CN102936460A - Asphalt rubber waterproof coating material - Google Patents
Asphalt rubber waterproof coating material Download PDFInfo
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- CN102936460A CN102936460A CN201210351566XA CN201210351566A CN102936460A CN 102936460 A CN102936460 A CN 102936460A CN 201210351566X A CN201210351566X A CN 201210351566XA CN 201210351566 A CN201210351566 A CN 201210351566A CN 102936460 A CN102936460 A CN 102936460A
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- asphalt waterproof
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- 238000000576 coating method Methods 0.000 title claims abstract description 21
- 239000011248 coating agent Substances 0.000 title claims abstract description 20
- 239000000463 material Substances 0.000 title abstract description 8
- 239000011387 rubberized asphalt concrete Substances 0.000 title description 2
- 239000010426 asphalt Substances 0.000 claims abstract description 28
- 229920001971 elastomer Polymers 0.000 claims abstract description 15
- 239000005060 rubber Substances 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000000049 pigment Substances 0.000 claims abstract description 9
- ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 7
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 7
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 claims abstract description 7
- 229920002401 polyacrylamide Polymers 0.000 claims abstract description 7
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910010271 silicon carbide Inorganic materials 0.000 claims abstract description 7
- 244000043261 Hevea brasiliensis Species 0.000 claims abstract description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 6
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229920003052 natural elastomer Polymers 0.000 claims abstract description 6
- 229920001194 natural rubber Polymers 0.000 claims abstract description 6
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 6
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000008117 stearic acid Substances 0.000 claims abstract description 6
- 229920003048 styrene butadiene rubber Polymers 0.000 claims abstract description 6
- 229920001169 thermoplastic Polymers 0.000 claims abstract description 6
- 239000004416 thermosoftening plastic Substances 0.000 claims abstract description 6
- 239000005038 ethylene vinyl acetate Substances 0.000 claims abstract description 5
- 239000004709 Chlorinated polyethylene Substances 0.000 claims abstract description 4
- 239000002994 raw material Substances 0.000 claims abstract description 4
- 239000013543 active substance Substances 0.000 claims description 14
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 9
- 239000004902 Softening Agent Substances 0.000 claims description 8
- 239000013530 defoamer Substances 0.000 claims description 8
- 229920000126 latex Polymers 0.000 claims description 7
- 239000000839 emulsion Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 239000011301 petroleum pitch Substances 0.000 claims description 6
- 239000011295 pitch Substances 0.000 claims description 6
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 5
- -1 polyoxyethylene Polymers 0.000 claims description 5
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 4
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 101100008049 Caenorhabditis elegans cut-5 gene Proteins 0.000 claims description 3
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 3
- 239000003945 anionic surfactant Substances 0.000 claims description 3
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical group [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- 238000010008 shearing Methods 0.000 claims description 3
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims description 3
- LAXBNTIAOJWAOP-UHFFFAOYSA-N 2-chlorobiphenyl Chemical group ClC1=CC=CC=C1C1=CC=CC=C1 LAXBNTIAOJWAOP-UHFFFAOYSA-N 0.000 claims description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 2
- ZLFVRXUOSPRRKQ-UHFFFAOYSA-N chembl2138372 Chemical compound [O-][N+](=O)C1=CC(C)=CC=C1N=NC1=C(O)C=CC2=CC=CC=C12 ZLFVRXUOSPRRKQ-UHFFFAOYSA-N 0.000 claims description 2
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 claims description 2
- 150000002790 naphthalenes Chemical class 0.000 claims description 2
- 229920001451 polypropylene glycol Polymers 0.000 claims description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 2
- 230000006378 damage Effects 0.000 abstract description 3
- 239000002518 antifoaming agent Substances 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 239000004014 plasticizer Substances 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- 239000003973 paint Substances 0.000 description 15
- 238000004078 waterproofing Methods 0.000 description 8
- 238000011056 performance test Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000032798 delamination Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002431 foraging effect Effects 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 229920001084 poly(chloroprene) Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
The present invention provides a rubber asphalt waterproof coating material, and belongs to the technical field of coating materials. The coating material is prepared from the following raw materials, by weight, 20-35 parts of a natural rubber, 10-15 parts of a thermoplastic styrene-butadiene rubber, 5-10 parts of acrylic resin, 3-5 parts of ethylene glycol ethyl ether, 20-30 parts of asphalt, 5-10 parts of chlorinated polyethylene, 1-2 parts of silicon carbide crystal whiskers, 3-6 parts of talc powder, 2-4 parts of diatomite , 2-4 parts of stearic acid, 3-8 parts of polyacrylamide, 6-9 parts of an ethylene-vinyl acetate copolymer, 3-5 parts of a plasticizer, 1-2 parts of a defoaming agent, 8-15 parts of a pigment, 2-3 parts of a surfactant, and 40-50 parts of water. The waterproof coating material provided by the embodiments still has good watertightness and good mechanical property after high temperature and high humidity destruction.
Description
Technical field
The invention provides a kind of rubber asphalt waterproof coating, belong to technical field of coatings.
Background technology
Building water-proof paint system is main body by synthesized polymer material, pitch, polymer modified asphalt, inorganic materials etc., mixes the water-proof material of solvent-borne type, water-soluble, water-latex type or powder-type that an amount of auxiliary agent, material modified, packing material etc. are processed into.Compare with waterproof roll, the waterproof paint construction is simple and convenient, is applicable to the basal plane of any shape, and can form fine and close seamless filming, and therefore, waterproof paint has been widely used in the various waterproofing works, and has obtained rapidly development.
Wherein, rubber asphalt class synthetic macromolecule class waterproof paint is just occupying increasing proportion in China's waterproofing work is used.Its raw material sources is extensive, and cost is lower, the general waterproofing work of large light of the amount of being applicable to.China has carried out relatively large work for improve petroleum pitch configuration waterproof paint aspect with superpolymer.Chloroprene rubber has appearred in the mid-1960s--asphalt waterproofing paint, and regenerated rubber has appearred in the initial stage seventies--asphalt waterproofing paint, and in the more successful application of engineering acquisition.Announced national standard " Technical code for roof engineering " in April, 1994, clear and definite regulation has all been made in specification of quality, coating waterproofing engineering design main points, constructional method, the acceptance of work and the maintenance of China's waterproof paint.
But some asphalt waterproofing paints still are not very good at aspects such as mechanical property, water resistance and weather resistance.At high temperature it the problems such as embrittlement delamination can occur occurring under creep trickling, the low temperature, has had influence on the water resistance of buildings.
Summary of the invention
For above commentary to prior art, technical problem to be solved by this invention is: the problem that the endurance quality of rubber asphalt waterproof coating is not good.Adopt following technical scheme:
A kind of rubber asphalt waterproof coating is made by the raw material of following weight part meter: 20～35 parts of natural rubbers, 10～15 parts of thermoplastic styrene butadiene rubbers, 5～10 parts of acrylic resins, 3～5 parts of ethylene glycol ethyl ethers, 20～30 parts of pitches, 5～10 parts of chlorinatedpolyethylenees, 1～2 part of silicon carbide whisker, 3～6 parts of talcum powder, 2～4 parts in diatomite, 2～4 parts of stearic acid, 3～8 parts of polyacrylamides, 6～9 parts of ethylene-vinyl acetate copolymers, 3～5 parts in softening agent, 1～2 part of defoamer, 8～15 parts of pigment, 2～3 parts in tensio-active agent, 40～50 parts in water.
Above-mentioned pitch is a kind of in 90# petroleum pitch, 10# petroleum pitch preferably.
Above-mentioned defoamer is one or more mixtures in polyoxyethylene glycol, polypropylene glycol, acetylenic glycol, polyvinyl alcohol preferably.
Above-mentioned softening agent is one or more mixtures in clorafin, chlorodiphenyl, chlorinated naphthalene, dibutyl phthalate preferably.
Above-mentioned tensio-active agent is preferably anion surfactant, more preferably is Sodium dodecylbenzene sulfonate.
Above-mentioned pigment can be selected from one or more mixtures in rutile type, phthalocyanine blue, fast light Huang, toluidine red, chromoxide green, red iron oxide, barba hispanica, the iron oxide yellow.Its preparation method is as follows:
S1: natural rubber, thermoplastic styrene butadiene rubber under 70～80 ℃ of conditions, are carried out after thin-pass plasticates, add the tensio-active agent of half weight, mixing evenly;
S2: enter shears behind the lower sheet, under 70～80 ℃ of conditions, to be rotated shearing under 500～600rpm rotating speed;
S3: again in the S2 products therefrom, add the tensio-active agent of half weight and the water of half weight, sheared 30 minutes, 800～900rpm rotating speed down cut 5 minutes, get rubber latex again;
S4: with asphalt heating to 140～160 ℃, insulation stirs, and adds remaining tensio-active agent and water again, stirs, and gets bitumen emulsion;
S5: rubber latex, bitumen emulsion are mixed with acrylic resin, ethylene glycol ethyl ether, chlorinatedpolyethylene, silicon carbide whisker, talcum powder, diatomite, stearic acid, polyacrylamide, ethylene-vinyl acetate copolymer, softening agent, defoamer, pigment, under 40～50 ℃, stir, let cool, and get final product.
Silicon carbide whisker in the waterproof paint provided by the invention, polyacrylamide and ethylene-vinyl acetate copolymer are organic dispersing agents, can make the homogeneous program of each component in the coating better, are easy to preparation and storage.Acrylic resin can make coating produce the performance of UV resistant, is difficult for aging, embrittlement, adds simultaneously ethylene glycol ethyl ether and can guarantee compatibility and workability.
Technique effect
Waterproof paint provided by the invention still has good watertightness and mechanical property through after the hot and humid destruction.Be applicable to the roofworks of common buildings and lavatory bathe between, the engineering waterproofing such as between the kitchen; Also be applicable to the protection against the tide of roofing and vault, body of wall etc.
Embodiment
Prepare each component by the weight ratio shown in the table 1.
The weight proportion of table 1 embodiment 1～embodiment 3
Above-mentioned pitch adopts 90# petroleum pitch.
Above-mentioned defoamer adopts polyoxyethylene glycol.
Above-mentioned softening agent adopts clorafin.
Above-mentioned tensio-active agent adopts Sodium dodecylbenzene sulfonate.
Above-mentioned pigment adopts red iron oxide.
Its preparation method is as follows:
Embodiment 1
S1: natural rubber, thermoplastic styrene butadiene rubber under 70～80 ℃ of conditions, are carried out after thin-pass plasticates, add the tensio-active agent of half weight, mixing evenly;
S2: enter shears behind the lower sheet, under 70 ℃ of conditions, to be rotated shearing under the 500rpm rotating speed;
S3: again in the S2 products therefrom, add the tensio-active agent of half weight and the water of half weight, sheared 30 minutes, 800rpm rotating speed down cut 5 minutes, get rubber latex again;
S4: with asphalt heating to 140 ℃, insulation stirs, and adds remaining tensio-active agent and water again, stirs, and gets bitumen emulsion;
S5: rubber latex, bitumen emulsion are mixed with acrylic resin, ethylene glycol ethyl ether, chlorinatedpolyethylene, silicon carbide whisker, talcum powder, diatomite, stearic acid, polyacrylamide, ethylene-vinyl acetate copolymer, softening agent, defoamer, pigment, under 40 ℃, stir, let cool, and get final product.
Embodiment 2
Be with the difference of embodiment 1: the temperature among the step S1 is 75 ℃; Temperature is 75 ℃ among the step S2, and rotating speed is 550rpm; Among the step S3, rotating speed is 850rpm; Temperature is 150 ℃ among the step S4; Temperature is 45 ℃ among the step S5.
Embodiment 3
Be with the difference of embodiment 1: the temperature among the step S1 is 80 ℃; Temperature is 80 ℃ among the step S2, and rotating speed is 600rpm; Among the step S3, rotating speed is 900rpm; Temperature is 160 ℃ among the step S4; Temperature is 50 ℃ among the step S5.
Performance test
The rubber asphalt waterproof coating of above-described embodiment gained is made a service test according to JC/T975-2005 " bridge waterproof paint ", and take commercially available conventional rubber asphalt waterproof coating as contrast.Test-results is as shown in table 2.
The performance test data of table 2 embodiment 1～embodiment 3 and reference examples
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Reference examples | |
| Tensile strength MPa | 1.3 | 1.4 | 1.3 | 1.1 |
| Elongation at break % | 850 | 860 | 850 | 800 |
| Low temperature flexibility degree ℃ | -30 | -29 | -30 | -21 |
| Watertightness (0.3MPa, 30min) | Ne-leakage | Ne-leakage | Ne-leakage | Ne-leakage |
In order to characterize the endurance quality of above embodiment waterproof paint, above-mentioned sample is placed constant temperature thermostat container (50 ℃, 80% humidity), took out afterwards in 30 days, repeat above-mentioned test subject, acquired results is as shown in table 3.
Table 3 embodiment 1～embodiment 3 and the performance test data of reference examples after rupture test
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Reference examples | |
| Tensile strength MPa | 1.2 | 1.3 | 1.3 | 0.8 |
| Elongation at break % | 760 | 770 | 760 | 530 |
| Low temperature flexibility degree ℃ | -30 | -28 | -27 | -18 |
[0046]
| Watertightness (0.3MPa, 30min) | Ne-leakage | Ne-leakage | Ne-leakage | Seepage appears |
Can see from table, the waterproof paint that the present embodiment provides still has good watertightness and mechanical property through after the hot and humid destruction.
Claims (7)
1. rubber asphalt waterproof coating, raw material by following weight part meter is made: 20～35 parts of natural rubbers, 10～15 parts of thermoplastic styrene butadiene rubbers, 5～10 parts of acrylic resins, 3～5 parts of ethylene glycol ethyl ethers, 20～30 parts of pitches, 5～10 parts of chlorinatedpolyethylenees, 1～2 part of silicon carbide whisker, 3～6 parts of talcum powder, 2～4 parts in diatomite, 2～4 parts of stearic acid, 3～8 parts of polyacrylamides, 6～9 parts of ethylene-vinyl acetate copolymers, 3～5 parts in softening agent, 1～2 part of defoamer, 8～15 parts of pigment, 2～3 parts in tensio-active agent, 40～50 parts in water, its preparation method is:
S1: natural rubber, thermoplastic styrene butadiene rubber under 70～80 ℃ of conditions, are carried out after thin-pass plasticates, add the tensio-active agent of half weight, mixing evenly;
S2: enter shears behind the lower sheet, under 70～80 ℃ of conditions, to be rotated shearing under 500～600rpm rotating speed;
S3: again in the S2 products therefrom, add the tensio-active agent of half weight and the water of half weight, sheared 30 minutes, 800～900rpm rotating speed down cut 5 minutes, get rubber latex again;
S4: with asphalt heating to 140～160 ℃, insulation stirs, and adds remaining tensio-active agent and water again, stirs, and gets bitumen emulsion;
S5: rubber latex, bitumen emulsion are mixed with acrylic resin, ethylene glycol ethyl ether, chlorinatedpolyethylene, silicon carbide whisker, talcum powder, diatomite, stearic acid, polyacrylamide, ethylene-vinyl acetate copolymer, softening agent, defoamer, pigment, under 40～50 ℃, stir, let cool, and get final product.
2. rubber asphalt waterproof coating according to claim 1 is characterized in that: described pitch is a kind of in 90# petroleum pitch, the 10# petroleum pitch.
3. rubber asphalt waterproof coating according to claim 1, it is characterized in that: described defoamer is one or more mixtures in polyoxyethylene glycol, polypropylene glycol, acetylenic glycol, the polyvinyl alcohol.
4. rubber asphalt waterproof coating according to claim 1, it is characterized in that: described softening agent is one or more mixtures in clorafin, chlorodiphenyl, chlorinated naphthalene, the dibutyl phthalate.
5. rubber asphalt waterproof coating according to claim 1, it is characterized in that: described tensio-active agent is anion surfactant.
6. rubber asphalt waterproof coating according to claim 5, it is characterized in that: described anion surfactant is Sodium dodecylbenzene sulfonate.
7. rubber asphalt waterproof coating according to claim 1, it is characterized in that: described pigment is one or more mixtures in rutile type, phthalocyanine blue, fast light Huang, toluidine red, chromoxide green, red iron oxide, barba hispanica, the iron oxide yellow.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210351566.XA CN102936460B (en) | 2012-09-20 | 2012-09-20 | Asphalt rubber waterproof coating material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210351566.XA CN102936460B (en) | 2012-09-20 | 2012-09-20 | Asphalt rubber waterproof coating material |
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| Publication Number | Publication Date |
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| CN102936460A true CN102936460A (en) | 2013-02-20 |
| CN102936460B CN102936460B (en) | 2015-01-21 |
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| CN201210351566.XA Active CN102936460B (en) | 2012-09-20 | 2012-09-20 | Asphalt rubber waterproof coating material |
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