CN102972865B - Preparation method of flavoring particles for cigarette filter tip by coating method, obtained product and use - Google Patents
Preparation method of flavoring particles for cigarette filter tip by coating method, obtained product and use Download PDFInfo
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- CN102972865B CN102972865B CN201210567396.9A CN201210567396A CN102972865B CN 102972865 B CN102972865 B CN 102972865B CN 201210567396 A CN201210567396 A CN 201210567396A CN 102972865 B CN102972865 B CN 102972865B
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- perfuming
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- cigarette filter
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- 239000002245 particle Substances 0.000 title claims abstract description 51
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 238000000576 coating method Methods 0.000 title claims abstract description 10
- 239000000463 material Substances 0.000 claims abstract description 39
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 28
- 238000000034 method Methods 0.000 claims abstract description 13
- 150000007524 organic acids Chemical class 0.000 claims abstract description 10
- 229920000620 organic polymer Polymers 0.000 claims abstract description 6
- 239000002904 solvent Substances 0.000 claims abstract description 5
- 239000011248 coating agent Substances 0.000 claims abstract description 4
- 239000002994 raw material Substances 0.000 claims abstract description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 13
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 11
- 238000007599 discharging Methods 0.000 claims description 11
- 241000208125 Nicotiana Species 0.000 claims description 10
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 9
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 8
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 6
- 235000002906 tartaric acid Nutrition 0.000 claims description 6
- 239000011975 tartaric acid Substances 0.000 claims description 6
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- 229920001800 Shellac Polymers 0.000 claims description 4
- ZLGIYFNHBLSMPS-ATJNOEHPSA-N shellac Chemical compound OCCCCCC(O)C(O)CCCCCCCC(O)=O.C1C23[C@H](C(O)=O)CCC2[C@](C)(CO)[C@@H]1C(C(O)=O)=C[C@@H]3O ZLGIYFNHBLSMPS-ATJNOEHPSA-N 0.000 claims description 4
- 239000004208 shellac Substances 0.000 claims description 4
- 229940113147 shellac Drugs 0.000 claims description 4
- 235000013874 shellac Nutrition 0.000 claims description 4
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 claims description 3
- 229910052808 lithium carbonate Inorganic materials 0.000 claims description 3
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 3
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 2
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 2
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 2
- 235000011090 malic acid Nutrition 0.000 claims description 2
- 239000001630 malic acid Substances 0.000 claims description 2
- 235000005985 organic acids Nutrition 0.000 claims description 2
- 229940072033 potash Drugs 0.000 claims description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 2
- 235000015320 potassium carbonate Nutrition 0.000 claims description 2
- 235000015165 citric acid Nutrition 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 7
- 239000000796 flavoring agent Substances 0.000 abstract description 2
- 235000019634 flavors Nutrition 0.000 abstract description 2
- 238000012216 screening Methods 0.000 abstract description 2
- 239000000779 smoke Substances 0.000 abstract description 2
- 230000000391 smoking effect Effects 0.000 abstract description 2
- 238000001035 drying Methods 0.000 abstract 2
- 238000002156 mixing Methods 0.000 abstract 1
- 230000003020 moisturizing effect Effects 0.000 abstract 1
- 230000002459 sustained effect Effects 0.000 abstract 1
- 239000002131 composite material Substances 0.000 description 8
- 230000015572 biosynthetic process Effects 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 239000011246 composite particle Substances 0.000 description 5
- 235000019441 ethanol Nutrition 0.000 description 5
- 239000003205 fragrance Substances 0.000 description 5
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- 229920006221 acetate fiber Polymers 0.000 description 3
- 239000003546 flue gas Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000009495 sugar coating Methods 0.000 description 2
- MIDXCONKKJTLDX-UHFFFAOYSA-N 3,5-dimethylcyclopentane-1,2-dione Chemical compound CC1CC(C)C(=O)C1=O MIDXCONKKJTLDX-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 241000233855 Orchidaceae Species 0.000 description 1
- 238000010669 acid-base reaction Methods 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 235000013736 caramel Nutrition 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 235000013409 condiments Nutrition 0.000 description 1
- 238000007596 consolidation process Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
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- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention relates to a preparation method of flavoring particles for a cigarette filter tip by a coating method, an obtained product and a use. According to the preparation method, a release base material and an organic polymer skeleton are used as main raw materials, and active release type cigarette flavoring particles are formed by processes including mixing, coating, granulating, curing, drying and the like, wherein the release base material is made from an organic acid and a release backing material; a flavoring curing agent is made from an anhydrous solvent, the organic polymer skeleton and a flavor; and the flavoring particles are obtained by rotary coating, drying and screening. According to the invention, the flavoring particles actively release flavoring materials and produce water after meeting a mainstream smoke, the reaction is sustained and stable, the cigarette style and the smoking quality can be enhanced, and the moisturizing effect is realized.
Description
[technical field]
The invention belongs to cigarette material technical field, the fragrant material of benefit particularly adding in cigarette filter and the preparation method of this material.
[background technology]
Lowering harm and decreasing coking problem is one of countries tobacco sixty-four dollar question.The first half of the year in 2011 whole nation cigarette list props up weighted average tar content and drops to below 11 milligrams, and part cigarette product tar content has dropped to below 10 milligrams.Also not rare on the cigarette market of 5 milligrams, 1 milligram even the cigarette of 0.1 milligram also come out.
For reaching the object of reducing tar and reducing harm, the technology industry such as filter tip, the fine composite filter of paper/vinegar, natural permeable degree tipping paper, online laser boring have been introduced.When their effectively reduce the harmful components in cigarette smoke, also can make the aspects such as original suction taste, mouthfeel, physiological strength of cigarette follow corresponding reduction.Especially the loss of fragrance matter and perfume quantity in cigarette, easily make taste lose original style, this just need to make up by adding other spices to carry out part, and one of effect of perfuming is when reducing cigarette harm, make up the loss of fragrance, to consumer, provide satisfied product.
Chinese invention patent 201010239046.0 discloses a kind of novel flavoring filter tip, choose diameter and cause fragrant particle in 20-40 object, by mouth rod forming machine, add equably 3 milligrams in the mouth rod tow of every millimeter described in, cause fragrant particle, make function mouth rod, described function mouth rod and the excellent Length Ratio by 10: 15 of base are rolled into flavoring filter tip by composite molding machine; Describedly cause fragrant particle and by following component, take by weight aluminosilicate and in comminutor, form as carrier: 4 parts of cloud and mist absolute oil; 1.5 parts of oak moss absolutes; 0.5 part of tree orchid essential oil; 4 parts of maltols; 15 parts of caramel colorants; 65 parts of propane diols; 10 parts, water.Yet through smokeing panel test, find that its flavouring effect is not ideal, inhale taste natural not, have comparatively significantly artificial fragrance breath.
[summary of the invention]
The inventor, through research, utilizes organic acid acid and carbonate mixture to meet water and reacts Heat of Formation or CO
2with the mechanism of water, set up flue gas Active Compensation system; Heat and CO
2while overflowing, can take the essence being added in soda acid particle out of reach flavor compensating effect, the generation of water has increased the effect that the moisture in flue gas reaches humectation; Due to the fragrance overflowing and the aerosol of moisture formation and the similitude of flue gas, make compensation effect more obvious.
For this reason, the invention provides a kind of coating method and prepare the method for perfuming particle for cigarette filter, step is as follows:
A, preparation discharge base-material: get respectively organic acid and be heated to be dried in 50-60 ℃ of baking oven with discharging bed material, in weight ratio take 1:2 ~ 3:2 through the organic acid of oven dry with discharge bed material, mix, obtain discharging base-material;
B, prepare perfuming curing agent: the anhydrous solvent and the organic polymer skeleton that in weight ratio, take 4:1 ~ 19:1, mix, obtain curing agent, then in weight ratio, take curing agent and the Zimbabwe's tobacco extract of 6:1 ~ 50:1, mix and obtain perfuming curing agent;
C, dressing: in weight ratio, take 7:30 ~ 1:2 perfuming curing agent and discharge base-material, pour in coating pan release base-material into rotation and mix and according to aforementioned proportion, perfuming curing agent is slowly sprayed into after 10min until sprayed completely, continue to make wet granular after rotation dressing 1h;
D, described wet granular is dried in the baking oven of 50-60 ℃, cross 100 mesh sieves, obtain described cigarette filter perfuming particle.
In the present invention, Zimbabwe's tobacco extract is can buy the product of acquisition on market, Zimbabwe's tobacco extract that for example Huabao Edible Essence & Condiment (Shanghai) sells.
In the present invention, the dressing of step c is undertaken by sugar coating machine, the BY-Chufa-type sugarcoating machine of for example selecting Jiangyin City Kang He Machinery Manufacturing Co., Ltd. to manufacture.
In the present invention, described organic acid is selected from one or more organic acids in citric acid, citric acid, tartaric acid and/or malic acid.
Described release bed material is selected from one or more release bed materials of sodium acid carbonate, saleratus, sodium carbonate, lithium carbonate and/or potash.
In step a, gained is discharged to base-material and sieve, choose more than particle diameter 40 orders particle as discharging base-material, as the raw material of step c.
Described anhydrous solvent is selected from ethanol, propane diols and/or acetone.
Described organic polymer skeleton is selected from lac, acetate fiber and/or PLA.
The invention still further relates to cigarette filter application in cigarette filter with perfuming particle that above-mentioned preparation method obtains, preferably with cigarette-filter tow length gauge, the addition of described perfuming particle is 0.5-35mg/mm.
Similarly, the perfuming particle that the present invention prepares can also be applied to that binary is compound, in tri compound, cavity composite filter.
Method of the present invention is simple, cost of manufacture is lower, and gained perfuming particle has consolidation homogeneous, the mellow and full advantage such as smooth.Utilize the cigarette filter that the inventive method prepares with material, to have nontoxic.Slowly disintegration after particle and main flume effect, produces CO
2can carry out active perfuming, can guarantee that fragrance uniformity, acid-base reaction stable and suction taste produce water and reach humectation effect as perfuming carrier with water.
[accompanying drawing explanation]
Fig. 1 is that coating method of the present invention is prepared the method step schematic diagram of perfuming particle for cigarette filter.
[specific embodiment]
By following embodiment, can understand better the present invention.
Embodiment 1
Make perfuming particle:
Take the citric acid 100g of having dried, tartaric acid 30g and saleratus 20g, sodium acid carbonate 100g, sodium carbonate 50g mixes, and obtains discharging base-material perfuming curing agent.
By acetone 135g and acetate fiber 12g, PLA 3g, Zimbabwe tobacco extract 3g, dissolving mixes, and obtains perfuming curing agent.
Perfuming curing agent is sprayed in the release base-material preparing and rotates dressing, then 50 ℃ of oven dry of baking oven, screening is chosen grade and as cigarette, is mended fragrant particle at 40 to 60 order particles.
Cigarette is mended to fragrant particle and by addition 25mg/mm, be applied to composite particles filter stick formation, make ternary cavity composite filter.Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, the active release type particle filter stick that tipping preparation is complete.
Cigarette is placed in to 22 ℃, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 ℃ of room temperatures, humidity 60% that ventilates, under environment, evaluate.
Embodiment 2
Make perfuming particle:
Take the citric acid 60g of having dried, tartaric acid 100g and saleratus 140g mix, and obtain discharging base-material perfuming curing agent.
By absolute ethyl alcohol 48g and shellac 12g Zimbabwe tobacco extract 10g, dissolving mixes, and obtains perfuming curing agent.
Perfuming curing agent is sprayed in the release base-material prepare and rotates dressing, and 50 ℃ of oven dry of gained particle baking oven, finally sieve, and choose grade and obtain described cigarette and mend fragrant particle with interior at 20 to 40 orders.
Gained particle is applied to composite particles filter stick formation by addition 2mg/mm, makes ternary cavity composite filter.Select the finished cigarettes of quality between 0.880-0.900g, as Yunnan Yuxi Cigarette Factory produces red plum board, remove original filter stick, the active release type particle filter stick that tipping preparation is complete.
Cigarette is placed in to 22 ℃, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 ℃ of room temperatures, humidity 60% that ventilates, under environment, evaluate again.
Embodiment 3
Make perfuming particle:
Take the citric acid 50g of having dried, citric acid 90g, sodium carbonate 60g, lithium carbonate 100g mixes, and obtains discharging base-material perfuming curing agent.
By absolute ethyl alcohol 108g and shellac 12g Zimbabwe tobacco extract (alcohol extracting part) 6g, dissolving mixes, and obtains perfuming curing agent.
Perfuming curing agent is sprayed in the release base-material preparing and rotates dressing.60 ℃, gained particle baking oven baking 1 hour, finally sieves, and chooses grade and obtains described cigarette and mend fragrant particle with interior at 20 to 40 orders.
Gained particle is applied to composite particles filter stick formation by addition 20mg/mm, makes ternary cavity composite filter.Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, the active release type particle filter stick that tipping preparation is complete.
Cigarette is placed in to 22 ℃, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 ℃ of room temperatures, humidity 60% that ventilates, under environment, evaluate again.
Embodiment 4
Make perfuming particle:
Take the tartaric acid 180g of having dried, sodium acid carbonate 120g mixes, and obtains discharging base-material perfuming curing agent.
By acetone 114g and acetate fiber 6g Zimbabwe tobacco extract (alcohol extracting part) 10g, dissolving mixes, and obtains perfuming curing agent.
Perfuming curing agent is sprayed in the release base-material preparing and rotates dressing;
By 60 ℃ of oven dry of gained particle baking oven, finally sieve, choose grade and obtain described cigarette and mend fragrant material with interior at 20 to 40 orders.
Gained particle is applied to composite particles filter stick formation by addition 2mg/mm, makes ternary cavity composite filter.
Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, the active release type particle filter stick that tipping preparation is complete.
Then cigarette is placed in to 22 ℃, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 ℃ of room temperatures, humidity 60% that ventilates, under environment, evaluate again.
Embodiment 5
Make perfuming particle:
Take the tartaric acid 130g of having dried, sodium acid carbonate 130g, sodium carbonate 60g mixes, and obtains discharging base-material perfuming curing agent.
Ethanol 114g and shellac 6g Zimbabwe tobacco extract (alcohol extracting part) 6g are dissolved also, and dissolving mixes, and obtains perfuming curing agent.
Perfuming curing agent is sprayed in the release base-material preparing and rotates dressing;
By 50 ℃, gained particle baking oven baking 2 hours, finally sieve, choose grade and obtain described cigarette and mend fragrant particle with interior at 20 to 40 orders.
Gained particle is applied to composite particles filter stick formation by addition 20mg/mm, makes ternary cavity composite filter.
Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, the active release type particle filter stick that tipping preparation is complete.
Cigarette is placed in to 22 ℃, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 ℃ of room temperatures, humidity 60% that ventilates, under environment, evaluate again.Smoking result is in Table 1.
Table 1
Claims (7)
1. coating method is prepared the method for perfuming particle for cigarette filter, it is characterized in that step is as follows:
A, preparation discharge base-material: get respectively organic acid and be heated to be dried in 50-60 ℃ of baking oven with discharging bed material, in weight ratio take 1:2～3:2 through the organic acid of oven dry with discharge bed material, mix, obtain discharging base-material;
B, prepare perfuming curing agent: the anhydrous solvent and the organic polymer skeleton that in weight ratio, take 4:1～19:1, mix, obtain curing agent, then in weight ratio, take curing agent and the Zimbabwe's tobacco extract of 6:1～50:1, mix and obtain perfuming curing agent; Described organic polymer skeleton is selected from lac or shellac;
C, dressing: in weight ratio, take 7:30～1:2 perfuming curing agent and discharge base-material, pour in coating pan release base-material into rotation and mix and according to aforementioned proportion, perfuming curing agent is slowly sprayed into after 10min until sprayed completely, continue to make wet granular after rotation dressing 1h;
D, described wet granular is dried in the baking oven of 50-60 ℃, cross 100 mesh sieves, obtain described cigarette filter perfuming particle.
2. method according to claim 1, is characterized in that described organic acid is selected from one or more organic acids in citric acid, citric acid, tartaric acid and malic acid.
3. method according to claim 1, is characterized in that described release bed material is selected from one or more release bed materials of sodium acid carbonate, saleratus, sodium carbonate, lithium carbonate and potash.
4. method according to claim 1, is characterized in that in step a, gained being discharged to base-material sieves, and chooses more than particle diameter 40 orders particle as discharging base-material, as the raw material of step c.
5. method according to claim 1, is characterized in that described anhydrous solvent elects ethanol, propane diols and/or acetone as.
6. the cigarette filter that in claim 1-5, described in any one claim, method obtains is the application in cigarette filter with perfuming particle.
7. the cigarette filter that in claim 1-5, described in any one claim, method obtains is the application in cigarette filter with perfuming particle, it is characterized in that with cigarette filter length gauge, and the addition of described perfuming particle is 0.5-35mg/mm.
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| CN109588774B (en) * | 2018-12-07 | 2021-08-13 | 云南中烟新材料科技有限公司 | Tea filter tip particles capable of prolonging aroma retention time and preparation method thereof |
| CN109497612B (en) * | 2018-12-12 | 2021-03-16 | 湖北中烟工业有限责任公司 | A heat-not-burn cigarette holder with tea aroma |
| CN110801049B (en) * | 2019-11-07 | 2022-02-01 | 云南中烟工业有限责任公司 | Cigarette filter tip aroma sustained-release particles and preparation method thereof |
| CN112772971B (en) * | 2019-11-11 | 2022-08-16 | 云南恩典科技产业发展有限公司 | Fragrant bead for hollow large-particle filter stick and preparation method thereof |
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| CN102533445A (en) * | 2012-02-05 | 2012-07-04 | 云南正邦生物技术有限公司 | Method for preparing active release type cigarette flavor complementing particles |
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