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CN102954926B - Capillary viscometer - Google Patents

Capillary viscometer Download PDF

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CN102954926B
CN102954926B CN201210304272.1A CN201210304272A CN102954926B CN 102954926 B CN102954926 B CN 102954926B CN 201210304272 A CN201210304272 A CN 201210304272A CN 102954926 B CN102954926 B CN 102954926B
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differential pressure
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fluid
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CN102954926A (en
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松崎政则
田岛一繁
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Saginomiya Seisakusho Inc
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • G01N11/02Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material
    • G01N11/04Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture
    • G01N11/08Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture by measuring pressure required to produce a known flow
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/22Fuels; Explosives

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Abstract

本发明提供细管式粘度计,能够消除在定流量泵、输送管上产生的被测定流体的流动的混乱,使被测定流体以层流状态在压差检测用细管内流动,而能够利用压差传感器来正确地检测压差检测用细管的入口端与出口端之间的压力差,从而能够可靠地进行粘度测定。在压差检测用细管的上游侧,设有具有比压差检测用细管的流道截面积大的流道截面积的流动控制室。

The present invention provides a narrow tube viscometer, which can eliminate the flow disturbance of the measured fluid generated on the constant flow pump and the delivery pipe, make the measured fluid flow in the thin tube for pressure difference detection in a laminar flow state, and can utilize the pressure The differential sensor accurately detects the pressure difference between the inlet end and the outlet end of the thin tube for pressure difference detection, thereby enabling reliable viscosity measurement. On the upstream side of the capillary for differential pressure detection, a flow control chamber having a flow channel cross-sectional area larger than that of the capillary for differential pressure detection is provided.

Description

细管式粘度计Capillary Viscometer

技术领域 technical field

本发明涉及如下构成的细管式粘度计,即,在压差检测用细管内流动例如A重油(MDO)、轻油(MGO)等被测定流体,用压差传感器来检测压差检测用细管的入口端与出口端的压差,由此来测定流体的粘度。The present invention relates to a capillary viscometer configured such that a fluid to be measured, such as A heavy oil (MDO) or light oil (MGO), flows through a capillary for differential pressure detection, and a differential pressure sensor detects the capillary for differential pressure detection. The pressure difference between the inlet end and the outlet end of the pipe is used to determine the viscosity of the fluid.

背景技术 Background technique

以往,使用如下细管式粘度计,即,在粘性流体以恒定流量的层流状态在具有恒定的内径的细管内流动的情况下,由细管内的上游侧与下游侧产生的压力差和流量的关系,根据哈根-泊肃叶(Hagen-Poiseuille)流的定律,来连续地求出粘度。Conventionally, thin tube viscometers have been used. When a viscous fluid flows in a thin tube with a constant inner diameter in a laminar flow state at a constant flow rate, the pressure difference and flow rate generated between the upstream and downstream sides of the narrow tube According to the relationship of Hagen-Poiseuille (Hagen-Poiseuille) flow law, to continuously find the viscosity.

即,所谓该哈根-泊肃叶流的式子,利用如下性质:在某流体以流量(q)的层流状态在内径半径(r)、长度(l)的细管内流动的情况下,细管的入口端与出口端之间的压力差(ΔP)与流体的粘度(η)成比例,如下述的式1表示。That is, the so-called Hagen-Poiseuille flow formula utilizes the following property: When a certain fluid flows in a thin tube with an inner diameter radius (r) and a length (l) in a laminar flow state of a flow rate (q), The pressure difference (ΔP) between the inlet port and the outlet port of the thin tube is proportional to the viscosity (η) of the fluid, as expressed by Equation 1 below.

数学式1:Mathematical formula 1:

ηη == πrπr 44 ΔPΔP 8181 qq

如上述式1所示,若已知细管的形状与流量,则通过检测细管的压差检测用细管(ΔP),能够测定流体的粘度(η)。As shown in the above formula 1, if the shape and flow rate of the capillary are known, the viscosity (η) of the fluid can be measured by detecting the capillary for differential pressure detection (ΔP) of the capillary.

图6是表示利用了该哈根-泊肃叶流的式子的以往的细管式粘度计的示意图。FIG. 6 is a schematic diagram showing a conventional thin-tube viscometer using the Hagen-Poiseuier flow equation.

如图6所示,以往的细管式粘度计100构成为,利用定流量泵104,经由吸入管102,从存积未图示的被测定流体的罐、配管等,抽出被测定流体。As shown in FIG. 6 , a conventional capillary viscometer 100 is configured such that a constant flow pump 104 draws a fluid to be measured through a suction pipe 102 from a tank, piping, etc. that stores a fluid to be measured (not shown).

而且,构成为,由定流量泵104抽出的被测定流体经由输送管106,并以层流状态在压差检测用细管108中流动,而从排出管110排出。Furthermore, the fluid to be measured is pumped by the constant flow pump 104 to flow through the delivery pipe 106 in a laminar flow state in the thin tube 108 for differential pressure detection, and is discharged from the discharge pipe 110 .

另一方面,高压检测管112从压差检测用细管108的入口端108a开始分支,并经由压差传感器114、低压检测管116,与压差检测用细管108的出口端108b连接,由此,向压差传感器114传递压力。On the other hand, the high pressure detection tube 112 branches from the inlet end 108a of the thin tube 108 for differential pressure detection, and is connected to the outlet end 108b of the thin tube 108 for differential pressure detection via the differential pressure sensor 114 and the low pressure detection tube 116. Therefore, the pressure is transmitted to the differential pressure sensor 114 .

由此,构成为,利用压差传感器114来检测高压检测管112的压力与低压检测管116的压力的压差,使用式1换算该压差,从而计算出粘度。Thus, the differential pressure sensor 114 detects the pressure difference between the pressure of the high-pressure detection pipe 112 and the pressure of the low-pressure detection pipe 116 , and converts the pressure difference using Equation 1 to calculate the viscosity.

现有技术文献prior art literature

专利文献1:日本专利第3796330号公报Patent Document 1: Japanese Patent No. 3796330

然而,近几年,为了防止环境破坏,例如,在陆地汽车、火力发电所等中加强排气限制。该排气限制对于海上的船舶也无例外,已经在一部分的海域开始了限制。However, in recent years, in order to prevent environmental damage, for example, exhaust gas regulation has been strengthened in land vehicles, thermal power plants, and the like. This exhaust gas regulation is not an exception for ships at sea, and regulation has already begun in some sea areas.

即,船舶的燃料强制性地在陆地的近海使用与至今使用的A重油(MDO)相比更加低硫黄(LSA)的轻油(MGO)。该轻油(MGO)是在15℃时的粘度为2mPa·s以下的非常低粘度的流体。That is, light oil (MGO) which is lower in sulfur (LSA) than A heavy oil (MDO) used hitherto is compulsorily used for the fuel of a ship in the offshore of land. This light oil (MGO) is a very low-viscosity fluid whose viscosity at 15° C. is 2 mPa·s or less.

然而,在对粘性流体通过细管内时产生的压力损失进行检测、并测定粘度的以往的细管式粘度计100中,压差检测用细管108内的被测定流体的流动为层流是重要的条件。However, in the conventional capillary viscometer 100 that detects the pressure loss that occurs when a viscous fluid passes through the capillary and measures the viscosity, it is important that the flow of the fluid to be measured in the capillary for pressure difference detection 108 be laminar. conditions of.

在该被测定流体的粘度高的情况下,层流在短距离形成,但是在被测定流体的粘度低的情况下,形成层流为止需要长的距离。When the viscosity of the fluid to be measured is high, laminar flow is formed over a short distance, but when the viscosity of the fluid to be measured is low, a long distance is required to form laminar flow.

另外,为了使细管式粘度计100小型化,如图6所示,若对从定流量泵104至压差检测用细管108为止的被测定流体的输送管106进行弯曲加工,则在例如轻油(MGO)之类被测定流体的粘度低的情况下,在弯曲部分中产生副流(二次流),由于该副流使测定流体混乱而不产生层流。其结果,压差检测用细管108内的被测定流体的流动不会成为层流,而给予测定大的影响。In addition, in order to reduce the size of the capillary viscometer 100, as shown in FIG. When the viscosity of the fluid to be measured such as light oil (MGO) is low, a side flow (secondary flow) occurs in the curved portion, and the measurement fluid is disturbed by this side flow so that laminar flow does not occur. As a result, the flow of the fluid to be measured in the thin tube for pressure difference detection 108 does not become a laminar flow, which greatly affects the measurement.

因此,在例如轻油(MGO)之类被测定流体的粘度低的情况下,若将从定流量泵104至压差检测用细管108为止的被测定流体的输送管106配置为直线状,并且将其距离变长,则在输送管106内,被测定流体的流动成为层流,并也不会产生副流(二次流)。Therefore, when the viscosity of the fluid to be measured such as light oil (MGO) is low, if the delivery pipe 106 of the fluid to be measured is arranged in a straight line from the constant flow pump 104 to the thin tube 108 for differential pressure detection, Furthermore, if the distance is made longer, the flow of the fluid to be measured becomes laminar in the delivery pipe 106 and no secondary flow (secondary flow) occurs.

然而,若像这样地将从定流量泵104至压差检测用细管108为止的被测定流体的输送管106配置为直线状,并且,将其距离变长,则细管式粘度计100大型化,并且,也有很多在构造上无法配置为直线状的情况。However, if the delivery pipe 106 of the fluid to be measured from the constant flow pump 104 to the capillary for differential pressure detection 108 is arranged in a straight line, and the distance thereof is increased, the capillary viscometer 100 will be large in size. In addition, there are many cases where the structure cannot be arranged in a straight line.

因此,专利文献1(专利第3796330号公报)中公开了如下粘度检测计单元,即,通过附设双联的齿轮泵,而在该泵的外周部螺旋状地形成粘度计测用的毛细管,来紧凑地形成装置整体。Therefore, Patent Document 1 (Patent No. 3796330) discloses a viscometer unit in which a double gear pump is attached, and a capillary for viscosity measurement is helically formed on the outer periphery of the pump. Compactly form the whole device.

然而,该专利文献1的粘度检测计单元中,必须配设双联的齿轮泵,从而构造复杂,并且,在例如轻油(MGO)之类被测定流体的粘度低的情况下,有在弯曲部分中产生副流(二次流)、给予测定大的影响的情况。However, in the viscosity detector unit of Patent Document 1, it is necessary to arrange a double gear pump, so that the structure is complicated, and when the viscosity of the fluid to be measured is low, such as light oil (MGO), there is a risk of bending. A side flow (secondary flow) is generated in a part, which has a great influence on the measurement.

发明内容 Contents of the invention

本发明鉴于这样的现状,其目的在于提供如下细管式粘度计,即,即使在例如轻油(MGO)之类被测定流体的粘度低的情况下,也能够消除在定流量泵、输送管上产生的被测定流体的流动的混乱,并且使被测定流体以层流状态在压差检测用细管内流动,能够利用压差传感器正确地对压差检测用细管的入口端与出口端之间的压力差进行检测,从而能可靠地进行粘度测定。In view of such circumstances, the present invention aims to provide a narrow tube type viscometer that can eliminate the need for constant flow pumps, delivery pipes, etc. The flow of the fluid to be measured is disturbed, and the fluid to be measured flows in the thin tube for pressure difference detection in a laminar flow state, and the differential pressure sensor can be used to accurately measure the difference between the inlet end and the outlet end of the thin tube for pressure difference detection. To detect the pressure difference between the two, so that the viscosity can be measured reliably.

另外,本发明的目的在于提供如下细管式粘度计,即,即使输送管内为副流(二次流)、乱流的状态,也能够消除该被测定流体的流动的混乱,并能够复杂地弯曲输送管,从而能够使用更加细的配管,进而也能够安装于复杂的构造体而提高设计的自由度。In addition, an object of the present invention is to provide a thin-tube viscometer that can eliminate the turbulence of the flow of the fluid to be measured even if the delivery pipe is in a state of secondary flow (secondary flow) or turbulent flow, and can complicate By bending the delivery tube, thinner piping can be used, and it can also be attached to a complex structure, thereby increasing the degree of freedom in design.

另外,本发明由于在流动控制室内一度成为平稳的流动,所以能够将直至压差检测用细管内的层流的完成为止的助起动间隔缩短,从而能够提供紧凑的细管式粘度计。In addition, since the present invention once becomes a stable flow in the flow control chamber, it is possible to shorten the start-up interval until the laminar flow in the pressure difference detection capillary is completed, thereby providing a compact capillary viscometer.

本发明是为了达成上述的以往技术中的课题以及目的而发明的,本发明的细管式粘度计构成为,The present invention was made to achieve the above-mentioned problems and objects in the prior art, and the capillary viscometer of the present invention is constituted as follows:

使被测定流体在压差检测用细管内流动,利用压差传感器来检测压差检测用细管的入口端与出口端的压差,由此来测定流体的粘度,该细管式粘度计的特征在于,The fluid to be measured flows in the thin tube for differential pressure detection, and the pressure difference between the inlet end and the outlet end of the thin tube for differential pressure detection is detected by the differential pressure sensor, thereby measuring the viscosity of the fluid. The characteristics of this narrow tube viscometer is that

在上述压差检测用细管的上游侧,设有流动控制室,该流动控制室具有比压差检测用细管的流道截面积大的流道截面积。On the upstream side of the capillary for differential pressure detection, a flow control chamber having a flow channel cross-sectional area larger than that of the capillary for differential pressure detection is provided.

通过这样构成,具有比压差检测用细管的流道截面积大的流道截面积的流动控制室设置于压差检测用细管的上游侧,所以被测定流体流入该流动控制室,由此流动控制室可以作为缓冲器发挥功能,而在流动控制室内降低流速,并使流体成为平稳的流动。With this configuration, the flow control chamber having a flow channel cross-sectional area larger than the flow channel cross-sectional area of the pressure difference detection capillary is provided on the upstream side of the pressure difference detection capillary, so the fluid to be measured flows into the flow control chamber, and the This flow control chamber can function as a damper, reducing the flow velocity within the flow control chamber and making the fluid a smooth flow.

因此,即使在例如轻油(MGO)之类被测定流体的粘度低的情况下,也能够消除在定流量泵、输送管上产生的被测定流体的流动的混乱,使被测定流体以层流状态在压差检测用细管内流动,能够利用压差传感器正确地检测压差检测用细管的入口端与出口端之间的压力差,从而能够可靠地进行粘度测定。Therefore, even when the viscosity of the measured fluid such as light oil (MGO) is low, the flow disturbance of the measured fluid generated on the constant flow pump and the delivery pipe can be eliminated, and the measured fluid can flow in a laminar flow. The state flows in the thin tube for differential pressure detection, and the differential pressure sensor can accurately detect the pressure difference between the inlet port and the outlet port of the thin tube for differential pressure detection, so that the viscosity can be measured reliably.

另外,能够提供如下细管式粘度计,即,即使输送管内为副流(二次流)、乱流的状态,也能够消除该被测定流体的流动的混乱,也能够将输送管复杂地弯曲,从而能够使用更加细的配管,进而也能够安装于复杂的构造体而提高设计的自由度。In addition, it is possible to provide a narrow tube type viscometer that can eliminate the turbulence of the flow of the fluid to be measured even if the inside of the delivery tube is in a state of secondary flow (secondary flow) or turbulent flow, and the delivery tube can be bent complicatedly. , so that thinner piping can be used, and it can also be installed in complex structures to increase the degree of freedom in design.

另外,在流动控制室内一度成为平稳的流动,所以能够将直至压差检测用细管内的层流的完成为止的助起动间隔缩短,从而能够提供紧凑的细管式粘度计。In addition, since the flow is once stable in the flow control chamber, it is possible to shorten the start-up interval until laminar flow in the pressure difference detection capillary is completed, thereby providing a compact capillary viscometer.

另外,本发明的细管式粘度计的特征在于,在上述流动控制室内,配置有压差检测用细管的至少一部分。In addition, the capillary viscometer of the present invention is characterized in that at least a part of the capillary for differential pressure detection is disposed in the flow control chamber.

这样,由于在流动控制室内,配置有压差检测用细管的至少一部分,所以流动控制室成为环绕有压差检测用细管的状态,从而能够紧凑地构成细管式粘度计。As described above, since at least a part of the capillary for differential pressure detection is arranged in the flow control chamber, the flow control chamber is surrounded by the capillary for differential pressure detection, and the capillary viscometer can be configured compactly.

另外,本发明的细管式粘度计的特征在于,将配置有上述压差传感器的支管的高压侧检测管的入口配置于上述流动控制室的下游侧。In addition, the narrow tube type viscometer according to the present invention is characterized in that the inlet of the high-pressure-side detecting tube of the branch pipe in which the differential pressure sensor is arranged is arranged on the downstream side of the flow control chamber.

这样,通过将配置压差传感器的支管的高压侧检测管的入口配置于上述流动控制室的下游侧,在流动控制室的下游侧有平稳的流动,流动的混乱消失,从而能够利用压差传感器来检测正确的高压侧的压力,其结果,能够可靠地进行粘度测定。In this way, by arranging the inlet of the high-pressure side detecting pipe of the branch pipe of the differential pressure sensor on the downstream side of the above-mentioned flow control chamber, there is a smooth flow on the downstream side of the flow control chamber, and the turbulence of the flow disappears, so that the differential pressure sensor can be used. To detect the correct pressure on the high pressure side, as a result, the viscosity can be measured reliably.

另外,本发明的细管式粘度计的特征在于,将配置有上述压差传感器的支管的高压侧检测管的入口配置于上述流动控制室的下游侧、且配置于上述压差检测用细管的上游侧端部附近。In addition, the capillary viscometer of the present invention is characterized in that the inlet of the high-pressure-side detection tube of the branch pipe in which the differential pressure sensor is disposed is disposed on the downstream side of the flow control chamber, and is disposed in the capillary for differential pressure detection. near the upstream end of the

这样,由于将配置有压差传感器的支管的高压侧检测管的入口配置于上述流动控制室的下游侧、且配置于上述压差检测用细管的上游侧端部附近,所以在流动控制室的下游侧、尤其压差检测用细管的上游侧端部附近,有平稳的流动,流动的混乱消失,从而能够利用压差传感器来检测正确的高压侧的压力,其结果,能够可靠地进行粘度测定。In this way, since the inlet of the high-pressure-side detecting pipe of the branch pipe of the differential pressure sensor is disposed on the downstream side of the flow control chamber and near the upstream end of the differential pressure detection capillary, the flow control chamber On the downstream side, especially in the vicinity of the upstream end of the thin tube for differential pressure detection, there is a smooth flow, and the turbulence of the flow disappears, so that the correct pressure on the high pressure side can be detected by the differential pressure sensor. As a result, it can be reliably performed. Viscosity determination.

本发明的效果如下。The effects of the present invention are as follows.

根据本发明,由于具有比压差检测用细管的流道截面积大的流道截面积的流动控制室设置于压差检测用细管的上游侧,所以被测定流体流入该流动控制室,由此流动控制室可以作为缓冲器来发挥功能,而在流动控制室内降低流速,并使流体成为平稳的流动。According to the present invention, since the flow control chamber having a flow channel cross-sectional area larger than that of the pressure difference detection capillary is provided on the upstream side of the pressure difference detection capillary, the fluid to be measured flows into the flow control chamber, Thus, the flow control chamber can function as a damper, and the flow velocity is reduced in the flow control chamber to make the fluid flow smoothly.

因此,即使在例如轻油(MGO)之类被测定流体的粘度低的情况下,也能够消除在定流量泵、输送管上产生的被测定流体的流动的混乱,使被测定流体以层流状态在压差检测用细管内流动,能够利用压差传感器来正确地检测压差检测用细管的入口端与出口端之间的压力差,从而能够可靠地进行粘度测定。Therefore, even when the viscosity of the measured fluid such as light oil (MGO) is low, the flow disturbance of the measured fluid generated on the constant flow pump and the delivery pipe can be eliminated, and the measured fluid can flow in a laminar flow. The state flows in the capillary for differential pressure detection, and the differential pressure sensor can accurately detect the pressure difference between the inlet port and the outlet port of the capillary for differential pressure detection, thereby enabling reliable viscosity measurement.

附图说明 Description of drawings

图1是表示本发明的细管式粘度计的示意图。Fig. 1 is a schematic diagram showing a narrow tube type viscometer of the present invention.

图2是图1的细管式粘度计的A-A线的剖视图。Fig. 2 is a sectional view taken along line A-A of the thin tube viscometer in Fig. 1 .

图3是图1的细管式粘度计的流动控制室的放大图。FIG. 3 is an enlarged view of the flow control chamber of the slim tube viscometer of FIG. 1 .

图4是表示本发明的其他的实施例的细管式粘度计的示意图。Fig. 4 is a schematic view showing a narrow tube viscometer according to another embodiment of the present invention.

图5是本发明的其他的实施例的细管式粘度计的流动控制室的放大图。Fig. 5 is an enlarged view of a flow control chamber of a narrow tube viscometer according to another embodiment of the present invention.

图6是表示以往的细管式粘度计的示意图。Fig. 6 is a schematic diagram showing a conventional narrow tube type viscometer.

图中:In the picture:

10—细管式粘度计,12—吸入管,14—定流量泵,16—输送管,16a—下游端,18—压差检测用细管,18a—口端,18b—出口端,20—排出管,22—高压检测管,22a—入口端,24—压差传感器,26—定流量泵,28—低压检测管,30—控制室,30a—前端部,30b—后端部,30c—下游端,30d—上游端,30e—上端,30f—下端,100—细管式粘度计,102—吸入管,104—定流量泵,106—输送管,108—压差检测用细管,108a—入口端,108b—出口端,110—排出管,112—高压检测管,114—压差传感器,116—低压检测管。10—thin tube viscometer, 12—suction pipe, 14—constant flow pump, 16—delivery pipe, 16a—downstream end, 18—thin tube for differential pressure detection, 18a—mouth port, 18b—outlet port, 20— Discharge pipe, 22—high pressure detection pipe, 22a—inlet port, 24—pressure difference sensor, 26—constant flow pump, 28—low pressure detection pipe, 30—control room, 30a—front end, 30b—rear end, 30c— Downstream end, 30d—upstream end, 30e—upper end, 30f—lower end, 100—thin tube viscometer, 102—suction pipe, 104—constant flow pump, 106—delivery pipe, 108—thin tube for differential pressure detection, 108a - inlet port, 108b - outlet port, 110 - discharge pipe, 112 - high pressure detection tube, 114 - differential pressure sensor, 116 - low pressure detection tube.

具体实施方式Detailed ways

以下,基于附图对本发明的实施方式(实施例)进一步进行详细说明。Hereinafter, embodiments (examples) of the present invention will be further described in detail based on the drawings.

实施例1Example 1

图1是表示本发明的细管式粘度计的示意图,图2是图1的细管式粘度计的A-A线的剖视图,图3是图1的细管式粘度计的流动控制室的放大图。Fig. 1 is a schematic view showing the capillary viscometer of the present invention, Fig. 2 is a sectional view of the line A-A of the capillary viscometer of Fig. 1 , and Fig. 3 is an enlarged view of the flow control chamber of the capillary viscometer of Fig. 1 .

图1中,符号10表示本发明的细管式粘度计整体。In FIG. 1 , reference numeral 10 denotes the whole thin tube type viscometer of the present invention.

如图1所示,细管式粘度计10构成为,利用定流量泵14,经由吸入管12、从未图示的存积例如轻油(MGO)之类粘度低的被测定流体的罐、配管等,抽出被测定流体。As shown in FIG. 1 , the capillary viscometer 10 is configured to use a constant flow pump 14 to pass through a suction pipe 12 , a tank (not shown) that stores a low-viscosity fluid to be measured, such as light oil (MGO), Piping, etc., to extract the fluid to be measured.

而且,构成为,在压差检测用细管18的上游侧设有流动控制室30,由定流量泵14抽出的被测定流体经由输送管16,而流入流动控制室30。Furthermore, a flow control chamber 30 is provided on the upstream side of the pressure difference detection capillary 18 , and the fluid to be measured pumped out by the constant flow pump 14 flows into the flow control chamber 30 through the delivery tube 16 .

即,输送管16的下游端16a与流动控制室30的长度方向的后端部30b(图1中,为右侧的流动控制室30的上游侧)连接。That is, the downstream end 16a of the delivery pipe 16 is connected to the longitudinal rear end portion 30b of the flow control chamber 30 (the upstream side of the right flow control chamber 30 in FIG. 1 ).

另外,在流动控制室30的长度方向的前端部30a(图1中,为左侧的流动控制室30的下游侧)分支有高压检测管22。即,在压差检测用细管18的上游侧端部附近、即压差检测用细管18的入口端18a的附近,配置有高压检测管22的入口端22a。In addition, a high-pressure detection tube 22 is branched at a front end portion 30 a in the longitudinal direction of the flow control chamber 30 (in FIG. 1 , the downstream side of the left flow control chamber 30 ). That is, the inlet end 22a of the high pressure detection tube 22 is disposed near the upstream end of the differential pressure detection capillary 18 , that is, near the inlet end 18a of the differential pressure detection capillary 18 .

而且,高压检测管22经由压差传感器24、低压检测管28而与压差检测用细管18的出口端18b连接,由此,向压差传感器24传递压力。Further, the high-pressure detection tube 22 is connected to the outlet end 18 b of the thin tube 18 for differential pressure detection via a differential pressure sensor 24 and a low-pressure detection tube 28 , thereby transmitting pressure to the differential pressure sensor 24 .

另一方面,以压差检测用细管18的入口端18a位于流动控制室30的长度方向的前端部30a附近的方式,在流动控制室30内配置压差检测用细管18的至少一部分。On the other hand, at least a part of the differential pressure detection capillary 18 is arranged in the flow control chamber 30 so that the inlet port 18a of the pressure difference detection capillary 18 is located near the longitudinal front end 30a of the flow control chamber 30 .

而且,构成为,经由输送管16而流入流动控制室30的被测定流体以层流状态在压差检测用细管18中流动,并从排出管20排出。Furthermore, the fluid to be measured flowing into the flow control chamber 30 through the delivery tube 16 flows in the thin tube 18 for differential pressure detection in a laminar flow state, and is discharged from the discharge tube 20 .

由此,利用压差传感器24来检测高压检测管22的压力与低压检测管28的压力的压差,并使用式1换算该压差,从而计算出粘度。Thus, the pressure difference between the pressure of the high pressure detection pipe 22 and the pressure of the low pressure detection pipe 28 is detected by the differential pressure sensor 24 , and the pressure difference is converted using Equation 1 to calculate the viscosity.

该情况下,如图1、图2所示,流动控制室30的流道截面积形成为具有比压差检测用细管18的流道截面积大的流道截面积。In this case, as shown in FIGS. 1 and 2 , the flow channel cross-sectional area of the flow control chamber 30 is formed to have a larger flow channel cross-sectional area than the flow channel cross-sectional area of the narrow tube 18 for pressure difference detection.

通过这样构成,如图1的箭头所示,利用定流量泵14而经由吸入管12被抽出的被测定流体经由输送管16、从输送管16的下游端16a,向流动控制室30的长度方向的后端部30b流入。With such a configuration, as shown by the arrow in FIG. 1 , the fluid to be measured that is drawn out through the suction pipe 12 by the constant flow pump 14 passes through the delivery pipe 16, from the downstream end 16a of the delivery pipe 16, to the longitudinal direction of the flow control chamber 30. The rear end 30b flows in.

而且,流入流动控制室30的被测定流体朝向流动控制室30的长度方向的前端部30a的方向流动。Then, the fluid to be measured flowing into the flow control chamber 30 flows toward the front end portion 30 a of the flow control chamber 30 in the longitudinal direction.

此时,由于流动控制室30的流道截面积具有比压差检测用细管18的流道截面积大的流道截面积,所以通过测定流体流入该流动控制室30,流动控制室可以作为缓冲器发挥功能,从而在流动控制室30内降低流速,并使流体成为平稳的流动。At this time, since the flow channel cross-sectional area of the flow control chamber 30 has a flow channel cross-sectional area larger than the flow channel cross-sectional area of the thin tube 18 for differential pressure detection, by measuring the flow of fluid into the flow control chamber 30, the flow control chamber can be used as The snubber functions to reduce the flow velocity within the flow control chamber 30 and bring the fluid into a smooth flow.

因此,即使在例如轻油(MGO)之类被测定流体的粘度低的情况下,也能够消除在定流量泵14、输送管16上产生的被测定流体的流动的混乱,使被测定流体以层流状态在压差检测用细管18内流动,能够利用压差传感器24正确地检测压差检测用细管18的入口端18a与出口端18b之间的压力差,从而能够可靠地进行粘度测定。Therefore, even when the viscosity of the fluid to be measured is low such as light oil (MGO), the disturbance of the flow of the fluid to be measured generated on the constant flow pump 14 and the delivery pipe 16 can be eliminated, so that the fluid to be measured can be measured at a low viscosity. The laminar flow state flows in the thin tube 18 for differential pressure detection, and the pressure difference between the inlet port 18a and the outlet port 18b of the thin tube 18 for differential pressure detection can be accurately detected by the differential pressure sensor 24, so that the viscosity can be reliably measured. Determination.

该情况下,由于在压差检测用细管18的上游侧端部附近、即压差检测用细管18的入口端18a的附近配置有高压检测管22的入口端22a,所以在流动控制室30的下游侧、尤其在压差检测用细管18的上游侧端部附近,为平稳的流动,流动的混乱消失,从而能够利用压差传感器24来检测准确的高压侧的压力,其结果,能够可靠地进行粘度测定。In this case, since the inlet end 22a of the high-pressure detection tube 22 is disposed near the upstream end of the thin tube 18 for differential pressure detection, that is, near the inlet end 18a of the thin tube 18 for differential pressure detection, the flow control chamber The downstream side of 30, especially in the vicinity of the upstream side end of the thin tube 18 for differential pressure detection, is a smooth flow, and the turmoil of the flow disappears, so that the pressure on the high pressure side can be accurately detected by the differential pressure sensor 24. As a result, Enables reliable viscosity measurement.

该情况下,例如,如图3所示,在压差检测用细管18的长度L1为大约150mm、压差检测用细管18的长度L1与流动控制室30的长度L2的比L1:L2为3:2的情况下,如图2所示,压差检测用细管18的流道截面积S1与流动控制室30的流道截面积S2的比S1:S2为1:30~1:50,此时被测定流体以层流状态在压差检测用细管18内流动,从而优选。In this case, for example, as shown in FIG. 3 , when the length L1 of the thin tube 18 for differential pressure detection is about 150 mm, the ratio L1:L2 of the length L1 of the thin tube 18 for differential pressure detection to the length L2 of the flow control chamber 30 In the case of 3:2, as shown in Figure 2, the ratio S1:S2 of the flow channel cross-sectional area S1 of the thin tube 18 for differential pressure detection to the flow channel cross-sectional area S2 of the flow control chamber 30 is 1:30~1: 50. At this time, the fluid to be measured flows in the thin tube 18 for differential pressure detection in a laminar flow state, which is preferable.

另外,如图2所示,压差检测用细管18的内径d1、压差检测用细管18的外径d2、流动控制室30的内径d3的关系优选为如下设定。In addition, as shown in FIG. 2 , the relationship between the inner diameter d1 of the differential pressure detection thin tube 18 , the outer diameter d2 of the pressure difference detection thin tube 18 , and the inner diameter d3 of the flow control chamber 30 is preferably set as follows.

即,压差检测用细管18的内径d1通过定流量泵14的排出量来计算,雷诺数Re优选设定为诺数Re<2300,以使当被测定流体的动粘度为1mm2/s(cSt)时,在压差检测用细管18流动的被测定流体可靠地成为层流。That is, the inner diameter d1 of the thin tube 18 for differential pressure detection is calculated by the discharge rate of the constant flow pump 14, and the Reynolds number Re is preferably set to be the number Re<2300, so that when the dynamic viscosity of the fluid to be measured is 1 mm 2 /s (cSt), the fluid to be measured flowing through the thin tube 18 for differential pressure detection reliably becomes a laminar flow.

该情况下,为了计算雷诺数,根据下述的雷诺数计算式来计算即可。In this case, in order to calculate the Reynolds number, it may be calculated according to the following Reynolds number calculation formula.

Re=vd/vRe=vd/v

其中,v是流速,d是压差检测用细管18的内径,ν是被测定流体的动粘度。Here, v is the flow velocity, d is the inner diameter of the thin tube 18 for differential pressure detection, and ν is the dynamic viscosity of the fluid to be measured.

另外,优选设定为,考虑压差检测细管的外径d2而流动控制室30的内径d3设为约6倍,在流动控制室30内流动的被测定流体的流速设为压差检测用细管18内的流速的约1/30。In addition, it is preferable to set the inner diameter d3 of the flow control chamber 30 to about 6 times the outer diameter d2 of the pressure difference detection capillary, and the flow velocity of the fluid to be measured flowing in the flow control chamber 30 is set to be used for pressure difference detection. About 1/30 of the flow velocity in narrow tube 18.

由此,1mm2/s的被测定流体在流动控制室30内流动时的雷诺数Re为Re≈200,并成为平稳的流动,从而在压差检测用细管18流动的被测定流体可靠地成为层流。As a result, the Reynolds number Re of the fluid to be measured at 1 mm 2 /s flowing in the flow control chamber 30 is Re≈200, and the flow becomes smooth, so that the fluid to be measured flowing in the thin tube 18 for differential pressure detection is reliably become laminar flow.

例如,优选将压差检测用细管18的内径d1设为约将压差检测用细管18的外径d2设为约将流动控制室30的内径d3设为约 For example, it is preferable to set the inner diameter d1 of the thin tube 18 for differential pressure detection to about Set the outer diameter d2 of the thin tube 18 for differential pressure detection to about Set the inner diameter d3 of the flow control chamber 30 to about

另外,如图3所示,优选将压差检测用细管18的长度L1设为比直至被测定流体的层流状态完成为止的助起动间隔长的长度。In addition, as shown in FIG. 3 , it is preferable to set the length L1 of the thin tube 18 for differential pressure detection to be longer than the start-up interval until the laminar flow state of the fluid to be measured is completed.

该情况下,通过下述的助起动间隔的计算式,来设定压差检测用细管18的长度L1即可。In this case, the length L1 of the thin tube 18 for differential pressure detection may be set by the following formula for calculating the start-up interval.

L1=k·Re/dL1=k·Re/d

其中,Re是雷诺数,d是压差检测用细管18的内径,系数k是0.06~0.065。Wherein, Re is the Reynolds number, d is the inner diameter of the thin tube 18 for pressure difference detection, and the coefficient k is 0.06-0.065.

另外,流动控制室30的长度L2不需要是在流动控制室30内完成层流的长度,只需要是使在定流量泵26与输送管16上产生的副流(二次流)、乱流的状态消失的距离的长度。In addition, the length L2 of the flow control chamber 30 does not need to be the length to achieve laminar flow in the flow control chamber 30, but only needs to be such that the secondary flow (secondary flow) and turbulent flow generated on the constant flow pump 26 and the delivery pipe 16 The length of the distance over which the state disappears.

此外,通过将输送管16的下游端16a与流动控制室30的长度方向的后端部30b(图1中为右侧的流动控制室30的上游侧)连接,能够将在流动控制室30内流动的被测定流体平稳地流动的距离变长。另外,流动控制室30的被测定流体的更换也变快。In addition, by connecting the downstream end 16a of the delivery pipe 16 to the rear end 30b in the longitudinal direction of the flow control chamber 30 (the upstream side of the flow control chamber 30 on the right in FIG. The distance over which the flowing fluid to be measured smoothly flows becomes longer. In addition, replacement of the fluid to be measured in the flow control chamber 30 is also quickened.

根据实验,如图2所示,可知,在使压差检测用细管18的内径d1为约使压差检测用细管18的外径d2为约使流动控制室30的内径d3为约的情况下,流动控制室30的长度L2设为压差检测用细管18的长度L1的1/2左右足够,但为了充裕而优选设为压差检测用细管18的长度L1的2/3。According to the experiment, as shown in Figure 2, it can be known that the inner diameter d1 of the capillary tube 18 for differential pressure detection is about Make the outer diameter d2 of the thin tube 18 for differential pressure detection be about Make the inner diameter d3 of the flow control chamber 30 be about In the case of the flow control chamber 30, it is sufficient to set the length L2 of the flow control chamber 30 to about 1/2 of the length L1 of the thin tube 18 for differential pressure detection, but it is preferable to set it to 2/2 of the length L1 of the thin tube 18 for differential pressure detection in order to have ample room. 3.

即,压差检测用细管18的长度L1与流动控制室30的长度L2的比L1:L2优选为3:2。That is, the ratio L1:L2 of the length L1 of the thin tube for pressure difference detection 18 to the length L2 of the flow control chamber 30 is preferably 3:2.

并且,流动控制室30的下游端30c(图1中,为左侧的流动控制室30的下游端30c)与压差检测用细管18的入口端18a之间的间隙L3优选设定为与压差检测用细管18的外径d2相同程度的大小,以使被测定流体的流速基本不变化。Furthermore, the gap L3 between the downstream end 30c of the flow control chamber 30 (in FIG. 1 , the downstream end 30c of the flow control chamber 30 on the left side) and the inlet end 18a of the thin tube 18 for differential pressure detection is preferably set to be equal to The outer diameter d2 of the thin tube 18 for differential pressure detection is about the same size so that the flow velocity of the fluid to be measured does not change substantially.

此外,流动控制室30的下游端30c和压差检测用细管18的入口端18a之间的间隙L3与流动控制室30的长度L2的比L3:L2优选为1:25。In addition, the ratio L3:L2 of the gap L3 between the downstream end 30c of the flow control chamber 30 and the inlet end 18a of the thin tube for pressure difference detection 18 and the length L2 of the flow control chamber 30 is preferably 1:25.

例如,优选将压差检测用细管18的长度L1设为约150mm,将流动控制室30的长度L2设为约100mm,将流动控制室30的下游端30c与压差检测用细管18的入口端18a之间的间隙L3设为约4mm。For example, it is preferable to set the length L1 of the thin tube 18 for differential pressure detection to about 150 mm, the length L2 of the flow control chamber 30 to be about 100 mm, and connect the downstream end 30c of the flow control chamber 30 to the thin tube 18 for differential pressure detection. The gap L3 between the inlet ports 18a was set at about 4 mm.

并且,如图3所示,对于输送管16的下游端16a的与流动控制室30连接的位置而言,从流动控制室30的上游端30d开始的距离L4优选设定为流动控制室30的长度L2的1/10以内。And, as shown in FIG. 3 , for the position where the downstream end 16 a of the delivery pipe 16 is connected to the flow control chamber 30 , the distance L4 from the upstream end 30 d of the flow control chamber 30 is preferably set to be the length of the flow control chamber 30 . Within 1/10 of the length L2.

此外,该实施例中,对流动控制室30的截面形状为圆形的情况进行了说明,但流动控制室30的流道截面积具有比压差检测用细管18的流道截面积大的流道截面积即可,例如,可以为椭圆形、三角形、矩形、多边形状等,没有特别限定,根据上述说明的基准,适当地设定即可。In addition, in this embodiment, the case where the cross-sectional shape of the flow control chamber 30 is circular has been described, but the flow passage cross-sectional area of the flow control chamber 30 has a flow passage cross-sectional area larger than the flow passage cross-sectional area of the thin tube 18 for differential pressure detection. The cross-sectional area of the flow channel is sufficient, and may be, for example, elliptical, triangular, rectangular, polygonal, etc., and is not particularly limited, and may be appropriately set based on the criteria described above.

实施例2Example 2

图4是表示本发明的其他的实施例的细管式粘度计的示意图。Fig. 4 is a schematic view showing a narrow tube viscometer according to another embodiment of the present invention.

该实施例的细管式粘度计10与图1~图3所示的细管式粘度计10基本上为相同的构成,对于相同的构成部件附注相同的参照编号,而省略其详细的说明。The narrow tube viscometer 10 of this embodiment basically has the same configuration as the narrow tube viscometer 10 shown in FIGS.

上述的实施例1的细管式粘度计10中,在流动控制室30内配置压差检测用细管18的至少一部分,但在该实施例的细管式粘度计10中,也可以如图4所示那样,压差检测用细管18不位于流动控制室30内。In the capillary viscometer 10 of the above-mentioned embodiment 1, at least a part of the capillary 18 for differential pressure detection is arranged in the flow control chamber 30, but in the capillary viscometer 10 of this embodiment, it may be as shown in FIG. As shown in FIG. 4 , the thin tube 18 for differential pressure detection is not located in the flow control chamber 30 .

即,该实施例的细管式粘度计10中,如图4所示,输送管16的下游端16a与流动控制室30的长度方向的前端部30a(图1中,为左侧的流动控制室30的上游侧)连接。That is, in the capillary viscometer 10 of this embodiment, as shown in FIG. The upstream side of chamber 30) is connected.

另外,压差检测用细管18的入口端18a与流动控制室30的下游端30c(图4中,为右侧的流动控制室30的下游端30c)连接。In addition, the inlet end 18a of the thin tube 18 for differential pressure detection is connected to the downstream end 30c of the flow control chamber 30 (in FIG. 4 , the downstream end 30c of the flow control chamber 30 on the right side).

并且,在流动控制室30的长度方向的后端部30b(图4中,为右侧的流动控制室30的下游侧),即在压差检测用细管18的入口端18a的附近,配置有高压检测管22的入口端22a。And, at the rear end portion 30b in the longitudinal direction of the flow control chamber 30 (in FIG. 4 , the downstream side of the flow control chamber 30 on the right side), that is, near the inlet end 18a of the thin tube 18 for differential pressure detection, a There is an inlet port 22a of the high pressure sensing tube 22 .

该实施例的细管式粘度计10中,也能够使在定流量泵26与输送管16上产生的被测定流体的流动的混乱成为平稳的流动。Also in the capillary viscometer 10 of this embodiment, it is possible to make the turbulence of the flow of the fluid to be measured generated in the constant flow pump 26 and the delivery pipe 16 into a smooth flow.

但是,压差检测用细管18需要为恒定的长度,从而无法使流动控制室30的长度L2变长。However, the thin tube 18 for differential pressure detection needs to have a constant length, and the length L2 of the flow control chamber 30 cannot be increased.

因此,例如,在图4的纸面使流动控制室30的纵深方向的长度变长,或者在流动控制室30为圆筒形状的情况下,使流动控制室30的内径d3变大,由此能够缩短流动控制室30的长度L2,但对此未图示。Therefore, for example, the length of the flow control chamber 30 in the depth direction is increased on the page of FIG. The length L2 of the flow control chamber 30 can be shortened, but this is not shown.

实施例3Example 3

图5是本发明的其他的实施例的细管式粘度计的流动控制室的放大图。Fig. 5 is an enlarged view of a flow control chamber of a narrow tube viscometer according to another embodiment of the present invention.

该实施例的细管式粘度计10与图4所示的细管式粘度计10基本上为相同的构成,对于相同的构成部件附注相同的参照编号,而省略其详细的说明。The capillary viscometer 10 of this embodiment basically has the same configuration as the capillary viscometer 10 shown in FIG. 4 , and the same components are assigned the same reference numerals, and detailed description thereof will be omitted.

上述的实施例2的细管式粘度计10中,若直线状(水平方向)配置输送管16与压差检测用细管18,则需要考虑由输送管16的流入口(输送管16的下游端16a)的流动的混乱对压差检测用细管18的影响。In the capillary viscometer 10 of the above-mentioned embodiment 2, if the conveying pipe 16 and the capillary for pressure difference detection 18 are arranged in a straight line (horizontal direction), it is necessary to consider The influence of the disturbance of the flow at end 16a) on the thin tube 18 for differential pressure detection.

这样,上述的实施例2的细管式粘度计10中,流动控制室30形成为长度方向为水平方向,但在该实施例中,流动控制室30如图5所示那样,在上下方向上配置。In this way, in the capillary viscometer 10 of the above-mentioned embodiment 2, the flow control chamber 30 is formed so that the longitudinal direction is the horizontal direction, but in this embodiment, the flow control chamber 30 is vertically vertical as shown in FIG. 5 . configuration.

即,输送管16的下游端16a配置于流动控制室30的上端30e附近,并且,压差检测用细管18的入口端18a配置于流动控制室30的下端30f附近。That is, the downstream end 16a of the delivery pipe 16 is disposed near the upper end 30e of the flow control chamber 30 , and the inlet end 18a of the thin tube 18 for differential pressure detection is disposed near the lower end 30f of the flow control chamber 30 .

通过这样构成,输送管16与压差检测用细管18的设置位置错开,并且,合成用于使在流动控制室30内流动的被测定流体的流动平稳的距离。With such a configuration, the installation positions of the delivery tube 16 and the pressure difference detection capillary 18 are shifted, and a distance is combined to stabilize the flow of the fluid to be measured flowing in the flow control chamber 30 .

以上,对本发明的优选的实施的方式进行了说明,但本发明不限定于此,例如,上述实施例中,用于例如轻油(MGO)之类粘度低的被测定流体,但也可以在对例如A重油(MDO)、C重油(MFO)之类粘度高的流体、并且油以外的其他的流体的粘度进行测定的情况下使用等,在不脱离本发明的目的的范围内能够有各种的变更。The preferred embodiment of the present invention has been described above, but the present invention is not limited thereto. For example, in the above-mentioned examples, it is used for a fluid to be measured with low viscosity such as light oil (MGO), but it may also be used in For example, when measuring the viscosity of high-viscosity fluids such as A heavy oil (MDO) and C heavy oil (MFO), and other fluids other than oil, it can be used in various ways without departing from the purpose of the present invention. species change.

产业上的可利用性Industrial availability

能够用于如下构成的细管式粘度计,即,通过使例如A重油(MDO)、轻油(MGO)等被测定流体在压差检测用细管内流动,而利用压差传感器来检测压差检测用细管的入口端与出口端的压差,来测定流体的粘度。It can be used in a capillary viscometer configured to detect differential pressure with a differential pressure sensor by flowing a fluid to be measured such as A heavy oil (MDO) or light oil (MGO) in a capillary for differential pressure detection The pressure difference between the inlet port and the outlet port of the thin tube is used to measure the viscosity of the fluid.

Claims (2)

1.一种细管式粘度计,其构成为,使被测定流体在压差检测用细管内流动,利用压差传感器来检测压差检测用细管的入口端与出口端的压差,由此来测定流体的粘度,该细管式粘度计的特征在于,1. A narrow tube type viscometer, which is constituted by making the fluid to be measured flow in the narrow tube for differential pressure detection, and using a differential pressure sensor to detect the pressure difference between the inlet end and the outlet end of the thin tube for differential pressure detection, thereby To measure the viscosity of the fluid, the capillary viscometer is characterized in that, 在所述压差检测用细管的上游侧设有流动控制室,该流动控制室具有比压差检测用细管的流道截面积大的流道截面积,上述流动控制室降低上述流体的流速并使上述流体平稳地流动,A flow control chamber is provided on the upstream side of the thin tube for differential pressure detection. The flow control chamber has a flow channel cross-sectional area larger than that of the thin tube for differential pressure detection. The flow control chamber reduces the flow rate of the fluid. flow rate and make the above fluid flow smoothly, 在所述流动控制室内,配置有压差检测用细管的至少一部分。In the flow control chamber, at least a part of the thin tube for differential pressure detection is disposed. 2.根据权利要求1所述的细管式粘度计,其特征在于,2. capillary viscometer according to claim 1, is characterized in that, 将配置有所述压差传感器的支管的高压侧检测管的入口配置于所述流动控制室的下游侧。An inlet of a high-pressure side detection pipe in which the branch pipe of the differential pressure sensor is arranged is arranged on the downstream side of the flow control chamber.
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