CN102864017A - Extracting method of chrysanthemum essential oil - Google Patents
Extracting method of chrysanthemum essential oil Download PDFInfo
- Publication number
- CN102864017A CN102864017A CN 201110188507 CN201110188507A CN102864017A CN 102864017 A CN102864017 A CN 102864017A CN 201110188507 CN201110188507 CN 201110188507 CN 201110188507 A CN201110188507 A CN 201110188507A CN 102864017 A CN102864017 A CN 102864017A
- Authority
- CN
- China
- Prior art keywords
- chrysanthemum
- essential oil
- extracting
- chrysanthemum essential
- extracting method
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000007516 Chrysanthemum Nutrition 0.000 title claims description 22
- 238000000034 method Methods 0.000 title claims description 19
- 239000000341 volatile oil Substances 0.000 title claims description 13
- 244000189548 Chrysanthemum x morifolium Species 0.000 title 1
- 241000723353 Chrysanthemum Species 0.000 claims description 21
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 12
- 239000003921 oil Substances 0.000 claims description 12
- 238000000605 extraction Methods 0.000 claims description 8
- 238000005516 engineering process Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 238000001556 precipitation Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- 230000006837 decompression Effects 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- 238000002386 leaching Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention discloses an extracting method of chrysanthemum essential oil, belonging to the technical field of chemical industries. With the adoption of the extracting method, the problems of excessive sediments and low purity in the extracting process of the chrysanthemum essential oil at present are solved; the oil yield of the chrysanthemum essential oil can be greatly improved; the impurity is reduced; and the chrysanthemum essential oil resource can be better used. The extracting method is characterized by comprising the following steps: carrying out dynamic leaching on the crushed chrysanthemum by petroleum ether; carrying out reflux extraction by ethyl acetate after petroleum ether is recovered from an extracting solution in a filtering manner; and concentrating the chrysanthemum liquid, adding water to dynamically extract; filtering, decompressing, concentrating, depositing in alcohol and purifying the extracting solution to obtain the chrysanthemum essential oil. The extracting process is simple and feasible, high in oil yield, and short in time, and is an ideal extracting method; and resources are saved, and no harmful substance is generated in the extracting process.
Description
Technical field
The present invention relates to a kind of extracting process of chrysanthemum essential oil, belong to chemical technology field.
Background technology
Chrysanthemum has the fabulous numerous effects such as heat, detoxifcation of reducing internal heat, drive, and chrysanthemum essential oil acetone equal solvent soluble in water, pure and mild is insoluble to sherwood oil, is slightly soluble in ethyl acetate.From extracting the method for chrysanthemum essential oil, mainly contain water extraction, water extract-alcohol precipitation and rare ethanol-extracted etc. at present.The processes such as concentrating and precipitating impurity elimination are all arranged, in this process, have precipitation capacity large, filter time consumption and energy consumption, the problem such as oil yield is low.
Summary of the invention
The objective of the invention is in order to disclose a kind of extracting process of chrysanthemum, simple for process, oil yield is high, the time is short, economize on resources, unharmful substance produces in leaching process, is a kind of desirable extracting process.
Technical scheme of the present invention: a kind of extracting process of chrysanthemum, its preparation technology is: (1) carries out dynamic lixiviate with the chrysanthemum of pulverizing with sherwood oil, after extracting solution reclaims sherwood oil after filtration; (2) carry out refluxing extraction with ethyl acetate again, concentrated chrysanthemum liquid adds water, dynamic extraction; (3) extracting solution through filtration, decompression, concentrated, alcohol precipitation, purifying, obtain chrysanthemum essential oil.
Beneficial effect of the present invention: extracting process of the present invention, too much in order to solve in the present chrysanthemum essential oil leaching process throw out, the problem such as purity is low.Can increase substantially the oil yield of chrysanthemum essential oil, impurity reduction uses the chrysanthemum essential oil resource better.This extraction process is simple, oil yield is high, the time is short, economize on resources, and unharmful substance produces in leaching process, is a kind of desirable extracting process.
Below in conjunction with embodiment, specify preparation technology of the present invention
Embodiment
A kind of extracting process of chrysanthemum essential oil, its preparation technology is: (1) carries out dynamic lixiviate with the chrysanthemum of pulverizing with sherwood oil, after extracting solution reclaims sherwood oil after filtration; (2) carry out refluxing extraction with ethyl acetate again, concentrated chrysanthemum liquid adds water, dynamic extraction; (3) extracting solution through filtration, decompression, concentrated, alcohol precipitation, purifying, obtain chrysanthemum essential oil.
This extraction process is simple, oil yield is high, the time is short, economize on resources, and unharmful substance produces in leaching process, is a kind of desirable extracting process.
Claims (1)
1. the extracting process of a chrysanthemum essential oil is characterized in that, its preparation technology is: (1) carries out dynamic lixiviate with the chrysanthemum of pulverizing with sherwood oil, after extracting solution reclaims sherwood oil after filtration; (2) carry out refluxing extraction with ethyl acetate again, concentrated chrysanthemum liquid adds water, dynamic extraction; (3) extracting solution through filtration, decompression, concentrated, alcohol precipitation, purifying, obtain chrysanthemum essential oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110188507 CN102864017A (en) | 2011-07-07 | 2011-07-07 | Extracting method of chrysanthemum essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110188507 CN102864017A (en) | 2011-07-07 | 2011-07-07 | Extracting method of chrysanthemum essential oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102864017A true CN102864017A (en) | 2013-01-09 |
Family
ID=47443150
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110188507 Pending CN102864017A (en) | 2011-07-07 | 2011-07-07 | Extracting method of chrysanthemum essential oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102864017A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103689158A (en) * | 2013-11-21 | 2014-04-02 | 深圳市深宝实业股份有限公司 | Preparation method of chrysanthemum morifolium extract |
| CN103937611A (en) * | 2014-04-04 | 2014-07-23 | 朱益锋 | Extraction method of chrysanthemum essence for textile |
| CN104152263A (en) * | 2014-08-18 | 2014-11-19 | 安徽中盛食用油科技有限公司 | Tea-seed oil extraction method with high oil yield |
| CN104513707A (en) * | 2014-12-16 | 2015-04-15 | 四川农业大学 | Method for extracting chrysanthemum essential oil and the extracted essential oil |
-
2011
- 2011-07-07 CN CN 201110188507 patent/CN102864017A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103689158A (en) * | 2013-11-21 | 2014-04-02 | 深圳市深宝实业股份有限公司 | Preparation method of chrysanthemum morifolium extract |
| CN103937611A (en) * | 2014-04-04 | 2014-07-23 | 朱益锋 | Extraction method of chrysanthemum essence for textile |
| CN104152263A (en) * | 2014-08-18 | 2014-11-19 | 安徽中盛食用油科技有限公司 | Tea-seed oil extraction method with high oil yield |
| CN104513707A (en) * | 2014-12-16 | 2015-04-15 | 四川农业大学 | Method for extracting chrysanthemum essential oil and the extracted essential oil |
| CN104513707B (en) * | 2014-12-16 | 2017-07-28 | 四川农业大学 | A kind of extracting method of chrysanthemum essential oil and the essential oil of extraction |
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| DD01 | Delivery of document by public notice |
Addressee: Liu Chang Document name: Notification of Publication of the Application for Invention |
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| DD01 | Delivery of document by public notice |
Addressee: Liu Chang Document name: Notification of before Expiration of Request of Examination as to Substance |
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| DD01 | Delivery of document by public notice |
Addressee: Liu Chang Document name: Notification that Application Deemed to be Withdrawn |
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| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20130109 |