CN103242974B - Fruit, vegetable and tableware detergent with good rheological property - Google Patents
Fruit, vegetable and tableware detergent with good rheological property Download PDFInfo
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Abstract
The invention discloses a fruit, vegetable and tableware detergent with a good rheological property. The detergent comprises the following raw material components in percentage by weight: 0.01-5.0% of a fluidity modifier, 5.0-40.0% of an anionic surfactant, 0.5-15.0% of a nonionic surfactant, 1.0-8.0% of an amphoteric surfactant, 0.1-8.0% of a viscosity modifier, 0.01-0.2% of an antiseptic agent, 0.01-0.5% of a chelating agent, 0.01-10% of other components, and the balance of deionized water. The invention relates to the detergent with viscosity characteristics, and the fluidity modifier is added into the detergent, so that the rheological property is improved, and the needs of consumers can be well satisfied.
Description
Technical field
The present invention relates to civilian sanitising agent technical field, specifically, the present invention relates to the fruits and vegetables dish washing detergent that a kind of rheological is good.
Background technology
Liquid detergent at high temperature sense organ is rarer, and under low temperature, liquid detergent rheological is poor, is difficult to topple over, and uses bring very big inconvenience to human consumer.There is bibliographical information, concerning liquid detergent system, in certain temperature range, the Arrhenius Equation can be adopted to investigate the situation of washing composition viscosity with temperature change, and the susceptibility of appraisement system viscosity temperature is carried out by the size of activation energy, the viscosity degree of washing composition is main relevant with the raw material of system to the susceptibility of temperature.
Be used for a small amount of inorganic salt of adjusting viscosity to the sensitivity effects of washing composition viscosity temperature little (Chen Zhifeng, Jin Yan, the viscosity temperature Study of Sensitivity of liquid washing agent, daily chemical industry, 2001, (3): 9-10) in system.Have studied the susceptibility of system viscosity to temperature described in this document, do not provide concrete terms of settlement.
Separately there is bibliographical information, by adding a small amount of high molecular polymer fast clean plain 68 in liquid detergent, the viscosity characteristics of liquid detergent can be changed, the peak viscosity of liquid detergent is adjusted to middle warm area, and viscosity when improve high-temperature zone, the viscosity stability of liquid detergent is improved relatively, ensure that relatively stable (Duan Yuchen, the Research on viscosity stability of dish washing detergent, the application chemical industry of product viscosity within the scope of cold zone and high-temperature zone, 2005, (5): 321-323).Fast clean plain 68 is vinylformic acid viscosity modifiers of a kind of modification, and can freeze under cryogenic, itself directly dissolves difficulty, by fast clean plain 68 and other surfactant compounds, slowly must add water after stirring, then adds buck and neutralize.
All there is the defect in use in above-mentioned all compositions being used for adjustment washing composition viscosity.Thus, how finding a kind of effective viscosity modifier is the technical barrier that one of ordinary skill in the art are badly in need of solving.
Summary of the invention
The object of the present invention is to provide that a kind of rheological is good, the fruits and vegetables dish washing detergent of excellent combination property.
The object of the invention to solve the technical problems realizes by the following technical solutions.The fruits and vegetables dish washing detergent that a kind of rheological proposed according to the present invention is good, it contains each feed composition of following weight percent: fluidity regulator 0.01-5.0%; Anion surfactant 5.0 ~ 40.0%; Nonionogenic tenside 0.5 ~ 15.0%; Amphoterics 1.0 ~ 8.0%; Viscosity modifier 0.1 ~ 8.0%; Sanitas 0.01 ~ 0.2%; Sequestrant 0.01 ~ 0.5%; Other component 0.01 ~ 10%; Deionized water surplus.
Fruits and vegetables dish washing detergent of the present invention, described anion surfactant is the mixture of more than at least one or two in polyoxyethylenated alcohol sodium sulfate, fatty alcohol-polyoxyethylene ether carboxylic acid sodium, alkyl sodium sulfonate, α-sodium olefin sulfonate.
Fruits and vegetables dish washing detergent of the present invention, described nonionogenic tenside is the mixture of more than at least one or two in fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-7, polyoxyethylene glycol, alkyl-glucoside, monoolein, sucrose ester, fatty acid methyl ester ethoxylate, polyglycerol fatty acid ester, amine oxide.
Fruits and vegetables dish washing detergent of the present invention, described amphoterics is any one or more mixture in lauryl L-Ala diethanolamine salt, lauryl Sodium L-alaninate, trimethyl-glycine.
Fruits and vegetables dish washing detergent of the present invention, described viscosity modifier is the mixture of more than at least one or two in sodium-chlor, sodium sulfate, ethanol, propylene glycol, cumene sodium sulfonate.
Fruits and vegetables dish washing detergent of the present invention, described sanitas is at least one in Sodium Benzoate, isothiazolinone, nipagin esters, potassium sorbate.
Fruits and vegetables dish washing detergent of the present invention, described sequestrant is at least one in EDTA-2Na, EDTA-4Na, citric acid.
Fruits and vegetables dish washing detergent of the present invention, described fluidity regulator is the mixture of more than at least one or two in PPG-20 methyl ether, PPG-10 methyl ether, glycerine, sodium xylene sulfonate.
Fruits and vegetables dish washing detergent of the present invention, other components described are acid-base modifier, pigment, photostabilizer, antioxidant, essence, and these components are the universaling component of washing composition, and kind does not do specific restriction.
By technique scheme, tool of the present invention has the following advantages and beneficial effect:
1, the washing composition containing fluidity regulator has good high/low temperature mobility, make product can not become g., jelly-like when low temperature, can pour out very easily, and also can suitably keep certain viscosity when high temperature, make product sensory unlikely excessively rare, make human consumer use convenient to product.
2, fluidity regulator of the present invention is all low stimulation readily biodegradable, and product gentleness does not hinder hand, and the form of fluidity regulator is liquid or solid, and epidemic situation comparison is stablized, can well and tensio-active agent dissolve each other, without the need to pre-treatment, be convenient to industrial production.
The effects such as 3, the present invention has decontamination, anti-hard water, wetting, emulsification, solubilising, and dispersion is bubbled, anticorrosion.
Embodiment
Know-why of the present invention is: the PPG-20 methyl ether of employing, PPG-10 methyl ether, and one or more mixtures in glycerine and sodium xylene sulfonate as fluidity regulator, and can be applied to industrial production very easily.There is source natural health, the advantages such as readily biodegradable.
Below in conjunction with embodiment, the present invention is described in further detail, but embodiments of the present invention are not limited thereto.Below by concrete preferred embodiment more detailed description washing composition of the present invention.
embodiment 1
The preparation method of the present embodiment is as follows:
1. add the deionized water measured, add sequestrant, stir until dissolve completely.
2. add Sodium dodecylbenzene sulfonate successively, polyoxyethylenated alcohol sodium sulfate, alkylamide propyl-betaine, alkyl glycoside, PPG-20 methyl ether (contrast sample need not add).Before adding, ensure that last raw material dissolves completely.
3. add sanitas, viscosity modifier, continue to be stirred to material and to dissolve completely, evenly.
Carry out Temperature-Viscosity mensuration to the washing composition of embodiment 1, detersive power measures, Stability Determination, and pH value measures, and test result is in table 1.
The performance measurement of the washing composition of table 1 embodiment 1 and contrast sample 1
As can be seen from Table 1, embodiment 1 has good detersive power and low-temperature stability, and pH value is close to human body skin.Embodiment 1 has added PPG-20 methyl ether, and the susceptibility of viscosity temperature obviously reduces many than the contrast sample do not added, and detersive power also promotes a little.Therefore, PPG-20 methyl ether add the high/low temperature rheological well improving embodiment 1.
embodiment 2
The preparation method of the present embodiment is as follows:
1. add the deionized water measured, add sequestrant, stir until dissolve completely.
2. add Sodium dodecylbenzene sulfonate successively, polyoxyethylenated alcohol sodium sulfate, alkylamide propyl ammonium oxide, alkyl glycoside, PPG-20 methyl ether (contrast sample need not add), PPG-10 methyl ether (contrast sample need not add).Before adding, ensure that last raw material dissolves completely.
3. add sanitas, viscosity modifier, continue to be stirred to material and to dissolve completely, evenly.
Carry out Temperature-Viscosity mensuration to the washing composition of embodiment 2, detersive power measures, Stability Determination, and pH value measures, and test result is in table 2.
The performance measurement of the washing composition of table 2 embodiment 2 and contrast sample 2
As can be seen from Table 2, embodiment 2 has good detersive power and low-temperature stability, and pH value is close to human body skin.Embodiment 2 has added the mixture of PPG-20 methyl ether and PPG-10 methyl ether, and the susceptibility of viscosity temperature obviously reduces many than the contrast sample do not added, and detersive power also promotes a little.Therefore, PPG-20 methyl ether, PPG-10 methyl ether add the high/low temperature rheological well improving embodiment 2.
embodiment 3
The preparation method of the present embodiment is as follows:
1. add the deionized water measured, add sequestrant, stir until dissolve completely.
2. add Sodium dodecylbenzene sulfonate successively, lauryl Sodium L-alaninate, alkylamide propyl ammonium oxide, PPG-10 methyl ether (contrast sample need not add), sodium xylene sulfonate (contrast sample need not add).Ensure before adding that last raw material dissolves completely.
3. add sanitas, viscosity modifier, continue to be stirred to material and to dissolve completely, evenly.
Carry out Temperature-Viscosity mensuration to the washing composition of embodiment 3, detersive power measures, Stability Determination, and pH value measures, and test result is in table 3.
The performance measurement of the washing composition of table 3 embodiment 3 and contrast sample 3
As can be seen from Table 3, embodiment 3 has good detersive power and low-temperature stability, and pH value is close to human body skin.Embodiment 3 has added PPG-10 methyl ether and sodium xylene sulfonate, and the susceptibility of viscosity temperature obviously reduces many than the contrast sample do not added, and detersive power also promotes a little.Therefore, PPG-10 methyl ether and sodium xylene sulfonate add the high/low temperature rheological well improving embodiment 3.
embodiment 4
The preparation method of the present embodiment is as follows:
1. add the deionized water measured, add sequestrant, stir until dissolve completely.
2. add Sodium dodecylbenzene sulfonate successively, lauryl L-Ala diethanolamine salt, α-sodium olefin sulfonate, fatty acid methyl ester ethoxylate, PPG-20 methyl ether (contrast sample need not add), sodium xylene sulfonate (contrast sample need not add).Ensure before adding that last raw material dissolves completely.
3. add sanitas, viscosity modifier, continue to be stirred to material and to dissolve completely, evenly.
Carry out Temperature-Viscosity mensuration to the washing composition of embodiment 4, detersive power measures, Stability Determination, and pH value measures, and test result is in table 4.
The performance measurement of the washing composition of table 4 embodiment 4 and contrast sample 4
Embodiment 4 has good detersive power and low-temperature stability as can be seen from Table 4, and pH value is close to human body skin.Embodiment 4 has added PPG-20 methyl ether and sodium xylene sulfonate, and the susceptibility of viscosity temperature obviously reduces many than the contrast sample do not added.Therefore, PPG-20 methyl ether and sodium xylene sulfonate add the high/low temperature rheological well improving embodiment 4.
embodiment 5
The preparation method of the present embodiment is as follows:
1. add the deionized water measured, add sequestrant, stir until dissolve completely.
2. add Sodium dodecylbenzene sulfonate successively, polyoxyethylenated alcohol sodium sulfate, alkylamide propyl ammonium oxide, α-sodium olefin sulfonate, lauryl Sodium L-alaninate, sodium xylene sulfonate (contrast sample need not add).Before adding, ensure that last raw material dissolves completely.
3. add sanitas, viscosity modifier, continue to be stirred to material and to dissolve completely, evenly.
Carry out Temperature-Viscosity mensuration to the washing composition of embodiment 5, detersive power measures, Stability Determination, and pH value measures, and test result is in table 5.
The performance measurement of the washing composition of table 5 embodiment 5 and contrast sample 5
Embodiment 5 has good detersive power and low-temperature stability as can be seen from Table 5, and pH value is close to human body skin.Embodiment 5 has added sodium xylene sulfonate, and the susceptibility of viscosity temperature obviously reduces many than the contrast sample do not added.Therefore, sodium xylene sulfonate add the high/low temperature rheological well improving embodiment 5.
embodiment 6
The preparation method of the present embodiment is as follows:
1. add the deionized water measured, add sequestrant, stir until dissolve completely.
2. add Sodium dodecylbenzene sulfonate successively, fatty alcohol-polyoxyethylene ether carboxylic acid sodium, alkylamide propyl-betaine, alkyl glycoside, sodium xylene sulfonate (contrast sample need not add), PPG-20 methyl ether (contrast sample need not add), PPG-10 methyl ether (contrast sample need not add).Ensure before adding that last raw material dissolves completely.
3. add sanitas, viscosity modifier, continue to be stirred to material and to dissolve completely, evenly.Carry out Temperature-Viscosity mensuration to the washing composition of embodiment 6, detersive power measures, Stability Determination, and pH value measures, and test result is in table 6.
The performance measurement of the washing composition of table 6 embodiment 6 and contrast sample 6
Embodiment 6 has good detersive power and low-temperature stability as can be seen from Table 6, and pH value is close to human body skin.Embodiment 6 has added sodium xylene sulfonate, PPG-10 methyl ether, PPG-20 methyl ether, and the susceptibility of viscosity temperature obviously reduces many than the contrast sample do not added.Therefore, sodium xylene sulfonate, PPG-10 methyl ether, PPG-20 methyl ether add the high/low temperature rheological well improving embodiment 6.
embodiment 7
The preparation method of the present embodiment is as follows:
1. add the deionized water measured, add sequestrant, stir until dissolve completely.
2. add polyoxyethylenated alcohol sodium sulfate successively, fatty alcohol-polyoxyethylene ether-9, lauryl Sodium L-alaninate, α-sodium olefin sulfonate, glycerine (contrast sample need not add), PPG-20 methyl ether (contrast sample need not add), PPG-10 methyl ether (contrast sample need not add).Ensure before adding that last raw material dissolves completely.
3. add sanitas, viscosity modifier, continue to be stirred to material and to dissolve completely, evenly.Carry out Temperature-Viscosity mensuration to the washing composition of embodiment 7, detersive power measures, Stability Determination, and pH value measures, and test result is in table 7.
The performance measurement of the washing composition of table 7 embodiment 7 and contrast sample 7
Embodiment 7 has good detersive power and low-temperature stability as can be seen from Table 7, and pH value is close to human body skin.Embodiment 7 has added glycerine, PPG-10 methyl ether, PPG-20 methyl ether, and the susceptibility of viscosity temperature obviously reduces many than the contrast sample do not added.Therefore, glycerine, PPG-10 methyl ether, PPG-20 methyl ether add the high/low temperature rheological well improving embodiment 7.
embodiment 8
The preparation method of the present embodiment is as follows:
1. add the deionized water measured, add sequestrant, stir until dissolve completely.
2. add polyoxyethylenated alcohol sodium sulfate successively, Sodium dodecylbenzene sulfonate, alkyl glycoside, alkylamide propyl-betaine, glycerine (contrast sample need not add).Ensure before adding that last raw material dissolves completely.
3. add sanitas, viscosity modifier, continue to be stirred to material and to dissolve completely, evenly.Carry out Temperature-Viscosity mensuration to the washing composition of embodiment 8, detersive power measures, Stability Determination, and pH value measures, and test result is in table 8.
The performance measurement of the washing composition of table 8 embodiment 8 and contrast sample 8
Embodiment 8 has good detersive power and low-temperature stability as can be seen from Table 8, and pH value is close to human body skin.Embodiment 8 has added glycerine, and the susceptibility of viscosity temperature obviously reduces many than the contrast sample do not added.Therefore, glycerine add the high/low temperature rheological well improving embodiment 8.
The above, it is only preferred embodiment of the present invention, not any pro forma restriction is done to the present invention, therefore everyly do not depart from technical solution of the present invention content, the any simple modification done above embodiment according to technical spirit of the present invention, equivalent variations and modification, all still belong in the scope of technical solution of the present invention.
Claims (4)
1. the fruits and vegetables dish washing detergent that rheological is good, is characterized in that: it contains each feed composition of following weight percent:
Fluidity regulator 0.01-5.0%; Described fluidity regulator is the mixture of any one or more in PPG-20 methyl ether, PPG-10 methyl ether, glycerine, sodium xylene sulfonate;
Anion surfactant 5.0 ~ 40.0%; Described anion surfactant is the mixture of any one or more in polyoxyethylenated alcohol sodium sulfate, fatty alcohol-polyoxyethylene ether carboxylic acid sodium, alkyl sodium sulfonate, α-sodium olefin sulfonate;
Nonionogenic tenside 0.5 ~ 15.0%; Described nonionogenic tenside is the mixture of any one or more in fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-7, polyoxyethylene glycol, alkyl-glucoside, monoolein, sucrose ester, fatty acid methyl ester ethoxylate, polyglycerol fatty acid ester, amine oxide;
Amphoterics 1.0 ~ 8.0%; Described amphoterics is any one or more mixture in lauryl L-Ala diethanolamine salt, lauryl Sodium L-alaninate, trimethyl-glycine;
Viscosity modifier 0.1 ~ 8.0%; Described viscosity modifier is the mixture of any one or more in sodium-chlor, sodium sulfate, ethanol, propylene glycol, cumene sodium sulfonate;
2. the fruits and vegetables dish washing detergent that rheological according to claim 1 is good, is characterized in that: described sanitas is at least one in Sodium Benzoate, isothiazolinone, nipagin esters, potassium sorbate.
3. the fruits and vegetables dish washing detergent that rheological according to claim 1 is good, is characterized in that: described sequestrant is at least one in EDTA-2Na, EDTA-4Na, citric acid.
4. the fruits and vegetables dish washing detergent that rheological according to claim 1 is good, it is characterized in that: other components described are acid-base modifier, pigment, photostabilizer, antioxidant, essence, these components are the universaling component of washing composition, and kind does not do specific restriction.
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