CN103109836A - Insecticide composition containing metaflumizone and dimehypo or cartap - Google Patents
Insecticide composition containing metaflumizone and dimehypo or cartap Download PDFInfo
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Abstract
本发明公开了一种含有氰氟虫腙的杀虫组合物，其中，由两种活性成分A和B组成，A成分是氰氟虫腙，B成分是杀虫双、杀螟丹的一种，所述两种活性成分A和B组成质量比为1：50～10：1。该杀虫组合物防治蔬菜、水稻、果树、棉花等作物的鳞翅目害虫，如小菜蛾、甜菜夜蛾、稻纵卷叶螟、二化螟、三化螟、卷叶蛾、棉铃虫等。本发明利用两种活性组份混配，根据用孙云沛法计算混剂的共毒系数CTC值，表明具有明显的增效作用，可减少有效成份用药量，延缓害虫对新药剂氰氟虫腙抗药性的产生。The invention discloses an insecticidal composition containing metaflumizone, wherein it consists of two active components A and B, component A is metaflumizone, and component B is a kind of dimehypo and cartap , the mass ratio of the two active ingredients A and B is 1:50-10:1. The pesticidal composition controls Lepidoptera pests in vegetables, rice, fruit trees, cotton and other crops, such as diamondback moth, beet armyworm, rice leaf roller, rice stem borer, rice stem borer, leaf roller moth, cotton bollworm, and the like. The present invention utilizes two kinds of active ingredients to mix, and according to the co-toxicity coefficient CTC value of the mixed agent calculated by Sun Yunpei's method, it shows that it has obvious synergistic effect, which can reduce the dosage of active ingredients and delay the resistance of pests to the new agent metaflumizone. medicinal production.
Description
The application is dividing an application of " Pesticidal combination that contains metaflumizone " application for a patent for invention, original application day: on January 5th, 2010, application number: 201010003850.9
Technical field
The present invention relates to a kind of composition pesticide, relate in particular to the Pesticidal combination that contains metaflumizone.
Background technology
The lepidoptera pests such as rice leaf roller, striped rice borer, paddy stem borer, diamond-back moth, cotton bollworm are the important pests on the crops such as paddy rice, vegetables, cotton.In recent years, owing to using continuously the insecticide that contains a kind of active constituent, these insects have produced pesticide resistance in various degree, and the medication increased frequency has caused that peasant burden increases the weight of, the destruction of environmental pollution and ecotope etc.
Metaflumizone (metaflumizone) is recent years abroad company a kind of noval chemical compound newly developed, belong to the semicarbazones insecticides, mechanism of action is unique, can effectively prevent and treat larva, the adult of the multiple lepidoptera pests such as diamond-back moth, rice leaf roller and some coleoptera, also can be used for preventing and treating the insects such as sanitary insect pest such as ant, termite, fly class, cockroach.Metaflumizone is a kind of insecticide of brand-new mechanism of action, on the acceptor that is attached to sodium-ion channel, hinders sodium ion current.Enter polypide after this medicine of insect's food-taking, the sodium-ion channel by on the mechanism of action blocking-up insect neuron axon film of uniqueness makes sodium ion can not pass through axolemma, and then suppress nerve impulse and make excessive the loosening of polypide, paralysis is after several hours, insect namely stops taking food, and is dead in 1～3 day.Metaflumizone can promptly be hydrolyzed and photodissociation in water birds, honeybee low toxicity.
In Chinese patent, also there is no the report of metaflumizone Pesticidal combination.
Advantage of the present invention and good effect are that the insecticide with two kinds of different structures, the different mechanisms of action carries out composite, be control resistant insect, expansion insecticidal spectrum and the effective way that improves drug effect, the more important thing is and avoid or delay insect to the generation of new composition metaflumizone resistance.
Summary of the invention
The object of the invention is to: for preventing the drug-fast generation of metaflumizone, provide the Pesticidal combination that contains metaflumizone of a kind of efficient, wide spectrum, low toxicity, with cause harm multiple lepidoptera pest on paddy rice, vegetables, fruit tree, cotton etc. of control.
To achieve these goals, technical scheme of the present invention is: a kind of Pesticidal combination that contains metaflumizone is provided, wherein, formed by two kinds of active components A and B, the A composition is metaflumizone, the B composition is a kind of of beta-cypermethrin, Cyhalothrin, Profenofos, chlorophos, diafenthiuron, pleocidin, worm hydrazides, HEXAFLUMURON, chlorfenapyr, pyridaben, Acetamiprid, Mobucin, dimehypo, cartap, and it is 1:50～10:1 that described two kinds of active components A and B form mass ratio.
Preferably, described two kinds of active components A and B mass accumulation percentage account for 1%～60% of gross mass.
Preferably, this Pesticidal combination contains the auxiliary compositions such as normally used solvent, auxiliary agent, carrier in pesticidal preparations, is convenient to make the formulation that is suitable for using, as wetting powder, water dispersible granules, suspending agent.
Preferably, the lepidoptera pest of the crops such as these Pesticidal combination control vegetables, paddy rice, fruit tree, cotton is as diamond-back moth, beet armyworm, rice leaf roller, striped rice borer, paddy stem borer, leaf roller, cotton bollworm etc.
The invention has the advantages that: the present invention utilizes two kinds of active constituents to be mixed, according to calculate the co-toxicity coefficient CTC value of mixture with the abundant method of Sun Yun, show to have obvious synergistic effect, can reduce the effective ingredient dosage, delay insect to the drug-fast generation of new medicament chlorine worm benzoyl.
Embodiment
The invention will be further described below in conjunction with preferred embodiment, but the present invention never is limited to following embodiment.In following examples, each component percentage composition all by quality ratio.
FORMULATION EXAMPLE 1
4% metaflumizone beta-cypermethrin, namely both mass ratioes are the wettable mealiness pulvis of 1:3
Above-mentioned each component is fully mixed afterwards, carried out drying, cooling, fine grinding, both must be mixed with 4% metaflumizone beta-cypermethrin wetting powder.
Described metaflumizone and beta-cypermethrin mass accumulation percentage account for 4% of gross mass.
FORMULATION EXAMPLE 2
5% metaflumizone Cyhalothrin, namely both mass ratioes are the wettable mealiness pulvis of 1:1
After above-mentioned each component is fully mixed, carry out drying, cooling, levigate, both must be mixed with 5% metaflumizone Cyhalothrin wetting powder.
Described metaflumizone and Cyhalothrin mass accumulation percentage account for 5% of gross mass.
FORMULATION EXAMPLE 3
11% metaflumizone Profenofos, namely both mass ratioes are the water dispersible granules of 1:10
After above-mentioned each component is fully mixed, carry out granulation after ultra-fine grinding, drying, screening, both made 11% metaflumizone Profenofos water dispersible granules.
Described metaflumizone and Profenofos mass accumulation percentage account for 11% of gross mass.
FORMULATION EXAMPLE 4
17.5% metaflumizone chlorophos, namely both mass ratioes are the wetting powder of 1:6
After above-mentioned each component is fully mixed, carry out drying, cooling, levigate, both must be mixed with 17.5% metaflumizone chlorophos wetting powder.
Described metaflumizone and chlorophos mass accumulation percentage account for 17.5% of gross mass.
FORMULATION EXAMPLE 5
30% metaflumizone diafenthiuron, namely both mass ratioes are the suspending agent of 1:5
Above-mentioned each component is fully mixed, add water 25g and fully grind, water complements to 100g, is mixed with 30% metaflumizone diafenthiuron suspending agent.
Described metaflumizone and diafenthiuron mass accumulation percentage account for 30% of gross mass.
FORMULATION EXAMPLE 6
4.5% metaflumizone pleocidin, namely both mass ratioes are the suspending agent of 2:1
Above-mentioned each component is fully mixed, add water 25g and fully grind, water complements to 100g, is mixed with 4.5% metaflumizone pleocidin suspension.
Described metaflumizone and pleocidin mass accumulation percentage account for 4.5% of gross mass.
FORMULATION EXAMPLE 7
10% metaflumizone worm hydrazides, namely both mass ratioes are the suspending agent of 1:1
Above-mentioned each component is fully mixed, add water 25g and fully grind, water complements to 100g, is mixed with 10% metaflumizone Tebufenozide suspending agent.
Described metaflumizone and worm hydrazides mass accumulation percentage account for 10% of gross mass.
FORMULATION EXAMPLE 8
10% metaflumizone HEXAFLUMURON, namely both mass ratioes are the wetting powder of 1:1
After above-mentioned each component is fully mixed, carry out drying, cooling, levigate, both be mixed with 10% metaflumizone HEXAFLUMURON wetting powder.
Described metaflumizone and HEXAFLUMURON mass accumulation percentage account for 10% of gross mass.
FORMULATION EXAMPLE 9
15% metaflumizone chlorfenapyr, namely both mass ratioes are the suspending agent of 1:2
After above-mentioned each component is fully mixed, add water 25g and fully grind, water complements to 100g, is mixed with 15% metaflumizone chlorfenapyr suspending agent.
Described metaflumizone and chlorfenapyr mass accumulation percentage account for 15% of gross mass.
FORMULATION EXAMPLE 10
20% metaflumizone pyridaben, namely both mass ratioes are the water dispersible granules of 1:3
After above-mentioned each component is fully mixed, mixture is carried out granulation after ultra-fine grinding, drying, screening, both made 20% metaflumizone pyridaben water dispersible granules.
Described metaflumizone and pyridaben mass accumulation percentage account for 20% of gross mass.
FORMULATION EXAMPLE 11
20% metaflumizone Acetamiprid, namely both mass ratioes are the wetting powder of 1:1
After above-mentioned each component is fully mixed, carry out drying, cooling, levigate, both must be mixed with 20% metaflumizone acetamiprid wettable powder.
Described metaflumizone and Acetamiprid mass accumulation percentage account for 20% of gross mass.
FORMULATION EXAMPLE 12
20% metaflumizone Mobucin, namely both mass ratioes are the wetting powder of 1:3
After above-mentioned each component is fully mixed, carry out drying, cooling, levigate, both must be mixed with 20% metaflumizone Mobucin wetting powder.
Described metaflumizone and Mobucin mass accumulation percentage account for 20% of gross mass.
FORMULATION EXAMPLE 13
2% metaflumizone dimehypo, namely both mass ratioes are the suspending agent of 1:1
After above-mentioned each component is fully mixed, add water 25g and fully grind, water complements to 100g, is mixed with 2% metaflumizone dimehypo suspending agent.
Described metaflumizone and dimehypo mass accumulation percentage account for 2% of gross mass.
FORMULATION EXAMPLE 14
41% metaflumizone cartap, namely both mass ratioes are the wetting powder of 1:40
After above-mentioned each component is fully mixed, carry out drying, cooling, levigate, both must be mixed with 41% metaflumizone cartap wetting powder.
Described metaflumizone and cartap mass accumulation percentage account for 41% of gross mass.
This Pesticidal combination contains the auxiliary compositions such as normally used solvent, auxiliary agent, carrier in pesticidal preparations, is convenient to make the formulation that is suitable for using, as wetting powder, water dispersible granules, suspending agent.The lepidoptera pest of the crops such as these Pesticidal combination control vegetables, paddy rice, fruit tree, cotton is as diamond-back moth, beet armyworm, rice leaf roller, striped rice borer, paddy stem borer, leaf roller, cotton bollworm etc.
By a large amount of screening tests, find that the composition that contains metaflumizone has obvious synergistic function to diamond-back moth, specifically is illustrated with following biological example.
Biological Examples one:
The examination worm is adopted the indoor diamond-back moth that connects the generation raising, and concrete grammar is:
Medicament preparation: test former medicine and provide former medicine for producer, made the preparation that needs by I company's product development center Drug Manufacturing Room.Before test, be mixed with different concentration gradients according to different mix proportion schemes, 6 concentration of every proportioning.
Connect worm: put into 3, cabbage leaves dish of the same size in the 9cm culture dish, select 3 instar larvaes of neat uniformity in culture dish, every ware connects 30 of worms.
Spraying: spray under 50PSI pressure with the POTT spray tower, spray 2 milliliters of medicines at every turn.Leaf dish positive and negative is all sprayed.Spraying is from low concentration, and blank sprays the equivalent clear water.Each proportioning arranges 6 concentration gradients, three wares of every concentration spray.Put into after having sprayed the insectary (25 ± 1 ℃, 12H/12H) in.
Investigation statistics: process and check dead borer population after 48 hours, with Abbott formula calculation correction lethality.The appliance computer program is obtained each for examination single dose lethal concentration of 50 LC50, and method abundant according to Sun Yun calculated the co-toxicity coefficient (CTC value) of mixed medicament, the CTC value greater than 120 be synergistic effect.Circular is as follows:
Setting a kind of single dose (A) is the standard single dose, and specifying its toxicity index (TI) is 100:
The percentage of TI * single dose in mixture of the theoretical toxicity index (TTI) of mixture=each single dose of Σ
Result of the test sees Table 1, table 2.
The virulence of each reagent agent of table 1 to diamond-back moth
| Medicament | LC50(ppm) |
| Metaflumizone | 13.56 |
| Beta-cypermethrin | 223.02 |
| Cyhalothrin | 218.24 |
| Profenofos | 272.46 |
| Chlorophos | 284.43 |
| Diafenthiuron | 59.50 |
| Pleocidin | 15.65 |
| The worm hydrazides | 78.90 |
| HEXAFLUMURON | 10.26 |
| Chlorfenapyr | 8.22 |
| Pyridaben | 340.25 |
| Acetamiprid | 380.76 |
| Mobucin | 270.11 |
| Dimehypo | 340.37 |
| Cartap | 355.41 |
Table 2 contains the composition of metaflumizone to the composite effect of diamond-back moth
| Composition | Ratio | LC50(ppm) | CTC |
| Metaflumizone+beta-cypermethrin | 1:3 | 35.77 | 128.23 |
| Metaflumizone+Cyhalothrin | 1:1 | 18.81 | 135.77 |
| Metaflumizone+Profenofos | 1:10 | 67.43 | 147.65 |
| Metaflumizone+chlorophos | 1:6 | 55.77 | 132.35 |
[0104]?
| Metaflumizone+diafenthiuron | 1:5 | 30.06 | 126.48 |
| Metaflumizone+pleocidin | 2:1 | 11.05 | 128.42 |
| Metaflumizone+worm hydrazides | 1:1 | 15.95 | 145.13 |
| Metaflumizone+HEXAFLUMURON | 1:1 | 8.45 | 138.28 |
| Metaflumizone+chlorfenapyr | 1:2 | 6.99 | 135.43 |
| Metaflumizone+pyridaben | 1:3 | 39.70 | 122.04 |
| Metaflumizone+Acetamiprid | 1:1 | 18.96 | 138.15 |
| Metaflumizone+Mobucin | 1:3 | 36.66 | 128.62 |
| Metaflumizone+dimehypo | 1:1 | 20.06 | 130.05 |
| Metaflumizone+cartap | 1:40 | 172.02 | 127.76 |
As can be seen from Table 1 and Table 2, with composite each composition of metaflumizone to the co-toxicity coefficient (CTC) of diamond-back moth all greater than 120, show, each composite effect all has synergistic effect to diamond-back moth.Each complex composition is processed into suitable formulation, but the multiple lepidoptera pests such as effectively preventing diamond-back moth, rice leaf roller, cotton bollworm, beet armyworm, prodenia litura, lima bean pod borer, leaf roller.Because diafenthiuron, chlorfenapyr and pyridaben have acaricidal activity, Acetamiprid and Mobucin, flea beetle, aleyrodid, plant hopper etc. there is good activity, so the built agent of the built agent of the built agent of metaflumizone and diafenthiuron or chlorfenapyr or pyridaben, metaflumizone and Acetamiprid, metaflumizone and Mobucin is except effective control lepidoptera pest, other insect also there is certain effect, enlarge insecticidal spectrum, reduced the medication number of times of agricultural chemicals.For the new medicament metaflumizone, delayed the generation of pest resistance to insecticide, can be used for preventing and treating the various pests that vegetables, paddy rice, cotton, fruit tree etc. occur.
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| CN101773132B (en) * | 2010-03-18 | 2012-08-29 | 陕西上格之路生物科学有限公司 | Insecticide composition containing metaflumizone |
| CN103283745A (en) * | 2012-03-01 | 2013-09-11 | 陕西韦尔奇作物保护有限公司 | Insecticide composition containing metaflumizone |
| CN103283772A (en) * | 2012-03-03 | 2013-09-11 | 陕西韦尔奇作物保护有限公司 | Pesticide composition containing metaflumizone and pyrethroids |
| CN105994270A (en) * | 2012-03-12 | 2016-10-12 | 陕西韦尔奇作物保护有限公司 | Chromafenozide-containing insecticidal composition |
| CN102630694A (en) * | 2012-03-31 | 2012-08-15 | 广西田园生化股份有限公司 | Ultralow-volume liquid containing metaflumizone and nicotine insecticide |
| CN102630688A (en) * | 2012-03-31 | 2012-08-15 | 广西田园生化股份有限公司 | Ultra low volume concentrate containing metaflumizone and carbamate insecticides |
| CN102657213B (en) * | 2012-04-16 | 2014-07-23 | 广西田园生化股份有限公司 | Ultra-low volume liquor containing metaflumizone and esbiothrin pesticides |
| CN102657204A (en) * | 2012-05-11 | 2012-09-12 | 湖南农业大学 | Synergetic insecticide composition |
| CN102894007A (en) * | 2012-11-19 | 2013-01-30 | 江苏钟山化工有限公司 | Synergistic insecticidal composition containing metaflumizone and beta-cypermethrin and application thereof |
| CN103053599A (en) * | 2012-12-29 | 2013-04-24 | 广东中迅农科股份有限公司 | Pesticide composition of metaflumizone and beta-cyfluthrin |
| CN103503912A (en) * | 2013-09-29 | 2014-01-15 | 江志鑫 | Acaricidal composite composition |
| CN103651458B (en) * | 2013-12-10 | 2016-08-17 | 南通纺都置业有限公司 | A kind of multiple killing teichomycin and the suspension emulsion of Mobucin and application |
| CN104082325B (en) * | 2014-06-19 | 2016-09-14 | 广东中迅农科股份有限公司 | A kind of containing chlorine chlorfenapyr with the Pesticidal combination of metaflumizone |
| CN105660673A (en) * | 2014-11-18 | 2016-06-15 | 陕西美邦农药有限公司 | Agricultural chemical insecticidal composition containing penflumizone |
| CN105613545A (en) * | 2014-11-26 | 2016-06-01 | 陕西美邦农药有限公司 | Insecticidal composition containing pentaflumizone and nereistoxin |
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| CN1471822A (en) * | 2003-07-15 | 2004-02-04 | 江苏省农药研究所有限公司 | Composition with insect killing activity |
| WO2009035908A1 (en) * | 2007-09-11 | 2009-03-19 | Wyeth | Compositions and their use for the treatment of protozoal infections comprising metaflumi zone |
| CN101564038B (en) * | 2009-04-23 | 2012-11-21 | 广东中迅农科股份有限公司 | Insecticidal composition containing metaflumizone |
| CN101524087A (en) * | 2009-04-28 | 2009-09-09 | 北京燕化永乐农药有限公司 | Pesticide composition containing metaflumizone and acephate |
| CN101584343B (en) * | 2009-07-06 | 2013-04-24 | 巴斯夫（中国）有限公司 | Metaflumizone and chlorpyrifos mixture insecticide |
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Change date: 20250122 Registration number: 2019460000007 Pledgor after: Hainan Zhengye Biotechnology Co.,Ltd. Pledgor before: HAINAN ZHENGYE ZHONGNONG HIGH TECHNOLOGY Co.,Ltd. |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20160413 Pledgee: Bank of Hainan Limited by Share Ltd. Pledgor: Hainan Zhengye Biotechnology Co.,Ltd. Registration number: 2019460000007 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Insecticidal composition containing cyhalothrin and insecticides such as imidacloprid or fenitrothion Granted publication date: 20160413 Pledgee: Bank of Hainan Limited by Share Ltd. Pledgor: Hainan Zhengye Biotechnology Co.,Ltd. Registration number: Y2025980008313 |