CN103184102A - A kind of extraction method of agarwood essential oil and application of agarwood essential oil - Google Patents
A kind of extraction method of agarwood essential oil and application of agarwood essential oil Download PDFInfo
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- CN103184102A CN103184102A CN2013100135733A CN201310013573A CN103184102A CN 103184102 A CN103184102 A CN 103184102A CN 2013100135733 A CN2013100135733 A CN 2013100135733A CN 201310013573 A CN201310013573 A CN 201310013573A CN 103184102 A CN103184102 A CN 103184102A
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- essential oil
- agalloch eaglewood
- extraction
- agarwood
- oil
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- 241000271309 Aquilaria crassna Species 0.000 title claims abstract description 80
- 239000000341 volatile oil Substances 0.000 title claims abstract description 79
- 238000000605 extraction Methods 0.000 title claims abstract description 57
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000000034 method Methods 0.000 claims abstract description 12
- 239000012530 fluid Substances 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims abstract description 9
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims abstract description 5
- 235000009414 Elaeocarpus kirtonii Nutrition 0.000 claims abstract description 4
- 235000013584 Tabebuia pallida Nutrition 0.000 claims abstract description 4
- 239000000284 extract Substances 0.000 claims description 14
- 244000144725 Amygdalus communis Species 0.000 claims description 10
- 235000011437 Amygdalus communis Nutrition 0.000 claims description 10
- 241000218691 Cupressaceae Species 0.000 claims description 10
- 239000008168 almond oil Substances 0.000 claims description 10
- 239000003921 oil Substances 0.000 claims description 10
- 235000019198 oils Nutrition 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- 230000000694 effects Effects 0.000 claims description 8
- 239000002270 dispersing agent Substances 0.000 claims description 4
- 239000003205 fragrance Substances 0.000 claims description 4
- 210000003205 muscle Anatomy 0.000 claims description 4
- 239000002304 perfume Substances 0.000 claims description 4
- 239000002893 slag Substances 0.000 claims description 4
- 244000236151 Tabebuia pallida Species 0.000 claims description 3
- 239000006071 cream Substances 0.000 claims description 3
- 239000006185 dispersion Substances 0.000 claims description 3
- 241000199223 Elaeocarpus kirtonii Species 0.000 abstract 1
- 238000003795 desorption Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 5
- OEYQBKYISMRWQB-UHFFFAOYSA-N Santal Chemical compound C=1C(OC)=CC(O)=C(C2=O)C=1OC=C2C1=CC=C(O)C(O)=C1 OEYQBKYISMRWQB-UHFFFAOYSA-N 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 206010002383 Angina Pectoris Diseases 0.000 description 1
- 206010007882 Cellulitis Diseases 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000001174 ascending effect Effects 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 230000004087 circulation Effects 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 208000029078 coronary artery disease Diseases 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 208000031225 myocardial ischemia Diseases 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 230000002485 urinary effect Effects 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
Abstract
本发明涉及一种沉香精油的提取方法，先砍伐白木香树，去掉白木，雕成沉香薄片；再将沉香薄片粉碎成40目筛的沉香粉；然后把沉香粉用正丁烷加到萃取釜，采用亚临界流体萃取技术直接提取沉香精油，其提取条件：提取时间为0.5～1.5小时，解析温度60℃，提取温度50℃，提取压力为0.4～0.5MPa；随后把第一次提取沉香精油后的渣用95％乙醇加到萃取釜进行第二次萃取，其提取条件为：按第一次提取沉香精油的同一提取条件提取沉香精油。本发明目的是提供一种沉香精油的提取方法及沉香精油的应用。The present invention relates to a method for extracting agarwood essential oil, firstly, felling white agarwood trees, removing white wood, and carving into agarwood slices; then crushing the agarwood slices into agarwood powder with a 40-mesh sieve; then adding the agarwood powder to an extraction kettle with n-butane, and directly extracting the agarwood essential oil by subcritical fluid extraction technology, and the extraction conditions are: extraction time is 0.5-1.5 hours, desorption temperature is 60°C, extraction temperature is 50°C, and extraction pressure is 0.4-0.5MPa; then, the residue after the first extraction of agarwood essential oil is added to the extraction kettle with 95% ethanol for a second extraction, and the extraction conditions are: extracting the agarwood essential oil according to the same extraction conditions of the first extraction of agarwood essential oil. The purpose of the present invention is to provide a method for extracting agarwood essential oil and the application of agarwood essential oil.
Description
Technical field
The present invention relates to a kind of extracting process, be specifically related to the application of a kind of agalloch eaglewood extracts essential oil method and agalloch eaglewood essential oil.
Background technology
Agalloch eaglewood tool promoting the circulation of QI to relieve pain, warming middle-JIAO to arrest vomiting, helping inspiration to relieve asthma, tranquilizing by nourishing the heart, the effect of the sending down abnormally ascending of promoting blood circulation, in treatment and prevention coronary heart disease, stenocardia, myocardial ischemia, diseases such as irregular pulse have significant curative effect.And traditional technology only adopts single extraction to extract the agalloch eaglewood essential oil, and obtainable linaloe oil is limited.Linaloe oil is very golden expensive, and how obtaining more linaloe oil becomes the purpose that everybody falls over each other to strive in the industry.
Summary of the invention
The object of the invention provides a kind of agalloch eaglewood extracts essential oil method.Twice extraction of this process using, relatively other technologies can obtain more linaloe oil, for the raw material sources of agalloch eaglewood series product find a new approach.
Another object of the present invention provides the application of agalloch eaglewood essential oil.
The present invention has adopted following technical proposals:
A kind of agalloch eaglewood extracts essential oil method, felling Lignum Aquilariae Resinatum tree is removed the whitewood earlier, carves the agalloch eaglewood thin slice; Again the agalloch eaglewood thin slice is ground into the agalloch eaglewood powder of 40 mesh sieves; Then the agalloch eaglewood powder is added to extraction kettle with normal butane, adopt the subcritical fluid extraction technology directly to extract the agalloch eaglewood essential oil, its extraction conditions: extraction time is 0.5～1 hour, and 60 ℃ of resolution temperatures extract 50 ℃ of temperature, and extraction pressure is 0.4～0.5MPa; Be added to extraction kettle with 95% ethanol and carry out extracting second time extraction agalloch eaglewood essential oil extracting for the first time slag behind the agalloch eaglewood essential oil subsequently, its extraction conditions: extraction time is 0.5～1.5 hour, 60 ℃ of resolution temperatures extract 50 ℃ of temperature, and extraction pressure is 0.4～0.5MPa.
Embodiment extracts one of application of agalloch eaglewood essential oil, with the agalloch eaglewood essential oil of extraction using alcohol, adds Laoshan wingceltis essential oil 1 ‰, adds ethanol 98%, and an amount of fixing agent is deployed into the Ligaloes perfumes that gives off a strong fragrance.Wherein fixing agent is face cream.
Embodiment, two of the application of extraction agalloch eaglewood essential oil, evenly make the muscle pressure of to releive by agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersant that the subcritical fluid extraction technology is extracted, skin had skin moisten effect agalloch eaglewood massage oil, wherein agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersion agent volume percent are: agalloch eaglewood essential oil 4%～8%, flores aurantii essential oil 1%～3%, cypress essential oil 1%～3%, sweet almond oil 86%～94%.
The present invention has following advantage and effect:
1, the present invention is added to extraction kettle to the agalloch eaglewood powder with normal butane, adopt the subcritical fluid extraction technology directly to extract the agalloch eaglewood essential oil, be added to extraction kettle with 95% ethanol and carry out extracting the second time extracting for the first time slag behind the agalloch eaglewood essential oil subsequently, twice extraction conditions is identical, production technique is simple, the relative other technologies of technology of the present invention can obtain more linaloe oil, for the raw material sources of agalloch eaglewood series product find a new approach.
2, use the agalloch eaglewood essential oil of extraction using alcohol, add Laoshan wingceltis essential oil 1 ‰, add ethanol 98%, an amount of fixing agent, be deployed into the Ligaloes perfumes that gives off a strong fragrance, the agalloch eaglewood essential oil has multi-efficiency to human body, as: improve the gas field, the pressure of releiving, anti-strongly fragrant, the conditioning body and mind and promote health new city metabolism etc. of sleeping peacefully.The santal essential oil is to the multiple curative effect of skin tool, is fit to aging, drying and lack of water skin.Urging property is strengthened and is breathed and urinary system, the treatment cellulitis.
3, agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and the dispersant of being extracted by the subcritical fluid extraction technology evenly made the agalloch eaglewood massage oil, and this agalloch eaglewood massage oil muscle pressure of can releiving has the skin moisten effect to skin.
Embodiment
The present invention is described in further detail below in conjunction with embodiment, but embodiments of the present invention are not limited thereto.
Embodiment, a kind of agalloch eaglewood extracts essential oil method, felling Lignum Aquilariae Resinatum tree is removed the whitewood earlier, carves the agalloch eaglewood thin slice; Again the agalloch eaglewood thin slice is ground into the agalloch eaglewood powder of 40 mesh sieves; Then the agalloch eaglewood powder is added to extraction kettle with normal butane, adopt the subcritical fluid extraction technology directly to extract the agalloch eaglewood essential oil, its extraction conditions: extraction time is 1 hour, and 60 ℃ of resolution temperatures extract 50 ℃ of temperature, and extraction pressure is 0.4～0.5MPa; Be added to extraction kettle with 95% ethanol and carry out extraction second time extracting for the first time slag behind the agalloch eaglewood essential oil subsequently, its extraction conditions is: by the same extraction conditions extraction agalloch eaglewood essential oil that extracts the agalloch eaglewood essential oil first time.
Extract one of application of agalloch eaglewood essential oil, with the agalloch eaglewood essential oil of extraction using alcohol, add Laoshan wingceltis essential oil 1 ‰, add ethanol 98%, an amount of face cream is deployed into the Ligaloes perfumes that gives off a strong fragrance as fixing agent.
Two of the application of extraction agalloch eaglewood essential oil, evenly make the muscle pressure of to releive by agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersant that the subcritical fluid extraction technology is extracted, skin had skin moisten effect agalloch eaglewood massage oil, wherein agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersion agent volume percent are: agalloch eaglewood essential oil 4%～8%, flores aurantii essential oil 1%～3%, cypress essential oil 1%～3%, sweet almond oil 86%～94%.
Claims (5)
1. an agalloch eaglewood extracts essential oil method is characterized in that, felling Lignum Aquilariae Resinatum tree is removed the whitewood earlier, carves the agalloch eaglewood thin slice; Again the agalloch eaglewood thin slice is ground into the agalloch eaglewood powder of 40 mesh sieves; Then the agalloch eaglewood powder is added to extraction kettle with normal butane, adopts the subcritical fluid extraction technology directly to extract the agalloch eaglewood essential oil; Be added to extraction kettle with 95% ethanol and carry out extracting second time extraction agalloch eaglewood essential oil extracting for the first time slag behind the agalloch eaglewood essential oil subsequently.
2. according to the described agalloch eaglewood extracts essential oil of claim 1 method, it is characterized in that: for the first time extraction conditions and for the second time extraction conditions be: extraction time is 0.5～1.5 hour, and 60 ℃ of resolution temperatures extract 50 ℃ of temperature, and extraction pressure is 0.4～0.5MPa.
3. the application of the described agalloch eaglewood essential oil of claim 1 is characterized in that, with the agalloch eaglewood essential oil of extraction using alcohol, adds Laoshan wingceltis essential oil 1 ‰, adds ethanol 98%, and an amount of fixing agent is deployed into the Ligaloes perfumes that gives off a strong fragrance.
4. the application of the described agalloch eaglewood essential oil of claim 2 is characterized in that, fixing agent is face cream.
5. the application of the described agalloch eaglewood essential oil of claim 1, it is characterized in that, evenly make the muscle pressure of to releive by agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersant that the subcritical fluid extraction technology is extracted, skin had skin moisten effect agalloch eaglewood massage oil, wherein agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersion agent volume percent are: agalloch eaglewood essential oil 4%～8%, flores aurantii essential oil 1%～3%, cypress essential oil 1%～3%, sweet almond oil 86%～94%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013100135733A CN103184102A (en) | 2013-01-14 | 2013-01-14 | A kind of extraction method of agarwood essential oil and application of agarwood essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013100135733A CN103184102A (en) | 2013-01-14 | 2013-01-14 | A kind of extraction method of agarwood essential oil and application of agarwood essential oil |
Publications (1)
| Publication Number | Publication Date |
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| CN103184102A true CN103184102A (en) | 2013-07-03 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN2013100135733A Pending CN103184102A (en) | 2013-01-14 | 2013-01-14 | A kind of extraction method of agarwood essential oil and application of agarwood essential oil |
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| Country | Link |
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| CN (1) | CN103184102A (en) |
Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103351954A (en) * | 2013-07-11 | 2013-10-16 | 大连卓尔高科技有限公司 | Process for extracting eaglewood essential oil by using supercritical carbon dioxide |
| CN103520435A (en) * | 2013-10-11 | 2014-01-22 | 中山市国林沉香科学研究所 | Agilawood health-care essential oil |
| CN103740467A (en) * | 2014-01-27 | 2014-04-23 | 陆燕 | Method for extracting plant essential oil |
| CN103789094A (en) * | 2014-01-21 | 2014-05-14 | 广州大学 | Method for extracting agilawood essential oil from agilawood chips |
| CN103923749A (en) * | 2014-04-30 | 2014-07-16 | 海口蜜香树科技有限公司 | Method for extracting Chinese eaglewood essential oil |
| CN104087420A (en) * | 2014-07-16 | 2014-10-08 | 贵州省华烁生物科技有限公司 | Subcritical extraction method capable of improving antioxidant activity of volatile oil in agarwood leaves |
| CN104792722A (en) * | 2015-04-30 | 2015-07-22 | 华南农业大学 | Method for establishing agilawood oil content near infrared spectral prediction model |
| CN104830528A (en) * | 2015-04-23 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and use method of aquilaria wood perfume |
| CN104830537A (en) * | 2015-04-30 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and application of aquilaria wood hydrolat |
| CN105647647A (en) * | 2016-01-07 | 2016-06-08 | 安阳市晶华油脂工程有限公司 | Energy-saving agilawood essential oil extraction complete plant and low-temperature extraction technique thereof |
| CN106176411A (en) * | 2016-08-22 | 2016-12-07 | 广州市香事文化传播有限公司 | A kind of agilawood essential oil and preparation method thereof |
| CN106833899A (en) * | 2017-02-07 | 2017-06-13 | 珠海市玖鑫化妆品有限公司 | The preparation technology and essential oil Deacne pack of a kind of linaloe oil |
| CN107216950A (en) * | 2017-07-29 | 2017-09-29 | 郑永如璧 | Agilawood spray and agilawood tobacco tar preparation method |
| CN107299002A (en) * | 2017-08-09 | 2017-10-27 | 中国热带农业科学院农产品加工研究所 | The extracting method of agilawood essential oil |
| CN110934797A (en) * | 2019-12-25 | 2020-03-31 | 芜湖市茅王香料植物科技有限公司 | Production process of lavender perfume capable of soothing nerves and helping sleep |
| CN111821222A (en) * | 2020-07-17 | 2020-10-27 | 茂名市瑜丰沉香创意产业有限公司 | A kind of agarwood massage oil and preparation method thereof |
| CN112159722A (en) * | 2020-09-01 | 2021-01-01 | 梁勇 | Preparation method of agilawood essential oil |
| CN116549340A (en) * | 2023-06-15 | 2023-08-08 | 山东爱香人香业有限公司 | Preparation method of durable agilawood sandalwood perfume |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1500477A (en) * | 2002-11-13 | 2004-06-02 | 丛繁滋 | Quick result aerosol with plant aroma and its preparation |
| CN1742752A (en) * | 2005-10-08 | 2006-03-08 | 晏四平 | Atomizing agent containing medicinal plant oil |
| CN101129316A (en) * | 2007-08-30 | 2008-02-27 | 中国热带农业科学院热带生物技术研究所 | Agarwood perfume and preparation method thereof |
-
2013
- 2013-01-14 CN CN2013100135733A patent/CN103184102A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1500477A (en) * | 2002-11-13 | 2004-06-02 | 丛繁滋 | Quick result aerosol with plant aroma and its preparation |
| CN1742752A (en) * | 2005-10-08 | 2006-03-08 | 晏四平 | Atomizing agent containing medicinal plant oil |
| CN101129316A (en) * | 2007-08-30 | 2008-02-27 | 中国热带农业科学院热带生物技术研究所 | Agarwood perfume and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 刘月蓉等: "天然植物精油提取技术——亚临界流体萃取", 《莆田学院学报》, vol. 18, no. 2, 30 April 2011 (2011-04-30), pages 67 - 70 * |
| 郭娟等: "洋葱精油的亚临界水提取", 《华南理工大学学报》, vol. 37, no. 4, 30 April 2009 (2009-04-30), pages 143 - 148 * |
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103351954A (en) * | 2013-07-11 | 2013-10-16 | 大连卓尔高科技有限公司 | Process for extracting eaglewood essential oil by using supercritical carbon dioxide |
| CN103520435A (en) * | 2013-10-11 | 2014-01-22 | 中山市国林沉香科学研究所 | Agilawood health-care essential oil |
| CN103789094A (en) * | 2014-01-21 | 2014-05-14 | 广州大学 | Method for extracting agilawood essential oil from agilawood chips |
| CN103740467A (en) * | 2014-01-27 | 2014-04-23 | 陆燕 | Method for extracting plant essential oil |
| CN103923749A (en) * | 2014-04-30 | 2014-07-16 | 海口蜜香树科技有限公司 | Method for extracting Chinese eaglewood essential oil |
| CN104087420B (en) * | 2014-07-16 | 2016-03-30 | 贵州省华烁生物科技有限公司 | A kind of subcritical extraction method improving volatile oil anti-oxidant activity in eaglewood leaf |
| CN104087420A (en) * | 2014-07-16 | 2014-10-08 | 贵州省华烁生物科技有限公司 | Subcritical extraction method capable of improving antioxidant activity of volatile oil in agarwood leaves |
| CN104830528A (en) * | 2015-04-23 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and use method of aquilaria wood perfume |
| CN104830537B (en) * | 2015-04-30 | 2018-05-18 | 东莞波顿香料有限公司 | A kind of preparation method and applications of agalloch eaglewood hydrosol |
| CN104830537A (en) * | 2015-04-30 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and application of aquilaria wood hydrolat |
| CN104792722A (en) * | 2015-04-30 | 2015-07-22 | 华南农业大学 | Method for establishing agilawood oil content near infrared spectral prediction model |
| CN105647647A (en) * | 2016-01-07 | 2016-06-08 | 安阳市晶华油脂工程有限公司 | Energy-saving agilawood essential oil extraction complete plant and low-temperature extraction technique thereof |
| CN106176411A (en) * | 2016-08-22 | 2016-12-07 | 广州市香事文化传播有限公司 | A kind of agilawood essential oil and preparation method thereof |
| CN106833899A (en) * | 2017-02-07 | 2017-06-13 | 珠海市玖鑫化妆品有限公司 | The preparation technology and essential oil Deacne pack of a kind of linaloe oil |
| CN107216950A (en) * | 2017-07-29 | 2017-09-29 | 郑永如璧 | Agilawood spray and agilawood tobacco tar preparation method |
| CN107299002A (en) * | 2017-08-09 | 2017-10-27 | 中国热带农业科学院农产品加工研究所 | The extracting method of agilawood essential oil |
| CN110934797A (en) * | 2019-12-25 | 2020-03-31 | 芜湖市茅王香料植物科技有限公司 | Production process of lavender perfume capable of soothing nerves and helping sleep |
| CN111821222A (en) * | 2020-07-17 | 2020-10-27 | 茂名市瑜丰沉香创意产业有限公司 | A kind of agarwood massage oil and preparation method thereof |
| CN112159722A (en) * | 2020-09-01 | 2021-01-01 | 梁勇 | Preparation method of agilawood essential oil |
| CN116549340A (en) * | 2023-06-15 | 2023-08-08 | 山东爱香人香业有限公司 | Preparation method of durable agilawood sandalwood perfume |
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Application publication date: 20130703 |