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CN102940228A - Composite sweetening agent applied to coffee and preparation method thereof - Google Patents

Composite sweetening agent applied to coffee and preparation method thereof Download PDF

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Publication number
CN102940228A
CN102940228A CN2012105009978A CN201210500997A CN102940228A CN 102940228 A CN102940228 A CN 102940228A CN 2012105009978 A CN2012105009978 A CN 2012105009978A CN 201210500997 A CN201210500997 A CN 201210500997A CN 102940228 A CN102940228 A CN 102940228A
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maltitol
fluidized bed
fluid bed
spraying
mixed material
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历冠廷
马力量
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Suzhou Industrial Park Shangrong Technology Co Ltd
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Suzhou Industrial Park Shangrong Technology Co Ltd
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Abstract

The invention relates to a composite sweetening agent applied to coffee and a preparation method thereof. The composite sweetening agent comprises the following components: 3.33-8.33 percent of sucralose, 45-65 percent of maltitol, 25-43 percent of erythritol, 1-4 percent of edible salt and 0.05-0.3 percent of sodium carboxymethylcellulose; and the process comprises the following steps of: putting the erythritol and the maltitol accounting for 60-70 percent of the total amount into a multi-dimensional blending machine for primary blending; adding the sucralose, the rest of the maltitol and other auxiliary materials into the water to obtain a mixed water liquid; allowing the materials which are primarily blended to enter a fluidized bed from the bottom of a spraying fluidized bed to increase the flowing from bottom to top under positive pressure; applying negative pressure to the upper part of the spraying fluidized bed to vibrate from top to bottom to boil the mixed materials up and down in the fluidized bed to form fine sugar alcohol small particulars; continuously spraying the mixed water liquid by a multi-point spray gun on the side of the fluidized bed and dispersing the mixed water solution to the sugar alcohol small particulars inside the fluidized bed to dry in hot air so as to prepare the composite sweetening agent.

Description

A kind of composite sweetener that is adapted at using in the coffee and preparation method thereof
Technical field
The present invention relates to a kind of food additives, be specifically related to a kind of composite sweetener that is adapted at using in the coffee and preparation method thereof.
Background technology
In the last few years, raising along with expanding economy and people's lives wealth, obesity, hypertension, diabetes, carious tooth etc. become the height morbidity among the crowd, and the generation of these high morbidities is considered to especially with the sucrose Excessive Intake substantial connection is arranged with eating habit and diet structure.Therefore, as the sweetener of food additives, one of its development priority is exactly safe, without nutritive value, empty calory or functional high sweetener extremely low in calories.The characteristics of functional high sweetener are use safe, and consumption is few, and sugariness is high, and use cost is generally all far below sucrose, and this also is the power place that Food Science man continually develops novel high-intensity sweetener.At present, about 20 kinds of the granted high sweetener in countries in the world obtains that kind that the majority state approval allows to use mainly contains that saccharin sodium, honey element, 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one 2,2-dioxide potassium salt, Aspartame, Sucralose, alitame, knob are sweet, glycyrrhizin, stevioside, Momordica grosvenori is sweet and Talin etc.These high sweeteners have plenty of artificial synthetic, and are sweet etc. such as Aspartame, Sucralose, knob; What have then is natural extract, sweet etc. such as sky chrysanthemum glycosides and arhat.No matter be artificial synthesis edulcorant or natural extraction sweetener, at sugariness, sweet taste, stable aspects its pluses and minuses arranged respectively all, therefore, want to give full play to the optimal efficacy of these sweeteners, reduce cost, the most frequently used means are exactly compound at present.By carrying out various sweeteners or sweet substance compound, bring into play may exist between the various sweeteners synergistic function, in the hope of as far as possible approaching or satisfy the requirement of desirable sweetener: safety non-toxic, sweet taste is pure similar to sucrose (this is to be popular generally accepted sweet tastes), high sugariness, low heat value or without calorific value, stable height, unlikely dental caries, reduction cost.
In the prior art, when being applied in coffee as main sweet composite sweetener is used as for sugar take Sucralose, with use traditional white granulated sugar to compare certain difference is arranged on the mouthfeel, particularly the sugariness of composite sweetener is high, consumption is few, so that the dense thick sense of coffee is lowered, the coffee bitter taste is given prominence to, is difficult to cover, thereby these composite sweeteners also are not easy to be accepted by masses.
Composite sweetener take Sucralose as main sweetening material in the prior art, can process by method or the spray-dired method of substep of simple blend, the composite sweetener that the simple blend method makes is with low cost, but be difficult to guarantee that main sweetening material Sucralose can be uniformly dispersed, and this point can affect the quality of composite sweetener product to a great extent.The spray-dired method of substep is that substep is dissolved in main sweetening material and each auxiliary sweetening material in the deionized water in batches, then the method by the wet spray drying is coated on each composition material on the granular sweetener by spraying respectively, the composite sweetener product sweetness that this method makes is uniformly dispersed, instant capacity is good, quality is better than the composite sweetener product that additive method makes, but its shortcoming is: material loss, the loss of especially main sweetening material is larger, machinery equipment power consumption is too high, the cost of product is significantly increased, and therefore this method also has been subject to certain restriction in implementation process.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of with low cost, sugariness is uniformly dispersed and mouthfeel is better composite sweetener that is adapted at using in the coffee and preparation method thereof is provided.
Purpose of the present invention is achieved through the following technical solutions:
A kind of composite sweetener that is adapted at using in the coffee comprises following percentage by weight composition: Sucralose 3.33~8.33%, maltitol 45~65%, antierythrite 25~43%, salt 1~4%, sodium carboxymethylcellulose 0.05~0.3%; Its preparation method comprises following processing step:
1. antierythrite and the maltitol that accounts for total amount 60 ~ 70% are dropped in the Multidimensionblender, mixed 20 ~ 50 minutes with the progression of 600 ~ 1000rpm, the granularity of control mixed material obtains the mixed material of antierythrite and maltitol at 80 ~ 130 orders;
2. the maltitol with Sucralose, salt, sodium carboxymethylcellulose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose, salt, sodium carboxymethylcellulose and maltitol;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
The preparation method of a kind of composite sweetener that is adapted at using in the coffee of the present invention comprises following processing step:
1. antierythrite and the maltitol that accounts for total amount 60 ~ 70% are dropped in the Multidimensionblender, mixed 20 ~ 50 minutes with the progression of 600 ~ 1000rpm, the granularity of control mixed material obtains the mixed material of antierythrite and maltitol at 80 ~ 130 orders;
2. the maltitol with Sucralose, salt, sodium carboxymethylcellulose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose, salt, sodium carboxymethylcellulose and maltitol;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
Further, the preparation method of above-mentioned a kind of composite sweetener that is adapted at using in the coffee, step 3. in, when mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 35 ~ 60 ℃, and the EAT of control fluid bed is at 70 ~ 90 ℃ during heated-air drying.
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
Composite sweetener of the present invention utilizes the synergy of sodium carboxymethylcellulose, salt and antierythrite, improve composite sweetener reduces coffee in coffee dense thick sense, make the bitter taste distinct issues, each composition collocation is scientific and reasonable in the composition of raw materials, pro rate is at optimum range, so that composite sweetener of the present invention is when being applied in the coffee, mouthfeel, local flavor are more near consumer's sweet taste demand.
The present invention drops into the auxiliary sweetening material of the part of composite sweetener in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and disperse dry by the disposable spraying of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy has reduced production cost (about 60 ~ 90 minutes of product manufacturing cycle of the present invention, and in batches about 2 ~ 3 hours of the manufacturing cycle of spray drying process).
The specific embodiment
Composite sweetener of the present invention, its composition is: Sucralose 3.33~8.33%, maltitol 45~65%, antierythrite 25~43%, salt 1~4%, sodium carboxymethylcellulose 0.05~0.3%.
The preparation technology of composite sweetener: first antierythrite and the maltitol that accounts for total amount 60 ~ 70% are dropped in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of antierythrite and maltitol at 80 ~ 130 orders; Maltitol with Sucralose, salt, sodium carboxymethylcellulose and surplus is dissolved in the deionized water again, obtains the mixed aqueous solution of Sucralose, salt, sodium carboxymethylcellulose and maltitol; Then mixed material is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 35 ~ 60 ℃, pass through again heated-air drying, the EAT of control fluid bed obtains described composite sweetener at 70 ~ 90 ℃ during heated-air drying.
Multidimensionblender used in the present invention adopts commercial 200 feather weight Multidimensionblenders, rotating speed level journey is 200 ~ 1800rpm, barrel is two taper, middle column, and during work, this Multidimensionblender can make the material in the barrel collide, pulverize and mix from a plurality of angles.
Embodiment 1:
(1) get in 35 kilograms of antierythrites, 40 kilograms of inputs of the maltitol Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixes 40 minutes, obtains the mixed material of antierythrite and maltitol, and granularity is between 80 ~ 130 orders;
(2) 20 kilograms of 3.33 kilograms of Sucraloses, 1.5 kilograms of salt, 0.17 kilogram of sodium carboxymethylcellulose, remaining maltitol are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose, salt, sodium carboxymethylcellulose and maltitol;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 35 ~ 60 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 90 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 2:
(1) get in 34 kilograms of antierythrites, 38 kilograms of inputs of the maltitol Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixes 40 minutes, obtains the mixed material of antierythrite and maltitol, and granularity is between 80 ~ 130 orders;
(2) 21 kilograms of 5 kilograms of Sucraloses, 1.75 kilograms of salt, 0.25 kilogram of sodium carboxymethylcellulose, remaining maltitol are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose, salt, sodium carboxymethylcellulose and maltitol;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 35 ~ 60 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 90 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 3:
(1) get in 35.58 kilograms of antierythrites, 36 kilograms of inputs of the maltitol Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixes 40 minutes, obtains the mixed material of antierythrite and maltitol, and granularity is between 80 ~ 130 orders;
(2) 19 kilograms of 6.67 kilograms of Sucraloses, 2.5 kilograms of salt, 0.25 kilogram of sodium carboxymethylcellulose, remaining maltitol are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose, salt, sodium carboxymethylcellulose and maltitol;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 35 ~ 60 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 90 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 4:
(1) get in 35.87 kilograms of antierythrites, 33.8 kilograms of inputs of the maltitol Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixes 35 minutes, obtains the mixed material of antierythrite and maltitol, and granularity is between 80 ~ 130 orders;
(2) 18.2 kilograms of 8.33 kilograms of Sucraloses, 3.5 kilograms of salt, 0.3 kilogram of sodium carboxymethylcellulose, remaining maltitol are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose, salt, sodium carboxymethylcellulose and maltitol;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 35 ~ 60 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 90 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
The composite sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
Figure 994866DEST_PATH_IMAGE002
Composite sweetener of the present invention utilizes the synergy of sodium carboxymethylcellulose, salt and antierythrite, improve composite sweetener reduces coffee in coffee dense thick sense, make the bitter taste distinct issues, each composition collocation is scientific and reasonable in the composition of raw materials, pro rate is at optimum range, so that composite sweetener of the present invention is when being applied in the coffee, mouthfeel, local flavor are more near consumer's sweet taste demand.
The present invention drops into the auxiliary sweetening material of the part of composite sweetener in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and disperse dry by the disposable spraying of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy, reduced production cost (about 60 ~ 90 minutes of product manufacturing cycle of the present invention, and about 2 ~ 3 hours of the manufacturing cycle of spray drying process in batches, and the present invention just the mixed power consumption that uses Multidimensionblender be approximately fluidized bed with spraying electricity consumption of equipment amount 1/24).
The sugariness degree of modification of composite sweetener of the present invention can be adjusted by the consumption of Sucralose according to actual needs, and the present invention is fit to the composite sweetener of 20~50 times of sucrose sweetness of preparation usually.
What need to understand is: the above only is preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.

Claims (3)

1. a composite sweetener that is adapted at using in the coffee is characterized in that comprising following percentage by weight composition: Sucralose 3.33~8.33%, maltitol 45~65%, antierythrite 25~43%, salt 1~4%, sodium carboxymethylcellulose 0.05~0.3%; Its preparation method comprises following processing step:
1. antierythrite and the maltitol that accounts for total amount 60 ~ 70% are dropped in the Multidimensionblender, mixed 20 ~ 50 minutes with the progression of 600 ~ 1000rpm, the granularity of control mixed material obtains the mixed material of antierythrite and maltitol at 80 ~ 130 orders;
2. the maltitol with Sucralose, salt, sodium carboxymethylcellulose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose, salt, sodium carboxymethylcellulose and maltitol;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
2. the preparation method of a kind of composite sweetener that is adapted at using in the coffee claimed in claim 1 is characterized in that comprising following processing step:
1. antierythrite and the maltitol that accounts for total amount 60 ~ 70% are dropped in the Multidimensionblender, mixed 20 ~ 50 minutes with the progression of 600 ~ 1000rpm, the granularity of control mixed material obtains the mixed material of antierythrite and maltitol at 80 ~ 130 orders;
2. the maltitol with Sucralose, salt, sodium carboxymethylcellulose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose, salt, sodium carboxymethylcellulose and maltitol;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
3. the preparation method of a kind of composite sweetener that is adapted at using in the coffee according to claim 2, it is characterized in that: step 3. in, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 35 ~ 60 ℃, and the EAT of control fluid bed is at 70 ~ 90 ℃ during heated-air drying.
CN2012105009978A 2012-11-30 2012-11-30 Composite sweetening agent applied to coffee and preparation method thereof Pending CN102940228A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105594944A (en) * 2015-12-21 2016-05-25 株洲千金药业股份有限公司 Semen cassiae instant coffee and preparation method thereof

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WO2011113799A1 (en) * 2010-03-15 2011-09-22 Nestec S.A. Artificial sweeteners and performance
CN102224920A (en) * 2011-05-11 2011-10-26 深圳市纽全德生物科技有限公司 Liquid table sweetener and preparation method thereof
CN102228175A (en) * 2011-05-11 2011-11-02 深圳市纽全德生物科技有限公司 Crystal-granular sweetener for dining, and preparation method thereof
CN102370027A (en) * 2011-10-14 2012-03-14 大连创达技术交易市场有限公司 Healthy instant coffee
CN102511774A (en) * 2011-12-15 2012-06-27 苏州工业园区尚融科技有限公司 Compound sugarless sweetener for drink and preparation method for same

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1254522A (en) * 1999-12-09 2000-05-31 北京恒毅利科贸有限责任公司 Method for preparing granular flavouring enriched food and its product
WO2011113799A1 (en) * 2010-03-15 2011-09-22 Nestec S.A. Artificial sweeteners and performance
CN102224920A (en) * 2011-05-11 2011-10-26 深圳市纽全德生物科技有限公司 Liquid table sweetener and preparation method thereof
CN102228175A (en) * 2011-05-11 2011-11-02 深圳市纽全德生物科技有限公司 Crystal-granular sweetener for dining, and preparation method thereof
CN102370027A (en) * 2011-10-14 2012-03-14 大连创达技术交易市场有限公司 Healthy instant coffee
CN102511774A (en) * 2011-12-15 2012-06-27 苏州工业园区尚融科技有限公司 Compound sugarless sweetener for drink and preparation method for same

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105594944A (en) * 2015-12-21 2016-05-25 株洲千金药业股份有限公司 Semen cassiae instant coffee and preparation method thereof

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Application publication date: 20130227