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CN103084135A - Horizontal impinging stream reactor - Google Patents

Horizontal impinging stream reactor Download PDF

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Publication number
CN103084135A
CN103084135A CN2013100474889A CN201310047488A CN103084135A CN 103084135 A CN103084135 A CN 103084135A CN 2013100474889 A CN2013100474889 A CN 2013100474889A CN 201310047488 A CN201310047488 A CN 201310047488A CN 103084135 A CN103084135 A CN 103084135A
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shell
pump
reactor
nozzle
guide shell
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CN103084135B (en
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杨侠
余蓓
罗燕
郭钊
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Wuhan Institute of Technology
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Abstract

本发明公开了一种卧式撞击流反应器,包括反应器壳体、进料管、卸料管、导流筒、泵和循环管道,所述进料管和卸料管设置在反应器壳体上,所述反应器壳体内水平同轴对称设置一对导流筒,导流筒用于引导物料分别被泵抽吸,其入口相对设置且间隔有第一设定距离以形成物料抽吸区,其出口分别通过循环管道与泵的入口相连通,其特征在于:所述反应器壳体上在导流筒之间沿垂直导流筒轴向的方向同轴对称设置一对喷嘴,喷嘴的出口相对设置且间隔有第二设定距离以形成物料相向撞击区,其入口通过循环管道与泵的出口相连通。它不仅提高了物料混合的效率,而且增强了反应器的稳定性和连续性,同时缩短了返混时间,结构简单,具有良好的经济性能。

Figure 201310047488

The invention discloses a horizontal impingement flow reactor, which comprises a reactor shell, a feed pipe, a discharge pipe, a draft tube, a pump and a circulation pipe, and the feed pipe and the discharge pipe are arranged on the reactor shell In terms of body, a pair of guide cylinders are arranged horizontally and coaxially and symmetrically in the reactor shell. The guide cylinders are used to guide the materials to be sucked by the pump respectively. zone, the outlets of which are respectively connected to the inlet of the pump through circulation pipes, and are characterized in that a pair of nozzles are coaxially and symmetrically arranged between the guide cylinders on the reactor shell along the direction vertical to the axial direction of the guide cylinders, and the nozzles The outlets of the outlets are arranged oppositely and separated by a second set distance to form a material-facing collision zone, and the inlets thereof communicate with the outlet of the pump through a circulation pipeline. It not only improves the efficiency of material mixing, but also enhances the stability and continuity of the reactor, and at the same time shortens the back-mixing time, and has a simple structure and good economic performance.

Figure 201310047488

Description

一种卧式撞击流反应器A horizontal impingement flow reactor

技术领域   technical field

本发明涉及一种化工领域的反应器,具体涉及一种用于液相反应过程的循环撞击流反应器。 The invention relates to a reactor in the field of chemical industry, in particular to a circulating impingement flow reactor used in a liquid phase reaction process.

背景技术  Background technique

撞击流反应器是一种应用于化工领域的新型反应器,利用两股高速流体相向撞击达到增大传热、传质速率的目的,已成功应用于吸收、混合、传热及结晶等化工过程。目前大多数的撞击流反应器是在导流筒内设置螺旋桨结构或者利用动力源等使得流体加速并相向撞击,设置螺旋桨结构的反应器虽然能达到混合强化的目的,但因安装螺旋桨的电机轴是悬臂结构,容易导致整个装置的不稳定和易损伤,由此减少反应器的使用寿命,利用动力源,比如通过泵的作用,给予物料一定的初速度,使其轴向相向撞击加强混合作用,但因泵连接的循环管道入口位于反应器底部,撞击混合后物料返混的时间太长,影响混合效率。 The impinging flow reactor is a new type of reactor used in the chemical industry. It uses two high-speed fluids to collide with each other to increase the heat transfer and mass transfer rate. It has been successfully used in chemical processes such as absorption, mixing, heat transfer and crystallization. . At present, most impinging flow reactors are equipped with a propeller structure in the guide tube or use a power source to accelerate the fluid and collide with each other. Although the reactor with the propeller structure can achieve the purpose of mixing and strengthening, the motor shaft installed with the propeller It is a cantilever structure, which can easily lead to instability and easy damage of the whole device, thus reducing the service life of the reactor. Using the power source, such as through the action of a pump, to give the material a certain initial velocity, so that the axial direction impacts each other to strengthen the mixing effect. , but because the inlet of the circulation pipe connected to the pump is located at the bottom of the reactor, the time for the material to mix back after impact mixing is too long, which affects the mixing efficiency.

发明内容  Invention content

本发明所要解决的技术问题在于提供一种卧式撞击流反应器,它不仅保持了螺旋桨结构撞击流反应器的高效混合性能,而且增强了反应器的稳定性和连续性,它结构简单,降低成本,易操作维修,同时缩短了返混时间,提高生产效率。 The technical problem to be solved by the present invention is to provide a horizontal impingement flow reactor, which not only maintains the high-efficiency mixing performance of the impingement flow reactor with propeller structure, but also enhances the stability and continuity of the reactor. It has a simple structure and reduces Low cost, easy operation and maintenance, while shortening the back-mixing time and improving production efficiency.

本发明为解决上述提出的问题所采取的技术方案是:包括反应器壳体、进料管、卸料管、第一导流筒、第二导流筒、第一泵、第二泵和循环管道,所述进料管和卸料管设置在所述反应器壳体上,所述反应器壳体内水平同轴对称设置第一导流筒和第二导流筒,其特征在于:所述第一导流筒和第二导流筒用于引导物料分别被第一泵和第二泵抽吸,所述第一导流筒和第二导流筒的入口相对设置且间隔有第一设定距离以形成物料抽吸区,其出口分别通过循环管道与第一泵和第二泵的入口相连通;所述反应器壳体上在第一导流筒和第二导流筒之间同轴对称设置第一喷嘴和第二喷嘴,所述第一喷嘴和第二喷嘴的出口相对设置且间隔有第二设定距离以形成物料相向撞击区,其入口通过循环管道与第一泵和第二泵的出口相连通。 The technical scheme adopted by the present invention to solve the above-mentioned problems is: comprising a reactor shell, a feed pipe, a discharge pipe, a first flow guide cylinder, a second flow guide cylinder, a first pump, a second pump and a circulation The pipe, the feed pipe and the discharge pipe are arranged on the reactor shell, and the first guide tube and the second guide tube are arranged horizontally and coaxially symmetrically in the reactor shell, which is characterized in that: The first guide cylinder and the second guide cylinder are used to guide the material to be sucked by the first pump and the second pump respectively, and the inlets of the first guide cylinder and the second guide cylinder are arranged oppositely and separated by a first setting A certain distance is used to form a material suction area, and its outlets are respectively connected to the inlets of the first pump and the second pump through circulation pipes; The first nozzle and the second nozzle are arranged axially symmetrically. The outlets of the first nozzle and the second nozzle are arranged opposite to each other and separated by a second set distance to form a material impact area. The outlets of the two pumps are connected.

按上述技术方案,所述第一导流筒和第二导流筒位于所述反应器壳体内的高度方向的中央位置,所述第一喷嘴和第二喷嘴位于所述反应器壳体上的长度方向的中央位置。 According to the above technical solution, the first guide tube and the second guide tube are located at the center of the reactor shell in the height direction, and the first nozzle and the second nozzle are located at the center of the reactor shell. Center position in the length direction.

按上述技术方案,所述物料抽吸区和物料相向撞击区相重合。 According to the above technical solution, the material suction area and the material facing impact area overlap.

按上述技术方案,所述反应器壳体上在第一导流筒和第二导流筒之间并排设置多对喷嘴,所述每对喷嘴同轴对置。 According to the above technical solution, multiple pairs of nozzles are arranged side by side between the first flow guide cylinder and the second flow guide cylinder on the reactor shell, and each pair of nozzles is coaxially opposed.

按上述技术方案,所述进料管设置在反应器壳体的上端。 According to the above technical solution, the feed pipe is arranged at the upper end of the reactor shell.

按上述技术方案,所述卸料管设置在反应器壳体的下端。 According to the above technical solution, the discharge pipe is arranged at the lower end of the reactor shell.

按上述技术方案,所述反应器壳体的形状为圆筒形,所述反应器壳体水平放置。 According to the above technical solution, the shape of the reactor shell is cylindrical, and the reactor shell is placed horizontally.

本发明的有益效果在于:通过设置一对喷嘴形成物料相向撞击区,使得物料经喷嘴喷出相向撞击进行混合,混合后的物料在泵的抽吸作用下沿导流筒再次快速进入循环管道,再次经喷嘴喷出相向撞击进行混合,如此循环,达到高效混合物料的效果。它不仅保持了螺旋桨结构撞击流反应器的高效混合性能,而且增强了反应器的稳定性和连续性,它结构简单,降低成本,易操作维修,同时缩短了返混时间,提高生产效率,具有良好的经济性能。 The beneficial effect of the present invention is that: a pair of nozzles is arranged to form a material collision area, so that the materials are sprayed out of the nozzles and mixed, and the mixed materials are quickly entered into the circulation pipe again along the guide tube under the suction of the pump. Once again, the nozzles are sprayed against each other for mixing, and this cycle achieves the effect of mixing materials efficiently. It not only maintains the high-efficiency mixing performance of the impingement flow reactor with propeller structure, but also enhances the stability and continuity of the reactor. It has a simple structure, reduces costs, is easy to operate and maintain, and at the same time shortens the back-mixing time and improves production efficiency. Good economic performance.

为了进一步缩短返混时间,采用多对喷嘴,通过循环管道与泵和导流筒形成多路循环管路,提高了物料混合效率。 In order to further shorten the back-mixing time, multiple pairs of nozzles are used to form multi-channel circulation pipelines through circulation pipelines, pumps and guide cylinders, which improves the mixing efficiency of materials.

附图说明  Description of drawings

图1为本发明设有一对喷嘴的实施例的结构示意图; Fig. 1 is the structural representation of the embodiment that the present invention is provided with a pair of nozzles;

图2是本发明设有两对喷组的实施例的结构示意图。 Fig. 2 is a structural schematic diagram of an embodiment of the present invention provided with two pairs of spray groups.

其中, 1进料管、2反应器壳体、3-1第一泵、3-2第二泵、4-1第一导流筒、4-2第二导流筒、5喷嘴、5-1第一喷嘴、5-2第二喷嘴、6循环管道、7卸料管。 Among them, 1 feed pipe, 2 reactor shell, 3-1 first pump, 3-2 second pump, 4-1 first guide tube, 4-2 second guide tube, 5 nozzle, 5- 1 first nozzle, 5-2 second nozzle, 6 circulation pipe, 7 discharge pipe.

具体实施方式 Detailed ways

为了使本发明的目的、技术方案及优点更加清楚明白,以下结合附图及实施例,对本发明进行进一步详细说明。应当理解,此处所描述的具体实施例仅用以解释本发明,并不用于限定本发明。 In order to make the object, technical solution and advantages of the present invention clearer, the present invention will be further described in detail below in conjunction with the accompanying drawings and embodiments. It should be understood that the specific embodiments described here are only used to explain the present invention, not to limit the present invention.

如图1所示,卧式撞击流反应器包括反应器壳体2、进料管1、卸料管7、第一导流筒4-1、第二导流筒4-2、第一泵5-1、第二泵5-2和循环管道6。反应器壳体2的形状为圆筒形,且水平放置,进料管1和卸料管7设置在反应器壳体2上,进料管1设置在反应器壳体2的上端,卸料管7设置在反应器壳体2的下端。反应器壳体2内水平同轴对称设置第一导流筒4-1和第二导流筒4-2,第一导流筒4-1和第二导流筒4-2用于引导物料分别被第一泵3-1和第二泵3-2抽吸,第一导流筒4-1和第二导流筒4-2的入口相对设置且间隔有第一设定距离以形成物料抽吸区,其出口分别通过循环管道6与第一泵3-1和第二泵3-2的入口相连通,反应器壳体2上在第一导流筒4-1和第二导流筒4-2之间沿垂直第一导流筒4-1和第二导流筒4-2轴向的方向同轴对称设置第一喷嘴5-1和第二喷嘴5-2,第一喷嘴5-1和第二喷嘴5-2的出口相对设置且间隔有第二设定距离以形成物料相向撞击区,其入口通过循环管道6与第一泵3-1和第二泵3-2的出口相连通。物料抽吸区和物料相向撞击区相重合。所述第一导流筒和第二导流筒位于所述反应器壳体内的高度方向的中央位置,所述第一喷嘴和第二喷嘴位于所述反应器壳体上的长度方向的中央位置。 As shown in Figure 1, the horizontal impinging flow reactor includes a reactor shell 2, a feed pipe 1, a discharge pipe 7, a first flow guide cylinder 4-1, a second flow guide cylinder 4-2, a first pump 5-1, the second pump 5-2 and the circulation pipeline 6. The shape of the reactor shell 2 is cylindrical and placed horizontally. The feed pipe 1 and the discharge pipe 7 are arranged on the reactor shell 2. The feed pipe 1 is arranged on the upper end of the reactor shell 2. A pipe 7 is provided at the lower end of the reactor shell 2 . In the reactor shell 2, a first flow guide cylinder 4-1 and a second flow guide cylinder 4-2 are arranged horizontally and coaxially symmetrically, and the first flow guide cylinder 4-1 and the second flow guide cylinder 4-2 are used to guide materials Suctioned by the first pump 3-1 and the second pump 3-2 respectively, the inlets of the first guide cylinder 4-1 and the second guide cylinder 4-2 are oppositely arranged and separated by a first set distance to form material In the suction area, its outlet is respectively connected to the inlet of the first pump 3-1 and the second pump 3-2 through the circulation pipe 6, and the reactor shell 2 is connected with the first guide tube 4-1 and the second guide tube 4-1. The first nozzle 5-1 and the second nozzle 5-2 are coaxially symmetrically arranged between the cylinders 4-2 along the direction perpendicular to the axial direction of the first guide cylinder 4-1 and the second guide cylinder 4-2, and the first nozzle 5-1 and the outlet of the second nozzle 5-2 are arranged opposite to each other and separated by a second set distance to form a material impact area, and its inlet passes through the circulation pipeline 6 and the first pump 3-1 and the second pump 3-2. The exit is connected. The material suction area and the material impact area coincide. The first guide cylinder and the second guide cylinder are located at the central position of the reactor shell in the height direction, and the first nozzle and the second nozzle are located at the central position of the reactor shell in the length direction .

如图2所示,卧式撞击流反应器还可以在反应器壳体2上在第一导流筒4-1和第二导流筒4-2之间沿垂直第一导流筒4-1和第二导流筒4-2轴向的方向并排设置两对喷嘴5,每对喷嘴同轴对置,其余结构与图1所示的结构相同。喷嘴5的数量、大小及位置可以随生产要求进行设置。 As shown in Figure 2, the horizontal impingement flow reactor can also be placed on the reactor shell 2 between the first draft tube 4-1 and the second draft tube 4-2 along the vertical first draft tube 4- 1 and the second guide tube 4-2 are provided with two pairs of nozzles 5 side by side in the axial direction, each pair of nozzles is coaxially opposed, and the rest of the structure is the same as that shown in FIG. 1 . The quantity, size and position of nozzles 5 can be set according to production requirements.

本发明提供的撞击流反应器的工作流程如下:物料由进料管进入反应器壳体,在泵的抽吸作用下,物料经导流筒引导再经循环管道由喷嘴高速喷出并在喷嘴出口形成的物料相向撞击区相向撞击以使物料混合,混合后的物料在泵的抽吸作用下再次沿导流筒快速进入循环管道,再次由喷嘴高速喷出并相向撞击以使物料混合,如此循环,最后待物料充分混合均匀通过卸料管排出。 The working process of the impinging flow reactor provided by the present invention is as follows: the material enters the reactor shell from the feed pipe, and under the suction of the pump, the material is guided by the guide tube and then sprayed out at a high speed by the nozzle through the circulation pipe and discharged at the nozzle. The materials formed at the outlet collide against the impact area to make the materials mix. The mixed materials quickly enter the circulation pipe along the guide tube under the suction of the pump, and are ejected from the nozzle at high speed again and collide with each other to make the materials mix. Circulation, and finally the material is fully mixed and discharged through the discharge pipe.

本发明提供的撞击流反应器可以进行循环撞击,既可以是间歇式操作,也可以是连续性操作。 The impingement flow reactor provided by the present invention can carry out cyclical impingement, either batch operation or continuous operation.

应当理解的是,对本领域普通技术人员来说,可以根据上述说明加以改进或变换,而所有这些改进和变换都应属于本发明所附权利要求的保护范围。 It should be understood that those skilled in the art can make improvements or changes based on the above description, and all these improvements and changes should belong to the protection scope of the appended claims of the present invention.

Claims (7)

1. horizontal impact flow reactor, comprise reactor shell, feed pipe, discharge duct, the first guide shell, the second guide shell, the first pump, the second pump and circulating line, described feed pipe and discharge duct are arranged on described reactor shell, in described reactor shell, horizontal coaxial-symmetrical arranges the first guide shell and the second guide shell, it is characterized in that: described the first guide shell and the second guide shell are used for directing material respectively by the first pump and the suction of the second pump, the entrance of described the first guide shell and the second guide shell is oppositely arranged and is separated with the first setpoint distance to form the material suction district, the outlet of the first guide shell and the second guide shell is connected by the entrance of circulating line with the first pump and the second pump respectively, on described reactor shell between the first guide shell and the second guide shell coaxial-symmetrical the first nozzle and second nozzle are set, the outlet of described the first nozzle and second nozzle is oppositely arranged and is separated with the second setpoint distance to form material impingement region in opposite directions, and the entrance of the first nozzle and second nozzle is connected with the first pump and the second delivery side of pump by circulating line.
2. horizontal impact flow reactor according to claim 1, it is characterized in that: described the first guide shell and the second guide shell are positioned at the middle position of the short transverse of described reactor shell, and described the first nozzle and second nozzle are positioned at the middle position of the length direction on described reactor shell.
3. horizontal impact flow reactor according to claim 1, it is characterized in that: described material suction district and material impingement region in opposite directions coincide.
4. horizontal impact flow reactor according to claim 1 is characterized in that: be arranged side by side manyly to nozzle on described reactor shell between the first guide shell and the second guide shell, described every pair of nozzle is coaxial opposed.
5. horizontal impact flow reactor according to claim 1, it is characterized in that: described feed pipe is arranged on the upper end of reactor shell.
6. horizontal impact flow reactor according to claim 1, it is characterized in that: described discharge duct is arranged on the lower end of reactor shell.
7. horizontal impact flow reactor according to claim 1 is characterized in that: described reactor shell be shaped as cylindrical shape, described reactor shell horizontal positioned.
CN201310047488.9A 2013-02-06 2013-02-06 Horizontal impinging stream reactor Expired - Fee Related CN103084135B (en)

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CN110016374A (en) * 2019-04-25 2019-07-16 西南石油大学 Method and equipment for direct separation of H2S in natural gas by hydrate method at wellhead
CN110026146A (en) * 2019-03-14 2019-07-19 中北大学 A kind of rotary packed bed device and method for preparing benzaldehyde of percussion flow
CN110542490A (en) * 2019-09-18 2019-12-06 昆明理工大学 A non-isothermal micro-impingement flow reactor testing method and device
US10985300B2 (en) 2015-09-11 2021-04-20 Quan Ke Encapsulation method for flip chip

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US10985300B2 (en) 2015-09-11 2021-04-20 Quan Ke Encapsulation method for flip chip
CN110026146A (en) * 2019-03-14 2019-07-19 中北大学 A kind of rotary packed bed device and method for preparing benzaldehyde of percussion flow
CN110026146B (en) * 2019-03-14 2021-05-18 中北大学 A kind of device and method for preparing benzaldehyde by impinging flow rotating packed bed
CN110016374A (en) * 2019-04-25 2019-07-16 西南石油大学 Method and equipment for direct separation of H2S in natural gas by hydrate method at wellhead
CN110016374B (en) * 2019-04-25 2021-05-11 西南石油大学 Method and equipment for directly separating H2S in natural gas by hydrate method at well head
CN110542490A (en) * 2019-09-18 2019-12-06 昆明理工大学 A non-isothermal micro-impingement flow reactor testing method and device

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