CN103181452A - Feed mildew inhibitor and preparation method - Google Patents
Feed mildew inhibitor and preparation method Download PDFInfo
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- CN103181452A CN103181452A CN2011104482283A CN201110448228A CN103181452A CN 103181452 A CN103181452 A CN 103181452A CN 2011104482283 A CN2011104482283 A CN 2011104482283A CN 201110448228 A CN201110448228 A CN 201110448228A CN 103181452 A CN103181452 A CN 103181452A
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- Prior art keywords
- feed
- preparation
- mildew inhibitor
- mixture
- mixing
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- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 239000003112 inhibitor Substances 0.000 title abstract description 8
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims abstract description 16
- WPYMKLBDIGXBTP-UHFFFAOYSA-N Benzoic acid Natural products OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims abstract description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 12
- OPGYRRGJRBEUFK-UHFFFAOYSA-L disodium;diacetate Chemical compound [Na+].[Na+].CC([O-])=O.CC([O-])=O OPGYRRGJRBEUFK-UHFFFAOYSA-L 0.000 claims abstract description 9
- 239000001632 sodium acetate Substances 0.000 claims abstract description 9
- 235000017454 sodium diacetate Nutrition 0.000 claims abstract description 9
- 235000019260 propionic acid Nutrition 0.000 claims abstract description 8
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims abstract description 8
- 239000005711 Benzoic acid Substances 0.000 claims abstract description 7
- 235000010233 benzoic acid Nutrition 0.000 claims abstract description 7
- BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 claims abstract description 6
- 239000004330 calcium propionate Substances 0.000 claims abstract description 6
- 235000010331 calcium propionate Nutrition 0.000 claims abstract description 6
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 6
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 6
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 6
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 6
- 238000007789 sealing Methods 0.000 claims abstract description 5
- 230000003449 preventive effect Effects 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 abstract description 7
- 230000002045 lasting effect Effects 0.000 abstract description 3
- WXBLLCUINBKULX-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1.OC(=O)C1=CC=CC=C1 WXBLLCUINBKULX-UHFFFAOYSA-N 0.000 abstract 2
- 238000007873 sieving Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 description 4
- LDCRTTXIJACKKU-ONEGZZNKSA-N dimethyl fumarate Chemical compound COC(=O)\C=C\C(=O)OC LDCRTTXIJACKKU-ONEGZZNKSA-N 0.000 description 3
- 229960004419 dimethyl fumarate Drugs 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 229910021536 Zeolite Inorganic materials 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical group COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 2
- 239000004459 forage Substances 0.000 description 2
- 230000000855 fungicidal effect Effects 0.000 description 2
- 239000000417 fungicide Substances 0.000 description 2
- 230000005923 long-lasting effect Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000010457 zeolite Substances 0.000 description 2
- 240000002234 Allium sativum Species 0.000 description 1
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
- 241000195493 Cryptophyta Species 0.000 description 1
- 239000005770 Eugenol Substances 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 240000002262 Litsea cubeba Species 0.000 description 1
- 235000012854 Litsea cubeba Nutrition 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 229960002217 eugenol Drugs 0.000 description 1
- 235000021393 food security Nutrition 0.000 description 1
- 238000003958 fumigation Methods 0.000 description 1
- 235000004611 garlic Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229920005610 lignin Polymers 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical class COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
Landscapes
- Fodder In General (AREA)
Abstract
The invention provides a feed mildew inhibitor and a preparation method. The feed mildew inhibitor comprises propionic acid, calcium propionate, sodium diacetate, sodium benzoate, benzoic acid and silica. The preparation method comprises the following steps: uniformly mixing propionic acid and silica, then adding calcium propionate, carrying out uniform mixing, sealing an obtained mixture and standing the mixture for 1 to 2 h; and sieving the mixture with a 40-mesh sieve and uniformly mixing the sieved mixture with sodium diacetate, sodium benzoate and benzoic acid. Each component of the mildew inhibitor accords with national feed hygiene standards in China, and the mildew inhibitor has the characteristics of safety, high efficiency, a lasting effect and low cost.
Description
Affiliated technical field
The invention belongs to the preservation technique field, provide a kind of with low cost, action time is lasting, safe Midew preventive for feed and preparation method.
Background technology
Contain a lot of nutriments in the feed, all mouldy than being easier to as corn, dregs of beans, oily chaff, inferior powder etc., even our fine in whole production process moisture control, feed still can be mouldy also along with the prolongation of period of storage.After feed was mouldy, the nutrition meeting of feed reduced, and the palatability of feed also can reduce, and also can cause great infringement to growth of animals or poultry by the toxin of mould secretion, food security that also can our meat, eggs and milk of remote-effects.Therefore, add mould inhibitor control fungus growth in Feed Manufacturing, the freshness date that prolongs feed is just very necessary.About the research to Midew preventive for feed, many inventors have proposed own scheme.
Provide a kind of long-lasting fungicide for composite feed as Chinese patent " CN1059454 long-lasting fungicide for composite feed ", be that main component and Chinese patent " CN1087471 Midew preventive for feed " provide a kind of for mould inhibitor with propionic acid and salt, dimethyl fumarate, sodium Diacetate, garlic and algae, it is by sodium Diacetate, dimethyl fumarate, nipagin esters and inserts etc.More than the dimethyl fumarate used in two patents because safety issue, use has been under an embargo.It is eugenol, litsea citrate oil, propionic acid, zeolite powder that Chinese patent " CN1141732 Midew preventive for feed " provides a kind of Midew preventive for feed, key component, and this invented technology is simple, has characteristics such as antibacterial, broad-spectrum antiseptic.But volatile ingredients all, persistence is not strong.It is sodium Diacetate, lignin, propylben, shitosan, benzoic acid, zeolite powder etc. that Chinese patent " CN102084941 Midew preventive for feed " provides a kind of Midew preventive for feed, component.Wherein lack the composition that to fumigate mould again.And above four kinds of patents all have at least one or two kind not to be the product that the Ministry of Agriculture issues to be had on " feedstuff additive product catalogue (2008) ", cause using in production practices.
Summary of the invention
Goal of the invention: technical problem solved by the invention provides a kind of Midew preventive for feed and production method, and every kind of composition of this mould inhibitor all meets forage health standard, and safety, efficient, lasting while have characteristics with low cost again.
Technical scheme: for achieving the above object, the present invention is based on following technical scheme:
1, adopt raw material sources wide, make simple, with low cost;
2, all be that the Ministry of Agriculture issues the product that " feedstuff additive product catalogue (2008) " go up the permission use;
3, the organic acid of existing fumigation action in the composition has again to continue to discharge hydrochlorate;
4, stable in properties does not produce any harmful substance
Each main component mass content umber is among the present invention
The invention still further relates to the preparation method of this product, this method is: earlier propionic acid and silica are mixed, after mixing with the adding calcium propionate, sealing was placed 1～2 hour again; Cross 40 mesh sieves, after mixing with sodium Diacetate, Sodium Benzoate, benzoic acid more namely.
Beneficial effect: the Midew preventive for feed according to the inventive method is produced compared with prior art, has following beneficial effect:
Cost of material is low, and it is guaranteed to originate; Bio-safety degree height all meets forage health standard; The sterilization of namely can tagging has stifling bactericidal action again concurrently, and under condition of the same race, anti-mold effect is good, and fresh keeping time is long.Be 0.05～0.1% o'clock at consumption, can make feed below 14% preserve two months not mouldy.
The specific embodiment
Further set forth the technical scheme that provided of the present invention in the mode of embodiment below.
Each constituent mass umber is
The preparation method is: earlier propionic acid and silica are mixed, after mixing with the adding calcium propionate, sealing was placed 1～2 hour again; Cross 40 mesh sieves, after mixing with sodium Diacetate, Sodium Benzoate, benzoic acid more namely.
Claims (2)
1. a Midew preventive for feed is characterized in that, its each component materials and mass fraction are:
The preparation method is: earlier propionic acid and silica are mixed, after mixing with the adding calcium propionate, sealing was placed 1～2 hour again; Cross 40 mesh sieves, after mixing with sodium Diacetate, Sodium Benzoate, benzoic acid more namely.
2. Midew preventive for feed as claimed in claim 1 is characterized in that, its each component materials and mass fraction are:
The preparation method is: earlier propionic acid and silica are mixed, after mixing with the adding calcium propionate, sealing was placed 1～2 hour again; Cross 40 mesh sieves, after mixing with sodium Diacetate, Sodium Benzoate, benzoic acid more namely.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011104482283A CN103181452A (en) | 2011-12-27 | 2011-12-27 | Feed mildew inhibitor and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011104482283A CN103181452A (en) | 2011-12-27 | 2011-12-27 | Feed mildew inhibitor and preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103181452A true CN103181452A (en) | 2013-07-03 |
Family
ID=48673112
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011104482283A Pending CN103181452A (en) | 2011-12-27 | 2011-12-27 | Feed mildew inhibitor and preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103181452A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103859216A (en) * | 2014-03-13 | 2014-06-18 | 侯伟革 | Composite mildew preventive for animal feed and application of composite mildew preventive |
| CN105341360A (en) * | 2015-12-07 | 2016-02-24 | 重庆华睿隆生物科技有限公司 | Carrier-free propionic acid solid feed mildew preventive and preparation and use thereof |
| CN105876142A (en) * | 2016-04-13 | 2016-08-24 | 西南科技大学 | Production method of straw feed preventing fungi and bacteria |
| CN106036034A (en) * | 2016-05-20 | 2016-10-26 | 四川爱客信生物科技有限公司 | Mixed liquid additive for feed and preparation method of mixed liquid additive |
| CN107836627A (en) * | 2017-11-30 | 2018-03-27 | 重庆华睿隆生物科技有限公司 | A kind of additive and its application method for preventing feed life acarid |
| CN107890002A (en) * | 2017-11-30 | 2018-04-10 | 重庆华睿隆生物科技有限公司 | A kind of propionic acid acetic acid sodium form Midew preventive for feed |
| CN107981060A (en) * | 2017-12-27 | 2018-05-04 | 高宗保 | A kind of milk cow forage of high yield milk and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101731451A (en) * | 2010-01-21 | 2010-06-16 | 鲁昊 | Compound mouldproof agent with acidizing effect and preparation method thereof |
| CN101766268A (en) * | 2009-01-07 | 2010-07-07 | 翁晓强 | Feed mould inhibitor |
-
2011
- 2011-12-27 CN CN2011104482283A patent/CN103181452A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101766268A (en) * | 2009-01-07 | 2010-07-07 | 翁晓强 | Feed mould inhibitor |
| CN101731451A (en) * | 2010-01-21 | 2010-06-16 | 鲁昊 | Compound mouldproof agent with acidizing effect and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 刘锦湖等: "饲料防霉剂的遴选", 《中国饲料》 * |
| 王春维: "双乙酸钠复合防霉剂的制备及防霉效果试验", 《中国饲料》 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103859216A (en) * | 2014-03-13 | 2014-06-18 | 侯伟革 | Composite mildew preventive for animal feed and application of composite mildew preventive |
| CN105341360A (en) * | 2015-12-07 | 2016-02-24 | 重庆华睿隆生物科技有限公司 | Carrier-free propionic acid solid feed mildew preventive and preparation and use thereof |
| CN105876142A (en) * | 2016-04-13 | 2016-08-24 | 西南科技大学 | Production method of straw feed preventing fungi and bacteria |
| CN106036034A (en) * | 2016-05-20 | 2016-10-26 | 四川爱客信生物科技有限公司 | Mixed liquid additive for feed and preparation method of mixed liquid additive |
| CN107836627A (en) * | 2017-11-30 | 2018-03-27 | 重庆华睿隆生物科技有限公司 | A kind of additive and its application method for preventing feed life acarid |
| CN107890002A (en) * | 2017-11-30 | 2018-04-10 | 重庆华睿隆生物科技有限公司 | A kind of propionic acid acetic acid sodium form Midew preventive for feed |
| CN107981060A (en) * | 2017-12-27 | 2018-05-04 | 高宗保 | A kind of milk cow forage of high yield milk and preparation method thereof |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20130703 |