CN102934717A - Dogbane tartary buckwheat tea and preparation process thereof - Google Patents
Dogbane tartary buckwheat tea and preparation process thereof Download PDFInfo
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- CN102934717A CN102934717A CN 201210442607 CN201210442607A CN102934717A CN 102934717 A CN102934717 A CN 102934717A CN 201210442607 CN201210442607 CN 201210442607 CN 201210442607 A CN201210442607 A CN 201210442607A CN 102934717 A CN102934717 A CN 102934717A
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- powder
- extract
- tartary buckwheat
- bitter buckwheat
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Landscapes
- Medicines Containing Plant Substances (AREA)
Abstract
Disclosed are a dogbane tartary buckwheat tea and a preparation process thereof. The tartary buckwheat tea is composed of 500 to 900 parts of tartary buckwheat husk powders, 300 to 400 parts of dogbane powders, 50 to 100 parts of folium mori powders, 50 to 100 parts of chrysanthemum powders, 50 to 100 parts of tartary buckwheat extract, 2 to 10 parts of guar gum, 2 to 10 parts of xanthan gum and 2 to 10 parts of konjac glucomannan. The preparation process of the tartary buckwheat tea includes breading, forming, drying and fragrance enhancing. The preparation process specifically includes firstly uniformly mixing the tartary buckwheat husk powders, the dogbane powders, the folium mori powders, the chrysanthemum powders, the tartary buckwheat extract, the guar gum, the xanthan gum and the konjac glucomannan until the colour and luster are uniform, still standing for 20 minutes, then taking out uniformly stirred tea powders, adding 25% to 40% of water, uniformly mixing by a pressurization forming machine, screening through a sieve with 30 meshes, performing granulation, placing formed tartary buckwheat tea particles in a plate, placing the plate in a hot air drying oven, drying at the temperature of 50 DEG C to 55 DEG C until the moisture content is within 8%, then placing the plate in a far infrared toaster, baking at the temperature of 200 DEG C to 220 DEG C for 2 to 3 minutes, naturally cooling, finally placing cooled tartary buckwheat tea in a rotary drum drying oven, and baking at the temperature of 110 DEG C to 145 DEG C until the moisture content is not more than 5%.
Description
Technical field
The present invention relates to a kind of bitter buckwheat tea and preparation technology thereof.
Background technology
Bitter buckwheat, be polygonaceae annual herb plant, is the health food that extremely the people parent looks at.Compendium of Material Medica is put down in writing the bitter buckwheat " effect of bitter, flat cold, useful strength, continuous spirit, sharp knowledge, wide chest, sending down abnormally ascending, stomach invigorating." modern study shows, bitter-buckwheat nutritive is worth high, and wherein protein content is about 10% left and right of dry weight, mainly contains glutelin, water-soluble albumin and salt dissolubility globulin and forms, approximate peas protein; Bitter buckwheat amino acid content is high and proportioning is suitable, and 8 seed amino acids of needed by human all contain, and especially are rich in arginine, lysine, tryptophan, histidine etc., and other food is had to good complementarity.Fat content is generally 2% to 3%, and containing nine kinds of aliphatic acid, human body is easy to the oleic acid of absorption and 80% left and right that linoleic acid accounts for bitter buckwheat aliphatic acid.Inorganic salt content in bitter buckwheat is abundant, and selenium, potassium, magnesium, copper, chromium, zinc, calcium, iron equal size all are much higher than cereal crop, the selenium element have an antitumaous effect.Bitter buckwheat is rich in vitamin B complex, vitamin E etc., unique distinction contains a large amount of Flavonoid substances rutins (being citrin) exactly, account for more than 2% of dry weight, human body is had to different physiological roles, can strengthen the permeability of capillary, improve cardiovascular system, suppress malignant growth and cancer etc.Bitter buckwheat also contains more dietary fiber, colloidal substance glucan especially, and abundant dietary fiber has the function of toxin-expelling and face nourishing, and diabetes and high fat of blood are also had to positive regulating action.The rate of exchange of bitter-buckwheat nutritive physiology are the outstanding grain medicine dual-purpose grain kind that the international food and agricultural organization of 73，Shi generally acknowledges, are that the typical case of China's integration of drinking and medicinal herbs culture embodies.
Bluish dogbane is the rare wild plant in the world, mainly is grown in the sandy ground on salt-soda soil, desert or riverbank, gully, hillside, in the most provinces and regions of northern China, distribution is arranged, wherein with the bluish dogbane performance optimal of deserts in Xinjiang.Modern study shows, be rich in flavone compound (as Quercetin, rue glucoside, flavonoid glycosides, Cardiac glycosides etc.), organic acid compound, several amino acids in bluish dogbane, and the mineral element such as calcium, magnesium, potassium, zinc, manganese, iron, selenium, thereby there is significantly hypotensive, reducing blood lipid, the anti-ageing effect of waiting for a long time.
The defect of prior art has: one, in the processing of traditional bitter buckwheat tea, dry longer drying time with Titian link process high-temperature, in bitter buckwheat, flavone compound very easily decomposes, thereby destroys the nutritional labeling in bitter buckwheat, reduces the health-care efficacy of bitter buckwheat.Two, bitter buckwheat, bluish dogbane all have reducing blood lipid preferably, hypoglycemic and hypotensive activity, however both share research less.
Summary of the invention
The invention provides formula and the preparation technology thereof of the bitter buckwheat tea of a kind of bluish dogbane, as a kind of tea-drinking product, the characteristics that it has mouthfeel delicate fragrance, endures repeated infusions, and health-care effect is outstanding, definite reducing blood lipid, blood sugar and blood pressure effect are arranged, wherein hypotensive particularly outstanding with effect for reducing blood fat.In addition, the present invention also provides the preparation technology of the bitter buckwheat tea of bluish dogbane, and this technique can retain the nutritional labeling of bitter buckwheat to greatest extent, and resource utilization is high, and process safety is stable, solvent recoverable, good economy performance.
Technical scheme is as follows:
The bitter buckwheat tea of bluish dogbane of the present invention, by tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan, formed, tartary buckwheat cortex powder 500-900 part wherein, bluish dogbane powder 300-400 part, mulberry leaf powder 50-100 part, chrysanthemum powder 50-100 part, tartary buckwheat extract 50-100 part, guar gum 2-10 part, xanthans 2-10 part, konjac glucomannan 2-10 part.
The bitter buckwheat tea of bluish dogbane of the present invention, preferably tartary buckwheat cortex powder is 800 parts, 360 parts, bluish dogbane powder, 50 parts of mulberry leaf powders, 50 parts of chrysanthemum powders, 80 parts of tartary buckwheat extracts, 4 parts of guar gums, 10 parts of xanthans, 2 parts of konjac glucomannans.
No. 9909 kinds of western agriculture that in the bitter buckwheat tea of bluish dogbane, the preferred Xibei Univ. of Agricultural & Forest Science & Technology of bitter buckwheat cultivates.
In the bitter buckwheat tea of bluish dogbane, the preparation technology of tartary buckwheat cortex powder is:
(1) screening: the bitter buckwheat seed that the selection grain is large, full, unit weight is high is for the production of processing.
(2) the first pulverizing: pulverize bitter buckwheat seed by mechanical grinding method, gained KUQIAOPI layer meal crossed 80 mesh sieves.
(3) ultramicro grinding: utilize fluid energy mill to carry out ultramicro grinding to KUQIAOPI layer meal, the gained fine powder is crossed 300 mesh sieves, obtains.
Before bitter buckwheat screening, it is carried out to pre-treatment in the bitter buckwheat tea of bluish dogbane, method is:
Bitter buckwheat seed is immersed in containing in the mixed aqueous solution of 0.008% copper sulphate, 0.048% zinc sulfate and 0.08% potassium dihydrogen phosphate, the thickness of seed in the aqueous solution is 1cm, soak 5 days, every day, ultra violet lamp was 1 hour, within 5 days, take out afterwards, clear water rinses, under 24KHz, 300W power condition ultrasonic 5 minutes, put the far-infrared oven low temperature drying, obtain.
The formula of the bitter buckwheat tea of bluish dogbane is preferred
(1) preparation technology of bluish dogbane powder is:
The mixture that the bluish dogbane powder is 90% Folium Apocyni Veneti powder and 10% bluish dogbane pollen.
Get the Folium Apocyni Veneti of plucking the first tenday period of a month in May, 25 ℃ of water rinses, spread and dry, in 25 ℃, 0.1MPa environment, place 4 hours, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 15 seconds, 4 ℃ cooling, pulverizes, and crosses 80 sieves, obtain the Folium Apocyni Veneti meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
Get the dogbane flower that early July plucks, spread and dry, place 4 hours in 25 ℃, 0.1MPa environment, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, and 150 ℃ of baking ovens toast 5 seconds, and 4 ℃ cooling, pulverize, cross 80 sieves, obtain the dogbane flower meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
(2) preparation technology of mulberry leaf powder is:
Get the mulberry leaf sheet after first frost, 25 ℃ of water rinses, spread and dry, in 25 ℃, 0.1MPa environment, place 4 hours, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 15 seconds, 4 ℃ cooling, pulverizes, and crosses 80 sieves, obtain the mulberry leaf meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
(3) preparation technology of chrysanthemum powder is:
Get chrysanthemum, spread and dry, place 4 hours in 25 ℃, 0.1MPa environment, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 5 seconds, and 4 ℃ cooling, pulverize, and cross 80 sieves, obtain the chrysanthemum meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
The formula of the bitter buckwheat tea of bluish dogbane is preferred
(1) tartary buckwheat extract comprises bitter buckwheat stem, leaf, root extract and Fagopyrum tataricum(L.)Gaertn. Bran extract two parts, and bitter buckwheat stem, leaf, root extract mix in the 1:1 ratio with Fagopyrum tataricum(L.)Gaertn. Bran extract;
(2) extraction process of bitter buckwheat stem, leaf, root extract is:
The mixture of the bitter buckwheat root of arbitrary proportion, stem and leaf, 12 times of amount 65% alcohol extracts, each 2 hours, extract 3 times, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain bitter buckwheat stem, leaf, root crude extract.
(3) extraction process of Fagopyrum tataricum(L.)Gaertn. Bran extract is:
Ultrasonic assisted Extraction is followed the example of the extraction tartary buckwheat bran, under 24KHz, 300W power ultrasonic condition, and 6 times of amount 80% ethanol, 0.5MPa pressure, 40 ℃, extract 2 times, each 2 hours, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain the tartary buckwheat bran crude extract.
(4) purifying process of tartary buckwheat extract is:
Adopt the DM-2 macroporous absorbent resin to be made with extra care tartary buckwheat extract: bitter buckwheat stem, leaf, root crude extract are mixed in the 1:1 ratio with the tartary buckwheat bran crude extract, and 70% ethanol dissolves, and makes concentration be decided to be 2mg/mL, regulating the pH value is 2, loading, the absorption flow velocity is 2mL/min, blade diameter length ratio 1:10; With 70% ethanol, macroporous absorbent resin is carried out to wash-out afterwards, regulating the pH value is 8.5, elution rate is 1mL/min, collects eluent, under 25 ℃ of conditions, eluent is carried out to the high speed centrifugation separation, centrifuge speed 4000rpm, centrifugal 20 minutes, filter eluent, filtrate is carried out to reduction vaporization drying (0.1MPa, 20 ℃), obtain tartary buckwheat extract.
The preparation technology of the bitter buckwheat tea of bluish dogbane of the present invention, comprise breading, moulding, drying, four steps of Titian, wherein:
(1) breading: tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan are mixed, until the color and luster homogeneous, standing 20 minutes.
(2) moulding: get the tea powder of mixing thoroughly, add water 25%-40%, adopt pressure forming machine to mix, cross 30 mesh sieves, granulate.
(3) drying: the bitter buckwheat tea granule dish out after moulding first is placed in to hot air drier, and 50-55 ℃ is dried in water content 8%, then puts into far-infrared oven, bakes and banks up with earth 2-3min for 200-220 ℃, naturally cooling.
(4) Titian: cooled bitter buckwheat tea is put into the roller drying case, bakes and banks up with earth to moisture not higher than 5% for 110-145 ℃.
The preparation technology of the bitter buckwheat tea of bluish dogbane is preferred
(1) first that guar gum, xanthans and konjac glucomannan is soluble in water, fully swelling, form colloidal solution, then add tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder and tartary buckwheat extract, then drops into the pressure forming machine mixed pelletization.
(2) controlling the mixer speed of mainshaft is 30rpm, mixing time 30 minutes.
Also can when breading, add the egg of 1% amount in the preparation technology of the bitter buckwheat tea of bluish dogbane.
Compared to the prior art, the technology of the present invention effect comprises:
1, the present invention chooses bitter buckwheat and bluish dogbane is primary raw material, and two Plants all have definite health care curative effect, and formula forms rationally.
2, the preferred Xibei Univ. of Agricultural & Forest Science & Technology of the present invention cultivates No. 9909 bitter buckwheat kinds of western agriculture successfully, and in the Shanxi plantation extensively, research shows that flavones ingredient wherein is abundant especially than other kind content to this kind.
3, the present invention has carried out the deep development utilization to bitter buckwheat and bluish dogbane, comprises bitter buckwheat root, stem, leaf, wheat bran and seed, and Folium Apocyni Veneti and flower, all fully uses, and farthest utilizes living resources.
4, the bitter buckwheat tea of gained of the present invention fragrance is pure and fresh, dark brown lucid and lively, and brewing property is good, suitable vast drunk by people.
5, adopt multiple extractive technique in preparation technology of the present invention, the active ingredient in bitter buckwheat is all retained.
6, preparation technology of the present invention adopts the low temperature drying technology, greatly shortens high temperature drying and Titian link process time, avoids flavones ingredient in bitter buckwheat to be damaged.
7, the present invention carries out system research to each parameter ratio in the bitter buckwheat tea ratio of adjuvant of bluish dogbane and process, draws optimised process, and the introducing of ultramicro grinding technique significantly raises the bitter buckwheat tea of bluish dogbane active ingredient stripping quantity.
8, the bitter buckwheat tea of gained bluish dogbane of the present invention after deliberation, has definite reducing blood lipid, hypoglycemic and blood pressure reduction effect, wherein hypotensive especially outstanding with blood fat reducing function.
The specific embodiment
Below in conjunction with specific embodiment, technical solution of the present invention is described in detail.
Embodiment 1:
Select the bitter buckwheat seed that grain is large, full, unit weight is high, by mechanical grinding method, it is pulverized, gained KUQIAOPI layer meal crossed 80 mesh sieves, utilizes fluid energy mill to carry out ultramicro grinding to KUQIAOPI layer meal, and the gained fine powder is crossed 300 mesh sieves, obtains.
Get the Folium Apocyni Veneti of plucking the first tenday period of a month in May, 25 ℃ of water rinses, spread and dry, in 25 ℃, 0.1MPa environment, place 4 hours, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 15 seconds, 4 ℃ cooling, pulverizes, and crosses 80 sieves, obtain the Folium Apocyni Veneti meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
Get the dogbane flower that early July plucks, spread and dry, place 4 hours in 25 ℃, 0.1MPa environment, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, and 150 ℃ of baking ovens toast 5 seconds, and 4 ℃ cooling, pulverize, cross 80 sieves, obtain the dogbane flower meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
The Folium Apocyni Veneti powder is mixed in the 9:1 ratio with bluish dogbane pollen, obtain the bluish dogbane powder.
Get bitter buckwheat root, stem and leaf, add 12 times of amount 65% alcohol extracts, each 2 hours, extract 3 times, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain bitter buckwheat root, stem, Leave extract.
Ultrasonic assisted Extraction is followed the example of the extraction tartary buckwheat bran, under 24KHz, 300W power ultrasonic condition, and 6 times of amount 80% ethanol, 0.5MPa pressure, 40 ℃, extract 2 times, each 2 hours, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain the tartary buckwheat bran crude extract.
Adopt the DM-2 macroporous absorbent resin to be made with extra care bitter buckwheat root, stem, leaf and Fagopyrum tataricum(L.)Gaertn. Bran extract: bitter buckwheat root, stem, Leave extract are mixed in the 1:1 ratio with the tartary buckwheat bran crude extract, 70% ethanol dissolves, make concentration be decided to be 2mg/mL, regulating the pH value is 2, loading, the absorption flow velocity is 2mL/min, blade diameter length ratio 1:10; With 70% ethanol, macroporous absorbent resin is carried out to wash-out afterwards, regulating the pH value is 8.5, elution rate is 1mL/min, collects eluent, under 25 ℃ of conditions, eluent is carried out to the high speed centrifugation separation, centrifuge speed 4000rpm, centrifugal 20 minutes, filter eluent, filtrate is carried out to reduction vaporization drying (0.1MPa, 20 ℃), obtain tartary buckwheat extract.
According to 900 parts of tartary buckwheat cortex powders, 300 parts, bluish dogbane powder, 50 parts of mulberry leaf powders, 100 parts of chrysanthemum powders, 100 parts of tartary buckwheat extracts, 8 parts of guar gums, 5 parts of xanthans, the ratio that konjac glucomannan is 5 parts measures tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan, tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan are mixed, until the color and luster homogeneous, standing 20 minutes.
Get the tea powder of mixing thoroughly, add water 35%, adopt pressure forming machine to mix, cross 30 mesh sieves, granulate.
Bitter buckwheat tea granule dish out after moulding first is placed in to hot air drier, and 50 ℃ are dried in water content 8%, then put into far-infrared oven, bake and bank up with earth 2min for 205 ℃, naturally cooling.
Cooled bitter buckwheat tea is put into the roller drying case, bakes and banks up with earth to moisture not higher than 5% for 110 ℃.
After testing, the rutin composition rate of transform is 97.4% to the bitter buckwheat tea of gained, dissolution rate 98.5%, and production technology is reasonable, the technique smoothness.
Embodiment 2:
Select the bitter buckwheat seed that grain is large, full, unit weight is high (No. 9909 kinds of western agriculture that Xibei Univ. of Agricultural & Forest Science & Technology cultivates), by mechanical grinding method, it is pulverized, gained KUQIAOPI layer powder crossed 80 mesh sieves, obtain duck wheat cortex meal, utilize fluid energy mill to carry out ultramicro grinding to KUQIAOPI layer meal, the gained fine powder is crossed 300 mesh sieves, obtains.
Get the Folium Apocyni Veneti of plucking the first tenday period of a month in May, 25 ℃ of water rinses, spread and dry, in 25 ℃, 0.1MPa environment, place 4 hours, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 15 seconds, 4 ℃ cooling, pulverizes, and crosses 80 sieves, obtain the Folium Apocyni Veneti meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
Get the dogbane flower that early July plucks, spread and dry, place 4 hours in 25 ℃, 0.1MPa environment, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, and 150 ℃ of baking ovens toast 5 seconds, and 4 ℃ cooling, pulverize, cross 80 sieves, obtain the dogbane flower meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
The Folium Apocyni Veneti powder is mixed in the 9:1 ratio with bluish dogbane pollen, obtain the bluish dogbane powder.
Get bitter buckwheat rhizome and leaf, add 12 times of amount 65% alcohol extracts, each 2 hours, extract 3 times, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain bitter buckwheat root, stem, Leave extract.
Ultrasonic assisted Extraction is followed the example of the extraction tartary buckwheat bran, under 24KHz, 300W power ultrasonic condition, and 6 times of amount 80% ethanol, 0.5MPa pressure, 40 ℃, extract 2 times, each 2 hours, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain the tartary buckwheat bran crude extract.
Adopt the DM-2 macroporous absorbent resin to be made with extra care bitter buckwheat root, stem, leaf and Fagopyrum tataricum(L.)Gaertn. Bran extract: bitter buckwheat root, stem, Leave extract are mixed in the 1:1 ratio with the tartary buckwheat bran crude extract, 70% ethanol dissolves, make concentration be decided to be 2mg/mL, regulating the pH value is 2, loading, the absorption flow velocity is 2mL/min, blade diameter length ratio 1:10; With 70% ethanol, macroporous absorbent resin is carried out to wash-out afterwards, regulating the pH value is 8.5, elution rate is 1mL/min, collects eluent, under 25 ℃ of conditions, eluent is carried out to the high speed centrifugation separation, centrifuge speed 4000rpm, centrifugal 20 minutes, filter eluent, filtrate is carried out to reduction vaporization drying (0.1MPa, 20 ℃), obtain tartary buckwheat extract.
According to 500 parts of tartary buckwheat cortex powders, 400 parts, bluish dogbane powder, 80 parts of mulberry leaf powders, 60 parts of chrysanthemum powders, 60 parts of tartary buckwheat extracts, 8 parts of guar gums, 10 parts of xanthans, the ratio that konjac glucomannan is 8 parts measures tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan, tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan are mixed, until the color and luster homogeneous, standing 20 minutes.
Get the tea powder of mixing thoroughly, add water 30%, adopt pressure forming machine to mix, cross 30 mesh sieves, granulate.
Bitter buckwheat tea granule dish out after moulding first is placed in to hot air drier, and 55 ℃ are dried in water content 8%, then put into far-infrared oven, bake and bank up with earth 2min for 215 ℃, naturally cooling.
Cooled bitter buckwheat tea is put into the roller drying case, bakes and banks up with earth to moisture not higher than 5% for 120 ℃.
After testing, the rutin composition rate of transform is 96.9% to the bitter buckwheat tea of gained, dissolution rate 97.1%, and production technology is reasonable, the technique smoothness.
Embodiment 3:
Bitter buckwheat seed (No. 9909 kinds of western agriculture that Xibei Univ. of Agricultural & Forest Science & Technology cultivates) is immersed in containing 0.008% copper sulphate, in the mixed aqueous solution of 0.048% zinc sulfate and 0.08% potassium dihydrogen phosphate, the thickness of seed in the aqueous solution is 1cm, soak 5 days, every day, ultra violet lamp was 1 hour, within 5 days, take out afterwards, clear water rinses, 24KHz, under the 300W power condition ultrasonic 5 minutes, put the far-infrared oven low temperature drying, select grain large, full, the bitter buckwheat seed that unit weight is high, by mechanical grinding method, it is pulverized, gained KUQIAOPI layer powder crossed 80 mesh sieves, obtain duck wheat cortex meal, utilize fluid energy mill to carry out ultramicro grinding to KUQIAOPI layer meal, the gained fine powder is crossed 300 mesh sieves, obtain.
Get the Folium Apocyni Veneti of plucking the first tenday period of a month in May, 25 ℃ of water rinses, spread and dry, in 25 ℃, 0.1MPa environment, place 4 hours, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 15 seconds, 4 ℃ cooling, pulverizes, and crosses 80 sieves, obtain the Folium Apocyni Veneti meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
Get the dogbane flower that early July plucks, spread and dry, place 4 hours in 25 ℃, 0.1MPa environment, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, and 150 ℃ of baking ovens toast 5 seconds, and 4 ℃ cooling, pulverize, cross 80 sieves, obtain the dogbane flower meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
The Folium Apocyni Veneti powder is mixed in the 9:1 ratio with bluish dogbane pollen, obtain the bluish dogbane powder.
Get bitter buckwheat rhizome and leaf, add 12 times of amount 65% alcohol extracts, each 2 hours, extract 3 times, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain bitter buckwheat root, stem, Leave extract.
Ultrasonic assisted Extraction is followed the example of the extraction tartary buckwheat bran, under 24KHz, 300W power ultrasonic condition, and 6 times of amount 80% ethanol, 0.5MPa pressure, 40 ℃, extract 2 times, each 2 hours, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain the tartary buckwheat bran crude extract.
Adopt the DM-2 macroporous absorbent resin to be made with extra care bitter buckwheat root, stem, leaf and Fagopyrum tataricum(L.)Gaertn. Bran extract: bitter buckwheat root, stem, Leave extract are mixed in the 1:1 ratio with the tartary buckwheat bran crude extract, 70% ethanol dissolves, make concentration be decided to be 2mg/mL, regulating the pH value is 2, loading, the absorption flow velocity is 2mL/min, blade diameter length ratio 1:10; With 70% ethanol, macroporous absorbent resin is carried out to wash-out afterwards, regulating the pH value is 8.5, elution rate is 1mL/min, collects eluent, under 25 ℃ of conditions, eluent is carried out to the high speed centrifugation separation, centrifuge speed 4000rpm, centrifugal 20 minutes, filter eluent, filtrate is carried out to reduction vaporization drying (0.1MPa, 20 ℃), obtain tartary buckwheat extract.
According to 600 parts of tartary buckwheat cortex powders, 350 parts, bluish dogbane powder, 60 parts of mulberry leaf powders, 50 parts of chrysanthemum powders, 50 parts of tartary buckwheat extracts, 5 parts of guar gums, 5 parts of xanthans, the ratio that konjac glucomannan is 5 parts measures tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan, tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan are mixed, until the color and luster homogeneous, standing 20 minutes.
Get the tea powder of mixing thoroughly, add water 35%, adopt pressure forming machine to mix, cross 30 mesh sieves, granulate.
Bitter buckwheat tea granule dish out after moulding first is placed in to hot air drier, and 52 ℃ are dried in water content 8%, then put into far-infrared oven, bake and bank up with earth 2min for 210 ℃, naturally cooling.
Cooled bitter buckwheat tea is put into the roller drying case, bakes and banks up with earth to moisture not higher than 5% for 130 ℃.
After testing, the rutin composition rate of transform is 97.8% to the bitter buckwheat tea of gained, dissolution rate 96.8%, and production technology is reasonable, the technique smoothness.
Embodiment 4:
Bitter buckwheat seed (No. 9909 kinds of western agriculture that Xibei Univ. of Agricultural & Forest Science & Technology cultivates) is immersed in containing 0.008% copper sulphate, in the mixed aqueous solution of 0.048% zinc sulfate and 0.08% potassium dihydrogen phosphate, the thickness of seed in the aqueous solution is 1cm, soak 5 days, every day, ultra violet lamp was 1 hour, within 5 days, take out afterwards, clear water rinses, 24KHz, under the 300W power condition ultrasonic 5 minutes, put the far-infrared oven low temperature drying, select grain large, full, the bitter buckwheat seed that unit weight is high, by mechanical grinding method, it is pulverized, gained KUQIAOPI layer powder crossed 80 mesh sieves, obtain duck wheat cortex meal, utilize fluid energy mill to carry out ultramicro grinding to KUQIAOPI layer meal, the gained fine powder is crossed 300 mesh sieves, obtain.
Get the Folium Apocyni Veneti of plucking the first tenday period of a month in May, 25 ℃ of water rinses, spread and dry, in 25 ℃, 0.1MPa environment, place 4 hours, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 15 seconds, 4 ℃ cooling, pulverizes, and crosses 80 sieves, obtain the Folium Apocyni Veneti meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
Get the dogbane flower that early July plucks, spread and dry, place 4 hours in 25 ℃, 0.1MPa environment, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, and 150 ℃ of baking ovens toast 5 seconds, and 4 ℃ cooling, pulverize, cross 80 sieves, obtain the dogbane flower meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
The Folium Apocyni Veneti powder is mixed in the 9:1 ratio with bluish dogbane pollen, obtain the bluish dogbane powder.
Get bitter buckwheat rhizome and leaf, add 12 times of amount 65% alcohol extracts, each 2 hours, extract 3 times, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain bitter buckwheat root, stem, Leave extract.
Ultrasonic assisted Extraction is followed the example of the extraction tartary buckwheat bran, under 24KHz, 300W power ultrasonic condition, and 6 times of amount 80% ethanol, 0.5MPa pressure, 40 ℃, extract 2 times, each 2 hours, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain the tartary buckwheat bran crude extract.
Adopt the DM-2 macroporous absorbent resin to be made with extra care bitter buckwheat root, stem, leaf and Fagopyrum tataricum(L.)Gaertn. Bran extract: bitter buckwheat root, stem, Leave extract are mixed in the 1:1 ratio with the tartary buckwheat bran crude extract, 70% ethanol dissolves, make concentration be decided to be 2mg/mL, regulating the pH value is 2, loading, the absorption flow velocity is 2mL/min, blade diameter length ratio 1:10; With 70% ethanol, macroporous absorbent resin is carried out to wash-out afterwards, regulating the pH value is 8.5, elution rate is 1mL/min, collects eluent, under 25 ℃ of conditions, eluent is carried out to the high speed centrifugation separation, centrifuge speed 4000rpm, centrifugal 20 minutes, filter eluent, filtrate is carried out to reduction vaporization drying (0.1MPa, 20 ℃), obtain tartary buckwheat extract.
According to 900 parts of tartary buckwheat cortex powders, 400 parts, bluish dogbane powder, 50 parts of mulberry leaf powders, 50 parts of chrysanthemum powders, 50 parts of tartary buckwheat extracts, 2 parts of guar gums, 10 parts of xanthans, the ratio that konjac glucomannan is 2 parts measures tartary buckwheat cortex powder, the bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan, first by guar gum, xanthans and konjac glucomannan (40% amount) soluble in water, abundant swelling, form colloidal solution, add again tartary buckwheat cortex powder, the bluish dogbane powder, mulberry leaf powder, chrysanthemum powder and tartary buckwheat extract, controlling the mixer speed of mainshaft is 30rpm, mixing time 30 minutes, then drop into pressure forming machine, cross 30 mesh sieves, granulate.
Bitter buckwheat tea granule dish out after moulding first is placed in to hot air drier, and 50 ℃ are dried in water content 8%, then put into far-infrared oven, bake and bank up with earth 2min for 200 ℃, naturally cooling.
Cooled bitter buckwheat tea is put into the roller drying case, bakes and banks up with earth to moisture not higher than 5% for 145 ℃.
After testing, the rutin composition rate of transform is 98.0% to the bitter buckwheat tea of gained, dissolution rate 95.8%, and production technology is reasonable, the technique smoothness.
Embodiment 5:
Bitter buckwheat seed (No. 9909 kinds of western agriculture that Xibei Univ. of Agricultural & Forest Science & Technology cultivates) is immersed in containing 0.008% copper sulphate, in the mixed aqueous solution of 0.048% zinc sulfate and 0.08% potassium dihydrogen phosphate, the thickness of seed in the aqueous solution is 1cm, soak 5 days, every day, ultra violet lamp was 1 hour, within 5 days, take out afterwards, clear water rinses, 24KHz, under the 300W power condition ultrasonic 5 minutes, put the far-infrared oven low temperature drying, select grain large, full, the bitter buckwheat seed that unit weight is high, by mechanical grinding method, it is pulverized, gained KUQIAOPI layer powder crossed 80 mesh sieves, obtain duck wheat cortex meal, utilize fluid energy mill to carry out ultramicro grinding to KUQIAOPI layer meal, the gained fine powder is crossed 300 mesh sieves, obtain.
Get the Folium Apocyni Veneti of plucking the first tenday period of a month in May, 25 ℃ of water rinses, spread and dry, in 25 ℃, 0.1MPa environment, place 4 hours, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 15 seconds, 4 ℃ cooling, pulverizes, and crosses 80 sieves, obtain the Folium Apocyni Veneti meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
Get the dogbane flower that early July plucks, spread and dry, place 4 hours in 25 ℃, 0.1MPa environment, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, and 150 ℃ of baking ovens toast 5 seconds, and 4 ℃ cooling, pulverize, cross 80 sieves, obtain the dogbane flower meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
The Folium Apocyni Veneti powder is mixed in the 9:1 ratio with bluish dogbane pollen, obtain the bluish dogbane powder.
Get bitter buckwheat rhizome and leaf, add 12 times of amount 65% alcohol extracts, each 2 hours, extract 3 times, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain bitter buckwheat root, stem, Leave extract.
Ultrasonic assisted Extraction is followed the example of the extraction tartary buckwheat bran, under 24KHz, 300W power ultrasonic condition, and 6 times of amount 80% ethanol, 0.5MPa pressure, 40 ℃, extract 2 times, each 2 hours, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain the tartary buckwheat bran crude extract.
Adopt the DM-2 macroporous absorbent resin to be made with extra care bitter buckwheat root, stem, leaf and Fagopyrum tataricum(L.)Gaertn. Bran extract: bitter buckwheat root is thick, stem, leaf extract are mixed in the 1:1 ratio with the tartary buckwheat bran crude extract, 70% ethanol dissolves, make concentration be decided to be 2mg/mL, regulating the pH value is 2, loading, the absorption flow velocity is 2mL/min, blade diameter length ratio 1:10; With 70% ethanol, macroporous absorbent resin is carried out to wash-out afterwards, regulating the pH value is 8.5, elution rate is 1mL/min, collects eluent, under 25 ℃ of conditions, eluent is carried out to the high speed centrifugation separation, centrifuge speed 4000rpm, centrifugal 20 minutes, filter eluent, filtrate is carried out to reduction vaporization drying (0.1MPa, 20 ℃), obtain tartary buckwheat extract.
According to 900 parts of tartary buckwheat cortex powders, 300 parts, bluish dogbane powder, 50 parts of mulberry leaf powders, 80 parts of chrysanthemum powders, 50 parts of tartary buckwheat extracts, 4 parts of guar gums, 10 parts of xanthans, 6 parts of konjac glucomannans, the ratio that egg is 14 parts measures tartary buckwheat cortex powder, the bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans, konjac glucomannan and egg, first by guar gum, xanthans, konjac glucomannan and egg (35% amount) soluble in water, abundant swelling, form colloidal solution, add again tartary buckwheat cortex powder, the bluish dogbane powder, mulberry leaf powder, chrysanthemum powder and tartary buckwheat extract, controlling the mixer speed of mainshaft is 30rpm, mixing time 30 minutes, then drop into pressure forming machine, cross 30 mesh sieves, granulate.
Bitter buckwheat tea granule dish out after moulding first is placed in to hot air drier, and 50 ℃ are dried in water content 8%, then put into far-infrared oven, bake and bank up with earth 3min for 200 ℃, naturally cooling.
Cooled bitter buckwheat tea is put into the roller drying case, bakes and banks up with earth to moisture not higher than 5% for 125 ℃.
After testing, the rutin composition rate of transform is 96.3% to the bitter buckwheat tea of gained, dissolution rate 95.5%, and production technology is reasonable, the technique smoothness.
Claims (10)
1. a bitter buckwheat tea, it is characterized in that, bitter buckwheat tea consists of tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan, tartary buckwheat cortex powder 500-900 part wherein, bluish dogbane powder 300-400 part, mulberry leaf powder 50-100 part, chrysanthemum powder 50-100 part, tartary buckwheat extract 50-100 part, guar gum 2-10 part, xanthans 2-10 part, konjac glucomannan 2-10 part.
2. a kind of bitter buckwheat tea as claimed in claim 1, is characterized in that, in bitter buckwheat tea, tartary buckwheat cortex powder is 700 parts, 350 parts, bluish dogbane powder, 60 parts of mulberry leaf powders, 100 parts of chrysanthemum powders, 90 parts of tartary buckwheat extracts, 4 parts of guar gums, 10 parts of xanthans, 6 parts of konjac glucomannans.
3. a kind of bitter buckwheat tea as claimed in claim 1, is characterized in that, bitter buckwheat is No. 9909 kinds of western agriculture that Xibei Univ. of Agricultural & Forest Science & Technology cultivates.
4. a kind of bitter buckwheat tea as claimed in claim 1, is characterized in that, the preparation technology of tartary buckwheat cortex powder is:
(1) screening: the bitter buckwheat seed that the selection grain is large, full, unit weight is high is for the production of processing.
(2) the first pulverizing: pulverize bitter buckwheat seed by mechanical grinding method, gained KUQIAOPI layer meal crossed 80 mesh sieves.
(3) ultramicro grinding: utilize fluid energy mill to carry out ultramicro grinding to KUQIAOPI layer meal, the gained fine powder is crossed 300 mesh sieves, obtains.
5. a kind of bitter buckwheat tea as claimed in claim 4, is characterized in that, before screening, bitter buckwheat carried out to pre-treatment, and method is:
Bitter buckwheat seed is immersed in containing in the mixed solution of 0.008% copper sulphate, 0.048% zinc sulfate and 0.08% potassium dihydrogen phosphate, the thickness of seed in solution is 1cm, soak 5 days, every day, ultra violet lamp was 1 hour, within 5 days, take out afterwards, clear water rinses, under 24KHz, 300W power condition ultrasonic 5 minutes, put the far-infrared oven low temperature drying, obtain.
6. a kind of bitter buckwheat tea as claimed in claim 1 is characterized in that:
(1) preparation technology of bluish dogbane powder is:
The mixture that the bluish dogbane powder is 90% Folium Apocyni Veneti powder and 10% bluish dogbane pollen.
Get the Folium Apocyni Veneti of plucking the first tenday period of a month in May, 25 ℃ of water rinses, spread and dry, in 25 ℃, 0.1MPa environment, place 4 hours, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 15 seconds, 4 ℃ cooling, pulverizes, and crosses 80 sieves, obtain the Folium Apocyni Veneti meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
Get the dogbane flower that early July plucks, spread and dry, place 4 hours in 25 ℃, 0.1MPa environment, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, and 150 ℃ of baking ovens toast 5 seconds, and 4 ℃ cooling, pulverize, cross 80 sieves, obtain the dogbane flower meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
(2) preparation technology of mulberry leaf powder is:
Get the mulberry leaf sheet after first frost, 25 ℃ of water rinses, spread and dry, in 25 ℃, 0.1MPa environment, place 4 hours, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 15 seconds, 4 ℃ cooling, pulverizes, and crosses 80 sieves, obtain the mulberry leaf meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
(3) preparation technology of chrysanthemum powder is:
Get chrysanthemum, spread and dry, place 4 hours in 25 ℃, 0.1MPa environment, 100 ℃ of steam beatings 5 minutes, room temperature is cooling, 150 ℃ of baking ovens toast 5 seconds, and 4 ℃ cooling, pulverize, and cross 80 sieves, obtain the chrysanthemum meal, meal is dropped into to fluid energy mill and carry out ultramicro grinding, product is crossed 300 mesh sieves, obtains.
7. a kind of bitter buckwheat tea as claimed in claim 1 is characterized in that:
(1) tartary buckwheat extract comprises bitter buckwheat stem, leaf, root extract and Fagopyrum tataricum(L.)Gaertn. Bran extract two parts, and bitter buckwheat stem, leaf, root extract mix in the 1:1 ratio with Fagopyrum tataricum(L.)Gaertn. Bran extract;
(2) extraction process of bitter buckwheat stem, leaf, root extract is:
12 times of amount 65% alcohol extracts, each 2 hours, extract 3 times, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain bitter buckwheat stem, leaf, root crude extract.
(3) extraction process of Fagopyrum tataricum(L.)Gaertn. Bran extract is:
Ultrasonic assisted Extraction is followed the example of the extraction tartary buckwheat bran, under 24KHz, 300W power ultrasonic condition, and 6 times of amount 80% ethanol, 0.5MPa pressure, 40 ℃, extract 2 times, each 2 hours, merge extract, reduction vaporization dry (0.1MPa, 20 ℃), obtain the tartary buckwheat bran crude extract.
(4) purifying process of tartary buckwheat extract is:
Adopt the DM-2 macroporous absorbent resin to be made with extra care tartary buckwheat extract: bitter buckwheat stem, leaf, root crude extract are mixed in the 1:1 ratio with the tartary buckwheat bran crude extract, and 70% ethanol dissolves, and makes concentration be decided to be 2mg/mL, regulating the pH value is 2, loading, the absorption flow velocity is 2mL/min, blade diameter length ratio 1:10; With 70% ethanol, macroporous absorbent resin is carried out to wash-out afterwards, regulating the pH value is 8.5, elution rate is 1mL/min, collects eluent, under 25 ℃ of conditions, eluent is carried out to the high speed centrifugation separation, centrifuge speed 4000rpm, centrifugal 20 minutes, filter eluent, filtrate is carried out to reduction vaporization drying (0.1MPa, 20 ℃), obtain tartary buckwheat extract.
8. the preparation technology as the bitter buckwheat tea of claim 1-7, is characterized in that, comprises breading, moulding, drying, four steps of Titian, wherein:
(1) breading: tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder, tartary buckwheat extract, guar gum, xanthans and konjac glucomannan are mixed, until the color and luster homogeneous, standing 20 minutes.
(2) moulding: get the tea powder of mixing thoroughly, add water 25%-40%, adopt pressure forming machine to mix, cross 30 mesh sieves, granulate.
(3) drying: the bitter buckwheat tea granule dish out after moulding first is placed in to hot air drier, and 50-55 ℃ is dried in water content 8%, then puts into far-infrared oven, bakes and banks up with earth 2-3min for 200-220 ℃, naturally cooling.
(4) Titian: cooled bitter buckwheat tea is put into the roller drying case, bakes and banks up with earth to moisture not higher than 5% for 110-145 ℃.
9. the preparation technology of a kind of bitter buckwheat tea as claimed in claim 8 is characterized in that:
(1) first that guar gum, xanthans and konjac glucomannan is soluble in water, fully swelling, form colloidal solution, then add tartary buckwheat cortex powder, bluish dogbane powder, mulberry leaf powder, chrysanthemum powder and tartary buckwheat extract, then drops into the pressure forming machine mixed pelletization.
(2) controlling the mixer speed of mainshaft is 30rpm, mixing time 30 minutes.
10. as the preparation technology of a kind of bitter buckwheat tea of claim 8 or 9, it is characterized in that, add the egg of 1% amount during breading.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103431116A (en) * | 2013-09-03 | 2013-12-11 | 西南大学 | Method for processing granulated folium mori green tea |
| CN105394759A (en) * | 2015-12-02 | 2016-03-16 | 上海大学 | Method for preparing mulberry leaves chrysanthemum compound tablets |
| CN107333954A (en) * | 2017-08-21 | 2017-11-10 | 西华大学 | A kind of preparation method of compound bitter buckwheat tea granule |
| CN109430482A (en) * | 2018-12-11 | 2019-03-08 | 南京益唯森生物科技有限公司 | A kind of organic tea of reducing blood pressure and regulating blood lipid and the preparation method and application thereof |
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2012
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103431116A (en) * | 2013-09-03 | 2013-12-11 | 西南大学 | Method for processing granulated folium mori green tea |
| CN105394759A (en) * | 2015-12-02 | 2016-03-16 | 上海大学 | Method for preparing mulberry leaves chrysanthemum compound tablets |
| CN105394759B (en) * | 2015-12-02 | 2018-08-07 | 上海大学 | A kind of preparation method of mulberry leaf-chrysanthemum composite tablet |
| CN107333954A (en) * | 2017-08-21 | 2017-11-10 | 西华大学 | A kind of preparation method of compound bitter buckwheat tea granule |
| CN109430482A (en) * | 2018-12-11 | 2019-03-08 | 南京益唯森生物科技有限公司 | A kind of organic tea of reducing blood pressure and regulating blood lipid and the preparation method and application thereof |
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