CN102775662A - Tire flat rubber material - Google Patents
Tire flat rubber material Download PDFInfo
- Publication number
- CN102775662A CN102775662A CN2012103127541A CN201210312754A CN102775662A CN 102775662 A CN102775662 A CN 102775662A CN 2012103127541 A CN2012103127541 A CN 2012103127541A CN 201210312754 A CN201210312754 A CN 201210312754A CN 102775662 A CN102775662 A CN 102775662A
- Authority
- CN
- China
- Prior art keywords
- rubber
- rubber powder
- carbon black
- tackifier
- rubber material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920001971 elastomer Polymers 0.000 title claims abstract description 57
- 239000005060 rubber Substances 0.000 title claims abstract description 46
- 239000000463 material Substances 0.000 title claims abstract description 13
- 239000000843 powder Substances 0.000 claims abstract description 27
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 26
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 22
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 22
- 230000003712 anti-aging effect Effects 0.000 claims description 14
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 11
- 239000005864 Sulphur Substances 0.000 claims description 11
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 11
- 239000006185 dispersion Substances 0.000 claims description 11
- 239000000806 elastomer Substances 0.000 claims description 11
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 11
- 229920003048 styrene butadiene rubber Polymers 0.000 claims description 11
- 239000011787 zinc oxide Substances 0.000 claims description 11
- 238000004513 sizing Methods 0.000 claims description 8
- 238000000227 grinding Methods 0.000 claims description 2
- 239000013536 elastomeric material Substances 0.000 claims 1
- 239000006229 carbon black Substances 0.000 abstract description 14
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 239000000428 dust Substances 0.000 abstract description 3
- 230000009969 flowable effect Effects 0.000 abstract 1
- 230000036449 good health Effects 0.000 abstract 1
- 230000000704 physical effect Effects 0.000 abstract 1
- 239000004594 Masterbatch (MB) Substances 0.000 description 10
- 239000011347 resin Substances 0.000 description 7
- 229920005989 resin Polymers 0.000 description 7
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 6
- 239000003292 glue Substances 0.000 description 6
- 239000004615 ingredient Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 239000003921 oil Substances 0.000 description 6
- WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Natural products O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 4
- YXIWHUQXZSMYRE-UHFFFAOYSA-N 1,3-benzothiazole-2-thiol Chemical compound C1=CC=C2SC(S)=NC2=C1 YXIWHUQXZSMYRE-UHFFFAOYSA-N 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- QHPQWRBYOIRBIT-UHFFFAOYSA-N 4-tert-butylphenol Chemical compound CC(C)(C)C1=CC=C(O)C=C1 QHPQWRBYOIRBIT-UHFFFAOYSA-N 0.000 description 2
- OUBMGJOQLXMSNT-UHFFFAOYSA-N N-isopropyl-N'-phenyl-p-phenylenediamine Chemical compound C1=CC(NC(C)C)=CC=C1NC1=CC=CC=C1 OUBMGJOQLXMSNT-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 230000002787 reinforcement Effects 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- -1 tertiary butyl phenol aldehyde Chemical class 0.000 description 2
- 208000028571 Occupational disease Diseases 0.000 description 1
- 102000007620 Pulmonary Surfactant-Associated Protein C Human genes 0.000 description 1
- 108010007125 Pulmonary Surfactant-Associated Protein C Proteins 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012628 flowing agent Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000010721 machine oil Substances 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- KUAZQDVKQLNFPE-UHFFFAOYSA-N thiram Chemical compound CN(C)C(=S)SSC(=S)N(C)C KUAZQDVKQLNFPE-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a tire flap rubber material, belonging to the field of manufacturing of rubber tires. According to the formula of the rubber material, 60-mesh rubber powder is added, carbon black is removed, and a tackifier and a flowable agent are added, thereby keeping the softness of the finished flat product for a long time, improving the hand feel of the finished flat product and lowering the production cost to some degree on the premise of not lowering the original physical properties. Meanwhile, the invention solves the problem that the carbon black can bring about massive dust and jeopardize good health of working personnel in working places.
Description
Technical field
The present invention relates to a kind of tire flap sizing material, belong to rubber tyre and make the field.
Background technology
Rim strip is claimed lining band again, press strip.Refer to be used to protect the inner tube of a tyre the endless rubber belt that the face of closing does not receive the wheel rim wearing and tearing.To the rim strip of making all kinds of all steels and half steel tire, require properties of rubber can resist flex crack, tear-resistant, heat-resisting and have a certain rigidity.The carbon black that has all added mix quality 5～6% in the existing sizing material plays reinforcement and filling effect.Sooty adds makes rubber unvulcanizate deposit after for some time or carbon black add-on degradation such as flexibility when big on the one hand, makes the dust of working space big on the other hand, and the harm staff's is healthy.
Summary of the invention
The present invention has overcome that rim strip softness that existing carbon black causes descends and problem such as the dust of worker's Working environment is big, and a kind of new tire flap sizing material is provided.This sizing material has added 60 purpose rubber powders in prescription; Removed carbon black; And add tackifier and flowing agent etc., and make it under the prerequisite that does not reduce original rerum natura, can not only keep the pliability of rim strip finished product for a long time; Improved the handling property of rim strip finished product, and production cost obtains reduction to a certain degree.The more important thing is the sanitary condition of production scene is greatly improved.
Technical scheme of the present invention is: a kind of tire flap sizing material; It is characterized in that; Its component and weight part thereof are tree elastomer 10～20, styrene-butadiene rubber(SBR) 10～30, shoddy 40～70, rubber powder (60 order) 9～12, light calcium carbonate 3～5, zinc oxide 2～3, Triple Pressed Stearic Acid 1.0～1.5, sulphur 1.0～1.5, anti-aging agent 1.0～2.0, promotor 0.5～0.8, tenderizer 3～5, tackifier 1～2, flow dispersion agent 0.5～1.0.
Said anti-aging agent is anti-aging agent RD, 4010NA or 4020 etc.; Said promotor is rubber accelerator M, DM, CZ, SP-C, TMTD, PZ etc.; Said tenderizer be molecular weight 300-600 hydro carbons or arene (like machine oil, paraffin oils, aromatic hydrocarbon oil, etc.); Said tackifier are octyl group phenolic tackifying resins (203-resin), p tert butylphenol formaldehyde resin or tertiary butyl phenol aldehyde tackifying resin; Said flow dispersion agent is conventional rubber flow dispersion agent HM-24 etc.
Said rubber powder is the Powdered elastomeric materials of 60 purposes for handling the granularity that obtains by junked tire through grinding and processing.The mixture of said shoddy for forming through pulverizing, regeneration (desulfurization) and refining by junked tire.
Preparing method: use rubber internal mixer; Order of addition(of ingredients) is: tree elastomer, styrene-butadiene rubber(SBR), shoddy and rubber powder drop into Banbury mixer and pressed bolt 2～3 minutes; Add light calcium carbonate, zinc oxide, Triple Pressed Stearic Acid, anti-aging agent, tackifier and flow dispersion agent then and pressed bolt 3～5 minutes; Add tenderizer then, discharge, extrude down sheet and form master batch; Master batch adds sulphur, promotor mixing at last, and following sheet is cooled to the making that room temperature is accomplished rim strip glue.
The invention has the beneficial effects as follows:
1, because rubber powder itself is a kind of sooty glue that contains; It can not only play sooty reinforcement, filling effect, and add-on can not cause the finished product changes in hardness bigger when strengthening; Thereby the pliability that has kept finished product, the while has also increased the stability of finished product hardness.
2, use 60 order rubber powders that the sanitary condition of the production scene of mixing process is greatly improved, everywhere unlike the carbon black that equally can find in the past to fly, the also bad cleaning of health of equipment simultaneously.Also guaranteeing that in varying degrees worker's Working environment improves, and has avoided the occupational illness because of using carbon black to cause.
3, because the price of 60 order rubber powders almost is about half of carbon black price; And the usage quantity of rubber powder be the carbon black usage quantity 1-2 doubly between; The consumption of other material of being adjusted in the prescription is fewer again, therefore makes whole formulation cost obtain decline to a certain degree.
Embodiment
Embodiment 1 (use rubber powder)
Proportioning (kilogram): tree elastomer 12, styrene-butadiene rubber(SBR) 16, shoddy 65, rubber powder (60 order) 12, light calcium carbonate 5, zinc oxide 2.5, Triple Pressed Stearic Acid 1.2, sulphur 1.2, anti-aging agent RD 1.4, promotor (rubber accelerator M) 0.6, tenderizer (aromatic hydrocarbon oil) 4, tackifier (203-resin) 1.5, flow dispersion agent (China steps chemical industry HM-24) 0.5.
Preparing method: use rubber internal mixer; Order of addition(of ingredients) is: tree elastomer, styrene-butadiene rubber(SBR), shoddy and rubber powder drop into Banbury mixer and pressed bolt 2.5 minutes; Add light calcium carbonate, zinc oxide, Triple Pressed Stearic Acid, anti-aging agent, tackifier and flow dispersion agent then and pressed bolt 4 minutes; Add tenderizer then, discharge, extrude down sheet and form master batch; Master batch adds sulphur, promotor mixing at last, and following sheet is cooled to the making that room temperature is accomplished rim strip glue.
Embodiment 2 (use carbon black)
Proportioning (kilogram): tree elastomer 12, styrene-butadiene rubber(SBR) 16, shoddy 65, carbon black 6, light calcium carbonate 5, zinc oxide 2.5, Triple Pressed Stearic Acid 1.1, sulphur 1.2, anti-aging agent RD 1.3, promotor (rubber accelerator M) 0.55, tenderizer (aromatic hydrocarbon oil) 2.5.
Preparing method: use rubber internal mixer; Order of addition(of ingredients) is: tree elastomer, styrene-butadiene rubber(SBR), shoddy and rubber powder drop into Banbury mixer and pressed bolt 2.5 minutes; Add light calcium carbonate, zinc oxide, Triple Pressed Stearic Acid and anti-aging agent then and pressed bolt 4 minutes; Add tenderizer then, discharge, extrude down sheet and form master batch; Master batch adds sulphur, promotor mixing at last, and following sheet is cooled to the making that room temperature is accomplished rim strip glue.
The finished product rim strip preserve separately of embodiment 1 and embodiment 2 16 hours with deposit 3 months experimental result shown in table 1 and table 2.
Park 16 hours experimental result behind the table 1 rim strip finished product
The experimental result of table 2 rim strip products storage after three months
Be not difficult to find out from the experimental data of table 1 and table 2, use all very approaching of carbon black and the rim strip finished product each item physical index that uses two different ingredients of 60 order rubber powders to produce.Above experimental data has also shown the finished product physical index of parking after three months and also has been to use the more stable of rubber powder, and performance the most significantly is exactly a Shao Er hardness, and the finished product Shao Er hardness that the prescription of use rubber powder is produced has kept relative stablizing.Simultaneously because the price of 60 order rubber powders almost is about half of carbon black price; Again because the amount ratio sooty consumption of rubber powder increases to some extent in prescription; Descend in that (unit price of embodiment 1 is 7.26 yuan/kilogram more than 0.15 yuan through the cost per kilogram of adjusting whole prescription; The unit price of embodiment 2 is 7.48 yuan/kilogram), the cost keeping of embodiment 1 and embodiment 2 respectively like table 3, shown in 4.
Table 3 embodiment 1 cost keeping table
Table 4 embodiment 2 cost keeping tables
Embodiment 3 (use rubber powder)
Proportioning (kilogram): tree elastomer 18, styrene-butadiene rubber(SBR) 22, shoddy 70, rubber powder (60 order) 12, light calcium carbonate 5, zinc oxide 2.8, Triple Pressed Stearic Acid 1.5, sulphur 1.5, anti-aging agent (antioxidant 4010NA) 1.4, promotor (rubber accelerator DM) 0.7, tenderizer (aromatic hydrocarbon oil) 4, tackifier (p tert butylphenol formaldehyde resin) 1.8, flow dispersion agent (China steps chemical industry HM-24) 0.7.
Preparing method: use rubber internal mixer; Order of addition(of ingredients) is: tree elastomer, styrene-butadiene rubber(SBR), shoddy and rubber powder drop into Banbury mixer and pressed bolt 3 minutes; Add light calcium carbonate, zinc oxide, Triple Pressed Stearic Acid, anti-aging agent, tackifier and flow dispersion agent then and pressed bolt 5 minutes; Add tenderizer then, discharge, extrude down sheet and form master batch; Master batch adds sulphur, promotor mixing at last, and following sheet is cooled to the making that room temperature is accomplished rim strip glue.
Embodiment 4 (use rubber powder)
Proportioning (kilogram): tree elastomer 10, styrene-butadiene rubber(SBR) 15, shoddy 40, rubber powder (60 order) 10, light calcium carbonate 4, zinc oxide 2, Triple Pressed Stearic Acid 1.0, sulphur 1.2, anti-aging agent (anti-aging agent 4020) 1.2, promotor (rubber accelerator DM) 0.5, tenderizer (aromatic hydrocarbon oil) 3.2, tackifier (tertiary butyl phenol aldehyde tackifying resin) 1.2, flow dispersion agent 0.6 (China steps chemical industry HM-24).
Preparing method: use rubber internal mixer; Order of addition(of ingredients) is: tree elastomer, styrene-butadiene rubber(SBR), shoddy and rubber powder drop into Banbury mixer and pressed bolt 2 minutes; Add light calcium carbonate, zinc oxide, Triple Pressed Stearic Acid, anti-aging agent, tackifier and flow dispersion agent then and pressed bolt 3 minutes; Add tenderizer then, discharge, extrude down sheet and form master batch; Master batch adds sulphur, promotor mixing at last, and following sheet is cooled to the making that room temperature is accomplished rim strip glue.
Claims (2)
1. tire flap sizing material; It is characterized in that; Its component and weight part thereof do; Tree elastomer 10～20, styrene-butadiene rubber(SBR) 10～30, shoddy 40～70, rubber powder 9～12, light calcium carbonate 3～5, zinc oxide 2～3, Triple Pressed Stearic Acid 1.0～1.5, sulphur 1.0～1.5, anti-aging agent 1.0～2.0, promotor 0.5～0.8, tenderizer 3～5, tackifier 1～2, flow dispersion agent 0.5～1.0, said rubber powder are 60 orders.
2. a kind of tire flap sizing material as claimed in claim 1 is characterized in that, said rubber powder is that junked tire is handled the Powdered elastomeric material that obtains through grinding and processing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210312754.1A CN102775662B (en) | 2012-08-29 | 2012-08-29 | Tire flat rubber material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210312754.1A CN102775662B (en) | 2012-08-29 | 2012-08-29 | Tire flat rubber material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102775662A true CN102775662A (en) | 2012-11-14 |
| CN102775662B CN102775662B (en) | 2014-01-29 |
Family
ID=47120785
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210312754.1A Active CN102775662B (en) | 2012-08-29 | 2012-08-29 | Tire flat rubber material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102775662B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103881164A (en) * | 2014-04-14 | 2014-06-25 | 柳州市颖航汽配有限公司 | Automotive rubber material and production method thereof |
| CN111320793A (en) * | 2020-01-13 | 2020-06-23 | 沈阳化工大学 | Preparation method of NR/SBR/tread reclaimed rubber/rubber powder combined truck tire flap |
| CN111333936A (en) * | 2020-01-13 | 2020-06-26 | 沈阳化工大学 | A kind of preparation method of NR/BR/tread reclaimed rubber/rubber powder combined with truck tire pad |
| CN111363215A (en) * | 2020-01-13 | 2020-07-03 | 沈阳化工大学 | Preparation method of BR/SBR/tread reclaimed rubber/rubber powder combined truck tire pad belt |
| CN111363216A (en) * | 2020-01-15 | 2020-07-03 | 沈阳化工大学 | Method for preparing truck tire pad belt by using reclaimed rubber and rubber powder together |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101492549A (en) * | 2008-01-21 | 2009-07-29 | 赛轮股份有限公司 | Tire flap sizing material |
-
2012
- 2012-08-29 CN CN201210312754.1A patent/CN102775662B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101492549A (en) * | 2008-01-21 | 2009-07-29 | 赛轮股份有限公司 | Tire flap sizing material |
Non-Patent Citations (2)
| Title |
|---|
| 欧阳涛: "De-link新生胶在垫带胶中的应用", 《轮胎工业》 * |
| 赵光贤: "胶粉及其应用", 《特种橡胶制品》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103881164A (en) * | 2014-04-14 | 2014-06-25 | 柳州市颖航汽配有限公司 | Automotive rubber material and production method thereof |
| CN111320793A (en) * | 2020-01-13 | 2020-06-23 | 沈阳化工大学 | Preparation method of NR/SBR/tread reclaimed rubber/rubber powder combined truck tire flap |
| CN111333936A (en) * | 2020-01-13 | 2020-06-26 | 沈阳化工大学 | A kind of preparation method of NR/BR/tread reclaimed rubber/rubber powder combined with truck tire pad |
| CN111363215A (en) * | 2020-01-13 | 2020-07-03 | 沈阳化工大学 | Preparation method of BR/SBR/tread reclaimed rubber/rubber powder combined truck tire pad belt |
| CN111363216A (en) * | 2020-01-15 | 2020-07-03 | 沈阳化工大学 | Method for preparing truck tire pad belt by using reclaimed rubber and rubber powder together |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102775662B (en) | 2014-01-29 |
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Owner name: LAIWUSHI FUQUAN RUBBER CO., LTD. Free format text: FORMER OWNER: LAIWU XINGQUAN RUBBER CO., LTD. Effective date: 20131224 |
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Effective date of registration: 20131224 Address after: 271100 Shandong province Laiwu City mountain high tech Development Zone, Road No. 15 Applicant after: Laiwu Fuquan Rubber Co., Ltd. Address before: Huitong road 271100 in Shandong province Laiwu City Laicheng Industrial Zone Applicant before: Laiwu Xingquan Rubber Co.,Ltd. |
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Address after: No. 15, Huitong East Road, Kou Town, Laiwu District, Jinan City, Shandong Province Patentee after: Jinan Laiwu Fuquan Rubber Co., Ltd Address before: 271100 Shandong province Laiwu City mountain high tech Development Zone, Road No. 15 Patentee before: LAIWU FUQUAN RUBBER Co.,Ltd. |