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CN102965843A - PET (polyethylene glycol terephthalate) fiber/teflon fiber composite sound absorbing cotton and preparation method of PET fiber/teflon fiber composite sound absorbing cotton - Google Patents

PET (polyethylene glycol terephthalate) fiber/teflon fiber composite sound absorbing cotton and preparation method of PET fiber/teflon fiber composite sound absorbing cotton Download PDF

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Publication number
CN102965843A
CN102965843A CN2012104781241A CN201210478124A CN102965843A CN 102965843 A CN102965843 A CN 102965843A CN 2012104781241 A CN2012104781241 A CN 2012104781241A CN 201210478124 A CN201210478124 A CN 201210478124A CN 102965843 A CN102965843 A CN 102965843A
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parts
fiber
controlled
pet
sound absorbing
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Pending
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CN2012104781241A
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Inventor
王黎明
孙益民
章云
厉曼
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WUHU YUEFEI NEW ACOUSTIC MATERIAL CO Ltd
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WUHU YUEFEI NEW ACOUSTIC MATERIAL CO Ltd
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Abstract

The invention discloses PET (polyethylene glycol terephthalate) fiber/teflon fiber composite sound absorbing cotton, which is prepared from the following ingredients in parts by weight: 70 to 80 parts of PET fibers, 40 to 50 parts of teflon fibers, 10 to 15 parts of emulsifying agents OP-30, 5 to 10 parts of peregal O-20, 80 to 100 parts of PP (propene polymer), 30 to 40 parts of HIPS (high impact polystyrene), 15 to 20 parts of activated clay, 10 to 15 parts of modified kieselguhr, 2 to 3 parts of stearic acid, 5 to 8 parts of dioctyl adipate, 4 to 6 parts of cresyl diphenyl phosphate, 2 to 3 parts of liquid paraffin, 1 to 2 parts of 3-aminopropyltrimethoxysilane, 2 to 3 parts of calcium stearate, 1 to 2 parts of barium stearate, 0.5 to 1.5 parts of anti-aging agents RD and 1 to 2 parts of antioxidants DLTP (dilauryl thiodipropionate). The sound absorbing cotton prepared by the invention has the advantages that the appearance evenness is good, the thickness is uniform, the hand feeling is soft, the product bonding degree is good, the tensile performance is high, the sound absorbing performance is excellent, the flame retardant effect is good, and the like.

Description

A kind of PET fiber/polytetrafluoroethylene fibre composite sound-absorbing cotton and preparation method thereof
Technical field
The present invention relates to Nonwovens In Technology, be specifically related to a kind of PET fiber/polytetrafluoroethylene fibre composite sound-absorbing cotton and preparation method thereof.
Background technology
Noise is one of three large public hazards of modern society's contaminated environment, and noise directly affects people's healthy progress along with society, and people have proposed more and more higher requirement to the Noise Prevention and Treatment of contaminated environment.Acoustical cotton can be converted to the kinetic energy of the fine count fiber of acoustical cotton inside with the high-frequency noises vibrational energy that produces in the life, and changes into heat energy and disappear, and reaches the function of absorbing sound and lowering noise.Therefore acoustical cotton has good sound-absorbing, heat-insulation warm keeping performance, is widely used in vehicles interior trim fields such as construction material, automobiles.But existing acoustical cotton product with and manufacture method all have many deficiencies, main manifestations is: adopt original manually-operated, use the cutter buttress, productivity ratio is low; Do not carry out flame treatment; The product bond degree not, easily loose, tension intensity is poor etc.
Summary of the invention
The object of the invention provides the PET fiber that a kind of fire resistance is good, intensity is high and sound-absorbing effect is good/polytetrafluoroethylene fibre composite sound-absorbing cotton and preparation method thereof for the deficiencies in the prior art.
The technical solution used in the present invention is as follows:
A kind of PET fiber/polytetrafluoroethylene fibre composite sound-absorbing is cotton, is made by the raw material of following weight portion: PET fiber 70-80, polytetrafluoroethylene fibre 40-50, polyoxyethylene nonylphenol ether-30 10-15, paregal O-20 5-10, PP 80-100, HIPS30-40, atlapulgite 15-20, modification infusorial earth 10-15, stearic acid 2-3, dioctyl adipate 5-8, phosphate toluene diphenyl ester 4-6, atoleine 2-3,3-aminopropyl trimethoxysilane 1-2, calcium stearate 2-3, barium stearate 1-2, anti-aging agent RD 0.5-1.5, anti-oxidant DLTP 1-2.
Described modification infusorial earth is made by following method: dried diatomite is dropped in the ball mill, the graphite, the vermiculite power of 1-2%, the sepiolite powder of 2-3%, the precipitated calcium carbonate of 3-5%, the waterglass of 2-3% and the polyvinyl alcohol of 3-5% that add 20-30%, behind the ball milling 8-12h, at 1050-1150 ℃ of lower calcining 2-3h, pulverizing grinds to form 200-300 order powder and gets final product.
The preparation method of PET fiber/polytetrafluoroethylene fibre composite sound-absorbing cotton may further comprise the steps:
(1) PET fiber and polytetrafluoroethylene fibre adding cotton blender machine are mixed, for making fiber softening, reducing the friction between the fiber, prevent static, before later process, add polyoxyethylene nonylphenol ether-30, paregal O-20 uniform stirring with the cloud point shape, balance 20-24h, make fiber level and smooth, have good saturability, be convenient to combing;
(2) the mixed fiber of step (1) is delivered to be carded to the uniform fiber web of thickness in the carding machine, output speed 100-120m/min, output fiber net mass area ratio is 200-300g/m 2
(3) the remaining raw materials such as PP, HIPS, atlapulgite, modification infusorial earth, stearic acid, dioctyl adipate are sent into carried out even blend in the screw extruder, screw rod one district's temperature is controlled at 160-180 ℃, two district's temperature are controlled at 210-225 ℃, three district's temperature are controlled at 220-240 ℃, four district's temperature are controlled at 240-250 ℃, and five district's temperature are controlled at 245-260 ℃;
(4) the above-mentioned fused mass of extruding is dropped into behind fondant filter, measuring pump in the spray silk machine silk is sprayed on the fiber web two sides on the lapper, spray silk die head temperature is controlled at 240-250 ℃, receiving range is controlled at 25-30cm, the jet-stream wind that is heated by air heater when melting and spraying enters spray silk die head dynamic analysis of spinning is carried out slenderizing, the temperature of jet-stream wind is 150-165 ℃, and jet angle is controlled at 55-60 °;
(5) semi-finished product with cold wind cooling, roll extrusion typing cut into various required size specifications after embossing is processed, and namely get the acoustical cotton finished product.
Beneficial effect of the present invention:
The present invention makes voluminous powder by diatomite is carried out modification, can improve the sound-absorbing effect of acoustical cotton, the present invention is by adjusting and process modification prescription, added atlapulgite, acoustical cotton has been had certain strengthening action, the mechanical performances such as the tensile strength of raising acoustical cotton, shock resistance.The present invention adopts the melt-spraying spinning method, have that technique is simple, controllability good, production efficiency is high, and industrializing implementation is easy, can guarantee the characteristics such as stable and reliable product quality, prepared acoustical cotton has that the smooth appearance degree is good, even thickness, soft, the advantages such as the product bond degree is good, tensile property is strong, sound absorption qualities is good, good flame retardation effect.
The specific embodiment
A kind of PET fiber/polytetrafluoroethylene fibre composite sound-absorbing is cotton, is made by the raw material of following weight portion: 78 parts of PET fibers, 42 parts of polytetrafluoroethylene fibres, polyoxyethylene nonylphenol ether-30 14 part, paregal O-20 8 part, 35 parts of 85 parts of PP, HIPS, 16 parts of atlapulgites, 15 parts of modification infusorial earths, 2.5 parts of stearic acid, 6 parts of dioctyl adipates, 5 parts of phosphate toluene diphenyl esters, 2 parts of atoleines, 1.5 parts of 3-aminopropyl trimethoxysilane, 2 parts of calcium stearates, 1.5 parts of barium stearates, 0.8 part of anti-aging agent RD, 1.5 parts of anti-oxidant DLTPs.
Wherein, described modification infusorial earth is made by following method: dried diatomite is dropped in the ball mill, add 28% graphite, 2% vermiculite power, 3% sepiolite powder, 4% precipitated calcium carbonate, 2.5% waterglass and 4% polyvinyl alcohol, behind the ball milling 10h, at 1150 ℃ of lower calcining 2h, pulverizing grinds to form 300 order powder and gets final product.
The preparation method of PET fiber/polytetrafluoroethylene fibre composite sound-absorbing cotton may further comprise the steps:
(1) PET fiber and polytetrafluoroethylene fibre adding cotton blender machine are mixed, for making fiber softening, reducing the friction between the fiber, prevent static, before later process, add polyoxyethylene nonylphenol ether-30, paregal O-20 uniform stirring with the cloud point shape, balance 22h, make fiber level and smooth, have good saturability, be convenient to combing;
(2) the mixed fiber of step (1) is delivered to be carded to the uniform fiber web of thickness in the carding machine, output speed 105m/min, output fiber net mass area ratio is 250g/m 2
(3) the remaining raw materials such as PP, HIPS, atlapulgite, modification infusorial earth, stearic acid, dioctyl adipate are sent into carried out even blend in the screw extruder, screw rod one district's temperature is controlled at 165 ℃, two district's temperature are controlled at 220 ℃, three district's temperature are controlled at 235 ℃, four district's temperature are controlled at 240 ℃, and five district's temperature are controlled at 250 ℃;
(4) the above-mentioned fused mass of extruding is dropped into behind fondant filter, measuring pump in the spray silk machine silk is sprayed on the fiber web two sides on the lapper, spray silk die head temperature is controlled at 245 ℃, receiving range is controlled at 25cm, the jet-stream wind that is heated by air heater when melting and spraying enters spray silk die head dynamic analysis of spinning is carried out slenderizing, the temperature of jet-stream wind is 160 ℃, jet velocity is 2400m/min, and jet angle is controlled at 57 °;
(5) semi-finished product with cold wind cooling, roll extrusion typing cut into various required size specifications after embossing is processed, and namely get the acoustical cotton finished product.
After tested, the distribution of fiber diameters of resulting materials is 1.6-1.8 μ m, and tearing strength is 548N/m, and the coefficient of heat conduction is 5.512W/ (m 2℃), oxygen index (OI) is 43%, noise reduction coefficient is 0.81.

Claims (3)

1. PET fiber/polytetrafluoroethylene fibre composite sound-absorbing is cotton, it is characterized in that, made by the raw material of following weight portion: PET fiber 70-80, polytetrafluoroethylene fibre 40-50, polyoxyethylene nonylphenol ether-30 10-15, paregal O-20 5-10, PP 80-100, HIPS 30-40, atlapulgite 15-20, modification infusorial earth 10-15, stearic acid 2-3, dioctyl adipate 5-8, phosphate toluene diphenyl ester 4-6, atoleine 2-3,3-aminopropyl trimethoxysilane 1-2, calcium stearate 2-3, barium stearate 1-2, anti-aging agent RD 0.5-1.5, anti-oxidant DLTP 1-2.
2. PET fiber according to claim 1/polytetrafluoroethylene fibre composite sound-absorbing is cotton, it is characterized in that, described modification infusorial earth is made by following method: dried diatomite is dropped in the ball mill, the graphite, the vermiculite power of 1-2%, the sepiolite powder of 2-3%, the precipitated calcium carbonate of 3-5%, the waterglass of 2-3% and the polyvinyl alcohol of 3-5% that add 20-30%, behind the ball milling 8-12h, at 1050-1150 ℃ of lower calcining 2-3h, pulverizing grinds to form 200-300 order powder and gets final product.
3. the preparation method of PET fiber as claimed in claim 1/polytetrafluoroethylene fibre composite sound-absorbing cotton is characterized in that may further comprise the steps:
(1) PET fiber and polytetrafluoroethylene fibre adding cotton blender machine are mixed, for making fiber softening, reducing the friction between the fiber, prevent static, before later process, add polyoxyethylene nonylphenol ether-30, paregal O-20 uniform stirring with the cloud point shape, balance 20-24h, make fiber level and smooth, have good saturability, be convenient to combing;
(2) the mixed fiber of step (1) is delivered to be carded to the uniform fiber web of thickness in the carding machine, output speed 100-120m/min, output fiber net mass area ratio is 200-300g/m 2
(3) the remaining raw materials such as PP, HIPS, atlapulgite, modification infusorial earth, stearic acid, dioctyl adipate are sent into carried out even blend in the screw extruder, screw rod one district's temperature is controlled at 160-180 ℃, two district's temperature are controlled at 210-225 ℃, three district's temperature are controlled at 220-240 ℃, four district's temperature are controlled at 240-250 ℃, and five district's temperature are controlled at 245-260 ℃;
(4) the above-mentioned fused mass of extruding is dropped into behind fondant filter, measuring pump in the spray silk machine silk is sprayed on the fiber web two sides on the lapper, spray silk die head temperature is controlled at 240-250 ℃, receiving range is controlled at 25-30cm, the jet-stream wind that is heated by air heater when melting and spraying enters spray silk die head dynamic analysis of spinning is carried out slenderizing, the temperature of jet-stream wind is 150-165 ℃, and jet angle is controlled at 55-60 °;
(5) semi-finished product with cold wind cooling, roll extrusion typing cut into various required size specifications after embossing is processed, and namely get the acoustical cotton finished product.
CN2012104781241A 2012-11-22 2012-11-22 PET (polyethylene glycol terephthalate) fiber/teflon fiber composite sound absorbing cotton and preparation method of PET fiber/teflon fiber composite sound absorbing cotton Pending CN102965843A (en)

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CN103696138A (en) * 2013-11-26 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Insulated non-woven fabric sound-absorbing cotton and preparation method thereof
CN103696131A (en) * 2013-11-25 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Flame-retardant sound-absorbing cotton and preparation method thereof
CN103696130A (en) * 2013-11-25 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Environment-friendly non-woven fabric noise-absorbing cotton and preparation method thereof
CN103696127A (en) * 2013-11-25 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Montmorillonite/isotactic polypropylene/polylactic acid composite sound absorbing cotton and preparation method thereof
CN103696134A (en) * 2013-11-26 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Flame-retardant non-woven fabric sound-absorbing cotton and preparation method thereof
CN103696133A (en) * 2013-11-26 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Refreshing glass down and preparation method thereof
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CN103692706A (en) * 2013-11-25 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Antistatic sound-absorbing cotton and preparation method thereof
CN103696135A (en) * 2013-11-26 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Noise-absorbing cotton containing Chinese herbal medicines and preparation method thereof
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CN103710863A (en) * 2013-11-25 2014-04-09 芜湖跃飞新型吸音材料股份有限公司 Natural-clay-containing light nonwoven material for sound absorbing cotton
CN103710866A (en) * 2013-11-25 2014-04-09 芜湖跃飞新型吸音材料股份有限公司 Elastic sound-absorbing cotton and preparation method thereof
CN103710860A (en) * 2013-11-25 2014-04-09 芜湖跃飞新型吸音材料股份有限公司 Palygorskite-containing nonwoven material for sound absorbing cotton
CN103710871A (en) * 2013-11-25 2014-04-09 芜湖跃飞新型吸音材料股份有限公司 Non-woven fabric sound-absorbing cotton capable of resisting irradiation aging
CN103710868A (en) * 2013-11-25 2014-04-09 芜湖跃飞新型吸音材料股份有限公司 Healthcare sound absorption cotton made of traditional Chinese medicine and method for manufacturing healthcare sound absorption cotton
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CN103757819A (en) * 2013-11-25 2014-04-30 芜湖跃飞新型吸音材料股份有限公司 High-density polyethylene sound-absorbing cotton and preparation method thereof
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CN103710872A (en) * 2013-11-25 2014-04-09 芜湖跃飞新型吸音材料股份有限公司 Nonwoven cloth sound absorbing cotton containing wood sawdust
CN103722829A (en) * 2013-11-25 2014-04-16 芜湖跃飞新型吸音材料股份有限公司 Renewable and environment-friendly activated carbon acoustic wool and preparation method thereof
CN103707582A (en) * 2013-11-25 2014-04-09 芜湖跃飞新型吸音材料股份有限公司 Modified isotatic polypropylene non-woven fabric sound-absorbing cotton and preparation method thereof
CN103710862A (en) * 2013-11-25 2014-04-09 芜湖跃飞新型吸音材料股份有限公司 Flame-retardant heat-preservation nonwoven material for sound absorbing cotton
CN103710876A (en) * 2013-11-26 2014-04-09 芜湖跃飞新型吸音材料股份有限公司 High-strength sound absorbing cotton and preparation method thereof
CN103696138A (en) * 2013-11-26 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Insulated non-woven fabric sound-absorbing cotton and preparation method thereof
CN103696135A (en) * 2013-11-26 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Noise-absorbing cotton containing Chinese herbal medicines and preparation method thereof
CN103696133A (en) * 2013-11-26 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Refreshing glass down and preparation method thereof
CN103696134A (en) * 2013-11-26 2014-04-02 芜湖跃飞新型吸音材料股份有限公司 Flame-retardant non-woven fabric sound-absorbing cotton and preparation method thereof
CN103710877A (en) * 2013-11-27 2014-04-09 芜湖跃飞新型吸音材料股份有限公司 Fluorescent whitened non-woven fabric and method for manufacturing same
CN103726223A (en) * 2013-11-27 2014-04-16 芜湖跃飞新型吸音材料股份有限公司 Flame-retardant non-woven cloth and manufacturing method thereof
CN103757821A (en) * 2013-11-27 2014-04-30 芜湖跃飞新型吸音材料股份有限公司 Nano pearl powder modified isotactic polypropylene non-woven fabric and preparation method thereof
CN103753875A (en) * 2013-11-27 2014-04-30 芜湖跃飞新型吸音材料股份有限公司 Chinese herbal medicine modified isotatic polypropylene non-woven fabric and preparation method thereof
CN103774344A (en) * 2014-01-02 2014-05-07 长春博超汽车零部件股份有限公司 Fibrilia composite material with low VOC nanometers and preparation method thereof
CN106128447A (en) * 2016-08-16 2016-11-16 苏州市云林电子有限公司 A kind of composite sound-absorbing foam

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Application publication date: 20130313