CN102935392A - Diffusion dish horizontal fixing device and using method thereof - Google Patents
Diffusion dish horizontal fixing device and using method thereof Download PDFInfo
- Publication number
- CN102935392A CN102935392A CN2012104771413A CN201210477141A CN102935392A CN 102935392 A CN102935392 A CN 102935392A CN 2012104771413 A CN2012104771413 A CN 2012104771413A CN 201210477141 A CN201210477141 A CN 201210477141A CN 102935392 A CN102935392 A CN 102935392A
- Authority
- CN
- China
- Prior art keywords
- support bar
- diffusion boat
- base
- elevating lever
- pressing plate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000009792 diffusion process Methods 0.000 title claims abstract description 63
- 238000000034 method Methods 0.000 title claims abstract description 11
- 230000003028 elevating effect Effects 0.000 claims description 31
- 239000005338 frosted glass Substances 0.000 claims description 17
- 239000003153 chemical reaction reagent Substances 0.000 claims description 3
- 239000007769 metal material Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 2
- 239000004033 plastic Substances 0.000 claims description 2
- 229920003023 plastic Polymers 0.000 claims description 2
- 239000002689 soil Substances 0.000 abstract description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 10
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 5
- 238000010521 absorption reaction Methods 0.000 abstract description 4
- 238000001514 detection method Methods 0.000 abstract 1
- 239000002585 base Substances 0.000 description 10
- 238000005516 engineering process Methods 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 2
- 239000004327 boric acid Substances 0.000 description 2
- 239000003337 fertilizer Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- MMDJDBSEMBIJBB-UHFFFAOYSA-N [O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[NH6+3] Chemical compound [O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[NH6+3] MMDJDBSEMBIJBB-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- XKMRRTOUMJRJIA-UHFFFAOYSA-N ammonia nh3 Chemical compound N.N XKMRRTOUMJRJIA-UHFFFAOYSA-N 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 125000001477 organic nitrogen group Chemical group 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000000565 sealant Substances 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
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- Sampling And Sample Adjustment (AREA)
- Devices For Use In Laboratory Experiments (AREA)
Abstract
一种扩散皿水平固定装置，属土壤检测装置技术领域。它包括底座、支撑杆、升降杆和压板,其特征在于，支撑杆为中空的直杆，垂直固定在底座边沿上，支撑杆中上部设置有固定螺丝；升降杆呈直角L形，升降杆的垂直部分插入支撑杆内，且能在支撑杆内做上下移动，支撑杆上的固定螺丝能对升降杆的垂直部分进行固定；升降杆横向部分的端部设置有有弹簧，弹簧下方水平方向固定连接压板，压板位于底座上方并和底座相对。本发明结构简单，使用方便安全，容易操作,解决了用扩散吸收法测定土壤中的碱解氮内外室溶液容易的混合，导致操作失败的技术问题。
A horizontal fixing device for a diffusion dish belongs to the technical field of soil detection devices. It includes a base, a support rod, a lifting rod and a pressure plate. It is characterized in that the supporting rod is a hollow straight rod, which is vertically fixed on the edge of the base, and the upper part of the supporting rod is provided with a fixing screw; the lifting rod is in a right-angle L shape, and the lifting rod The vertical part is inserted into the support rod and can move up and down in the support rod. The fixing screw on the support rod can fix the vertical part of the lifting rod; the end of the horizontal part of the lifting rod is provided with a spring, and the horizontal direction below the spring is fixed. Connect the pressure plate, the pressure plate is located above the base and opposite to the base. The invention has the advantages of simple structure, convenient and safe use, and easy operation, and solves the technical problem that the inner and outer chamber solutions of the alkali-hydrolyzed nitrogen in the soil are easily mixed by the diffusion absorption method, resulting in operation failure.
Description
Technical field
The present invention relates to the horizontal fixture of a kind of diffusion boat, dependent territory earth checkout gear technical field.
Background technology
The soil alkali-hydrolyzable nitrogen comprises labile, the fairly simple organic nitrogen of appearance in inorganic nitrogen and the part organic matter, and it is the summation of the protein of ammonium nitrogen, nitrate nitrogen, amino acid, acid amides and facile hydrolysis.It can reflect at no distant date nitrogen supply situation of soil, so be called again soil available nitrogen.Measure the content of soil alkali-hydrolyzable nitrogen to understanding the confession nitrogen ability of soil, instruct the rational application of fertilizer to have definite meaning.Therefore the alkali-hydrolyzable nitrogen that how can measure fast and accurately in the soil is problem in the soil and fertilizer research field always.Comparatively commonly used is to adopt the diffusion absorption method at present, normal operation glass diffusion boat, the inside and outside chamber of ware body adds respectively boric acid and soil sample, smear the sealants such as alkaline glycerine at the external edge of ware, the cover plate that frosted glass is made covers and rotates for several times, make ware limit and frosted glass cover plate fully bonding, gradually rotate again and remove the frosted glass cover plate on one side, add alkali lye at the diffusion boat exocoel after exposing a slit, then cover tightly immediately, tight with the rubber band circle again, the frosted glass cover plate is fixed, to guarantee with the diffusion boat sealing fully.Put into subsequently insulating box and placed 24 hours, then take out dismantle rubber band and frosted glass, the boric acid absorption liquid is carried out titration.This assay method result is stable, equipment is simple, but in operating process especially when bundle is torn rubber band open, need to guarantee diffusion boat careful operation on horizontal plane, the careless slightly mixing that just can cause interior exocoel solution, so that operation failure, rework rate is high, and time-consuming.The horizontal fixture of diffusion boat is not also appeared in the newspapers at present.
Summary of the invention
For solving the problems of the technologies described above, for the defective described in the background technology and deficiency, the invention provides the horizontal fixture of a kind of diffusion boat, to realize that the diffusion boat seal process easily and fast, finish safely.
Technical scheme of the present invention is as follows:
The horizontal fixture of a kind of diffusion boat comprises base, support bar, elevating lever and pressing plate, it is characterized in that, support bar is the straight-bar of hollow, is vertically fixed on the base edge, and the support bar middle and upper part is provided with fixed screw; Elevating lever is at right angles L shaped, and the vertical component of elevating lever inserts in the support bar, and can do in support bar and move up and down, and the fixed screw on the support bar can be fixed the vertical component of elevating lever; The end of elevating lever lateral part is provided with spring, and spring lower horizontal direction is fixedly connected with pressing plate, and pressing plate is positioned at base top and relative with base.
The present invention is preferred, and described pressing plate bottom surface is covered with one deck cushion pad, and further preferred, described cushion pad is valve rubber.Cushion pad effectively cushions pressing plate for the pressure of diffusion boat, and guarantee pressing plate to the diffusion boat surface stressed evenly, prevent from damaging diffusion boat.
The present invention is preferred, and the height of described support bar is 0.5～2cm, and the height of the vertical component of elevating lever is less than the height of support bar.
The present invention is preferred, and the width of described pressing plate is greater than mistress's diameter of diffusion boat.
Described base, support bar, elevating lever and pressing plate are metal material or rigid plastics material.
The present invention also provides the using method of the horizontal fixture of a kind of diffusion boat, may further comprise the steps:
(1), will be stamped the diffusion boat that frosted glass cover plate, inside contain testing sample and reagent and place on the base of the horizontal fixture of diffusion boat,
(2), unclamp fixed screw, adjust the elevating lever height, the vertical component of elevating lever is done in support bar and is moved up and down, when pressing plate contacts with the frosted glass cover plate, the fixed screw on the screwed support bar; The elastic force of spring is horizontally fixed on the base frosted glass cover plate and diffusion boat simultaneously,
(3), frosted glass cover plate and the diffusion boat that fixes moved in the insulating box together with the horizontal fixture of diffusion boat, for subsequent use.
The present invention is preferred, and the diffusion boat in the step (1) is the multilayer diffusion boat, and the multilayer diffusion boat is stacked placing on the base up and down.
The invention has the beneficial effects as follows:
1, the present invention is simple in structure, convenient fixing, the frosted glass cover plate can be fixed on the diffusion boat by the up-down adjustment elevating lever and by the elastic force of spring, to guarantee the diffusion boat sealing fully, in fixation procedure, diffusion boat is on the horizontal plane always, prevents the diffusion boat inclination and causes diffusion boat inner room and mistress's solution to mix, solve the interior mistress's solution of alkali-hydrolyzable nitrogen of measuring in the soil with the diffusion absorption method and be easy to mix, caused the technical problem of operation failure.The horizontal fixture of diffusion boat of the present invention is the accuracy rate original text fixedly, safety easy to use, and easily operation is time saving and energy saving, has improved operating efficiency.
2, convenient disassembly of the present invention unclamps fixed screw, and to the adjusted elevating lever, level is taken off diffusion boat and got final product.
3, pressing plate of the present invention bottom surface is covered with one deck cushion pad, and cushion pad effectively cushions pressing plate for the pressure of diffusion boat, and guarantee pressing plate to the diffusion boat surface stressed evenly.
Description of drawings
Fig. 1 is structural representation of the present invention;
Wherein: 1, base, 2, support bar, 3, elevating lever, 4, the elevating lever lateral part, 5, spring, 6, pressing plate, 7, fixed screw, 8, valve rubber.
The specific embodiment
The invention will be further described below in conjunction with drawings and Examples, but be not limited to this.
Embodiment 1:
The horizontal fixture of a kind of diffusion boat, structure comprise base 1, support bar 2 and elevating lever 3 as shown in Figure 1, and support bar 2 is the straight-bar of hollow, are vertically fixed on base 1 edge, and support bar 2 middle and upper parts are provided with fixed screw 7; Elevating lever 3 is at right angles L shaped, and the vertical component of elevating lever 3 inserts in the support bar 2, and can do in support bar 2 and move up and down, and the fixed screw 7 on the support bar 2 can be fixed the vertical component of elevating lever 3; The end of elevating lever lateral part 4 is provided with spring 5, and spring 5 lower horizontal directions are fixedly connected with pressing plate 6, and pressing plate 6 is positioned at base 1 top and relative with base 1.
The bottom surface of pressing plate 6 is covered with one deck valve rubber 8, valve rubber 8 effectively the buffering pressing plates for the pressure of diffusion boat, and guarantee pressing plate to the diffusion boat surface stressed evenly, prevent from damaging diffusion boat.
The height of support bar 2 is 0.5cm, and the height of the vertical component of elevating lever 3 is less than the height of support bar 2.
For making 6 pairs of diffusion boats of pressing plate stressed evenly, the width of pressing plate 6 is greater than mistress's diameter of diffusion boat.
Embodiment 2:
The horizontal fixture of a kind of diffusion boat as described in Example 1, difference is: the height of support bar 2 is 2cm.
Embodiment 3:
The using method of the horizontal fixture of embodiment 1 described diffusion boat may further comprise the steps:
1, will be stamped the diffusion boat that frosted glass cover plate, inside contain testing sample and reagent and place on the base 1 of the horizontal fixture of diffusion boat,
2, unclamp fixed screw 7, adjust elevating lever 3 height, the vertical component of elevating lever 3 is done in support bar 2 and is moved up and down, when pressing plate 6 contacts with the frosted glass cover plate, and the fixed screw 7 on the screwed support bar 2; The elastic force of spring is horizontally fixed on the base frosted glass cover plate and diffusion boat simultaneously,
3, frosted glass cover plate and the diffusion boat that fixes moved in the insulating box together with the horizontal fixture of diffusion boat, for subsequent use.
Claims (6)
1. the horizontal fixture of diffusion boat comprises base, support bar, elevating lever and pressing plate, it is characterized in that, support bar is the straight-bar of hollow, is vertically fixed on the base edge, and the support bar middle and upper part is provided with fixed screw; Elevating lever is at right angles L shaped, and the vertical component of elevating lever inserts in the support bar, and can do in support bar and move up and down, and the fixed screw on the support bar can be fixed the vertical component of elevating lever; The end of elevating lever lateral part has been provided with spring, and spring lower horizontal direction is fixedly connected with pressing plate, and pressing plate is positioned at base top and relative with base.
2. the horizontal fixture of diffusion boat according to claim 1, it is characterized in that: described pressing plate bottom surface is covered with one deck cushion pad, and further preferred, described cushion pad is valve rubber.
3. the horizontal fixture of diffusion boat according to claim 2, it is characterized in that: the height of described support bar is 0.5～2cm, and the height of the vertical component of elevating lever is less than the height of support bar.
4. the horizontal fixture of diffusion boat according to claim 2, it is characterized in that: the width of described pressing plate is greater than mistress's diameter of diffusion boat.
5. the horizontal fixture of diffusion boat according to claim 2, it is characterized in that: described base, support bar, elevating lever and pressing plate are metal material or rigid plastics material.
6. the using method of the horizontal fixture of diffusion boat as claimed in claim 1 may further comprise the steps:
(1), will be stamped the diffusion boat that frosted glass cover plate, inside contain testing sample and reagent and place on the base of the horizontal fixture of diffusion boat,
(2), unclamp fixed screw, adjust the elevating lever height, the vertical component of elevating lever is done in support bar and is moved up and down, when pressing plate is pressed in the diffusion boat level on the base, fixed screw on the screwed support bar, frosted glass cover plate and diffusion boat are horizontally fixed on the base simultaneously
(3), frosted glass cover plate and the diffusion boat that fixes moved in the insulating box together with the horizontal fixture of diffusion boat, for subsequent use.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210477141.3A CN102935392B (en) | 2012-11-21 | 2012-11-21 | Horizontally fixing device of diffusion vessel and use method of horizontally fixing device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210477141.3A CN102935392B (en) | 2012-11-21 | 2012-11-21 | Horizontally fixing device of diffusion vessel and use method of horizontally fixing device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102935392A true CN102935392A (en) | 2013-02-20 |
| CN102935392B CN102935392B (en) | 2014-09-17 |
Family
ID=47694331
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210477141.3A Expired - Fee Related CN102935392B (en) | 2012-11-21 | 2012-11-21 | Horizontally fixing device of diffusion vessel and use method of horizontally fixing device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102935392B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109470835A (en) * | 2018-10-23 | 2019-03-15 | 中国科学院合肥物质科学研究院 | A kind of alkaline hydrolysis nitrogen treatment device for soil testing |
| CN112505292A (en) * | 2020-11-17 | 2021-03-16 | 中国环境科学研究院 | Culture device and culture method for nitrogen hydrolysis experiment |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5998202A (en) * | 1997-02-26 | 1999-12-07 | Synthecon, Inc. | Multiple chamber diffusion vessel |
| CN201243891Y (en) * | 2008-09-02 | 2009-05-27 | 周柯秋成 | Rack for placing dishware |
| CN201648393U (en) * | 2010-04-14 | 2010-11-24 | 张桂玲 | Culture dish retainer |
| CN202533320U (en) * | 2012-05-07 | 2012-11-14 | 景德镇陶瓷学院 | Fixture for ceramic ware |
-
2012
- 2012-11-21 CN CN201210477141.3A patent/CN102935392B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5998202A (en) * | 1997-02-26 | 1999-12-07 | Synthecon, Inc. | Multiple chamber diffusion vessel |
| CN201243891Y (en) * | 2008-09-02 | 2009-05-27 | 周柯秋成 | Rack for placing dishware |
| CN201648393U (en) * | 2010-04-14 | 2010-11-24 | 张桂玲 | Culture dish retainer |
| CN202533320U (en) * | 2012-05-07 | 2012-11-14 | 景德镇陶瓷学院 | Fixture for ceramic ware |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109470835A (en) * | 2018-10-23 | 2019-03-15 | 中国科学院合肥物质科学研究院 | A kind of alkaline hydrolysis nitrogen treatment device for soil testing |
| CN112505292A (en) * | 2020-11-17 | 2021-03-16 | 中国环境科学研究院 | Culture device and culture method for nitrogen hydrolysis experiment |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102935392B (en) | 2014-09-17 |
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Granted publication date: 20140917 Termination date: 20151121 |
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