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CN102972861B - A kind of fire-cured tobacco type electronic cigarette tobacco liquid - Google Patents

A kind of fire-cured tobacco type electronic cigarette tobacco liquid Download PDF

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Publication number
CN102972861B
CN102972861B CN201110263484.5A CN201110263484A CN102972861B CN 102972861 B CN102972861 B CN 102972861B CN 201110263484 A CN201110263484 A CN 201110263484A CN 102972861 B CN102972861 B CN 102972861B
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China
Prior art keywords
tobacco
electronic cigarette
fire
type electronic
cured
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Application number
CN201110263484.5A
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Chinese (zh)
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CN102972861A (en
Inventor
姚继徳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hengxin Hongtu International Holdings Co ltd
Hengxin Yongji Technology Shenzhen Co Ltd
Original Assignee
Shenzhen Hangsen Star Technology Co Ltd
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Priority to CN201110263484.5A priority Critical patent/CN102972861B/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention provides a kind of fire-cured tobacco type electronic cigarette tobacco liquid.This fire-cured tobacco type electronic cigarette tobacco liquid, comprise the component of following quality proportioning: Yunnan Flue-cured Tobacco extract 5-50%, tobacco ketone 1035? 1-10%, tobacco alcohol 1036? 1-10%, tobacco essence 0.5-5%, natural nicotine 0.1-2.5%, medical glycerine 5-25%, distilled water 1-10%, edible alcohol 1-15%, surplus is propane diols.According to fire-cured tobacco type electronic cigarette tobacco liquid of the present invention, the traditional substitute of tobacco being beneficial to health meeting Chinese smoker needs is provided, there is the Yunnan Flue-cured Tobacco fragrance that nature is strong, inhale taste graceful fine and smooth, fragrance is abundant to be met, and strength is moderate, pleasant impression is pure, Hui Tian promotes the production of body fluid, and harmful substance is few, is beneficial to smoker healthy.

Description

A kind of fire-cured tobacco type electronic cigarette tobacco liquid
Technical field
The present invention relates to electronic cigarette, particularly relate to a kind of fire-cured tobacco type electronic cigarette tobacco liquid.
Background technology
In recent years, electronic cigarette obtains in the world extensively to be approved and achieves great development, people have generally had science and objectively judgement more to electronic cigarette, and the progress of electronic cigarette product self is also being accelerated and promoting this industry towards optimum and healthy future development.Electronic cigarette mainly comprises smoking set and cigarette bullet, is mounted with tobacco juice in cigarette bullet, by smoking set, tobacco juice is atomized and produces smoking effect, can get rid of the larger material of traditional nicotinism and have the substitution effect of traditional smoking.But, existing electronic cigarette tobacco liquid, or the taste belonging to that import does not meet Chinese smoker, or containing more harmful components in tobacco juice, be unfavorable for the health of smoker.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of fire-cured tobacco type electronic cigarette tobacco tar is provided.
For realizing above object, the technical solution used in the present invention is:
A kind of fire-cured tobacco type electronic cigarette tobacco liquid, comprise the component of following quality proportioning: Yunnan Flue-cured Tobacco extract 5-50%, tobacco ketone 10351-10%, tobacco alcohol 10361-10%, tobacco essence 0.5-5%, natural nicotine 0.1-2.5%, medical glycerine 5-25%, distilled water 1-10%, edible alcohol 1-15%, surplus is propane diols.
In the preferred technical scheme of one, comprise the component of following quality proportioning: Yunnan Flue-cured Tobacco extract 5-20%, tobacco ketone 10352-10%, tobacco alcohol 10363-8%, tobacco essence 1-2%, natural nicotine 0.5-1%, medical glycerine 18-20%, distilled water 2-5%, edible alcohol 1-2%, surplus propane diols.
The purity of described natural nicotine is greater than 98%.
The ethanol content of described edible alcohol is greater than 95%.
Described propane diols is the special propane diols of food flavor.
Beneficial effect of the present invention: provide the traditional substitute of tobacco being beneficial to health meeting Chinese smoker needs, have the Yunnan Flue-cured Tobacco fragrance that nature is strong, inhales taste graceful fine and smooth, fragrance is abundant to be met, and strength is moderate, and pleasant impression is pure, Hui Tian promotes the production of body fluid, and harmful substance is few, is beneficial to smoker healthy.
Detailed description of the invention
In the present invention, the extraction preparation method of Yunnan Flue-cured Tobacco extract, tobacco ketone 1035 and tobacco alcohol 1036: the Yunnan Flue-cured Tobacco tobacco leaf getting natural ageing in 3 years, according to tobacco leaf and mixed solvent (glycerine: propane diols: alcohol: water=1: 2: 3: 4) ratio of 1: 10 feeds intake, conventional heating (heating-up temperature 80-85 DEG C) Effect of Alcohol Extracting Procedureto Total is adopted to extract 6 hours in rustless steel container, filter after cool to room temperature, filtrate is Yunnan Flue-cured Tobacco extract.Get the Yunnan Flue-cured Tobacco tobacco leaf (moisture requirement 12.5%) of natural ageing in more than 3 years, sieve through 100 mesh sieve after pulverizing, add benzinum (the boiling range 60-90 DEG C) heating and refluxing extraction 3 hours (Extracting temperature 80 ± 2 DEG C) of 10 times of weight, cooled and filtered, filter residue adds 5 times of benzinums again and extracts filtration by above-mentioned technique, merges twice petroleum ether extract.Mixed petroleum ether extract is concentrated, obtains the tobacco extract A of oily, extract A is taken out filtration afterwards with freezing 24 hours (subzero 10 degree) after the absolute ethyl alcohol back dissolving of 10 times, filtrate heating is concentrated to obtain extract B.What extract B is adopted on molecular distillation equipment following process conditions respectively carries out molecular clock: extract B is at 0.15Mpa, and 175 DEG C are carried out molecular clock, and steaming thing is C, and residue is D; Residue D is at 0.10Mpa, and 220 DEG C are carried out molecular clock, and steaming thing is E, and residue is F; Residue F is at 0.08Mpa, and 250 DEG C are carried out molecular clock, and steaming thing is G, and residue is H.Test by analysis, steaming thing C main component is natural nicotine, content >=75%, high-purity nicotine of the acquisition more than 98.5% that can be used for purifying further.Steaming thing E main component is the mixture that nerol, linalool, benzyl carbinol etc. are rich in alcohols, and total alcohol content >=30%, by this mixture called after tobacco alcohol 1036.Steaming thing G main component is the mixture of ketone compounds, by this mixture called after tobacco ketone 1035, wherein Megastigmatrienone content >=2%, damascenone content >=1.5%, oxidation isophorone content >=1%, the composition that other content is greater than 0.1% also has geranyl acetone, 2,3-diacetyl, damascone solanone.
Example 1
The formula of fire-cured tobacco type electronic cigarette 1# tobacco tar is (quality is than content): Yunnan Flue-cured Tobacco extract accounts for 20%, tobacco ketone 1035 accounts for 5%, tobacco alcohol 1036 accounts for 3%, tobacco essence 1% (uses the special aromatising prods of electronic cigarette tobacco tar of Yuxi De Xin Bioisystech Co., Ltd development here, product type YN001), natural nicotine (purity is greater than 98%) accounts for 0.5%, medical glycerine accounts for 20%, distilled water accounts for 5%, edible alcohol (content 95%) accounts for 2%, and surplus is the special propane diols of food flavor.Mixing after above-mentioned raw materials weighs according to fixed proportion and sequencing, stirs and is packaged in Brown Glass Brown glass bottles and jars only after 30 minutes, gets supernatant liquor (1# tobacco tar) and be directly added in electronic cigarette device to be atomized and suck after quiet 72 hours.
Example 2
The formula of fire-cured tobacco type electronic cigarette 2# tobacco tar is (quality is than content): Yunnan Flue-cured Tobacco extract accounts for 10%, tobacco ketone 1035 accounts for 2%, tobacco alcohol 1036 accounts for 8%, tobacco essence 1% (uses the special aromatising prods of electronic cigarette tobacco tar of Yuxi De Xin Bioisystech Co., Ltd development here, product type YN001), natural nicotine (purity is greater than 98%) accounts for 0.8%, medical glycerine accounts for 18%, distilled water accounts for 2%, edible alcohol (content 95%) accounts for 2%, and surplus is the special propane diols of food flavor.Mixing after above-mentioned raw materials weighs according to fixed proportion and sequencing, stirs and is packaged in Brown Glass Brown glass bottles and jars only after 30 minutes, gets supernatant liquor (2# tobacco tar) and be directly added in electronic cigarette device to be atomized and suck after quiet 72 hours.
Example 3
The formula of fire-cured tobacco type electronic cigarette 3# tobacco tar is (quality is than content): Yunnan Flue-cured Tobacco extract accounts for 5%, tobacco ketone 1035 accounts for 10%, tobacco alcohol 1036 accounts for 5%, tobacco essence 2% (uses the special aromatising prods of electronic cigarette tobacco tar of Yuxi De Xin Bioisystech Co., Ltd development here, product type YN001), natural nicotine (purity is greater than 98%) accounts for 1%, medical glycerine accounts for 20%, distilled water accounts for 3%, edible alcohol (content 95%) accounts for 1%, and surplus is the special propane diols of food flavor.Mixing after above-mentioned raw materials weighs according to fixed proportion and sequencing, stirs and is packaged in Brown Glass Brown glass bottles and jars only after 30 minutes, gets supernatant liquor (3# tobacco tar) and be directly added in electronic cigarette device to be atomized and suck after quiet 72 hours.
Above content is in conjunction with concrete preferred embodiment further description made for the present invention, can not assert that specific embodiment of the invention is confined to these explanations.For general technical staff of the technical field of the invention, without departing from the inventive concept of the premise, make concrete change or change and all belong to protection scope of the present invention.

Claims (5)

1. a fire-cured tobacco type electronic cigarette tobacco liquid, it is characterized in that the component comprising following quality proportioning: Yunnan Flue-cured Tobacco extract 5-50%, tobacco ketone 10351-10%, tobacco alcohol 10361-10%, tobacco essence 0.5-5%, natural nicotine 0.1-2.5%, medical glycerine 5-25%, distilled water 1-10%, edible alcohol 1-15%, surplus is propane diols; Wherein, the mixture of tobacco ketone 1035 to be main component be ketone compounds, Megastigmatrienone content >=2%, damascenone content >=1.5%, oxidation isophorone content >=1%, the composition that other content is greater than 0.1% also has geranyl acetone, 2,3-diacetyl, damascone solanone; Wherein, the mixture that tobacco alcohol 1036 is main component is nerol, linalool, benzyl carbinol are rich in alcohols, total alcohol content >=30%.
2. fire-cured tobacco type electronic cigarette tobacco liquid according to claim 1, it is characterized in that the component comprising following quality proportioning: Yunnan Flue-cured Tobacco extract 5-20%, tobacco ketone 10352-10%, tobacco alcohol 10363-8%, tobacco essence 1-2%, natural nicotine 0.5-1%, medical glycerine 18-20%, distilled water 2-5%, edible alcohol 1-2%, surplus propane diols.
3. fire-cured tobacco type electronic cigarette tobacco liquid according to claim 1 and 2, is characterized in that: the purity of described natural nicotine is greater than 98%.
4. fire-cured tobacco type electronic cigarette tobacco liquid according to claim 1 and 2, is characterized in that: the ethanol content of described edible alcohol is greater than 95%.
5. fire-cured tobacco type electronic cigarette tobacco liquid according to claim 1 and 2, is characterized in that: described propane diols is the special propane diols of food flavor.
CN201110263484.5A 2011-09-07 2011-09-07 A kind of fire-cured tobacco type electronic cigarette tobacco liquid Active CN102972861B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI732965B (en) 2017-10-18 2021-07-11 日商日本煙草產業股份有限公司 Battery unit, flavor inhaling device, power charger, method for detecting abnormality of power supply, and computer program product

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* Cited by examiner, † Cited by third party
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CN103919281A (en) * 2013-01-16 2014-07-16 深圳瀚星翔科技有限公司 Electronic cigarette atomized liquid
WO2014177693A1 (en) * 2013-05-02 2014-11-06 Jt International Sa Vaporisable material
CN103263080A (en) * 2013-05-23 2013-08-28 红云红河烟草(集团)有限责任公司 Preparation method of sweet and fragrant type electric heating cigarette liquid
CN103610229A (en) * 2013-12-09 2014-03-05 李建伟 Nicotine liquid of electronic cigarette
CN103859580A (en) * 2014-01-22 2014-06-18 红云红河烟草(集团)有限责任公司 Preparation method of electric heating type non-combustion cigarette paste
CN104068469B (en) * 2014-06-25 2016-07-27 湖南中烟工业有限责任公司 A kind of electronic cigarette liquid with sootiness fragrance
CN104489929B (en) * 2014-11-24 2017-04-19 安徽中烟工业有限责任公司 Cigar type electronic cigarette liquid
CN104489901B (en) * 2014-12-03 2016-06-29 河南中烟工业有限责任公司 One grows tobacco taste tobacco juice for electronic smoke
CN104585859A (en) * 2015-01-15 2015-05-06 中国烟草总公司郑州烟草研究院 Preparation method of electronic cigarette juice
CN105219530A (en) * 2015-10-08 2016-01-06 中烟施伟策(云南)再造烟叶有限公司 A kind of tobacco spice preparation method reinforced for reconstituted tobacco
CN105533793B (en) * 2016-02-24 2016-12-28 江西中烟工业有限责任公司 A kind of preparation method of Dark sun-cured tobacco extract
CN108185539B (en) * 2018-03-21 2021-03-05 福建中烟工业有限责任公司 Electronic cigarette with improved sensory quality and manufacturing method thereof
CN109171011A (en) * 2018-10-12 2019-01-11 武汉醉吟茶品茶业科技有限公司 One kind replacing cigarette sifting tea
CN111227295A (en) * 2020-01-20 2020-06-05 深圳梵活生命科学股份有限公司 Smokeless electronic atomized liquid and preparation method thereof

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100594809C (en) * 2008-02-29 2010-03-24 修运强 An electronic analog cigarette and its atomized liquid
CN101461566B (en) * 2009-01-08 2012-01-18 华健 Atomized liquid of electronic smoke
CN101933654A (en) * 2010-08-16 2011-01-05 深圳市如烟生物科技有限公司 Cigarette liquid for tooth whitening and strengthening health care electronic cigarettes

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI732965B (en) 2017-10-18 2021-07-11 日商日本煙草產業股份有限公司 Battery unit, flavor inhaling device, power charger, method for detecting abnormality of power supply, and computer program product

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Effective date of registration: 20151215

Address after: Five road in Longgang District of Shenzhen City, Guangdong province 518112 Buji Street No. 3 Hisense Gan Li innovation industrial city 9 building 501, 901, 1001

Applicant after: Shenzhen Hangsen Star Technology Co., Ltd.

Address before: 518000, Guangdong, Shenzhen province Longgang District Buji Street cloth Road, li long letter letter science and Technology Park Economic Center building, 6 floor

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Address after: Five road in Longgang District of Shenzhen City, Guangdong province 518112 Buji Street No. 3 Hisense Gan Li innovation industrial city 9 building 501, 901, 1001

Patentee after: Shenzhen Hangsen Star Technology Co., Ltd.

Patentee after: HENGSEN INTERNATIONAL GROUP LIMITED

Address before: Five road in Longgang District of Shenzhen City, Guangdong province 518112 Buji Street No. 3 Hisense Gan Li innovation industrial city 9 building 501, 901, 1001

Patentee before: Shenzhen Hangsen Star Technology Co., Ltd.

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Address after: 1b, building 6, saitu digital industrial plant, 137 Bulan Road, gankeng community, Jihua street, Shenzhen City, Guangdong Province

Patentee after: Hengxin Yongji Technology (Shenzhen) Co.,Ltd.

Patentee after: HENGXIN HONGTU INTERNATIONAL HOLDINGS Co.,Ltd.

Address before: 518112 Room 501, 901, 1001, building 9, China Hisense innovation industry city, No. 3, ganliwu Road, Buji street, Longgang District, Shenzhen City, Guangdong Province

Patentee before: SHENZHEN HANGSEN STAR TECHNOLOGY Co.,Ltd.

Patentee before: HENGXIN HONGTU INTERNATIONAL HOLDINGS Co.,Ltd.

CP03 Change of name, title or address