester aroma substances.
本发明方法具有如下有益效果: The inventive method has the following beneficial effects:
与传统小曲白酒酿造工艺相比,采用本发明所提供的方法,可将小曲白酒发酵周期由传统的7天左右延长至20天,明显提升了小曲白酒的酯香味,同时有效的控制了高级醇的生成,所酿造出的小曲白酒总酸含量为:1.48 g/L,总酯含量为:3.01 g/L,高级醇含量为:1.23g/L,酒体柔和,清亮透明,醇香清雅,回甜爽口。 Compared with the traditional brewing process of Xiaoqu Baijiu, the method provided by the present invention can extend the fermentation period of Xiaoqu Baijiu from about 7 days to 20 days, significantly improve the ester aroma of Xiaoqu Baijiu, and effectively control the higher alcohol content. The total acid content of the brewed Xiaoqu Baijiu is 1.48 g/L, the total ester content is 3.01 g/L, and the higher alcohol content is 1.23 g/L. Sweet and refreshing.
具体实施方式 Detailed ways
以下通过具体实施例,对本发明进行更为详细的说明: Below by specific embodiment, the present invention is described in more detail:
(1)称取2Kg稻谷,用72~75℃温水浸泡12h,泡粮水漫过粮面2~3cm,泡粮结束后,进行初蒸20min,闷水60min,再复蒸60min,得到的熟粮柔熟、裂口、收汗,含水量51%~55%; (1) Weigh 2Kg of rice, soak it in warm water at 72-75°C for 12 hours, soak the grain water over the surface of the grain for 2-3cm, after soaking the grain, steam for 20 minutes, steam for 60 minutes, and steam again for 60 minutes to obtain cooked rice The grain is soft and cooked, cracked, and sweated, with a water content of 51% to 55%;
(2)将步骤(1)所得到的熟粮摊晾至30℃左右,加入4g安琪酿酒曲(增香高产),翻拌均匀,摊晾至23℃; (2) Spread the cooked grain obtained in step (1) to about 30°C, add 4g of Angel Brewing Koji (increasing aroma and high yield), mix well, and let it dry to 23°C;
(3)对步骤(2)所得到的粮糟按照10cm的厚度进行做箱,培菌糖化22h; (3) Make a box for the grain grains obtained in step (2) according to the thickness of 10cm, and cultivate and saccharify for 22 hours;
(4)糖化结束后,将步骤(3)所得到的甜糟4.5Kg进行摊晾冷却至25℃,加入6.75Kg摊晾至25℃左右的醅糟,翻拌混合均匀; (4) After the saccharification is completed, spread 4.5Kg of sweet grains obtained in step (3) to cool down to 25°C, add 6.75Kg of fermented grains that are spread to about 25°C, and mix well;
(5)控制步骤(4)所得到的甜、醅混合糟温度在16℃,进入发酵罐,放置于20℃的恒温箱,密封发酵20天; (5) Control the temperature of the sweet and unstrained spirits mixed grains obtained in step (4) at 16°C, enter the fermenter, place in a thermostat at 20°C, and seal and ferment for 20 days;
(6)发酵结束后,对发酵糟进行蒸馏,分段摘酒,取中段酒与按照传统工艺发酵7天后蒸馏得到的中段酒进行感官品评和理化指标检测。 (6) After the fermentation is over, the fermented grains are distilled, the wine is harvested in sections, and the middle wine and the middle wine distilled after 7 days of fermentation according to the traditional process are used for sensory evaluation and physical and chemical index detection.
表1发酵周期为20天的小曲白酒感官品评 Table 1 Sensory evaluation of Xiaoqu Baijiu with a fermentation period of 20 days
表2发酵周期为7天的小曲白酒感官品评 Table 2 Sensory evaluation of Xiaoqu Baijiu with a fermentation period of 7 days
表3发酵周期为20天的小曲白酒的理化指标 Table 3 The physical and chemical indicators of Xiaoqu Baijiu with a fermentation period of 20 days
表4发酵周期为7天的小曲白酒的理化指标 Table 4 The physical and chemical indicators of Xiaoqu Baijiu with a fermentation period of 7 days
从表1、2可以看出,发酵周期为20天的小曲白酒品质明显优于发酵周期为7天的小曲白酒,尤其是口味。 It can be seen from Tables 1 and 2 that the quality of Xiaoqu liquor with a fermentation period of 20 days is obviously better than that of Xiaoqu liquor with a fermentation period of 7 days, especially the taste.
从表3、4可以看出,发酵周期为20天的小曲白酒较发酵周期为7天的小曲白酒的理化指标主要是总酯含量大大增加,总酸含量略升,由于整个发酵过程采用低温缓慢的发酵方式,虽然将发酵周期延长但高级醇的含量反而略降。 It can be seen from Tables 3 and 4 that the physical and chemical indicators of Xiaoqu Baijiu with a fermentation period of 20 days compared with Xiaoqu Baijiu with a fermentation period of 7 days are mainly that the total ester content is greatly increased, and the total acid content is slightly increased. Although the fermentation period is prolonged, the content of higher alcohols decreases slightly.
上述实施例仅为本发明的较佳实施方式之一,并非以此限制本发明的保护范围,故:凡依本发明的方法所做的等效变化,只要在本发明的要旨范围内,均应涵盖于本发明的保护范围之内。 The above-described embodiment is only one of the preferred embodiments of the present invention, and is not intended to limit the protection scope of the present invention, so: all equivalent changes made according to the method of the present invention, as long as they are within the gist of the present invention, are all Should be covered within the protection scope of the present invention.
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310197665.1A CN103243002B (en) | 2013-05-24 | 2013-05-24 | Method for improving quality of smaller lumped koji distilled spirit |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310197665.1A CN103243002B (en) | 2013-05-24 | 2013-05-24 | Method for improving quality of smaller lumped koji distilled spirit |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103243002A CN103243002A (en) | 2013-08-14 |
CN103243002B true CN103243002B (en) | 2014-10-22 |
Family
ID=48922882
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310197665.1A Expired - Fee Related CN103243002B (en) | 2013-05-24 | 2013-05-24 | Method for improving quality of smaller lumped koji distilled spirit |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103243002B (en) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103937642A (en) * | 2014-05-05 | 2014-07-23 | 劲牌有限公司 | Method for producing soft-yeast flavored liquor with high acid content and high ester content |
CN103952264B (en) * | 2014-05-26 | 2016-05-18 | 董长河 | A kind of Solid Fermentation of Uncooked Material, liquid distillate are prepared the method for white wine |
CN105524773A (en) * | 2014-09-30 | 2016-04-27 | 宁夏鼎夏酒业有限公司 | Process for producing Chinese koji baijiu |
CN104673610B (en) * | 2015-03-20 | 2017-07-18 | 云南谷冠生物科技有限公司 | A kind of truffle buckwheat health-care wine and preparation method thereof |
CN105002063A (en) * | 2015-09-10 | 2015-10-28 | 郑成宣 | Brewing method of ecological rice xiaoqu liquor |
CN105039114A (en) * | 2015-09-10 | 2015-11-11 | 郑成宣 | Brewing method of sticky rice ecological Xiaoqu liquor |
CN105062792A (en) * | 2015-09-10 | 2015-11-18 | 郑成宣 | Brewage method of wheat ecological Xiaoqu liquor |
CN105062796A (en) * | 2015-09-10 | 2015-11-18 | 郑成宣 | Brewing method of rice ecological Xiaoqu wine |
CN106085693A (en) * | 2016-06-14 | 2016-11-09 | 四川凸酒酒业有限公司 | The production method of Xiaoqu liquor by solid fermentation without bran |
CN106085780A (en) * | 2016-08-31 | 2016-11-09 | 泰山恒信有限公司 | A kind of distilled liquor brewage process and equipment |
CN107345184A (en) * | 2017-08-02 | 2017-11-14 | 合江县白沙镇燕坪酒厂 | The brewage process of Yi Zhong Ao arracks |
CN110499223A (en) * | 2019-06-28 | 2019-11-26 | 浙江致中和实业有限公司 | Distilled liquor brewage process |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101260352A (en) * | 2008-04-17 | 2008-09-10 | 广东省蕉岭县一线天酒业有限责任公司 | Method for brewing rice-fragrant type Xiaoqu rice wine |
CN102978064A (en) * | 2012-12-04 | 2013-03-20 | 宣汉巴人地窖酒厂 | Multi-grain fen-flavor liquor and preparation method thereof |
-
2013
- 2013-05-24 CN CN201310197665.1A patent/CN103243002B/en not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101260352A (en) * | 2008-04-17 | 2008-09-10 | 广东省蕉岭县一线天酒业有限责任公司 | Method for brewing rice-fragrant type Xiaoqu rice wine |
CN102978064A (en) * | 2012-12-04 | 2013-03-20 | 宣汉巴人地窖酒厂 | Multi-grain fen-flavor liquor and preparation method thereof |
Non-Patent Citations (10)
Title |
---|
小曲清香型燕麦酒的研制;王超凯等;《食品与发酵科技》;20121031;第48卷(第5期);第86-88页 * |
小曲白酒的生产工艺及质量控制;易良建;《中国科技信息》;20120430(第7期);第122、130页 * |
干红毛樱桃酒酿造工艺研究;高海生等;《中国食品学报》;20020331;第2卷(第1期);第17-21页 * |
张宇赤.控制低温缓慢发酵 提高白酒质量.《酿酒》.2003,第30卷(第2期),第1页第2-7段. |
张美莉.用糯高粱与小麦酿制小曲白酒.《农产品加工》.2010,(第4期),第16-17页第2、3节. |
控制低温缓慢发酵 提高白酒质量;张宇赤;《酿酒》;20030331;第30卷(第2期);第1页第2-7段 * |
易良建.小曲白酒的生产工艺及质量控制.《中国科技信息》.2012,(第7期),第122、130页. |
王超凯等.小曲清香型燕麦酒的研制.《食品与发酵科技》.2012,第48卷(第5期),第86-88页. |
用糯高粱与小麦酿制小曲白酒;张美莉;《农产品加工》;20100430(第4期);第16-17页第2、3节 * |
高海生等.干红毛樱桃酒酿造工艺研究.《中国食品学报》.2002,第2卷(第1期),第17-21页. |
Also Published As
Publication number | Publication date |
---|---|
CN103243002A (en) | 2013-08-14 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103243002B (en) | Method for improving quality of smaller lumped koji distilled spirit | |
CN104450399B (en) | A kind of liquid fermentation produces the method for rice spirit | |
CN103666927B (en) | Process for preparing fresh scent strong-flavor Chinese spirit | |
CN107488602B (en) | Abnormal Wickerhamia yeast GJYD15 and application thereof in preparation of low-temperature Daqu | |
CN107227237B (en) | Pure brewing method of white spirit | |
CN105505721A (en) | Production process of fragrant faint scent type liquor | |
CN108277132A (en) | A method of shortening aromatic Chinese spirit fermentation period by storing outer esterification | |
CN105349400A (en) | Cave type pit, pit mud and method of brewing highly flavored type basic liquor by cave type pit and pit mud | |
CN104987970A (en) | Highly-esterified Daqu preparation method | |
CN107058143A (en) | A kind of heat-resisting, acidproof, saccharomyces cerevisiae of resistance to ethanol and brewing fermentation agent | |
CN101280268A (en) | Purebred rose vinegar and preparation method thereof | |
CN111560304B (en) | A kind of wine containing superoxide dismutase SOD activity | |
CN101735921B (en) | High temperature inverted rice wine and preparation method thereof | |
CN115058345B (en) | A kind of Aspergillus flavus strain HJ-3 and brewing method for improving liquor quality | |
CN110499224A (en) | A kind of process preparing strengthening porcelain using monascus | |
CN104987972A (en) | Preparation method of liquid fermentum rubrum for brewing | |
CN102352287B (en) | Method for increasing ester-aroma substances in Fen-flavor liquor by utilizing liquor tailing | |
CN105176729B (en) | A kind of method for producing delicate fragrance type high-ester flavouring wine | |
CN104762163B (en) | A kind of method preparing biological song | |
CN107083336B (en) | A kind of production method of compound nucleoside functional song | |
CN103205344B (en) | Method for preparing red yeast white spirit by vinasse, two yeasts and three segments of large jars | |
CN103805394B (en) | A kind of liquor brewing method | |
CN107586647B (en) | Liquor produced by discarding lees of Xiaoqu Qingxiang liquor and its production method | |
CN103525682B (en) | Vinegar brewing method preventing mycoderm and vinegar flies from being generated | |
CN103966050B (en) | Production method for micro-molecule wine |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141022 Termination date: 20170524 |