CN103084227A - Device for chemical experiment aiming at magnetic composite particle turbid liquid separation procedure - Google Patents
Device for chemical experiment aiming at magnetic composite particle turbid liquid separation procedure Download PDFInfo
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- CN103084227A CN103084227A CN2012105869781A CN201210586978A CN103084227A CN 103084227 A CN103084227 A CN 103084227A CN 2012105869781 A CN2012105869781 A CN 2012105869781A CN 201210586978 A CN201210586978 A CN 201210586978A CN 103084227 A CN103084227 A CN 103084227A
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- permanent magnet
- packaging bag
- magnetic
- velcro
- composite particle
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- 239000011246 composite particle Substances 0.000 title claims abstract description 23
- 238000002474 experimental method Methods 0.000 title claims abstract description 20
- 239000000126 substance Substances 0.000 title claims abstract description 14
- 238000000034 method Methods 0.000 title abstract description 11
- 238000000926 separation method Methods 0.000 title abstract 3
- 239000007788 liquid Substances 0.000 title description 6
- 238000004806 packaging method and process Methods 0.000 claims abstract description 46
- 239000000463 material Substances 0.000 claims abstract description 23
- 239000000725 suspension Substances 0.000 claims abstract description 18
- 238000002955 isolation Methods 0.000 claims abstract description 11
- 239000002131 composite material Substances 0.000 claims abstract 2
- 239000011859 microparticle Substances 0.000 claims abstract 2
- 238000007789 sealing Methods 0.000 claims description 14
- 239000011521 glass Substances 0.000 claims description 11
- 239000011247 coating layer Substances 0.000 claims description 10
- 229910001047 Hard ferrite Inorganic materials 0.000 claims description 5
- 229910001172 neodymium magnet Inorganic materials 0.000 claims description 5
- 239000004033 plastic Substances 0.000 claims description 3
- 229920003023 plastic Polymers 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000000919 ceramic Substances 0.000 claims 1
- 238000004458 analytical method Methods 0.000 abstract description 11
- 230000008569 process Effects 0.000 abstract description 7
- 239000003795 chemical substances by application Substances 0.000 description 14
- 239000012528 membrane Substances 0.000 description 8
- 238000010219 correlation analysis Methods 0.000 description 4
- 230000005415 magnetization Effects 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 238000005204 segregation Methods 0.000 description 3
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- 238000000576 coating method Methods 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- -1 pottery Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
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- 238000012546 transfer Methods 0.000 description 2
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 229940072056 alginate Drugs 0.000 description 1
- 235000010443 alginic acid Nutrition 0.000 description 1
- 229920000615 alginic acid Polymers 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
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- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical class OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 1
- 229920005547 polycyclic aromatic hydrocarbon Polymers 0.000 description 1
- 125000005575 polycyclic aromatic hydrocarbon group Chemical group 0.000 description 1
- 238000004094 preconcentration Methods 0.000 description 1
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Images
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- Laminated Bodies (AREA)
Abstract
本发明涉及一种针对磁性复合微粒悬浊液离析程序的化学实验用装置，属于分析测试领域。分析化学实验室中现有的惯常的针对磁性复合微粒悬浊液的离析用装置过于简陋，以至于影响到了相关离析操作的便捷性，本案针对该问题。本案用其相互粘搭状态易于拆解的两条粘扣带一左一右地从两侧连接内含永磁体的柔性材质的兜状的永磁体封装袋，将它束缚定位在非磁性容器侧壁外表面上，其附着形态的轮廓状似腰包；如此，在以磁场离析捕集剂的整个操作过程中，免除了相关分析实验操作人员用手拿捏、按压定位滑溜的永磁体这样一种紧张度较高的动作；应用本案装置，相关分析实验人员可以相对放松地进行相关磁性复合微粒悬浊液离析操作。
The invention relates to a chemical experiment device for the separation procedure of magnetic composite microparticle suspension, which belongs to the field of analysis and testing. The existing customary isolation devices for magnetic composite particle suspensions in analytical chemistry laboratories are too simple to affect the convenience of related isolation operations. This case addresses this problem. In this case, two Velcro tapes, which are easily disassembled, are used to connect the pocket-shaped permanent magnet packaging bag of flexible material containing permanent magnets from both sides, and bind it to the side of the non-magnetic container. On the outer surface of the wall, the outline of its attachment form is like a waist bag; in this way, during the whole operation process of isolating the trapping agent with a magnetic field, the relevant analysis experiment operators are relieved of the tension of holding and pressing the slippery permanent magnet with their hands. With the application of the device in this case, the relevant analysis and experiment personnel can perform the separation operation of the relevant magnetic composite particle suspension in a relatively relaxed manner.
Description
Technical field
The present invention relates to a kind of chemical experiment device for magnetic composite particle suspension segregation program, belong to the analytical test field.
Background technology
In the analytical test experimental work, for the water analysis object, with micron order or nano level magnetic composite particle trapping agent absorption object, then separate with permanent magnet the magnetic composite particle trapping agent that has adsorbed object, adsorbed from this through elution program again the magnetic composite particle trapping agent of object and isolated object, for Instrumental Analysis sample introduction thereafter, this is the standby sample means of a kind of very efficient Instrumental Analysis among at present flourish.
Described standby sample means can also be expressed as the pre-treatment means.
The standby sample means of described Instrumental Analysis take analytical test as purpose only relate to tens of milligrams usually to micron order or the nano level magnetic composite particle trapping agent of number gram, and its volume of water analysis object that relates to also only has hundreds of milliliters usually to the amount of several liters.
micron order or nano level magnetic composite particle trapping agent are scattered among the water analysis object, form suspension, with the close non magnetic container that holds this suspension of permanent magnet, effect due to magnetic field, magnetic composite particle trapping agent in suspension carries its object that captures and moves, assembles to high magnetic field area together, and this moves, accumulation process continues approximately tens of seconds to the number minutes, this case institute problems of concern just appears at this trapping agent isolation operation link: situation about recognizing at present is, experiment and correlation analysis operating personnel are being affectedly bashful the naked permanent magnet without any additional equipment to remove to be adjacent to described non magnetic container with hand, always like this in whole trapping agent isolation operation process, at toppling over of thereafter remaining liquid, in the discharging operation process, also like this, namely, be affectedly bashful on the other hand, press permanent magnet, the described non magnetic container of another holds, carry out toppling over of remaining liquid with a kind of relatively nervous operating attitude, discharging operation.The normally hundreds of milliliters of described non magnetic container are to several glass beakers that rise capacity, comprise above-mentioned the whole trapping agent isolation operation process that remaining liquid topples over, equally be smooth glass and so on container wall on hard, smooth permanent magnet by being pressed in hand, carry out simultaneously described remaining liquid and topple over action, its operation tensity is apparent.If be engaged in for a long time the operation that such needs tighten one's nerve, so, it will cause to experiment and correlation analysis personnel's physical and mental health recessive infringement.
Therefore, how improving the simple operation of magnetic composite particle suspension segregation link in relevant chemical experiment, is a problem that merits attention.
Its research and development and the application in the analytical test field of related magnetic composite particle trapping agent as an example, can be 201210099400.3 Chinese invention patent application case referring to application number.
About its research and development and the application in the analytical test field of magnetic composite particle trapping agent, also can be referring to following paper information: Zhang S X, Niu H Y, Cai Y Q, et al.Barium alginate cagedFe
3O
4@C18magnetic nanoparticles for the pre-concentration of polycyclicaromatic hydrocarbons and phthalate esters from environmental watersamples[J] .Analytica Chimica Acta, 2010,665:167-175.
Summary of the invention
Technical problem to be solved by this invention is, for the present situation not easily of magnetic composite particle suspension segregation link operation in above-mentioned chemical experiment, research and develop a kind of magnetic composite particle suspension that is applicable to chemical laboratory that helps to address this problem and emanate and use device.
the present invention is by the described technical problem of following solution, this scheme provides a kind of chemical experiment device for magnetic composite particle suspension segregation program, this installs its construction package and comprises tubbiness, the non magnetic container of cup-shaped or ampuliform, described its material of non magnetic container is glass, pottery, plastics or stainless steel, and, tabular, block, strip, disc-shaped, cylindric, the permanent magnet of pie or ring-type, this permanent magnet is Nd-Fe-B permanent magnet or hard ferrite permanent magnet, emphasis is, the structure of this device also comprises the permanent magnet packaging bag of flexible material, this permanent magnet packaging bag is satchel or pocketed thing, offer on this permanent magnet packaging bag for the sack to the inner filling of this permanent magnet packaging bag permanent magnet, described permanent magnet is the inside that filling is installed in this permanent magnet packaging bag, and, article two, magic tape, the both sides of this permanent magnet packaging bag respectively connect a described magic tape, its position that is connected with the permanent magnet packaging bag of the described magic tape of each is a termination at this magic tape, the remainder of these two magic tapes like as two arms around filling the span of a man's arms on the sidewall outer surface of described non magnetic container, these two magic tapes and mutual sticking taking, described magic tape has another name called the glochild pull stap, mutually sticking these two magic tapes of taking its pull strength and cause described permanent magnet packaging bag to be close on the sidewall outer surface of this non magnetic container, one of function of these two magic tapes is that described permanent magnet packaging bag is positioned on the sidewall outer surface of this non magnetic container together with its content constraint, two of the function of these two magic tapes is to give this apparatus structure dismounting mobility convenient to both, attach around ground these two magic tapes be installed on described non magnetic container side wall outer surface together with its overall profile shape of described permanent magnet packaging bag that combines with these two magic tapes like purse, this permanent magnet packaging bag can sticking taken the releasing of its state and removed from non magnetic container side wall outer surface in the lump with these two magic tapes along with described together with its content.
Itself art-recognized meanings of described flexible material one word is known.
The flexible material that can be selected for the described permanent magnet packaging bag of preparation is of a great variety, can be selected arbitrarily as required.Related flexible material market is on sale.
Itself art-recognized meanings of described magic tape one word is known for the manufacturing professional of magic tape.
Preferred magic tape is to have the flexible stretch sticking cingulum of degree of tightness.It is on sale that this has the flexible stretch sticking cingulum of degree of tightness market.Described degree of tightness elasticity is optional.
Described permanent magnet can be the permanent magnet of cited any shape, and its direction of magnetization can be any selected direction of magnetization, and its material can be any in Nd-Fe-B permanent magnet or hard ferrite permanent magnet.
Described non magnetic container can be the non magnetic container of cited any material, and described non magnetic container can be the non magnetic container of cited any shape, and still, preferably this non magnetic container is glass beaker.
For reaching better this case target, can also install rubber membrane or application elastic coating layer attaching of this permanent magnet packaging bag on that face of non magnetic container, this rubber membrane or elastic coating layer thickness between 0.5 millimeter and 3.0 millimeters, the function of this rubber membrane or elastic coating layer is to increase frictional resistance and contain by this its sliding transfer of permanent magnet packaging bag.
The material markets such as related rubber membrane and elastic coating are on sale.
The described non magnetic word of this case refers to its material does not here have serious obstruction for penetrating of magnetic field, rather than says that its material is to the response of magnetic field without any magnitude.
The sack of permanent magnet packaging bag can take various ways to seal, described sealing mode for example: slide fastener sealing mode, sticking sealing mode or the hasp sealing mode of taking.
Its assembly of this device of this case can also comprise some annexes, described annex for example: be used for to observe the Special illuminating light of magnetic trapping agent absorption running process terminal point, as shot-light etc.; Described annex is also for example: be used for determining the Chronograph timepiece of magnetic trapping agent absorption running process terminal point, as timer clock etc.; Described annex is more for example: the glass bar that uses with the liquid cooperation that inclines etc.; Described annex is optional.
Advantage of the present invention is, mutually stickingly take two magic tapes that state is easy to disassemble and permanent magnet is fettered in the lump together with the packaging bag of the pocketed of its flexible material be positioned on non magnetic container side wall outer surface with it, its profile shape that adheres to form is like purse, so, in the whole operating process with magnetic field segregation trapping agent, exempted experiment and correlation analysis operating personnel and be affectedly bashful, pressed the smooth higher action of a kind of like this tensity of permanent magnet in location with hand; Use this case device, experiment and correlation analysis personnel can relatively carry out magnetic composite particle suspension isolation operation with loosening.
Its structure of this case device and be easy to the dismounting; This structure is a kind of structure that facilitates independent assortment to use.
Description of drawings
Fig. 1 is the schematic diagram of this case apparatus structure.
In figure, 1,7 is respectively the different magic tape in two-strip structure position, the 2nd, the permanent magnet packaging bag of flexible material, the 3rd, permanent magnet, the 4th, non magnetic container, the 5th, slide fastener, the 6th, the pull head of slide fastener, two of the left and right in figure arrow are indicated two of left and right magic tape mutually to close up and are mutually glued the direction of action of taking.
The specific embodiment
in this case embodiment that Fig. 1 shows, this installs its construction package and comprises tubbiness, the non magnetic container 4 of cup-shaped or ampuliform, described non magnetic container 4 its materials are glass, pottery, plastics or stainless steel, and, tabular, block, strip, disc-shaped, cylindric, the permanent magnet 3 of pie or ring-type, this permanent magnet 3 is Nd-Fe-B permanent magnet or hard ferrite permanent magnet, emphasis is, the structure of this device also comprises the permanent magnet packaging bag 2 of flexible material, this permanent magnet packaging bag 2 is satchel or pocketed thing, offer on this permanent magnet packaging bag 2 for the sack to the inner filling permanent magnet 3 of this permanent magnet packaging bag 2, described permanent magnet 3 is the inside that filling is installed in this permanent magnet packaging bag 2, and, article two, magic tape, these two magic tapes are respectively magic tape 1 and magic tape 7, the both sides of this permanent magnet packaging bag 2 are connected with magic tape 1 and magic tape 7 respectively, magic tape 1 and magic tape 7 are all to be connected with permanent magnet packaging bag 2 with separately a termination, the remainder of magic tape 1 and magic tape 7 like as two arms around filling the span of a man's arms on the sidewall outer surface of described non magnetic container 4, magic tape 1 and magic tape 7 and mutual sticking taking, described magic tape has another name called the glochild pull stap, mutually the sticking magic tape 1 of taking and magic tape 7 its pull strength and cause described permanent magnet packaging bag 2 to be close on the sidewall outer surface of this non magnetic container 4, one of function of magic tape 1 and magic tape 7 is that described permanent magnet packaging bag 2 is positioned on the sidewall outer surface of this non magnetic container 4 together with its content constraint, two of the function of magic tape 1 and magic tape 7 is to give this apparatus structure dismounting mobility convenient to both, attach around ground the magic tape 1 be installed on described non magnetic container 4 sidewall outer surfaces and magic tape 7 together with described permanent magnet packaging bag 2 its overall profile shapes that combine with magic tape 1 and magic tape 7 like purse, this permanent magnet packaging bag 2 can sticking taken the releasing of its state and removed from non magnetic container 4 sidewall outer surfaces in the lump with magic tape 1 and magic tape 7 along with described together with its content.
This is a kind of apparatus structure that is easy to disassemble.
Itself art-recognized meanings of related flexible material one word is known.
Described magic tape market is on sale.
Implement related magic tape and preferably have the flexible stretch sticking cingulum of degree of tightness.Stretch sticking cingulum market is on sale.
Described permanent magnet 3 can be the permanent magnet of cited any shape, and its direction of magnetization can be any selected direction of magnetization, and its material can be any in Nd-Fe-B permanent magnet or hard ferrite permanent magnet.
Described non magnetic container 1 can be the non magnetic container of cited any material, and described non magnetic container 1 can be the non magnetic container of cited any shape, and still, preferably this non magnetic container 1 is glass beaker.The instant glass beaker of non magnetic container of showing in legend; Glass beaker is only an example.
Among enforcement, can also install rubber membrane or application elastic coating layer attaching of this permanent magnet packaging bag 2 on that face of non magnetic container 1, this rubber membrane or elastic coating layer thickness between 0.5 millimeter and 3.0 millimeters, any selected one-tenth-value thickness 1/10 in this thickness range is all the thickness enforcement value that this case allows, and the function of this rubber membrane or elastic coating layer is increase frictional resistance and contain by this permanent magnet packaging bag 2 its sliding transfers.
The material markets such as related rubber membrane and elastic coating are on sale.
Do not show this rubber layer or elastic coating layer in legend.
Described permanent magnet packaging bag can utilize any selected flexible material to make by techniques such as sewing, bonding, splicings.
The sack of permanent magnet packaging bag 2 can take various ways to seal, described sealing mode for example: slide fastener sealing mode, sticking sealing mode or the hasp sealing mode of taking.What show in legend is slide fastener sealing mode, and this is only an example; The sealing mode of described sack is not limited to this; Other sealing mode of described sack is not showed with legend.
This case device also is applicable to the indoor experiment of chemical experiment certainly with itself a small amount of preparation procedure of magnetic composite particle material, also is suitable for the isolation operation of the magnetic composite particle suspension under this situation.
The concrete enforcement of this case is not limited to this case accompanying drawing legend.
Claims (5)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210586978.1A CN103084227B (en) | 2012-12-13 | 2012-12-13 | Chemical experiment device for magnetic composite particle suspension isolation procedures |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210586978.1A CN103084227B (en) | 2012-12-13 | 2012-12-13 | Chemical experiment device for magnetic composite particle suspension isolation procedures |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103084227A true CN103084227A (en) | 2013-05-08 |
| CN103084227B CN103084227B (en) | 2016-08-03 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210586978.1A Expired - Fee Related CN103084227B (en) | 2012-12-13 | 2012-12-13 | Chemical experiment device for magnetic composite particle suspension isolation procedures |
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| Country | Link |
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| CN (1) | CN103084227B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112570050A (en) * | 2019-09-27 | 2021-03-30 | 厦门大学 | Fluid transportation control system and method |
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|---|---|---|---|---|
| US4793973A (en) * | 1985-07-08 | 1988-12-27 | Serono Diagnostic Partners | Container for adding antibodies or antigens to a biological liquid |
| US5647994A (en) * | 1993-06-21 | 1997-07-15 | Labsystems Oy | Method and apparatus for separating magnetic particles from a solution |
| WO2004011146A1 (en) * | 2002-07-29 | 2004-02-05 | Campbell Andrew T | A device and method for manipulating magnetic particles |
| US7105357B1 (en) * | 1998-05-27 | 2006-09-12 | Max-Planck-Gesellschaft Zur Forderung Der Wissenschaften E. V. | Method and device for processing extremely small substance quantities |
| CN101010592A (en) * | 2004-07-26 | 2007-08-01 | 拜奥默里克斯有限公司 | Device and method for separating, mixing and concentrating magnetic particles with a fluid and use thereof in purification methods |
| CN101423973A (en) * | 2008-10-21 | 2009-05-06 | 宁波大学 | Experimental device applying to researching intervention of magnetic field conditional for complex crystallization |
| CN201345894Y (en) * | 2008-12-12 | 2009-11-18 | 司徒家超 | Self-service feeding inflatable bag |
| CN201375355Y (en) * | 2009-04-02 | 2010-01-06 | 赵延 | Heat insulating cup cover |
| CN201602296U (en) * | 2009-12-31 | 2010-10-13 | 徐琨 | Extensible water cup heat preservation bag |
| CN102362183A (en) * | 2009-03-23 | 2012-02-22 | 皇家飞利浦电子股份有限公司 | Manipulation of magnetic particles in a biological sample |
-
2012
- 2012-12-13 CN CN201210586978.1A patent/CN103084227B/en not_active Expired - Fee Related
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4793973A (en) * | 1985-07-08 | 1988-12-27 | Serono Diagnostic Partners | Container for adding antibodies or antigens to a biological liquid |
| US5647994A (en) * | 1993-06-21 | 1997-07-15 | Labsystems Oy | Method and apparatus for separating magnetic particles from a solution |
| US7105357B1 (en) * | 1998-05-27 | 2006-09-12 | Max-Planck-Gesellschaft Zur Forderung Der Wissenschaften E. V. | Method and device for processing extremely small substance quantities |
| WO2004011146A1 (en) * | 2002-07-29 | 2004-02-05 | Campbell Andrew T | A device and method for manipulating magnetic particles |
| CN101010592A (en) * | 2004-07-26 | 2007-08-01 | 拜奥默里克斯有限公司 | Device and method for separating, mixing and concentrating magnetic particles with a fluid and use thereof in purification methods |
| CN101423973A (en) * | 2008-10-21 | 2009-05-06 | 宁波大学 | Experimental device applying to researching intervention of magnetic field conditional for complex crystallization |
| CN201345894Y (en) * | 2008-12-12 | 2009-11-18 | 司徒家超 | Self-service feeding inflatable bag |
| CN102362183A (en) * | 2009-03-23 | 2012-02-22 | 皇家飞利浦电子股份有限公司 | Manipulation of magnetic particles in a biological sample |
| CN201375355Y (en) * | 2009-04-02 | 2010-01-06 | 赵延 | Heat insulating cup cover |
| CN201602296U (en) * | 2009-12-31 | 2010-10-13 | 徐琨 | Extensible water cup heat preservation bag |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112570050A (en) * | 2019-09-27 | 2021-03-30 | 厦门大学 | Fluid transportation control system and method |
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| Publication number | Publication date |
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| CN103084227B (en) | 2016-08-03 |
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