CN103126047B - The application of extractive of agaric in cigarette - Google Patents
The application of extractive of agaric in cigarette Download PDFInfo
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- CN103126047B CN103126047B CN201310091173.4A CN201310091173A CN103126047B CN 103126047 B CN103126047 B CN 103126047B CN 201310091173 A CN201310091173 A CN 201310091173A CN 103126047 B CN103126047 B CN 103126047B
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 241000208125 Nicotiana Species 0.000 claims abstract description 21
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 21
- 238000010438 heat treatment Methods 0.000 claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 claims abstract description 8
- 239000012535 impurity Substances 0.000 claims abstract description 6
- 238000005903 acid hydrolysis reaction Methods 0.000 claims abstract description 5
- 230000007071 enzymatic hydrolysis Effects 0.000 claims abstract description 5
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 claims abstract description 5
- 239000012141 concentrate Substances 0.000 claims abstract description 3
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 235000000023 Auricularia auricula Nutrition 0.000 claims description 37
- 241001149430 Auricularia auricula-judae Species 0.000 claims description 37
- 239000000284 extract Substances 0.000 claims description 34
- 241000221377 Auricularia Species 0.000 claims description 26
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 15
- 239000000843 powder Substances 0.000 claims description 15
- 241000233866 Fungi Species 0.000 claims description 13
- 239000002253 acid Substances 0.000 claims description 9
- 238000002791 soaking Methods 0.000 claims description 9
- 238000000605 extraction Methods 0.000 claims description 8
- 210000001124 body fluid Anatomy 0.000 claims description 6
- 239000010839 body fluid Substances 0.000 claims description 6
- 230000007062 hydrolysis Effects 0.000 claims description 6
- 238000006460 hydrolysis reaction Methods 0.000 claims description 6
- 230000001737 promoting effect Effects 0.000 claims description 6
- 108091005804 Peptidases Proteins 0.000 claims description 5
- 239000004365 Protease Substances 0.000 claims description 5
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 5
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- 230000008961 swelling Effects 0.000 claims description 5
- 102000004190 Enzymes Human genes 0.000 claims description 4
- 108090000790 Enzymes Proteins 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 239000006228 supernatant Substances 0.000 claims description 2
- 102000004169 proteins and genes Human genes 0.000 abstract description 6
- 108090000623 proteins and genes Proteins 0.000 abstract description 6
- 230000008859 change Effects 0.000 abstract description 4
- 238000004090 dissolution Methods 0.000 abstract description 3
- 229920002521 macromolecule Polymers 0.000 abstract description 2
- 239000000470 constituent Substances 0.000 abstract 2
- 230000008014 freezing Effects 0.000 abstract 2
- 238000007710 freezing Methods 0.000 abstract 2
- 230000008018 melting Effects 0.000 abstract 2
- 238000002844 melting Methods 0.000 abstract 2
- 150000001720 carbohydrates Chemical class 0.000 abstract 1
- 235000014633 carbohydrates Nutrition 0.000 abstract 1
- 230000029087 digestion Effects 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
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- 239000004480 active ingredient Substances 0.000 description 4
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- 241001506047 Tremella Species 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
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- 230000006870 function Effects 0.000 description 3
- 238000010298 pulverizing process Methods 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- SHZGCJCMOBCMKK-UHFFFAOYSA-N D-mannomethylose Natural products CC1OC(O)C(O)C(O)C1O SHZGCJCMOBCMKK-UHFFFAOYSA-N 0.000 description 2
- -1 D-wood sugar Chemical compound 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- SHZGCJCMOBCMKK-DHVFOXMCSA-N L-fucopyranose Chemical compound C[C@@H]1OC(O)[C@@H](O)[C@H](O)[C@@H]1O SHZGCJCMOBCMKK-DHVFOXMCSA-N 0.000 description 2
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- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 2
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- 229910052791 calcium Inorganic materials 0.000 description 2
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- OILXMJHPFNGGTO-UHFFFAOYSA-N (22E)-(24xi)-24-methylcholesta-5,22-dien-3beta-ol Natural products C1C=C2CC(O)CCC2(C)C2C1C1CCC(C(C)C=CC(C)C(C)C)C1(C)CC2 OILXMJHPFNGGTO-UHFFFAOYSA-N 0.000 description 1
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- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- LRYZPFWEZHSTHD-HEFFAWAOSA-O 2-[[(e,2s,3r)-2-formamido-3-hydroxyoctadec-4-enoxy]-hydroxyphosphoryl]oxyethyl-trimethylazanium Chemical class CCCCCCCCCCCCC\C=C\[C@@H](O)[C@@H](NC=O)COP(O)(=O)OCC[N+](C)(C)C LRYZPFWEZHSTHD-HEFFAWAOSA-O 0.000 description 1
- CFWRDBDJAOHXSH-SECBINFHSA-N 2-azaniumylethyl [(2r)-2,3-diacetyloxypropyl] phosphate Chemical compound CC(=O)OC[C@@H](OC(C)=O)COP(O)(=O)OCCN CFWRDBDJAOHXSH-SECBINFHSA-N 0.000 description 1
- OQMZNAMGEHIHNN-UHFFFAOYSA-N 7-Dehydrostigmasterol Natural products C1C(O)CCC2(C)C(CCC3(C(C(C)C=CC(CC)C(C)C)CCC33)C)C3=CC=C21 OQMZNAMGEHIHNN-UHFFFAOYSA-N 0.000 description 1
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 241000437273 Auricularia cornea Species 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- DNVPQKQSNYMLRS-NXVQYWJNSA-N Ergosterol Natural products CC(C)[C@@H](C)C=C[C@H](C)[C@H]1CC[C@H]2C3=CC=C4C[C@@H](O)CC[C@]4(C)[C@@H]3CC[C@]12C DNVPQKQSNYMLRS-NXVQYWJNSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- PNNNRSAQSRJVSB-SLPGGIOYSA-N Fucose Natural products C[C@H](O)[C@@H](O)[C@H](O)[C@H](O)C=O PNNNRSAQSRJVSB-SLPGGIOYSA-N 0.000 description 1
- 241000287828 Gallus gallus Species 0.000 description 1
- 229920001503 Glucan Polymers 0.000 description 1
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 1
- SHZGCJCMOBCMKK-PQMKYFCFSA-N L-Fucose Natural products C[C@H]1O[C@H](O)[C@@H](O)[C@@H](O)[C@@H]1O SHZGCJCMOBCMKK-PQMKYFCFSA-N 0.000 description 1
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 description 1
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 1
- KDXKERNSBIXSRK-YFKPBYRVSA-N L-lysine Chemical compound NCCCC[C@H](N)C(O)=O KDXKERNSBIXSRK-YFKPBYRVSA-N 0.000 description 1
- PNNNRSAQSRJVSB-UHFFFAOYSA-N L-rhamnose Natural products CC(O)C(O)C(O)C(O)C=O PNNNRSAQSRJVSB-UHFFFAOYSA-N 0.000 description 1
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 1
- 239000004472 Lysine Substances 0.000 description 1
- MSFSPUZXLOGKHJ-UHFFFAOYSA-N Muraminsaeure Natural products OC(=O)C(C)OC1C(N)C(O)OC(CO)C1O MSFSPUZXLOGKHJ-UHFFFAOYSA-N 0.000 description 1
- 108010013639 Peptidoglycan Proteins 0.000 description 1
- 244000252132 Pleurotus eryngii Species 0.000 description 1
- 235000001681 Pleurotus eryngii Nutrition 0.000 description 1
- 241000195474 Sargassum Species 0.000 description 1
- 241000264279 Sargassum fusiforme Species 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- GZCGUPFRVQAUEE-KVTDHHQDSA-N aldehydo-D-mannose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)C=O GZCGUPFRVQAUEE-KVTDHHQDSA-N 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
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- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000010100 anticoagulation Effects 0.000 description 1
- 239000006286 aqueous extract Substances 0.000 description 1
- PYMYPHUHKUWMLA-WDCZJNDASA-N arabinose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)C=O PYMYPHUHKUWMLA-WDCZJNDASA-N 0.000 description 1
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 description 1
- 235000003704 aspartic acid Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 description 1
- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
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- 230000007812 deficiency Effects 0.000 description 1
- 210000005069 ears Anatomy 0.000 description 1
- ZKQRGSXITBHHPC-VVQHAZRASA-N ergosta-5,7-dien-3beta-ol Chemical compound C1[C@@H](O)CC[C@]2(C)[C@@H](CC[C@@]3([C@@H]([C@H](C)CC[C@H](C)C(C)C)CC[C@H]33)C)C3=CC=C21 ZKQRGSXITBHHPC-VVQHAZRASA-N 0.000 description 1
- DNVPQKQSNYMLRS-SOWFXMKYSA-N ergosterol Chemical compound C1[C@@H](O)CC[C@]2(C)[C@H](CC[C@]3([C@H]([C@H](C)/C=C/[C@@H](C)C(C)C)CC[C@H]33)C)C3=CC=C21 DNVPQKQSNYMLRS-SOWFXMKYSA-N 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000000054 fungal extract Substances 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 235000013922 glutamic acid Nutrition 0.000 description 1
- 239000004220 glutamic acid Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
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- 239000000787 lecithin Substances 0.000 description 1
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- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention provides an application of an extractive of agaric in cigarettes. The extractive of the agaric is added into the cigarettes, and therefore, processability of cut tobacco can be improved remarkably, offensive odor and irritation can be reduced, a sense of engender liquid can be increased and the whole quality of sucking the cigarettes can be improved. The extractive can be prepared by the following steps; steps of drying the agaric, getting rid of impurity, meshing the agaric, immersing the agaric, freezing and melting the agaric repeatedly, dealing with the agaric with enzymatic hydrolysis, heating and digestion, separating clear liquid and residues, dealing the residues with acid hydrolysis again, filtering the clear liquid, combining the clear liquid to concentrate and gaining the extractive of the agaric. The application is characterized by using the method of freezing and melting repeatedly to improve a dissolution rate of effective constituents of the agaric, getting rid of protein of cigarette-smoking taste through an adoption of an enzymic method, improving a use ration of the effective constituents of the agaric by further hydrolyzing macromolecule carbohydrates which are bad in solubleness. The application has the advantages of being simple and efficient, prone to amplify the craft of extracting from water and applying the extractive into the cigarettes without the change of initial performance and processing craft, and therefore, the application has the advantages of possessing meaning and value of practical production.
Description
Technical field
The present invention relates to the preparations and applicatio of cigarette additive, be specifically related to the application of Auricularia extract in cigarette.The application of this technology does not change the existing processing technology of cigarette, can improve sucking quality and the sense organ comfort level of cigarette.
Background technology
Auricularia auriculajudae has another name called the ears or side handles of a utensil, cloud ear, tree chicken, wooden moth, wood fungus, is a kind of self-sow or the fungi of artificial cultivation on various rotten wood.Auricularia auriculajudae is nutritious, and food flavor is delicious, not only has very high nutritive value, and has very high medical value.Auricularia auriculajudae property is put down, and taste is sweet, has cool blood, invigorates blood circulation, effect that pain relieving and beneficial gas are kept fit.
Auricularia auriculajudae aboundresources and containing abundant nutritional labeling, the in recent years extensive concern of extremely Chinese scholars.Auricularia auriculajudae protein content up to more than 10%, wherein containing abundant essential amino acid, as aspartic acid, glutamic acid, lysine etc. to have the composition of important function to human development and health.Be rich in the mineral matter element of the needed by human such as calcium, zinc in auricularia auriculajudae, wherein iron content is higher than meat 100 times, and calcium content is then 30-70 times of meat.Also containing ergosterol, dihydroergosterol, lecithin, cephalin and sphingomyelins etc. in auricularia auriculajudae.Polysaccharide is the main active substances of auricularia auriculajudae, primarily of compositions such as L-fucose, Arabinose, D-wood sugar, D-MANNOSE, D-Glucose, glucuronic acids.It is reported, Auricularia polysaccharide has anticoagulation, antitumor, anti-inflammatory etc. cytoprotection, also has reducing blood lipid, hypoglycemic, the anti-ageing effect of waiting for a long time.Melanin is another important active substances of auricularia auriculajudae, be made up of Blackfungus polyhexose and protein, in dark purple black, there is certain bacteriostasis, its structure is by not having coloured glucose, fucose, galactolipin and a series of small peptide by regular connection, the folding peptidoglycan with certain function, black fungus pigment can strengthen body immunity, anti-oxidant, delay senility, and also has certain antifungal activity.
Still there is certain deficiency in current domestic cigarette product, the exploitation of novel cigarette additive is an important solution route in flavouring essence quality and sense organ comfort level etc.Vast territory and abundant resources in China, and natural resources are of a great variety, and the composition of contained active ingredient also respectively has feature, for the exploitation of cigarette additive provides rich in natural resources.By different modes method, extraction and isolation is carried out to its active ingredient, and for the feature of cigarette product, extract is applied in cigarette in different forms, to improve the overall quality of cigarette.Current natural extract is widely used at Field of Tobacco, and achieving significant effect, the natural extract related to mainly contains Hijiki polysaccharide (ZL 200610128282.9), sargassum fusiforme aqueous extract (ZL 200610128283.3), sargassum fusifome alcohol extract (ZL 200610128284.8), natural built-up extract (ZL 03140229.1) etc.
About the application of fungal extract in cigarette has been reported, Chen Qun etc. disclose the extracting method of the extracting method of white fungus Thick many candies and the application (CN 102796204 A) in tobacco and white fungus water extracting liquid and the application (CN 102793263 A) in tobacco thereof, and two kinds of dried tremella extracts all have the effect reducing dry sensation, improve mouthfeel and humectation.Compared with white fungus, same containing saccharide compound and protein in water soluble ingredient in auricularia auriculajudae, but tremella polysaccharides is based on α-(1 → 3)-D-mannosan, and Auricularia polysaccharide also comprises β-(1 → 3)-D-glucan except α-(1 → 3)-D-mannosan.The research of the present inventor shows, protein in extract has to be increased flue gas and to mix the negative effect of gas, and white fungus and auricularia auriculajudae all have higher protein content level (Wang Fengfang. pleurotus eryngii compares with common edible mushroom Middle nutrition composition. Shanghai Institute Of Technology's journal, 2003(3): 48-51), therefore Deproteinated technique is adopted to be very important in leaching process.In addition, the melanin in Auricularia extract has anti-oxidant and function that is scavenging free radicals, is the active material of the uniqueness not available for dried tremella extract.But black fungus pigment combines with protein and sugar compounds usually, enzyme process or acid system can be adopted to be hydrolyzed, thus improve melanic dissolution efficiency.
Summary of the invention
The present invention studies auricularia auriculajudae based on above-mentioned present Research just, fully utilize various technology, water soluble ingredient in abundant extraction auricularia auriculajudae, set up extraction process that is simply effective, that be easy to amplification, and Auricularia extract is put in cigarette, object is sucking quality and the sense organ comfort level of improving cigarette.
The object of the invention is to be achieved through the following technical solutions:
The application of a kind of Auricularia extract in cigarette, feature adds Auricularia extract in pipe tobacco, pipe tobacco processing characteristics significantly improves, assorted gas and excitant reduce, sense of promoting the production of body fluid increases, overall sucking quality is improved, and described extract is prepared from by the following method: dried fungus → removal of impurities pulverizes → soaks → multigelation → enzymatic hydrolysis → heating lixiviate → isolated by filtration clear liquid and filter residue → filter residue again through acid hydrolysis → filter clear liquid → clear liquid merges and concentrates → Auricularia extract.
The addition of described Auricularia extract is the 0.005-0.05% of pipe tobacco weight, is evenly sprayed onto pipe tobacco during use.
Soaking in step, water: auricularia auriculajudae dry powder=1 ~ 2:1(w/w), soaking at room temperature 1 ~ 5h.
In multigelation step, auricularia auriculajudae swelling after water soaking is placed 1 ~ 5h in-18 DEG C, after 30 ~ 60 DEG C of heating are thawed, then be placed in-18 DEG C of placement 1 ~ 5h, repeatedly carry out 2 ~ 4 times.
In enzymatic hydrolysis step, the enzyme preparation added is protease, and addition is 0.5 ~ 1% of auricularia auriculajudae dry powder quality, hydrolysis temperature 40 ~ 60 DEG C, enzymolysis time 1 ~ 2h.
In heating lixiviate step, amount of water is 5 ~ 15 times of auricularia auriculajudae dry powder quality, extraction temperature 70 ~ 90 DEG C, extraction time 3 ~ 5h.
In acid hydrolysis step, the acid added is citric acid, and make the acid concentration in system be 1 ~ 5 mol/L, hydrolysis temperature is 70 ~ 90 DEG C, hydrolysis time 1 ~ 30min.
In merging concentration step, centrifuged supernatant is 10 ~ 30% through being evaporated to solid content.
The present invention has following characteristics: (1) adopts multigelation method wall breaking technology to improve the dissolution rate of auricularia auriculajudae active ingredient; (2) enzyme process is adopted to remove the protein affecting cigarette odor-absorbing; (3) poor to dissolubility in auricularia auriculajudae large molecule glucide is further hydrolyzed, and improves the utilization rate of auricularia auriculajudae active ingredient.The present invention establishes simply effectively, is easy to the auricularia auriculajudae extraction process by water of amplification, and Auricularia extract is applied in cigarette, do not change original performance of cigarette, do not change the original processing technology of cigarette, improve processing characteristics and the sense organ comfort level of cigarette, assorted gas and excitant can be made to reduce, and sense of promoting the production of body fluid increases, and therefore has more the meaning and value of actual production.
Accompanying drawing explanation
Fig. 1 is preparation technology's flow process of Auricularia extract in the present invention.
Detailed description of the invention
The present invention is described further below in conjunction with embodiment, but does not limit the present invention.
embodiment 1:
Dried fungus obtains auricularia auriculajudae dry powder through removal of impurities, pulverizing, adds the water of 1 times of weight, soak at room temperature 2h.Auricularia auriculajudae swelling after water soaking places 1h in-18 DEG C, after 60 DEG C of heating are thawed, then is placed in-18 DEG C of placement 2h, repeatedly carries out 2 times.Regulation system temperature to 45 DEG C, the protease adding auricularia auriculajudae dry powder weight 0.5% keeps 1h.Add the water that quality is 10 times of auricularia auriculajudae dry powder quality, be heated to 70 DEG C of backflow 5h, filter while hot after stopping heating, clear liquid is for subsequent use.Adding citric acid to system acid concentration in filter residue is 1mol/L, and 70 DEG C of heating 1h, filter while hot after stopping heating, merging clear liquid, through being evaporated to solid content 10%, obtaining Auricularia extract.
Auricularia extract is dissolved in water, is evenly sprayed onto on pipe tobacco by 0.005% of pipe tobacco weight, after baking, rolls into cigarette.The pipe tobacco processing characteristics of adding polysaccharide significantly improves, the soft exquisiteness of cigarette smoke, and assorted gas excitant reduces, and sense of promoting the production of body fluid increases.
embodiment 2:
Dried fungus obtains auricularia auriculajudae dry powder through removal of impurities, pulverizing, adds the water of 2 times of weight, soak at room temperature 2h.Auricularia auriculajudae swelling after water soaking places 1h in-18 DEG C, after 50 DEG C of heating are thawed, then is placed in-18 DEG C of placement 2h, repeatedly carries out 3 times.Regulation system temperature to 50 DEG C, the protease adding auricularia auriculajudae dry powder weight 0.7% keeps 1.5h.Add the water that quality is 12 times of auricularia auriculajudae dry powder quality, be heated to 80 DEG C of backflow 3h, filter while hot after stopping heating, clear liquid is for subsequent use.Adding citric acid to system acid concentration in filter residue is 2mol/L, and 80 DEG C of heating 1h, filter while hot after stopping heating, merging clear liquid, through being evaporated to solid content 20%, obtaining Auricularia extract.
Auricularia extract is dissolved in water, is evenly sprayed onto on pipe tobacco by 0.01% of pipe tobacco weight, after baking, rolls into cigarette.The pipe tobacco processing characteristics of adding polysaccharide significantly improves, the soft exquisiteness of cigarette smoke, and assorted gas excitant reduces, and sense of promoting the production of body fluid increases.
embodiment 3:
Dried fungus obtains auricularia auriculajudae dry powder through removal of impurities, pulverizing, adds the water of 2 times of weight, soak at room temperature 3h.Auricularia auriculajudae swelling after water soaking places 1h in-18 DEG C, after 40 DEG C of heating are thawed, then is placed in-18 DEG C of placement 2h, repeatedly carries out 3 times.Regulation system temperature to 55 DEG C, the protease adding auricularia auriculajudae dry powder weight 0.1% keeps 1h.Add the water that quality is 8 times of auricularia auriculajudae dry powder quality, be heated to 90 DEG C of backflow 2h, filter while hot after stopping heating, clear liquid is for subsequent use.Adding citric acid to system acid concentration in filter residue is 1mol/L, and 90 DEG C of heating 1h, filter while hot after stopping heating, merging clear liquid, through being evaporated to solid content 30%, obtaining Auricularia extract.
Auricularia extract is dissolved in water, is evenly sprayed onto on pipe tobacco by 0.008% of pipe tobacco weight, after baking, rolls into cigarette.The pipe tobacco processing characteristics of adding polysaccharide significantly improves, the soft exquisiteness of cigarette smoke, and assorted gas excitant reduces, and sense of promoting the production of body fluid increases.
Claims (5)
1. the application of Auricularia extract in cigarette, it is characterized in that: in pipe tobacco, add Auricularia extract, pipe tobacco processing characteristics significantly improves, assorted gas and excitant reduce, sense of promoting the production of body fluid increases, overall sucking quality is improved, and described extract is prepared from by the following method: dried fungus → removal of impurities pulverizes → soaks → multigelation → enzymatic hydrolysis → heating lixiviate → isolated by filtration clear liquid and filter residue → filter residue again through acid hydrolysis → filter clear liquid → clear liquid merges and concentrates → Auricularia extract;
In multigelation step, auricularia auriculajudae swelling after water soaking is placed 1 ~ 5h in-20 ~-10 DEG C, after 30 ~ 60 DEG C of heating are thawed, then be placed in-20 ~-10 DEG C of placement 1 ~ 5h, repeatedly carry out 2 ~ 4 times;
In enzymatic hydrolysis step, the enzyme preparation added is protease, and addition is 0.5 ~ 1% of auricularia auriculajudae dry powder quality, hydrolysis temperature 40 ~ 60 DEG C, enzymolysis time 1 ~ 2h;
In acid hydrolysis step, the acid added is citric acid, and make the acid concentration in system be 1 ~ 5 mol/L, hydrolysis temperature is 70 ~ 90 DEG C, hydrolysis time 1 ~ 30min.
2. the application of Auricularia extract according to claim 1 in cigarette, is characterized in that: the addition of Auricularia extract is the 0.005-0.05% of pipe tobacco weight, is evenly sprayed onto pipe tobacco during use.
3. the application of Auricularia extract according to claim 1 in cigarette, is characterized in that: soaking in step, water: auricularia auriculajudae dry powder=1 ~ 2:1, soaking at room temperature 1 ~ 5h.
4. the application of Auricularia extract according to claim 1 in cigarette, is characterized in that: in heating lixiviate step, amount of water is 5 ~ 15 times of auricularia auriculajudae dry powder quality, extraction temperature 70 ~ 90 DEG C, extraction time 3 ~ 5h.
5. the application of Auricularia extract according to claim 1 in cigarette, is characterized in that: in merging concentration step, centrifuged supernatant is 10 ~ 30% through being evaporated to solid content.
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| CN116875384A (en) * | 2023-08-07 | 2023-10-13 | 河南中烟工业有限责任公司 | A tobacco flavor that improves taste and its application in heated cigarettes |
Citations (5)
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|---|---|---|---|---|
| GB1089361A (en) * | 1964-01-22 | 1967-11-01 | Desmond Walter Molins | Improvements relating to tobacco processing |
| CN1409997A (en) * | 2002-11-16 | 2003-04-16 | 何伟平 | Black fungus health care food and its making method |
| CN102060934A (en) * | 2010-12-11 | 2011-05-18 | 中国计量学院 | Enzymatic extraction method for auricularia auricula polysaccharides |
| CN102321189A (en) * | 2011-10-24 | 2012-01-18 | 周伯扬 | Comprehensive extraction process for auricularia auricula polysaccharide |
| CN102793263A (en) * | 2012-08-27 | 2012-11-28 | 福建中烟工业有限责任公司 | Extraction method of tremella water extract concentrate and application of concentrate in tobaccos |
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| WO2007013613A1 (en) * | 2005-07-29 | 2007-02-01 | Suntory Limited | Composition containing fucoidan or fucoidan hydrolysate and immunopotentiating material |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1089361A (en) * | 1964-01-22 | 1967-11-01 | Desmond Walter Molins | Improvements relating to tobacco processing |
| CN1409997A (en) * | 2002-11-16 | 2003-04-16 | 何伟平 | Black fungus health care food and its making method |
| CN102060934A (en) * | 2010-12-11 | 2011-05-18 | 中国计量学院 | Enzymatic extraction method for auricularia auricula polysaccharides |
| CN102321189A (en) * | 2011-10-24 | 2012-01-18 | 周伯扬 | Comprehensive extraction process for auricularia auricula polysaccharide |
| CN102793263A (en) * | 2012-08-27 | 2012-11-28 | 福建中烟工业有限责任公司 | Extraction method of tremella water extract concentrate and application of concentrate in tobaccos |
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